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Separations, Volume 9, Issue 10

2022 October - 61 articles

Cover Story: Gonadal steroid hormones—17β-testosterone (17β-T), 11-ketotestosterone (11-KT), and 17β-estradiol (17β-E2)—can modulate normal sexual behaviour in early developed or adult fish, and can also regulate many other critical physiological processes. However, many androgen and anty-androgen active compounds enter the aquatic environment and, even at low concentrations, affect fish, causing a modification of behaviour and sexual or immune function. Therefore, it is important to determine the concentrations of hormones in fish gonads. The goal of this work is to develop a method for the determination of 17β-T, 11-11-KT, and 17β-E2 in sea salmon gonads through the application of high-performance liquid chromatography–mass spectrometry (HPLC-MS) as an analysis technique. This method was applied to determining 17β-T, 11-KT, and 17β-E2 in real samples of female and male sea trout gonads. View this paper
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Articles (61)

  • Article
  • Open Access
10 Citations
3,116 Views
16 Pages

Mixotrophic denitrification has showed great potential for treating wastewater with a low C/N ratio. Mixotrophic denitrification is the process combining autotrophic denitrification and heterotrophic denitrification in one system. It can compensate t...

(This article belongs to the Section Environmental Separations)
  • Article
  • Open Access
69 Citations
5,275 Views
24 Pages

Synthesis of Gum Arabic Magnetic Nanoparticles for Adsorptive Removal of Ciprofloxacin: Equilibrium, Kinetic, Thermodynamics Studies, and Optimization by Response Surface Methodology

  • Abdullahi Haruna Birniwa,
  • Rania Edrees Adam Mohammad,
  • Mujahid Ali,
  • Muhammad Faisal Rehman and ,
  • Shehu Sa’ad Abdullahi,
  • Sayed M. Eldin,
  • Suwaiba Mamman,
  • Abubakar Chadi Sadiq and
  • Ahmad Hussaini Jagaba
  • + 4 authors+ 0 author

Given the increasing risks that antibiotic abuse poses to microecology and human health, it is imperative to develop incredibly powerful adsorbents. This study investigated the use of environmentally sustainable polymeric nanocomposite based on gum a...

(This article belongs to the Special Issue Separation Processes for Effective Removal of Emerging Contaminants from Water and Wastewater)
  • Article
  • Open Access
4 Citations
4,363 Views
26 Pages

Amelioration of Alcoholic Liver Disease by Activating PXR-Cytochrome P450s Axis with Blackberry Extract

  • Ting Xiao,
  • Zhenghong Guo,
  • Min Fu,
  • Jiaoyan Huang and ,
  • Xiaowei Wang,
  • Yuqing Zhao,
  • Ling Tao and
  • Xiangchun Shen
  • + 3 authors+ 0 author

Blackberry is widely used in diets for its rich biological phytochemicals and health benefits. However, the relationship between the effect of blackberry extract (BBE) on ameliorating alcoholic liver disease (ALD) and the PXR-Cytochrome P450s axis in...

(This article belongs to the Topic Discovery of Bioactive Compounds from Natural Organisms and Their Molecular Mechanisms against Diseases)
  • Article
  • Open Access
3 Citations
2,873 Views
14 Pages

Effect of Oily Aerosol Charge Characteristics on the Filtration Efficiency of an Electrostatically Enhanced Fibrous Filter System

  • Yi Yu,
  • Di Pan,
  • Kai Kang,
  • Shu-Pei Bai and ,
  • Hao Han,
  • Hua Song and
  • Jian Kang
  • + 2 authors+ 0 author

The synergistic effect of electrostatically enhanced fibrous filtration originates from the charging characteristics of aerosol particles and electret fibers in an electric field. Two electrostatically enhanced fibrous filter systems are designed in...

(This article belongs to the Section Environmental Separations)
  • Article
  • Open Access
15 Citations
3,343 Views
14 Pages

Vegetables and fruits can potentially accumulate cyanotoxins after water contaminated with cyanobacteria is used for irrigation. We developed and validated an analytical method to quantify eight microcystin congeners (MCs) and nodularin (NOD) using u...

(This article belongs to the Special Issue Development of Highly Efficient Separation-Based Analytical Methods for Food Integrity Assurance)
  • Article
  • Open Access
6 Citations
3,220 Views
12 Pages

Hydrophobic Natural Eutectic Solvents for the Gas Chromatographic Determination of Suspected Allergens in Fragrances by Dispersive Liquid-Liquid Microextraction

  • Gaia Bechis,
  • Giulia Mastellone,
  • Arianna Marengo,
  • Barbara Sgorbini and ,
  • Cecilia Cagliero and
  • Patrizia Rubiolo
  • + 1 author+ 0 author

The fragrance industry plays a key role in the global economy, producing a wide range of personal care and household products. However, some fragrance ingredients have been linked to allergic reactions in sensitive people, and their concentrations ar...

(This article belongs to the Section Materials in Separation Science)
  • Article
  • Open Access
6 Citations
4,299 Views
14 Pages

Tecoma stans is an ornamental perennial tropical and subtropical plant belonging to the Bignoniaceae family with green leaves and yellow attractive fragrance flowers and commonly known as yellow trumpetbush or yellow bells. The plant originated in th...

  • Article
  • Open Access
7 Citations
3,041 Views
17 Pages

Cobalt Biosorption in Fixed-Bed Column Using Greenhouse Crop Residue as Natural Sorbent

  • Gabriel Blázquez,
  • María Ángeles Martín-Lara,
  • Irene Iáñez-Rodríguez,
  • Inés Morales and ,
  • Antonio Pérez and
  • Mónica Calero
  • + 1 author+ 0 author

Intensive greenhouse agriculture annually produces large amounts of residues. The present work focused on the study of the dynamic adsorption of cobalt from aqueous solutions over a vegetal residue from intensive greenhouse cultivation. The influence...

(This article belongs to the Special Issue Removal of Metals or Other Toxic Substances from Wastewaters by Natural Sorbents)
  • Article
  • Open Access
10 Citations
2,781 Views
10 Pages

Surface Acidification of BiOI/TiO2 Composite Enhanced Efficient Photocatalytic Degradation of Benzene

  • Ziwang Zhao,
  • Hao Wang,
  • Chunyu Wang,
  • Yuan Sun and ,
  • Hao Han,
  • Jian Kang,
  • Yanchun Dong and
  • Lei Wang
  • + 3 authors+ 0 author

A novel BiOI/TiO2 nano-heterojunction was prepared using hydrothermal and sol-gel methods. The composite material was characterized by X-ray diffraction, ultraviolet-visible diffuse reflection spectroscopy, scanning electron microscopy, and transmiss...

(This article belongs to the Section Environmental Separations)
  • Article
  • Open Access
11 Citations
4,055 Views
11 Pages

Taraxacum kok-saghyz Rodin (TKS) is a potential edible resource plant that is rich in inulin, lipid, protein and other active ingredients. In this study, HS-SPME/GC–MS was used to analyze volatile compounds (VCs) and profile the fatty acids in...

(This article belongs to the Special Issue Development of Highly Efficient Separation-Based Analytical Methods for Food Integrity Assurance)
  • Article
  • Open Access
4 Citations
6,937 Views
13 Pages

Application of Humic and Fulvic Acids as an Alternative Method of Cleaning Water from Plant Protection Product Residues

  • Eirini A. Makrigianni,
  • Eirini S. Papadaki,
  • Theodoros Chatzimitakos,
  • Vassilis Athanasiadis and ,
  • Eleni Bozinou and
  • Stavros I. Lalas
  • + 1 author+ 0 author

Humic acids (HAs) and fulvic acids (FAs) are naturally occurring compounds that influence the fate and transportation of various compounds in the soil. Although HAs and FAs have multiple uses, the reports about their sorbent potential for environment...

(This article belongs to the Special Issue Novel Applications of Separation Technology)
  • Article
  • Open Access
26 Citations
5,377 Views
15 Pages

Qualitative and Quantitative Detection of Acacia Honey Adulteration with Glucose Syrup Using Near-Infrared Spectroscopy

  • Maja Benković,
  • Tamara Jurina,
  • Lucija Longin,
  • Franjo Grbeš and ,
  • Davor Valinger,
  • Ana Jurinjak Tušek and
  • Jasenka Gajdoš Kljusurić
  • + 2 authors+ 0 author

Honey adulteration with cheap sweeteners such as corn syrup or invert syrup results in honey of lesser quality that can harm the objectives of both manufacturers and consumers. Therefore, there is a growing interest for the development of a fast and...

(This article belongs to the Special Issue Novel Applications of Separation Technology)
  • Article
  • Open Access
30 Citations
3,052 Views
24 Pages

Appreciatively Efficient Sorption Achievement to U(VI) from the El Sela Area by ZrO2/Chitosan

  • Sameh H. Negm,
  • Mahmoud O. Abd El-Magied,
  • Wael M. El Maadawy,
  • Mostafa M. Abdel Aal and ,
  • Samia M. Abd El Dayem,
  • Mahmoud A. Taher,
  • Khaled A. Abd El-Rahem,
  • Mohamed N. Rashed and
  • Mohamed F. Cheira
  • + 4 authors+ 0 author

The need to get uranium out of leaching liquid is pushing scientists to come up with new sorbents. This study uses the wet technique to improve the U(VI) sorption properties of ZrO2/chitosan composite sorbent. To validate the synthesis of ZrO2/CS com...

(This article belongs to the Special Issue Photocatalysis and Adsorption Techniques in Water and Wastewater Treatment)
  • Article
  • Open Access
26 Citations
5,625 Views
13 Pages

Potential Use of Low-Cost Agri-Food Waste as Biosorbents for the Removal of Cd(II), Co(II), Ni(II) and Pb(II) from Aqueous Solutions

  • Lorena Sánchez-Ponce,
  • Margarita Díaz-de-Alba,
  • María José Casanueva-Marenco,
  • Jesús Gestoso-Rojas and ,
  • Marta Ortega-Iguña,
  • María Dolores Galindo-Riaño and
  • María Dolores Granado-Castro
  • + 2 authors+ 0 author

We evaluated the potential use of agri-food waste for the removal of heavy metal ions from aqueous solutions and its application in different processes (e.g., water remediation, in the production of biomass enriched in nutritionally significant eleme...

(This article belongs to the Special Issue Removal of Emerging Pollutants and Environmental Analysis)
  • Article
  • Open Access
11 Citations
4,386 Views
18 Pages

The objective of this study was to develop and validate a near-infrared (NIR) spectroscopy based method for in-line quantification during the second alcohol precipitation process of Astragali radix. In total, 22 calibration experiments were carefully...

(This article belongs to the Special Issue Separation, Extraction and Purification of Natural Products from Plants)
  • Article
  • Open Access
5 Citations
5,912 Views
16 Pages

Plant Poisons in the Garden: A Human Risk Assessment

  • Samantha L. Bowerbank,
  • Matteo D. Gallidabino and
  • John R. Dean

A study of the plants, and their associated poisons, in the Poison Garden at The Alnwick Garden was undertaken across a calendar year. By selecting 25 plants in the Poison Garden, we have been able to develop a single chromatographic method for the d...

(This article belongs to the Section Environmental Separations)
  • Review
  • Open Access
92 Citations
29,421 Views
27 Pages

Nitrogen oxide (NOx) is a major gaseous pollutant in flue gases from power plants, industrial processes, and waste incineration that can have adverse impacts on the environment and human health. Many denitrification (de-NOx) technologies have been de...

(This article belongs to the Section Environmental Separations)
  • Article
  • Open Access
5,293 Views
24 Pages

Synthesis and Characterization with Computational Studies of Metal Complexes of Methyl 2-((4-cyanophenyl)(hydroxy) methyl)acrylate: A New Biologically Active Multi-Functional Adduct

  • Shazia Ishfaq,
  • Shazia Nisar,
  • Amtul Qayum,
  • Sadaf Iqbal and ,
  • Nasreen Fatima,
  • Fatmah Ali Alasmary,
  • Amani Salem Almalki,
  • ElSayed M. Tag El Din,
  • Muhammad Sufyan Javed and
  • Patrizia Bocchetta
  • + 5 authors+ 0 author

The title ligand (L”x), methyl 2-((4-cyanophenyl)(hydroxy)methyl)acrylate was synthesized following the Morita-Baylis-Hillman reaction scheme. Spectroscopic techniques such as: UV- Visible, FT-IR, ESI-MS, and 1H NMR helped in characterization o...

(This article belongs to the Topic Discovery of Bioactive Compounds from Natural Organisms and Their Molecular Mechanisms against Diseases)
  • Article
  • Open Access
4 Citations
2,786 Views
17 Pages

Numerical Simulation of Critical Production Pressure Drop of Injection and Production Wells in Gas Storage Based on Gas-Solid Coupling

  • Yiyong Sui,
  • Mengying Luo,
  • Tangmao Lin,
  • Guihua Liu and ,
  • Yuan Zhao,
  • Yazhou Wu and
  • Lanqing Ren
  • + 2 authors+ 0 author

The periodic injection-production process of natural gas in underground gas storage make the rock bear alternating load under the gas-solid coupling. The alternating load changes the physical properties of rock, and then influence the critical produc...

(This article belongs to the Topic Oil, Gas and Water Separation Research)
  • Article
  • Open Access
8 Citations
5,109 Views
17 Pages

Separation and Purification of Taxanes from Crude Taxus cuspidata Extract by Antisolvent Recrystallization Method

  • Yajing Zhang,
  • Zirui Zhao,
  • Wenlong Li,
  • Yuanhu Tang and ,
  • Huiwen Meng and
  • Shujie Wang
  • + 1 author+ 0 author

Taxanes are natural compounds with strong antitumor activity. In this study, we first enriched taxanes by ultrasonic extraction and liquid–liquid extraction from Taxus cuspidata, then purified these taxanes by the antisolvent recrystallization...

(This article belongs to the Collection Recent Trends in the Separation of Natural Products and Pharmaceuticals)
  • Article
  • Open Access
12 Citations
4,437 Views
10 Pages

Development and Validation of HPLC-DAD Method for the Determination of Favipiravir and Studying the Impact of Vitamin C on the Pharmacokinetics of COVID-19 Antiviral Drug Favipiravir

  • Mohammad Hailat,
  • Israa Al-Ani,
  • Zainab Zakareia,
  • Ramadan Al-Shdefat and ,
  • Osaid Al-Meanazel,
  • Md. Khalid Anwer,
  • Mohammed Hamad,
  • Walid Abu Rayyan,
  • Riad Awad and
  • Wael Abu Dayyih
  • + 5 authors+ 0 author

A novel, sensitive, and low-cost HPLC method for the rapid determination of favipiravir (FVR) in rat plasma was developed and validated, and the effect of vitamin C on FVR pharmacokinetic parameters was investigated. FVR and oxcarbazepine (IS) were s...

(This article belongs to the Special Issue HPLC: A Key Tool for Analytical Chemistry)
  • Article
  • Open Access
36 Citations
5,436 Views
17 Pages

Evaluation of Pulsed Electric Field-Assisted Extraction on the Microstructure and Recovery of Nutrients and Bioactive Compounds from Mushroom (Agaricus bisporus)

  • Mara Calleja-Gómez,
  • Juan Manuel Castagnini,
  • Ester Carbó,
  • Emilia Ferrer and ,
  • Houda Berrada and
  • Francisco J. Barba
  • + 1 author+ 0 author

Pulsed electric field (PEF) is a sustainable innovative technology that allows for the recovery of nutrients and bioactive compounds from vegetable matrices. A. bisporus was chosen for its nutritional value and the effect of PEF pretreatment was eval...

(This article belongs to the Special Issue Development and Application of Green or Sustainable Strategies in Analytical Chemistry)
  • Article
  • Open Access
6 Citations
4,868 Views
11 Pages

Comparison of Validation Parameters for the Determination of Vitamin D3 in Commercial Pharmaceutical Products Using Traditional and Greener HPTLC Methods

  • Mohammed H. Alqarni,
  • Faiyaz Shakeel,
  • Ahmed I. Foudah,
  • Tariq M. Aljarba and ,
  • Aftab Alam,
  • Sultan Alshehri and
  • Prawez Alam
  • + 2 authors+ 0 author

Several analytical methods are documented for the estimation of vitamin D3 (VD3) in pharmaceuticals, food supplements, nutritional supplements, and biological samples. However, greener analytical methods for VD3 analysis are scarce in the literature....

(This article belongs to the Special Issue Development and Application of Green or Sustainable Strategies in Analytical Chemistry)
  • Article
  • Open Access
10 Citations
5,040 Views
12 Pages

Simultaneous Detection of Chlorzoxazone and Paracetamol Using a Greener Reverse-Phase HPTLC-UV Method

  • Ahmed I. Foudah,
  • Faiyaz Shakeel,
  • Mohammed H. Alqarni,
  • Tariq M. Aljarba and ,
  • Sultan Alshehri and
  • Prawez Alam
  • + 1 author+ 0 author

In the literature, greener/eco-friendly analytical techniques for simultaneous estimation of chlorzoxazone (CZN) and paracetamol (PCT) are scarce. As a consequence, greener reverse-phase high-performance thin-layer chromatography with ultraviolet (HP...

(This article belongs to the Special Issue Development and Application of Green or Sustainable Strategies in Analytical Chemistry)
  • Article
  • Open Access
16 Citations
5,413 Views
17 Pages

In Vitro Cytotoxicity and Spectral Analysis-Based Phytochemical Profiling of Methanol Extract of Barleria hochstetteri, and Molecular Mechanisms Underlying Its Apoptosis-Inducing Effect on Breast and Lung Cancer Cell Lines

  • Saad Ahmed Alkahtani,
  • Ali Mohamed Alshabi,
  • Ibrahim Ahmed Shaikh,
  • Mohamed A. A. Orabi and ,
  • Basel A. Abdel-Wahab,
  • Ismail A. Walbi,
  • Mohammed Shafiuddin Habeeb,
  • Masood Medleri Khateeb,
  • Arun K. Shettar and
  • Joy H. Hoskeri
  • + 5 authors+ 0 author

The objectives of this research were to carry out GC–MS and LC–MS-based phytochemical profiling of Barleria hochstetteri, as well as flow cytometry-based mechanistic investigations of the cytotoxic effect of its extracts against breast an...

(This article belongs to the Section Analysis of Food and Beverages)
  • Article
  • Open Access
9 Citations
3,605 Views
20 Pages

Characterization of Chemical Constituents of Oxytropis microphylla (Pall.) DC. by Ultra-High-Performance Liquid Chromatography Coupled with Quadrupole-Time-of Flight Tandem Mass Spectrometry

  • Mengqi Xia,
  • Min Yao,
  • Junmao Li,
  • Jianjian Zhang and ,
  • Yayun Yu,
  • Shilin Yang,
  • Guoyue Zhong,
  • Na Pei,
  • Hui Ouyang and
  • Yulin Feng
  • + 5 authors+ 0 author

Oxytropis microphylla (Pall.) DC. is a traditional Tibetan medicine used as an external preparation for clearing heat and detoxification, healing sore muscles, astringent vein hemostasis, defecation, and treating plague, constipation, anthrax, and sw...

(This article belongs to the Section Analysis of Natural Products and Pharmaceuticals)
  • Article
  • Open Access
11 Citations
3,487 Views
18 Pages

Inhibitory Effect and Mechanism of Dill Seed Essential Oil on Neofusicoccum parvum in Chinese Chestnut

  • Tian-Tian Liu,
  • Lin-Jing Gou,
  • Hong Zeng,
  • Gao Zhou and ,
  • Wan-Rong Dong,
  • Yu Cui,
  • Qiang Cai and
  • Yu-Xin Chen
  • + 3 authors+ 0 author

The chestnut postharvest pathogen Neofusicoccum parvum (N. parvum) is an important postharvest pathogen that causes chestnut rot. Chestnut rot in postharvest reduces food quality and causes huge economic losses. This study aimed to evaluate the inhib...

(This article belongs to the Special Issue Separation, Extraction and Purification of Natural Products from Plants)
  • Article
  • Open Access
34 Citations
11,810 Views
24 Pages

This study analyses the concept of a novel multi-crystallization system to achieve zero liquid discharge (ZLD) for desalination plants using an innovative heat recovery system consisting of a heat transfer fluid and a compressor to reduce energy cons...

(This article belongs to the Special Issue Separation Technologies in Water and Wastewater Treatment and Resources Recovery)
  • Article
  • Open Access
6 Citations
2,731 Views
12 Pages

Phthalates are widely used in industry, but adverse effects on human health have been reported due to exposure to these chemicals. In the human body, they are metabolized into phthalic monoesters, which are used to monitor human exposure and assess r...

(This article belongs to the Section Materials in Separation Science)
  • Article
  • Open Access
2 Citations
3,007 Views
15 Pages

Development of Analytical Procedure for the Determination of 17β-Testosterone, 11-Ketotestosterone and 17β-Estradiol in the Sea Trout (Salmo trutta L.) Gonads

  • Iwona Matraszek-Żuchowska,
  • Alicja Kłopot,
  • Sebastian Witek,
  • Agnieszka Pękala-Safińska and
  • Andrzej Posyniak

Steroid hormones, such as 17β-testosterone, 11-ketotestorenone and 17β-estradiol, play an essential role not only in reproductive function but also are potential biomarkers of numerous additional functions in teleost fish. The presence of e...

(This article belongs to the Special Issue Chromatography-Mass Spectrometry Technology Research)
  • Article
  • Open Access
7 Citations
4,601 Views
19 Pages

Research on the sources of microplastics (MP) in the environment and the parameters that lead to the loss of microfibers from synthetic textiles during washing have recently attracted public attention. Considering the involvement of a variety of stru...

(This article belongs to the Section Environmental Separations)
  • Article
  • Open Access
44 Citations
6,977 Views
9 Pages

Retention Time Prediction with Message-Passing Neural Networks

  • Sergey Osipenko,
  • Eugene Nikolaev and
  • Yury Kostyukevich

Retention time prediction, facilitated by advances in machine learning, has become a useful tool in untargeted LC-MS applications. State-of-the-art approaches include graph neural networks and 1D-convolutional neural networks that are trained on the...

(This article belongs to the Section Chromatographic Separations)
  • Article
  • Open Access
11 Citations
11,184 Views
14 Pages

Cordycepin (3′-deoxyadenosine) is a potent bioactive metabolite of the medicinal fungus Cordyceps militaris, which has been increasingly exploited to treat various chronic diseases in humans. However, the current synthesis and purification proc...

(This article belongs to the Special Issue Separation, Extraction and Purification of Natural Products)
  • Article
  • Open Access
6 Citations
4,639 Views
18 Pages

Identification of Photodegradation Products of Escitalopram in Surface Water by HPLC-MS/MS and Preliminary Characterization of Their Potential Impact on the Environment

  • Veronica Termopoli,
  • Viviana Consonni,
  • Davide Ballabio,
  • Roberto Todeschini and ,
  • Marco Orlandi and
  • Fabio Gosetti
  • + 1 author+ 0 author

The study concerns the photodegradation of the antidepressant escitalopram (ESC), the S-enantiomer of the citalopram raceme, both in ultrapure and surface water, considering the contribution of indirect photolysis through the presence of nitrate and...

(This article belongs to the Section Environmental Separations)
  • Article
  • Open Access
2 Citations
2,073 Views
16 Pages

Increasing the Accuracy and Optimizing the Structure of the Scale Thickness Detection System by Extracting the Optimal Characteristics Using Wavelet Transform

  • Abdulilah Mohammad Mayet,
  • Tzu-Chia Chen,
  • Seyed Mehdi Alizadeh,
  • Ali Awadh Al-Qahtani and ,
  • Ramy Mohammed Aiesh Qaisi,
  • Hala H. Alhashim and
  • Ehsan Eftekhari-Zadeh
  • + 2 authors+ 0 author

Loss of energy, decrement of efficiency, and decrement of the effective diameter of the oil pipe are among the consequences of scale inside oil condensate transfer pipes. To prevent these incidents and their consequences and take timely action, it is...

(This article belongs to the Section Environmental Separations)
  • Article
  • Open Access
2 Citations
2,336 Views
11 Pages

A rapid and sensitive protein determination method that uses electromembrane extraction (EME) and is coupled with matrix-assisted laser desorption/ionization mass spectrometry (MALDI/MS) is developed. A flat nylon membrane is used to collect proteins...

(This article belongs to the Section Materials in Separation Science)
  • Article
  • Open Access
9 Citations
4,806 Views
16 Pages

The identification of isomeric drugs is gaining increasing importance in forensics and doping control. Isomers vary in terms of safety, effectiveness, and regulation, particularly for amphetamine-related drugs (ARDs). This study developed and validat...

  • Article
  • Open Access
2 Citations
2,815 Views
8 Pages

The Effect of Molecular Mass of Hydroxyethyl Cellulose on the Performance of Capillary Electrophoretic Separation of Proteins

  • Jiaxin Huang,
  • Chunxian Tao,
  • Zhenqing Li,
  • Erika Miyake and ,
  • Qingxiang You,
  • Wen Xiao,
  • Dawei Zhang and
  • Yoshinori Yamaguchi
  • + 3 authors+ 0 author

Capillary electrophoresis (CE) is a versatile analytical separation method in the field of biochemistry. Although it has been proved that the relative molecular mass (Mr) of the polymers determines the threshold concentration of the entangled polymer...

(This article belongs to the Section Chromatographic Separations)
  • Article
  • Open Access
32 Citations
4,911 Views
19 Pages

Efficient Removal of Eriochrome Black T Dye Using Activated Carbon of Waste Hemp (Cannabis sativa L.) Grown in Northern Morocco Enhanced by New Mathematical Models

  • Fouad El Mansouri,
  • Guillermo Pelaz,
  • Antonio Morán,
  • Joaquim C. G. Esteves Da Silva and ,
  • Francesco Cacciola,
  • Hammadi El Farissi,
  • Hatim Tayeq,
  • Mohammed Hassani Zerrouk and
  • Jamal Brigui
  • + 4 authors+ 0 author

In the present work, the adsorption behavior of Eriochrome Black T (EBT) on waste hemp activated carbon (WHAC) was examined. The surface of the WHAC was modified by H3PO4 acid treatment. The surface and structural characterization of the adsorbents w...

(This article belongs to the Special Issue Extraction and Analysis of Plant Active Ingredients)
  • Article
  • Open Access
6 Citations
2,286 Views
12 Pages

In the present study, a rapid, practical, selective and sensitive method was proposed for simultaneous determination of dopamine (DA) and uric acid (UA). Kinetic profiles of analytes were recorded and transformed by different mother wavelets. The con...

(This article belongs to the Special Issue Novel Applications of Separation Technology)
  • Communication
  • Open Access
6 Citations
2,548 Views
7 Pages

The purpose of this study was to simultaneously develop anti-hyperuricemic and anti-wrinkle source using Camellia japonica leaf (CJ). CJ extract was prepared. Its contents of biomarkers and biological activities were then analyzed. First, we investig...

(This article belongs to the Section Analysis of Food and Beverages)
  • Article
  • Open Access
24 Citations
6,429 Views
13 Pages

The Essential Oil Composition of Helichrysum italicum (Roth) G. Don: Influence of Steam, Hydro and Microwave-Assisted Distillation

  • Zvonimir Jažo,
  • Mateo Glumac,
  • Ivana Drventić,
  • Ljilja Žilić and ,
  • Tea Dujmović,
  • Danica Bajić,
  • Marko Vučemilo,
  • Ena Ivić,
  • Sanida Bektić and
  • Mila Radan
  • + 6 authors+ 1 author

Helichrysum italicum (Roth) G. Don (Asteraceae), also known as immortelle, usually grows in the Mediterranean area. The composition of the essential oil (EO) of immortelle is a mixture of various aromatic substances, mainly monoterpenes and sesquiter...

(This article belongs to the Special Issue Separation and Quantitative Analysis of Natural Product Extracts)
  • Article
  • Open Access
4 Citations
3,734 Views
19 Pages

Pinus roxburghii and Nauplius graveolens Extracts Elevate Apoptotic Gene Markers in C26 Colon Carcinoma Cells Induced in a BALB/c Mouse Model

  • Mosab Gad,
  • Hassan Z. Hassouna,
  • Khaled Mahmoud,
  • Ahmed A. Abd-Rabou and ,
  • Amal S. Abdel-Azeem,
  • Amany M. Hegazy,
  • Mohamed S. Abdel-Lattife,
  • Fouad A. Ahmed,
  • Fatih Oz and
  • Ahmed A. Zaky
  • + 6 authors+ 1 author

The present study aimed to evaluate the chemopreventive potential of Pinus roxburghii branch (P. roxburghii) and Nauplius graveolens (N. graveolens) extracts against human colorectal cancer (CRC) induced by C26 murine cells in a BALB/c mouse model. R...

(This article belongs to the Special Issue Novel Applications of Separation Technology)
  • Article
  • Open Access
5 Citations
2,262 Views
10 Pages

This study discusses the impact of two different ecological restoration approaches on the distribution of soil particle size and organic carbon, expecting to provide references for research on the effects of ecological restoration on the soil carbon...

(This article belongs to the Section Environmental Separations)
  • Article
  • Open Access
5 Citations
3,521 Views
16 Pages

Anti-Allergic and Antioxidant Potential of Polyphenol-Enriched Fractions from Cyclopia subternata (Honeybush) Produced by a Scalable Process

  • Carla Dippenaar,
  • Hitoshi Shimbo,
  • Kazunobu Okon,
  • Neil Miller and ,
  • Elizabeth Joubert,
  • Tadashi Yoshida and
  • Dalene de Beer
  • + 2 authors+ 0 author

Anti-allergic activity was previously demonstrated for extracts of Cyclopia subternata Vogel plant material, containing substantial amounts of xanthones, benzophenones, dihydrochalcones, flavanones and flavones. Fractionation of a hot water extract o...

(This article belongs to the Special Issue Isolation, Elucidation and Synthesis of Bioactive Natural Products)
  • Article
  • Open Access
7 Citations
3,640 Views
15 Pages

Integrated Electro-Ozonation and Fixed-Bed Column for the Simultaneous Removal of Emerging Contaminants and Heavy Metals from Aqueous Solutions

  • Amin Mojiri,
  • Noriatsu Ozaki,
  • John L. Zhou,
  • Reza Andasht Kazeroon and ,
  • Mohammad Ali Zahed,
  • Shahabaldin Rezania,
  • Mohammadtaghi Vakili,
  • Shahin Gavanji and
  • Hossein Farraji
  • + 4 authors+ 0 author

In the current study, an integrated physiochemical method was utilized to remove tonalide (TND) and dimethyl phthalate (DMP) (as emerging contaminants, ECs), and nickel (Ni) and lead (Pb) (as heavy metals), from synthetic wastewater. In the first ste...

(This article belongs to the Special Issue Separation Processes for Effective Removal of Emerging Contaminants from Water and Wastewater)
  • Article
  • Open Access
36 Citations
5,541 Views
12 Pages

Greenness Assessment of Chromatographic Methods Used for Analysis of Empagliflozin: A Comparative Study

  • Eman Y. Santali,
  • Ibrahim A. Naguib,
  • Abdullah M. Alshehri,
  • Yazeed A. Alzahrani and ,
  • Abdullah E. Alharthi,
  • Turki S. Alosaimi,
  • Bandar D. Alsayali,
  • Izzeddin Alsalahat,
  • Albandary Almahri and
  • Fatma F. Abdallah
  • + 6 authors+ 1 author

The analytical chemistry community is attempting to incorporate green chemistry concepts in the development of analytical techniques to redefine analytical methods and dramatically modify the philosophy of analytical technique development. Each green...

(This article belongs to the Section Analysis of Natural Products and Pharmaceuticals)
  • Article
  • Open Access
12 Citations
3,446 Views
19 Pages

Recovery of Palladium and Gold from PGM Ore and Concentrates Using ZnAl-Layered Double Hydroxide@zeolitic Imidazolate Framework-8 Nanocomposite

  • Nkositetile Raphael Biata,
  • Silindokuhle Jakavula,
  • Anele Mpupa,
  • Richard M. Moutloali and
  • Philiswa Nosizo Nomngongo

30 September 2022

Gold (Au) and palladium (Pd) are platinum group metals (PGMs) that are considered critical in society because they are required in several industrial applications. Their shortage has caused the urgent need for their recovery from secondary resources....

(This article belongs to the Special Issue Separation Technologies in Water and Wastewater Treatment and Resources Recovery)

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Separations - ISSN 2297-8739