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3,102 Results Found

  • Article
  • Open Access
586 Views
18 Pages

5 November 2025

This study investigates the pyrolysis behavior of tung seed shells (TSSs), an underutilized lignocellulosic residue from Vernicia fordii, using thermogravimetric analysis (TGA) and in situ TG–FTIR spectroscopy. The thermal decomposition process...

  • Article
  • Open Access
9 Citations
2,608 Views
15 Pages

18 February 2022

The article analyzes the thermal degradation in the inert and oxidative atmosphere of waste vinyl panels, the main component of which is PVC. Both pyrolysis and incineration of plastic waste are difficult, complex and multifaceted processes due to se...

  • Article
  • Open Access
64 Citations
5,502 Views
15 Pages

26 February 2021

Recently, the pyrolysis process has been adapted as a sustainable strategy to convert metallized food packaging plastics waste (MFPW) into energy products (paraffin wax, biogas, and carbon black particles) and to recover aluminum. Usually, catalysts...

  • Article
  • Open Access
14 Citations
4,332 Views
11 Pages

Chip-Based MEMS Platform for Thermogravimetric/Differential Thermal Analysis (TG/DTA) Joint Characterization of Materials

  • Wenhan Zhou,
  • Xinyu Li,
  • Fanglan Yao,
  • Haozhi Zhang,
  • Ke Sun,
  • Fang Chen,
  • Pengcheng Xu and
  • Xinxin Li

16 March 2022

Combined use of thermal analysis techniques can realize complementarity of different characterization methods. Comprehensive thermal analysis with both thermogravimetric analysis and differential thermal analysis (TG/DTA) can measure not only mass ch...

  • Article
  • Open Access
643 Views
16 Pages

Evolved Gas Analysis of Waste Polypropylene, Cardboard, Wood Biomass and Their Blends: A TG–FTIR Approach

  • Martinson Joy Dadson Bonsu,
  • Md Sydur Rahman,
  • Lachlan H. Yee,
  • Ernest Du Toit,
  • Graeme Palmer and
  • Shane McIntosh

4 December 2025

In this study, the evolved gas analysis of polypropylene (PP), mixed wood biomass (WB), cardboard (CB), and their blends was investigated using a coupled thermo-gravimetric analysis–Fourier transform infrared spectroscopy (TG–FTIR) approa...

  • Article
  • Open Access
9 Citations
8,387 Views
15 Pages

Uncertainty Determination Methodology, Sampling Maps Generation and Trend Studies with Biomass Thermogravimetric Analysis

  • Jose A. Pazó,
  • Enrique Granada,
  • Ángeles Saavedra,
  • Pablo Eguía and
  • Joaquín Collazo

28 September 2010

This paper investigates a method for the determination of the maximum sampling error and confidence intervals of thermal properties obtained from thermogravimetric analysis (TG analysis) for several lignocellulosic materials (ground olive stone, almo...

  • Article
  • Open Access
2 Citations
1,214 Views
20 Pages

10 March 2025

This study investigated the influence of particle size on combustion performance using equivalent characteristic spectrum analysis (ECSA) on a TG-MS platform. The experiments were conducted at heating rates of 10 °C/min and 20 °C/min for thre...

  • Article
  • Open Access
13 Citations
10,380 Views
14 Pages

Biomass Thermogravimetric Analysis: Uncertainty Determination Methodology and Sampling Maps Generation

  • Jose A. Pazó,
  • Enrique Granada,
  • Ángeles Saavedra,
  • Pablo Eguía and
  • Joaquín Collazo

15 July 2010

The objective of this study was to develop a methodology for the determination of the maximum sampling error and confidence intervals of thermal properties obtained from thermogravimetric analysis (TG), including moisture, volatile matter, fixed carb...

  • Article
  • Open Access
93 Citations
6,420 Views
16 Pages

21 June 2019

Thermal decomposition of solids often includes simultaneous occurrence of the overlapping processes with unequal contributions in a specific physical quantity variation during the overall reaction (e.g., the opposite effects of decomposition and evap...

  • Article
  • Open Access
30 Citations
6,970 Views
13 Pages

30 January 2017

A thickness gradient interpenetrating polymer network (IPN) was easily created that takes advantage of the relatively poor compatibility and curing rates discrepancy between epoxy (EP) and polyurethane (PU). Ultraviolet absorption spectrum (UV-Vis),...

  • Feature Paper
  • Article
  • Open Access
12 Citations
4,250 Views
10 Pages

Thermal Behavior and Structural Study of SiO2/Poly(ε-caprolactone) Hybrids Synthesized via Sol-Gel Method

  • Stefano Vecchio Ciprioti,
  • Riccardo Tuffi,
  • Alessandro Dell’Era,
  • Francesco Dal Poggetto and
  • Flavia Bollino

10 February 2018

SiO2-based organic-inorganic hybrids (OIHs) are versatile materials whose properties may change significantly because of their thermal treatment. In fact, after their preparation at low temperature by the sol-gel method, they still have reactive sila...

  • Article
  • Open Access
3 Citations
2,556 Views
16 Pages

17 June 2022

New heterotrinuclear complexes with the general formula [Cu2Ln(H2L)(HL)(NO3)2]·MeOH (Ln = Ho (1), Er (2), H4L = N,N′-bis(2,3-dihydroxybenzylidene)-1,3-diaminopropane) were synthesized using compartmental Schiff base ligand in conjugation...

  • Article
  • Open Access
54 Citations
5,560 Views
18 Pages

Pyrolysis Kinetic Behaviour of Glass Fibre-Reinforced Epoxy Resin Composites Using Linear and Nonlinear Isoconversional Methods

  • Samy Yousef,
  • Justas Eimontas,
  • Nerijus Striūgas,
  • Marius Praspaliauskas and
  • Mohammed Ali Abdelnaby

11 May 2021

Due to the increasing demand for glass fibre-reinforced epoxy resin composites (GFRC), huge amounts of GFRC waste are produced annually in different sizes and shapes, which may affect its thermal and chemical decomposition using pyrolysis technology....

  • Article
  • Open Access
205 Views
14 Pages

28 February 2026

Background/Objectives: This study aimed to evaluate the predictive value of the triglyceride-glucose index with body mass index (TyG-BMI) and the triglyceride-to-high-density lipoprotein-cholesterol (TG/HDL-C) ratio for predicting the occurrence of m...

  • Article
  • Open Access
36 Citations
6,327 Views
15 Pages

Microglial Activation in the Retina of a Triple-Transgenic Alzheimer’s Disease Mouse Model (3xTg-AD)

  • Elena Salobrar-García,
  • Ana C. Rodrigues-Neves,
  • Ana I. Ramírez,
  • Rosa de Hoz,
  • José A. Fernández-Albarral,
  • Inés López-Cuenca,
  • José M. Ramírez,
  • António F. Ambrósio and
  • Juan J. Salazar

Alzheimer’s disease (AD) is the most common type of dementia in the world. The main biomarkers associated with AD are protein amyloid-β (Aβ) plaques and protein tau neurofibrillary tangles, which are responsible for brain neuroinflamm...

  • Article
  • Open Access
63 Citations
7,877 Views
15 Pages

16 October 2018

To fill the shortages in the knowledge of the pyrolysis and combustion properties of new and aged polyvinyl chloride (PVC) sheaths, several experiments were performed by thermogravimetric analysis (TG), Fourier transform infrared (FTIR), microscale c...

  • Article
  • Open Access
3 Citations
3,033 Views
14 Pages

25 January 2025

Numerous fire disasters have involved thermoplastic expanded polystyrene (EPS) external thermal insulation composite systems (ETICS) on building façades. This study evaluates the flame-retardant efficiency of expandable graphite (EG)-blended E...

  • Review
  • Open Access
18 Citations
13,094 Views
18 Pages

The Effect of Walnut Intake on Lipids: A Systematic Review and Meta-Analysis of Randomized Controlled Trials

  • Saeed Mastour Alshahrani,
  • Reham M. Mashat,
  • Diaa Almutairi,
  • Alaa Mathkour,
  • Sahar Saad Alqahtani,
  • Amirah Alasmari,
  • Abdullah Hassan Alzahrani,
  • Reem Ayed,
  • Mohammed Yahya Asiri and
  • Abdullah Alsabaani
  • + 1 author

23 October 2022

Cardiovascular diseases (CVD) are the leading causes of death worldwide. Dyslipidemia is a cardiometabolic risk factor of CVD, yet it can be modifiable. Walnuts have been suggested as a dietary intervention to improve the lipid profile. Therefore, we...

  • Article
  • Open Access
18 Citations
8,905 Views
13 Pages

Study on Thermal Decomposition Behavior, Gaseous Products, and Kinetic Analysis of Bis-(Dimethylglyoximato) Nickel(II) Complex Using TG-DSC-FTIR-MS Technique

  • Ergang Yao,
  • Siyu Xu,
  • Fengqi Zhao,
  • Taizhong Huang,
  • Haijian Li,
  • Ningning Zhao,
  • Jianhua Yi,
  • Yanjing Yang and
  • Changjian Wang

15 March 2020

The fiber-like bis-(dimethylglyoximato) nickel(II) complex, Ni(DMG)2 was successfully synthesized. The obtained samples were characterized by SEM-EDS, FT-IR, XRD, and XPS. The TG-DSC-FTIR-MS coupling technique was used to characterize the thermal dec...

  • Article
  • Open Access
42 Citations
8,678 Views
15 Pages

Pyrolysis Process of Mixed Microplastics Using TG-FTIR and TED-GC-MS

  • Min-Hyun Cho,
  • Yu-Jin Song,
  • Chan-Joo Rhu and
  • Byung-Rye Go

3 January 2023

Microplastics have become a ubiquitous contaminant in the environment. The present study focuses on the identification, characterization, and quantification techniques for tracking microplastics. Due to their unique compositional structure, unambiguo...

  • Article
  • Open Access
6 Citations
3,197 Views
19 Pages

The Theoretical and Experimental Investigation of the Fluorinated Palladium β-Diketonate Derivatives: Structure and Physicochemical Properties

  • Svetlana I. Dorovskikh,
  • Denis E. Tryakhov,
  • Darya D. Klyamer,
  • Alexander S. Sukhikh,
  • Irina V. Mirzaeva,
  • Natalia B. Morozova and
  • Tamara V. Basova

28 March 2022

To search for new suitable Pd precursors for MOCVD/ALD processes, the extended series of fluorinated palladium complexes [Pd(CH3CXCHCO(R))2] with β-diketone [tfa−1,1,1-trifluoro-2,4-pentanedionato (1); pfpa−5,5,6,6,6-pentafluoro-2,4-...

  • Article
  • Open Access
11 Citations
4,006 Views
17 Pages

Analysis of the Fuel Properties of the Seed Shell of the Neem Plant (Azadirachta indica)

  • Francisco Simão Neto,
  • Maria Melo Neta,
  • Ana Sousa,
  • Luana Damasceno,
  • Bruna Sousa,
  • Samuel Medeiros,
  • Rafael Melo,
  • Ada Lopes,
  • José Santos and
  • Maria Rios

14 August 2023

The energetic potential of the seed shell of the Neem plant (Azadirachta indica) was investigated using proximate analysis, Higher Heating Value (HHV), thermal analysis (TG-DTG and DSC) in inert and oxidative atmospheres, and X-ray fluorescence (XRF)...

  • Article
  • Open Access
5 Citations
4,150 Views
19 Pages

1 November 2024

Recent incidents of fire accidents attributed to oil combustion have emerged as a significant threat to both industrial safety and environmental conservation. In this study, the thermal oxidation and thermal analysis kinetics parameters of transforme...

  • Article
  • Open Access
2 Citations
1,655 Views
17 Pages

14 November 2023

Realizing the utilization of reclaimed asphalt binder (RAB) and rice husk (RH) to reduce environmental pollution and expand the reutilization technique of reclaimed asphalt pavement (RAP), co-pyrolysis of RAB with RH has great potential. In this stud...

  • Article
  • Open Access
28 Citations
14,241 Views
15 Pages

22 January 2025

To grasp the decomposition reaction rule of calcium carbonate in cement raw material, the thermogravimetric analyzer (TG), derivative thermogravimetric (DTG), and differential scanning calorimeter (DSC) were used for analysis. Calcium carbonate sampl...

  • Article
  • Open Access
14 Citations
3,547 Views
15 Pages

Observational Constraints and Cosmographic Analysis of f(T,TG) Gravity and Cosmology

  • Harshna Balhara,
  • Jainendra Kumar Singh,
  • Shaily and
  • Emmanuel N. Saridakis

2 October 2024

We perform observational confrontation and cosmographic analysis of f(T,TG) gravity and cosmology. This higher-order torsional gravity is based on both the torsion scalar, as well as on the teleparallel equivalent of the Gauss–Bonnet combinatio...

  • Article
  • Open Access
14 Citations
7,778 Views
13 Pages

Recovery of Iron from Mill Scale by Reduction with Carbon Monoxide

  • Krzysztof Nowacki,
  • Tomasz Maciąg and
  • Teresa Lis

17 May 2021

The mill scale is a waste from the iron and steel industry. Due to the high content of iron in the form of oxides, it is an attractive material for the recovery of metallic iron by reduction. The product of mill scale reduction is an iron with a very...

  • Feature Paper
  • Article
  • Open Access
8 Citations
3,029 Views
22 Pages

6 September 2021

This paper presents the impact of thermal lag on the progress of different coal types’ gasification by CO2. The analysis was performed using thermogravimetry and numerical modeling. Experiments were carried out at a heating rate of 1–50 Kmin−1 and a...

  • Article
  • Open Access
22 Citations
5,459 Views
11 Pages

1 December 2017

Sewage sludge in China has the characteristics of low organic content and low heating value compared with other developed countries. Self-sustaining combustion of Chinese sludge cannot be achieved when the moisture content is high. Co-combusting a sm...

  • Review
  • Open Access
119 Citations
19,229 Views
26 Pages

This paper reviews the application of carbonation technology to the environmental industry as a way of reducing carbon dioxide (CO2), a green house gas, including the presentation of related projects of our research group. An alternative technology t...

  • Article
  • Open Access
25 Citations
5,286 Views
17 Pages

RETRACTED: Thermal Analysis of a Metal–Organic Framework ZnxCo1-X-ZIF-8 for Recent Applications

  • Moustafa Ahmed,
  • Yas M Al-Hadeethi,
  • Ahmed Alshahrie,
  • Arwa T Kutbee,
  • Essam R. Shaaban and
  • Ahmed F. Al-Hossainy

22 November 2021

Zeolitic imidazolate frameworks (ZIFs) are interesting materials for use in several aspects: energy storage material, gas sensing, and photocatalysis. The thermal stability and pyrolysis process are crucial in determining the active phase of the mate...

  • Article
  • Open Access
1,076 Views
15 Pages

11 February 2025

The aim of this study was to optimize a method for qualitative and quantitative determination of gaseous degradation products formed in the process of thermal decomposition in the sample. The toxicometric index was determined with the use of the coup...

  • Feature Paper
  • Article
  • Open Access
15 Citations
3,867 Views
19 Pages

26 August 2021

Catalysts are usually used in the thermal conversion of waste tires to enhance the efficiency of the process and the quality of pyrolytic products. Recently, it has already been proved that Ni/Fe bimetallic catalysts had an effective catalytic effect...

  • Data Descriptor
  • Open Access
265 Views
18 Pages

16 February 2026

This dataset provides synchronized multimodal behavioral measurements from 36 mice across four experimental groups: wild-type and rTg4510 tauopathy mice, each tested with or without doxycycline-mediated suppression of mutant tau expression. Of these,...

  • Article
  • Open Access
45 Citations
13,031 Views
9 Pages

Thermal Behavior of Hydrated Iron Sulfate in Various Atmospheres

  • Ndue Kanari,
  • Nour-Eddine Menad,
  • Etleva Ostrosi,
  • Seit Shallari,
  • Frederic Diot,
  • Eric Allain and
  • Jacques Yvon

19 December 2018

Iron sulfate, in particular FeSO4·7H2O, is derived from titanium dioxide production and the steel pickling process. Regarding TiO2 manufacturing, the amount of the resultant FeSO4·7H2O can be as high as 6 tons per ton of produced TiO2,...

  • Article
  • Open Access
6 Citations
1,852 Views
25 Pages

Influence of Spanish Broom Fibre Treatment, Fibre Length, and Amount and Harvest Year on Reinforced Cement Mortar Quality

  • Sandra Juradin,
  • Dražan Jozić,
  • Ivanka Netinger Grubeša,
  • Anita Pamuković,
  • Anđela Čović and
  • Frane Mihanović

The use of natural materials, such as natural fibres, in the construction industry is becoming more frequent. The source of natural fibres should be sought in local plants, such as Spanish Broom in the Mediterranean area. The fibre treatment process...

  • Article
  • Open Access
1 Citations
1,087 Views
19 Pages

The Torrefaction of Agricultural and Industrial Residues: Thermogravimetric Analysis, Characterization of the Products and TG-FTIR Analysis of the Gas Phase

  • Danijela Urbancl,
  • Deniz Agačević,
  • Eva Gradišnik,
  • Anja Šket,
  • Nina Štajnfelzer,
  • Darko Goričanec and
  • Aleksandra Petrovič

1 September 2025

Four biomass residues–rosemary pomace, rosemary cake, grape seed and apple pomace–were torrefied at 250, 350 and 450 °C, and the physical, chemical and structural changes were characterized. The mass and energy yield decreased with in...

  • Article
  • Open Access
658 Views
19 Pages

17 October 2025

Lithium slag (LS), a solid waste generated during lithium smelting, exhibits significant potential for geopolymer preparation. However, the high shrinkage of lithium slag geopolymer mortar (LSGM) severely restricts its engineering application. Curren...

  • Article
  • Open Access
17 Citations
9,042 Views
20 Pages

Association between ADIPOQ +45T>G Polymorphism and Type 2 Diabetes: A Systematic Review and Meta-Analysis

  • Yaofu Fan,
  • Kun Wang,
  • Shuhang Xu,
  • Guofang Chen,
  • Hongjie Di,
  • Meng Cao and
  • Chao Liu

30 December 2014

Recently, a number of studies have reported the association between the single nucleotide polymorphisms (SNPs) +45T>G polymorphism in the adiponectin (ADIPOQ) gene and type 2 diabetes mellitus (T2DM) risk, though the results are inconsistent. In o...

  • Article
  • Open Access
4,560 Views
22 Pages

5 September 2024

RaTG13 is phylogenomically the closest related coronavirus to SARS-CoV-2; consequently, understanding the provenance of this high-value genome sequence is important in understanding the origin of SARS-CoV-2. While RaTG13 was described as being genera...

  • Article
  • Open Access
25 Citations
4,946 Views
12 Pages

4 April 2022

The calcium hydroxide (Ca(OH)2) content is one of the main indices of cement hydration degree. In order to accurately determine the calcium hydroxide content of ethylene and vinyl acetate (EVA) copolymer-modified cement paste, a dual atmosphere therm...

  • Article
  • Open Access
1,489 Views
17 Pages

8 March 2025

Measuring molecular mobility (Mm) in solid food is challenging due to the rigid and heterogeneous nature of these matrices. The thermodynamic parameter Strength (S) fails to account for molecular displacement distances. This study emphasizes the role...

  • Article
  • Open Access
5 Citations
3,355 Views
13 Pages

Transcriptomic Analysis in the Hippocampus and Retina of Tg2576 AD Mice Reveals Defective Mitochondrial Oxidative Phosphorylation and Recovery by Tau 12A12mAb Treatment

  • Giovanna Morello,
  • Maria Guarnaccia,
  • Valentina La Cognata,
  • Valentina Latina,
  • Pietro Calissano,
  • Giuseppina Amadoro and
  • Sebastiano Cavallaro

12 September 2023

Increasing evidence implicates decreased energy metabolism and mitochondrial dysfunctions among the earliest pathogenic events of Alzheimer’s disease (AD). However, the molecular mechanisms underlying bioenergetic dysfunctions in AD remain, to...

  • Article
  • Open Access
13 Citations
3,377 Views
21 Pages

Analysis of the Pyrolysis Kinetics, Reaction Mechanisms, and By-Products of Rice Husk and Rice Straw via TG-FTIR and Py-GC/MS

  • Li Lin,
  • Yang E,
  • Qiang Sun,
  • Yixuan Chen,
  • Wanning Dai,
  • Zhengrong Bao,
  • Weisheng Niu and
  • Jun Meng

24 December 2024

This study employed thermogravimetric analysis (TGA), Fourier transform infrared spectroscopy (FTIR), and pyrolysis gas chromatography/mass spectrometry (Py-GC/MS) to characterize and provide insights into the pyrolysis behaviors and by-products of r...

  • Article
  • Open Access
38 Citations
4,786 Views
13 Pages

Composites of Unsaturated Polyester Resins with Microcrystalline Cellulose and Its Derivatives

  • Artur Chabros,
  • Barbara Gawdzik,
  • Beata Podkościelna,
  • Marta Goliszek and
  • Przemysław Pączkowski

21 December 2019

The paper investigates the properties of unsaturated polyester resins and microcrystalline cellulose (MCC) composites. The influence of MCC modification on mechanical, thermomechanical, and thermal properties of obtained materials was discussed. In o...

  • Article
  • Open Access
90 Citations
10,512 Views
13 Pages

Structural Determination of Pectins by Spectroscopy Methods

  • Agata Kozioł,
  • Kamila Środa-Pomianek,
  • Agata Górniak,
  • Agnieszka Wikiera,
  • Konrad Cyprych and
  • Magdalena Malik

18 April 2022

Plant polysaccharides include pectins, which are responsible for an important role in plant physiology and are part of the plant cell wall. These compounds are known as gelling and stabilizing agents, which are widely used in the food industry. The s...

  • Article
  • Open Access
7 Citations
2,776 Views
15 Pages

25 June 2021

Two coordination polymers, [Co(µ4-L)(H2O)2]n (1) and [Ni(µ-L)(H2O)4]n (2), were solvothermally assembled from the corresponding metal(II) chlorides and biphenyl-4,4-dioxydiacetic acid (H2L) as a flexible dicarboxylate linker. The cobalt(II) compound...

  • Feature Paper
  • Article
  • Open Access
6 Citations
2,559 Views
17 Pages

A Thermal Study on Peat Oxidation Behavior in the Presence of an Iron-Based Catalyst

  • Mohammed A. Khelkhal,
  • Semen E. Lapuk,
  • Nikita E. Ignashev,
  • Alexey A. Eskin,
  • Mikhail Yu. Glyavin,
  • Nikolay Yu. Peskov,
  • Tatiana O. Krapivnitskaia and
  • Alexey V. Vakhin

9 November 2021

Peat is a resource used for heat and energy, particularly in countries where peat is abundant and conventional fuels are not available. Some countries have made extensive use of peat resources to produce electricity and heat in addition to light hydr...

  • Article
  • Open Access
11 Citations
2,891 Views
14 Pages

24 September 2020

The topic raised in this paper concerns an important aspect regarding the possibilities of the combustion and co-combustion of biomass substrates (energetic willow/sewage sludge), in light of the renewable energy source (RES) regulations, with fuel f...

  • Article
  • Open Access
8 Citations
3,232 Views
25 Pages

Thermally Stable Nitrothiacalixarene Chromophores: Conformational Study and Aggregation Behavior

  • Anton Muravev,
  • Tatiana Gerasimova,
  • Robert Fayzullin,
  • Olga Babaeva,
  • Ildar Rizvanov,
  • Ayrat Khamatgalimov,
  • Marsil Kadirov,
  • Sergey Katsyuba,
  • Igor Litvinov and
  • Igor Antipin
  • + 2 authors

21 September 2020

Achieving high thermal stability and control of supramolecular organization of functional dyes in sensors and nonlinear optics remains a demanding task. This study was aimed at the evaluation of thermal behavior and Langmuir monolayer characteristics...

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