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114 Results Found

  • Article
  • Open Access
36 Citations
8,592 Views
11 Pages

A Gas Chromatographic System for the Detection of Ethylene Gas Using Ambient Air as a Carrier Gas

  • Nayyer Abbas Zaidi,
  • Muhammad Waseem Tahir,
  • Michael J. Vellekoop and
  • Walter Lang

7 October 2017

Ethylene gas is a naturally occurring gas that has an influence on the shelf life of fruit during their transportation in cargo ships. An unintentional exposure of ethylene gas during transportation results in a loss of fruit. A gas chromatographic s...

  • Article
  • Open Access
16 Citations
4,955 Views
11 Pages

7 August 2018

In this paper, a novel ceramic preconcentrator is manufactured using aluminum nitride (ALN) ceramics. The preconcentrator consists of a heater, a preconcentrator body, a gas inlet and a gas outlet. The adsorption material, Carbosieve SII, is loaded i...

  • Article
  • Open Access
24 Citations
5,683 Views
7 Pages

17 August 2018

In this work, a mini monitoring system integrated with a microfabricated metal oxide array sensor and a micro packed gas chromatographic (GC) column was developed for monitoring environmental gases. The microfabricated packed GC column with a 1.6 m l...

  • Letter
  • Open Access
6 Citations
5,461 Views
12 Pages

Low-Cost Benzene Toluene Xylene Measurement Gas System Based on the Mini Chromatographic Cartridge

  • Emiliano Zampetti,
  • Paolo Papa,
  • Joshua Avossa,
  • Andrea Bearzotti,
  • Catia Balducci,
  • Giovanna Tranfo and
  • Antonella Macagnano

28 December 2020

Benzene, toluene and xylene (BTX) are an important part of the volatile organic compounds (VOCs) to be detected and monitored in the air, due to their toxicity towards human health. One of the most reliable technique used in BTX detection is gas chro...

  • Article
  • Open Access
2 Citations
6,851 Views
12 Pages

27 February 2013

Static headspace gas chromatographic (SHS-GC) analysis was performed to determine the release of 13 odorants in hydrocolloid model systems containing original or regio-selectively carboxylated cellulose at different pH values. The release of most od...

  • Article
  • Open Access
5 Citations
3,477 Views
11 Pages

Fast Sampling Field Deployable Mud Gas Carbon Isotope Analyzer

  • Sheng Wu,
  • Andrei Deev,
  • Yan Zhuang,
  • Le Lu,
  • Zhengyou Wang,
  • Yongchun Tang and
  • Andrew Sneddon

4 September 2020

We report the details of a field deployable mud gas carbon isotope analyzer for mud gas analysis based on coupling a gas chromatograph with a mid-infrared spectrometer using a quantum cascade laser and hollow waveguide. The GC–IR2 (gas chromatograph–...

  • Article
  • Open Access
70 Citations
7,976 Views
16 Pages

Development of an Exhaled Breath Monitoring System with Semiconductive Gas Sensors, a Gas Condenser Unit, and Gas Chromatograph Columns

  • Toshio Itoh,
  • Toshio Miwa,
  • Akihiro Tsuruta,
  • Takafumi Akamatsu,
  • Noriya Izu,
  • Woosuck Shin,
  • Jangchul Park,
  • Toyoaki Hida,
  • Takeshi Eda and
  • Yasuhiro Setoguchi

10 November 2016

Various volatile organic compounds (VOCs) in breath exhaled by patients with lung cancer, healthy controls, and patients with lung cancer who underwent surgery for resection of cancer were analyzed by gas condenser-equipped gas chromatography-mass sp...

  • Article
  • Open Access
8 Citations
4,076 Views
15 Pages

Polymeric Ionic Liquids Derived from L-Valine for the Preparation of Highly Selective Silica-Supported Stationary Phases in Gas Chromatography

  • Jorge González-Rodríguez,
  • Adriana Valls,
  • Pilar Arias Abrodo,
  • María Dolores Gutiérrez Álvarez,
  • Jaime González-Álvarez,
  • Belén Altava and
  • Santiago V. Luis

14 October 2020

A series of silica-supported polymeric ionic liquid (PIL)-based stationary phases derived from a vinylic L-valine ionic liquid monomer and divinylbenzene (DVB) as the crosslinking agent have been prepared and studied as gas chromatographic stationary...

  • Abstract
  • Open Access
1,264 Views
3 Pages

Efficient Methods for Training and Validation of Odor Sensors

  • Gina Zeh,
  • Maximilian Koehne and
  • Tilman Sauerwald

The correlation between a gas sensor pattern and its corresponding odor impression on human noses remains a scientific challenge for the development of technical odor detection systems. Small, inexpensive gas sensors, for example, those based on a me...

  • Article
  • Open Access
6 Citations
4,311 Views
16 Pages

Every human body is a source of a unique scent, which can be used for medical or forensic purposes. Human skin scent is a complex mixture of more or less volatile compounds with different chemical and physical properties, which often differ significa...

  • Article
  • Open Access
1,710 Views
13 Pages

11 October 2024

The essential oil components of traditional Chinese medicine in-hospital preparation were complex, and one-dimensional chromatographic separation was difficult to completely separate them due to the limited peak capacity. This study was carried out t...

  • Proceeding Paper
  • Open Access
1,636 Views
5 Pages

Novel Methodology Based on Thick Film Gas Sensors to Monitor the Hydraulic Oil Ageing

  • Ambra Fioravanti,
  • Antonino Bonanno,
  • Maria Cristina Carotta,
  • Giorgio Paolo Massarotti,
  • Sara Morandi,
  • Nicolò Riboni and
  • Federica Bianchi

10 December 2018

A new methodology for the real time monitoring of hydraulic oil aging based on the vapor analysis using metal oxide semiconductor (MOX) gas sensors has been successfully developed. A dedicated hydraulic test bench was designed and realized to age the...

  • Review
  • Open Access
31 Citations
8,107 Views
27 Pages

Recent Advances in Ethylene Gas Detection

  • Xiaohu Chen,
  • Ryan Wreyford and
  • Noushin Nasiri

23 August 2022

The real-time detecting and monitoring of ethylene gas molecules could benefit the agricultural, horticultural and healthcare industries. In this regard, we comprehensively review the current state-of-the-art ethylene gas sensors and detecting techno...

  • Article
  • Open Access
35 Citations
9,101 Views
15 Pages

Kinetics of the Formation and Dissociation of Gas Hydrates from CO2-CH4 Mixtures

  • Kristine Horvat,
  • Prasad Kerkar,
  • Keith Jones and
  • Devinder Mahajan

6 July 2012

Sequestration of carbon dioxide (CO2) in the form of its hydrates in natural methane (CH4) hydrate reservoirs, via CO2/CH4 exchange, is an attractive pathway that also yields valuable CH4 gas as product. In this paper, we describe a macroscale experi...

  • Article
  • Open Access
4 Citations
3,723 Views
11 Pages

12 August 2020

Considering the adverse effects of gasoline additives and aromatic compounds on the quality of the water supply and the ecological environment of the water, a methodology, with short chromatographic separation time (22.5 min) and high separation qual...

  • Article
  • Open Access
3,177 Views
11 Pages

25 April 2022

The phenomenon of abnormal CO emergence occurred in a working face of Tangshan mine, and the CO source was analyzed from the two perspectives of CO detection method optimization and microstructure changes in the low-temperature environment of the coa...

  • Article
  • Open Access
2 Citations
2,767 Views
18 Pages

23 June 2022

Multidimensional gas chromatography is, presently, an established and powerful analytical tool, due to higher resolving power than the classical 1D chromatographic approaches. Applied to multiple areas, it allows to isolate, detect and identify a lar...

  • Article
  • Open Access
18 Citations
6,256 Views
26 Pages

In the last few years, the flavored beer market has increased significantly. In particular, consumers showed a growing interest in citrus-flavored beers. Citrus fruits contain, among other class of compounds, terpenes and terpenoids and oxygenated he...

  • Article
  • Open Access
7 Citations
4,611 Views
14 Pages

High-Pressure and Automatized System for Study of Natural Gas Hydrates

  • Luiz F. Rodrigues,
  • Alessandro Ramos,
  • Gabriel de Araujo,
  • Edson Silveira,
  • Marcelo Ketzer and
  • Rogerio Lourega

9 August 2019

Due to the declining of oil reserves in the world in the coming decades, gas hydrate (GH) is seen as the great promise to supply the planet’s energy demand. With this, the importance of studying the behavior of GH, several researchers have been...

  • Article
  • Open Access
4 Citations
2,946 Views
16 Pages

29 September 2021

Biohydrogen production in small laboratory scale culture vessels is often difficult to perform and quantitate. One problem is that commonly used silicon tubing and improvised plastic connections used for constructing apparatus are cheap and easy to c...

  • Article
  • Open Access
9 Citations
1,807 Views
14 Pages

17 November 2023

During the depletion development of condensate gas reservoirs, when the formation pressure drops below the dew point pressure, the condensate oil and natural gas systems are in the non-equilibrium state of foggy retrograde condensation. The rational...

  • Article
  • Open Access
40 Citations
5,590 Views
24 Pages

High-Performance VOC Quantification for IAQ Monitoring Using Advanced Sensor Systems and Deep Learning

  • Yannick Robin,
  • Johannes Amann,
  • Tobias Baur,
  • Payman Goodarzi,
  • Caroline Schultealbert,
  • Tizian Schneider and
  • Andreas Schütze

10 November 2021

With air quality being one target in the sustainable development goals set by the United Nations, accurate monitoring also of indoor air quality is more important than ever. Chemiresistive gas sensors are an inexpensive and promising solution for the...

  • Article
  • Open Access
18 Citations
5,605 Views
17 Pages

10 September 2021

Pesticides have been used to control pests in agricultural fields and storage systems before circulating agricultural products to markets. A tandem mass spectrometry, equipped with gas chromatographic separation (GC–MS/MS) or ultra-performance liquid...

  • Article
  • Open Access
28 Citations
4,879 Views
26 Pages

24 August 2022

Taking into account the international policies in the field of environmental protection in the world in general, and in the European Union in particular, the reduction of greenhouse gas (GHG) emissions, and primarily of carbon dioxide, has become one...

  • Proceeding Paper
  • Open Access
2 Citations
2,684 Views
4 Pages

Microscale Gas Chromatography with Microsensor Array Detection: Challenges and Prospects

  • Junqi Wang,
  • Nicolas Nuñovero,
  • Changhua Zhan,
  • Robert Nidetz,
  • William H. Steinecker,
  • Seth J. Peterson,
  • Bryan M. Brookover and
  • Edward T. Zellers

The capability to analyze complex mixtures of airborne volatile organic compounds (VOCs) at low concentrations; in situ; has implications for environmental monitoring; worker exposure assessment; biomedical diagnostics; and population security. Since...

  • Article
  • Open Access
1 Citations
2,244 Views
14 Pages

Measurement Uncertainty in the Totalisation of Quantity and Energy Measurement in Gas Grids

  • Adriaan M. H. van der Veen,
  • Kjetil Folgerø and
  • Federica Gugole

3 April 2025

The total quantity and energy delivered through a gas grid is calculated using simple formulæ that sum the increments measured at regular time intervals. These calculations are described in international standards (e.g., ISO 15112 and EN 1776)...

  • Article
  • Open Access
8 Citations
7,802 Views
17 Pages

Long-Term Outdoor Reliability Assessment of a Wireless Unit for Air-Quality Monitoring Based on Nanostructured Films Integrated on Micromachined Platforms

  • Matteo Leccardi,
  • Massimiliano Decarli,
  • Leandro Lorenzelli,
  • Paolo Milani,
  • Petteri Mettala,
  • Risto Orava and
  • Emanuele Barborini

13 June 2012

We have fabricated and tested in long-term field operating conditions a wireless unit for outdoor air quality monitoring. The unit is equipped with two multiparametric sensors, one miniaturized thermo-hygrometer, front-end analogical and digital elec...

  • Article
  • Open Access
1 Citations
1,910 Views
21 Pages

Optimizing Low-Cost Gas Analysis with a 3D Printed Column and MiCS-6814 Sensor for Volatile Compound Detection

  • Nela Skowronkova,
  • Martin Adamek,
  • Magdalena Zvonkova,
  • Jiri Matyas,
  • Anna Adamkova,
  • Stepan Dlabaja,
  • Martin Buran,
  • Veronika Sevcikova,
  • Jiri Mlcek and
  • Martina Cernekova
  • + 1 author

13 October 2024

This paper explores an application of 3D printing technology on the food industry. Since its inception in the 1980s, 3D printing has experienced a huge rise in popularity. This study uses cost-effective, flexible, and sustainable components that enab...

  • Article
  • Open Access
1 Citations
1,734 Views
14 Pages

Optimizing a Hydrogen and Methane Blending System Through Design and Simulation

  • Ştefan Ionuţ Spiridon,
  • Bogdan Florian Monea and
  • Eusebiu Ilarian Ionete

10 April 2025

Hydrogen–methane gas mixtures are increasingly recognized as a viable path toward achieving carbon neutrality, leveraging existing natural gas infrastructure while reducing greenhouse gas emissions. This study investigates a novel static mixing...

  • Article
  • Open Access
15 Citations
6,196 Views
18 Pages

Characterizing the Performance of a Compact BTEX GC-PID for Near-Real Time Analysis and Field Deployment

  • Isis Frausto-Vicencio,
  • Alondra Moreno,
  • Hugh Goldsmith,
  • Ying-Kuang Hsu and
  • Francesca M. Hopkins

17 March 2021

In this study, we test the performance of a compact gas chromatograph with photoionization detector (GC-PID) and optimize the configuration to detect ambient (sub-ppb) levels of benzene, toluene, ethylbenzene, and xylene isomers (BTEX). The GC-PID sy...

  • Article
  • Open Access
12 Citations
5,102 Views
14 Pages

A MEMS-Enabled Deployable Trace Chemical Sensor Based on Fast Gas-Chromatography and Quartz Enhanced Photoacousic Spectoscopy

  • Stefano Zampolli,
  • Sandro Mengali,
  • Nicola Liberatore,
  • Ivan Elmi,
  • Luca Masini,
  • Michele Sanmartin and
  • Roberto Viola

24 December 2019

This paper reports on a portable selective chemical sensor for hazardous vapors at trace levels, which combines a two-stage purge and trap vapor pre-concentration system, a Micro-Electro-Mechanical-System (MEMS) based fast gas-chromatographic (FAST-G...

  • Article
  • Open Access
16 Citations
3,761 Views
16 Pages

Two-in-One Sensor Based on PV4D4-Coated TiO2 Films for Food Spoilage Detection and as a Breath Marker for Several Diseases

  • Mihai Brinza,
  • Stefan Schröder,
  • Nicolai Ababii,
  • Monja Gronenberg,
  • Thomas Strunskus,
  • Thierry Pauporte,
  • Rainer Adelung,
  • Franz Faupel and
  • Oleg Lupan

11 May 2023

Certain molecules act as biomarkers in exhaled breath or outgassing vapors of biological systems. Specifically, ammonia (NH3) can serve as a tracer for food spoilage as well as a breath marker for several diseases. H2 gas in the exhaled breath can be...

  • Article
  • Open Access
4 Citations
1,736 Views
17 Pages

20 November 2024

Large-scale underground hydrogen storage (UHS) is a critical component in the emerging hydrogen economy. Knowledge of multiphase flow behavior involving hydrogen in storage reservoir formations is crucial to characterizing hydrogen transport properti...

  • Review
  • Open Access
24 Citations
8,553 Views
22 Pages

Plastic particles smaller than 5 mm accumulate in aqueous, terrestrial, and atmospheric environments and their discovery has been a serious concern when it comes to eco-toxicology and human health risk assessment. In the following review, the potenti...

  • Article
  • Open Access
7 Citations
3,230 Views
23 Pages

12 July 2023

Procedures for determination of the residual solvent and volatile impurity content in pharmaceutical products usually rely on dissolution in a solvent, followed by headspace-gas chromatography (HS-GC) analysis. Whereas chromatographic systems can uti...

  • Article
  • Open Access
9 Citations
6,665 Views
13 Pages

Development of an Atmospheric Pressure Chemical Ionization Interface for GC-MS

  • Christian Lipok,
  • Florian Uteschil and
  • Oliver J. Schmitz

16 July 2020

A closed atmospheric pressure chemical ionization (APCI) ion source as interface between a gas chromatograph (GC) and a triple quadrupole mass spectrometer (QqQ-MS) was developed. The influence of different ion source conditions, such as humidity, ma...

  • Article
  • Open Access
8 Citations
4,413 Views
13 Pages

Evaluation of the SOA Formation in the Reaction of Furfural with Atmospheric Oxidants

  • Inmaculada Colmenar,
  • Pilar Martín,
  • Beatriz Cabañas,
  • Sagrario Salgado,
  • Florentina Villanueva and
  • Bernabe Ballesteros

30 August 2020

An experimental product study of the reactions of furfural with the main tropospheric oxidants (Cl, OH and NO3) has been carried out using a Fourier Transform Infrared spectrophotometer (FTIR) and a gas chromatograph–mass spectrometer with a ti...

  • Article
  • Open Access
12 Citations
3,709 Views
12 Pages

Compact GC-QEPAS for On-Site Analysis of Chemical Threats

  • Nicola Liberatore,
  • Roberto Viola,
  • Sandro Mengali,
  • Luca Masini,
  • Federico Zardi,
  • Ivan Elmi and
  • Stefano Zampolli

27 December 2022

This paper reports on a compact, portable, and selective chemical sensor for hazardous vapors at trace levels, which is under development and validation within the EU project H2020 “RISEN”. Starting from the prototype developed for a prev...

  • Article
  • Open Access
1 Citations
1,109 Views
11 Pages

The Impact of Selected Eutectic Solvents on the Volatile Composition of Citrus lemon Essential Oil

  • Giacomo Luigi Petretto,
  • Andrea Mele,
  • Giorgio Pintore and
  • Alberto Mannu

30 October 2024

The development of new materials for the controlled release of molecules represents a topic of primary importance in medicine, as well as in food science. In recent years, eutectic solvents have been applied as releasing media due to their improved c...

  • Article
  • Open Access
14 Citations
3,463 Views
9 Pages

Diurnal Tree Stem CH4 and N2O Flux Dynamics from a Riparian Alder Forest

  • Thomas Schindler,
  • Katerina Machacova,
  • Ülo Mander,
  • Jordi Escuer-Gatius and
  • Kaido Soosaar

30 June 2021

Tree stems play an important role in forest methane (CH4) and nitrous oxide (N2O) flux dynamics. Our paper aimed to determine the unknown diurnal variability of CH4 and N2O exchange in grey alder tree stems. The gas fluxes in tree stems and adjacent...

  • Article
  • Open Access
8 Citations
3,371 Views
13 Pages

26 October 2019

We applied a thermal-desorption gas-chromatograph mass-spectrometer (TD-GC–MS) system to identify the marker volatile organic compounds (VOCs) in the aroma of red wine. After obtaining the marker VOC, we utilized surface acoustic waves (SAWs) t...

  • Review
  • Open Access
7 Citations
4,165 Views
16 Pages

Condensed Phase Membrane Introduction Mass Spectrometry: A Direct Alternative to Fully Exploit the Mass Spectrometry Potential in Environmental Sample Analysis

  • Veronica Termopoli,
  • Maurizio Piergiovanni,
  • Davide Ballabio,
  • Viviana Consonni,
  • Emmanuel Cruz Muñoz and
  • Fabio Gosetti

17 February 2023

Membrane introduction mass spectrometry (MIMS) is a direct mass spectrometry technique used to monitor online chemical systems or quickly quantify trace levels of different groups of compounds in complex matrices without extensive sample preparation...

  • Article
  • Open Access
12 Citations
6,005 Views
12 Pages

The gas chromatographic retention behaviour of 16 polycyclic aromatic hydrocarbons (PAHs) and alkylated PAHs on a new ionic liquid stationary phase, 1,12-di(tripropylphosphonium) dodecane bis(trifluoromethanesulfonyl)imide (SLB®-ILPAH) intended f...

  • Article
  • Open Access
44 Citations
9,762 Views
8 Pages

CuO Nanorods-Decorated Reduced Graphene Oxide Nanocatalysts for Catalytic Oxidation of CO

  • Yan Wang,
  • Zhihui Wen,
  • Huoli Zhang,
  • Guohua Cao,
  • Qi Sun and
  • Jianliang Cao

21 December 2016

Developing an efficient non-noble catalyst for CO oxidation with high catalytic activity remains a challenge for practical applications. In this work, CuO nanorods decorated reduced graphene oxide (RGO) nanocatalysts were prepared via a facile one-st...

  • Article
  • Open Access
6 Citations
3,291 Views
13 Pages

In recent years, nuclear medicine has gained great interest, partly due to the success story of [177Lu]Lu-PSMA-617 (PluvictoTM). Still, in-depth preclinical characterization of radiopharmaceuticals mainly happens at centers that allow working with ra...

  • Article
  • Open Access
5 Citations
3,971 Views
29 Pages

26 May 2022

Understanding the phase behaviour of (CO2 + water + permanent gas) systems is critical for implementing carbon capture and storage (CCS) processes, a key technology in reducing CO2 emissions. In this paper, phase behaviour data for (H2O + N2) and (CO...

  • Feature Paper
  • Article
  • Open Access
1 Citations
1,525 Views
15 Pages

26 October 2024

To eliminate the problem of the aging of cellulose insulation in the manufacturing stage, a new drying method is being developed based on the use of methanol vapors. Previous studies have shown that the complete removal of methanol from the cellulose...

  • Article
  • Open Access
1 Citations
1,620 Views
17 Pages

Exploitation and Utilization of Generated Oil and Gas by Pyrolysis Simulation Modeling of Shale Source Rocks under the Condition of In Situ Conversion

  • Xia Luo,
  • Lianhua Hou,
  • Zhongying Zhao,
  • Senhu Lin,
  • Zhenglian Pang,
  • Lijun Zhang,
  • Wenxue Han and
  • Yong Li

3 January 2024

Previous studies have mainly focused on the source rocks of the 7th Member of Yanchang Formation (Chang 7 Member) in the Ordos Basin, with very few studies focusing on the extracts from the source rocks. These extracts have important guiding signific...

  • Article
  • Open Access
23 Citations
6,777 Views
13 Pages

Unmasking of Olive Oil Adulteration Via a Multi-Sensor Platform

  • Marco Santonico,
  • Simone Grasso,
  • Francesco Genova,
  • Alessandro Zompanti,
  • Francesca Romana Parente and
  • Giorgio Pennazza

31 August 2015

Methods for the chemical and sensorial evaluation of olive oil are frequently changed and tuned to oppose the increasingly sophisticated frauds. Although a plethora of promising alternatives has been developed, chromatographic techniques remain the m...

  • Article
  • Open Access
4 Citations
3,436 Views
14 Pages

18 January 2021

This paper reports a multi-valve module with high chemical inertness and embedded flow heating for microscale gas chromatography (µGC) systems. The multi-valve module incorporates a monolithically microfabricated die stack, polyimide valve memb...

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