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Materials

Materials is an international peer-reviewed, open access journal on materials science and engineering published semimonthly online by MDPI.
The Spanish Materials Society (SOCIEMAT), Manufacturing Engineering Society (MES) and Chinese Society of Micro-Nano Technology (CSMNT) are affiliated with Materials and their members receive discounts on the article processing charges.
Indexed in PubMed | Quartile Ranking JCR - Q2 (Metallurgy and Metallurgical Engineering | Physics, Applied | Physics, Condensed Matter)

All Articles (54,143)

Porosity formation due to solidification shrinkage and inadequate liquid metal feeding during the casting of Sn-0.3Ag-0.7Cu (SAC0307) is a critical issue that impairs quality and subsequent processing. However, the opacity of the casting process often obscures the quantitative relationships between process parameters and defect formation, creating a significant barrier to science-based optimization. To address this, the present study utilizes finite element method (FEM) analysis to systematically investigate the influence of pouring temperature (PCT, 290–390 °C) and interfacial heat transfer coefficient (HTC, 900–5000 W/(m2·K)) on this phenomenon. The results reveal that PCT exerts a non-monotonic effect on porosity by modulating the solidification mode, which governs the accumulation of dispersed microporosity. In contrast, HTC plays a critical role in determining porosity morphology by controlling both the solidification rate and mode. Consequently, an optimal processing window was identified at 350 °C PCT and 3000 W/(m2·K) HTC, which significantly enhances interdendritic feeding and improves the ingot’s internal soundness. The efficacy of these optimized parameters was experimentally validated through macro- and microstructural characterization. This work not only elucidates the governing mechanisms of solidification quality but also demonstrates the value of numerical simulation for process optimization, offering a reliable scientific basis for the industrial production of high-quality SAC0307 alloys.

5 January 2026

Three-dimensional (3D) model and volume mesh discretization of the casting system: (a) geometric setup, (b) mold volume mesh, (c) casting volume mesh, (d) heat transfer interfaces.

Fibres can markedly enhance the uniaxial compressive strength (UCS) of cemented paste backfill (CPB). However, previous studies have mainly verified the effectiveness of polypropylene and straw fibres in improving the UCS of CPB experimentally, while systematic multi-factor evaluation remains limited. In this study, laboratory experiments were conducted on polypropylene- and straw fibre-reinforced CPB to construct a reliable dataset. The factors influencing the intensity of uniaxial compressive strength were divided into four aspects (mixture proportions, physical properties of the cement–tailings mixture, chemical characteristics of tailings, and fibre properties), and four intelligent models were developed for effectiveness analysis and UCS prediction. SHapley Additive exPlanations (SHAP) were employed to quantify the contributions of individual features, and the findings were experimentally validated. The GWO–LGBM model outperformed the SVR, ANN, and LGBM models, achieving R2 = 0.907, RMSE = 0.78, MAE = 0.515, and MAPE = 0.157 for the training set, and R2 = 0.949, RMSE = 0.627, MAE = 0.38, and MAPE = 0.115 for the testing set, respectively. Feature analysis reveals that mixture proportions contribute the most to UCS, followed by the tailings’ physical properties, the fibre properties, and the tailings’ chemical characteristics. This study found that cement content and tailings gradation control CPB structural compactness and fibres enhance bonding between hydration products and tailings aggregates, while the chemical composition of the tailings plays an inert role, functioning mainly as an aggregate.

5 January 2026

Particle size distribution of cement and tailings.

Improper disposal of granite sawdust from stone processing and heavy metal-containing tailings sand can pose severe threats to the environment and human health. Based on their physicochemical properties, granite sawdust was used to synthesize a zeolite-based stabilizer (GFAS) for immobilizing lead (Pb) and zinc (Zn) in tailings waste. The stabilizer was prepared through an alkali fusion–hydrothermal method, followed by phosphoric acid modification. Characterization by XRD, SEM-EDS, and BET revealed that GFAS possesses a Na-P1 zeolite structure (Na6Al6Si10O32) with a micro-mesoporous texture and a specific surface area of 35.00 m2/g, representing a 10-fold increase over raw sawdust. The cation exchange capacity (CEC) of GFAS reached 57.08 cmol+/kg, a 116-fold enhancement. The stabilization mechanism involved synergistic physical adsorption, chemical precipitation (e.g., Pb3(PO4)2, Zn(OH)2), and ion exchange. This study presents a sustainable “waste-treats-waste” strategy for effectively reducing the mobility of heavy metals in tailings waste, thereby contributing to the remediation of seepage from tailings pond foundations.

5 January 2026

Application of granite sawdust in various fields.

Ultra-High-Performance Concrete (UHPC) is being increasingly utilized in major engineering projects due to its excellent mechanical properties, strong durability, and superior overall performance. Nevertheless, the widespread use of premium cementitious materials leads to high expenses and a substantial environmental impact. In this work, crushed recycled paste was calcined at 600 °C for two hours to produce calcined recycled fine powder (RFP) with varying hydration reactivity. UHPC was produced using the RFP in place of some of the cement. Chemical activation was accomplished by adding a composite activator system made up of Ca(OH)2, Na2SO4, Na2SiO3·9H2O, and K2SO4 in order to further improve the performance of UHPC. Particle size, viscosity, fluidity, mechanical properties, and hydration products were analyzed to establish the best activator type and dosage, as well as the ideal activation procedure for recycled fine powder. By mass replacement of cementitious materials, when 15.0% of the calcined recycled fine powder was added, the compressive strength of UHPC reached 149.1 MPa, a 23.2% increase over reference UHPC without calcined recycled fine powder. The results show that the calcined recycled fine powder ground for 60 min exhibits the highest activity. More hydrated products were formed in UHPC as a result of the addition of Ca(OH)2. The compressive strength peaked at 162.2 MPa at an incorporation rate of 1.5%, which is 8.8% higher than UHPC without an activator.

5 January 2026

Particle size distribution of raw material.

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Materials - ISSN 1996-1944