Journal Description
Metals
Metals
is an international, peer-reviewed, open access journal published monthly online by MDPI. The Spanish Materials Society (SOCIEMAT) is affiliated with Metals and their members receive discounts on the article processing charges.
- Open Access— free for readers, with article processing charges (APC) paid by authors or their institutions.
- High Visibility: indexed within Scopus, SCIE (Web of Science), Inspec, Ei Compendex, CAPlus / SciFinder, and other databases.
- Journal Rank: JCR - Q2 (Metallurgy and Metallurgical Engineering) / CiteScore - Q1 (Metals and Alloys)
- Rapid Publication: manuscripts are peer-reviewed and a first decision is provided to authors approximately 18.7 days after submission; acceptance to publication is undertaken in 2.7 days (median values for papers published in this journal in the second half of 2025).
- Recognition of Reviewers: reviewers who provide timely, thorough peer-review reports receive vouchers entitling them to a discount on the APC of their next publication in any MDPI journal, in appreciation of the work done.
- Companion journals for Metals include: Compounds, Alloys and Iron.
Impact Factor:
2.5 (2024);
5-Year Impact Factor:
2.8 (2024)
Latest Articles
Physics-Informed Decision Framework for Reuse of Reclaimed Steel Members Under Uncertainty
Metals 2026, 16(2), 171; https://doi.org/10.3390/met16020171 (registering DOI) - 1 Feb 2026
Abstract
Structural steel reuse can gain large embodied-carbon savings, yet it is still not widely adopted since approval depends on the quality of the evidence, how uncertainty is handled, and if the design requirements are followed, not just on resistance. Reclaimed members frequently lack
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Structural steel reuse can gain large embodied-carbon savings, yet it is still not widely adopted since approval depends on the quality of the evidence, how uncertainty is handled, and if the design requirements are followed, not just on resistance. Reclaimed members frequently lack dependable documentation regarding material grade, loading history, boundary conditions, connection status, and degradation. For reuse decisions, conservative default assumptions protect safety but frequently eliminate qualified reuse options. This research examines data-driven and physics-informed computational methods from a decision-making standpoint, contending that their significance resides in facilitating an auditable approval process, not in supplanting deterministic verification. We differentiate feasibility, acceptability, and approval as distinct engineering phases. Data-driven models are thought of as tools for quickly screening candidates, surrogate evaluation, inverse reasoning, and stock-to-demand matching. Their goal is to reduce the list of candidates and prioritize evidence collection. Physics-informed approaches are examined as admissibility filters that impose restrictions of equilibrium, compatibility, stability, and plausible boundary-condition envelopes; therefore, minimizing mechanically invalid predictions under partial information. Next, we consider uncertainty quantification and explainability to be essential for reuse decisions. We suggest practical outputs for approval packages, such as resistance bounds within specified assumption envelopes, sensitivity rankings of decision-critical unknowns, low-support flags, and evidence actions for conditional acceptance. This document is organized into a process from audit to approval. It also states the open issues in reuse-specific datasets, standardized evidence capturing, decision-relevant validation under degradation, and regulatory acceptance. The resulting framework clarifies how advanced computational tools can enable adaptable, conservative, and transparent steel reuse in practice.
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(This article belongs to the Special Issue Novel Insights and Advances in Steels and Cast Irons (2nd Edition))
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Open AccessArticle
Microstructure and Mechanical Properties of Ultrafine-Grained CrMnFeCoNi High-Entropy Alloy Prepared via Powder Metallurgy
by
Sunghyuk Jang, Seonghyun Park and Jae-Gil Jung
Metals 2026, 16(2), 170; https://doi.org/10.3390/met16020170 (registering DOI) - 1 Feb 2026
Abstract
We studied the microstructural evolution and mechanical properties of ultrafine-grained CrMnFeCoNi high-entropy alloys fabricated by mechanical alloying of various additives and spark plasma sintering. The additives were 1 wt.% process control agent (stearic acid) + 1 wt.% graphene nanofiber (GNF) (PG) or 1
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We studied the microstructural evolution and mechanical properties of ultrafine-grained CrMnFeCoNi high-entropy alloys fabricated by mechanical alloying of various additives and spark plasma sintering. The additives were 1 wt.% process control agent (stearic acid) + 1 wt.% graphene nanofiber (GNF) (PG) or 1 wt.% Y2O3 + 1 wt.% GNF (YG) to modify the constituting phase of the sintered alloy. The PG and YG powders exhibited a single FCC phase. The YG powders had a larger powder size and a smaller crystallite size than the PG powders. Ultrafine-grained FCC matrices with average particle sizes of 0.57 μm and 0.71 μm, respectively, were formed through the SPS process of PG and YG powders. The absence of PCA in YG alloys resulted in a bimodal distribution of fine and coarse grains (due to incomplete mechanical alloying) and formation of a lesser and finer Cr7C3 phase (due to reduced C content). The sintered PG alloy contained coarse (~60 nm) spinel Mn3O4 oxides along grain boundaries, whereas the YG alloy exhibited coarse Mn3O4 and fine (~17 nm) Y2O3 oxide particles along grain boundaries. Additionally, the YG alloy contained tiny (~5 nm) Y2O3 oxide particles with a cube-on-cube orientation relationship within the FCC matrix. YG alloy exhibited higher hardness and compressive yield strength than PG alloy, mainly due to the oxide dispersion strengthening of finely dispersed Y2O3 particles. The addition of Y2O3 reinforcing particles had a minimal effect on the ultimate compressive strength and fracture strain of the sintered alloy.
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(This article belongs to the Special Issue Feature Papers in Entropic Alloys and Meta-Metals)
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Open AccessArticle
The Effect of High Heat Input on the Microstructure and Impact Toughness of EH36 Steel Welded Joints
by
Zhenteng Li, Pan Zhang, Gengzhe Shen, Fujian Guo, Yanmei Zhang, Liuyan Zhang, Qunye Gao and Xuelin Wang
Metals 2026, 16(2), 169; https://doi.org/10.3390/met16020169 (registering DOI) - 1 Feb 2026
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Ultra-high heat input welding offers high efficiency for large-scale offshore engineering, but excessive heat input can degrade low-temperature toughness. This study investigates the microstructural evolution and impact toughness of EH36 ship steel under high heat inputs (300–500 kJ/cm) using Gleeble-3500 thermal simulation, Charpy
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Ultra-high heat input welding offers high efficiency for large-scale offshore engineering, but excessive heat input can degrade low-temperature toughness. This study investigates the microstructural evolution and impact toughness of EH36 ship steel under high heat inputs (300–500 kJ/cm) using Gleeble-3500 thermal simulation, Charpy impact tests, and multi-scale characterization (OM, SEM, EBSD). Results show that impact toughness peaks at 400 kJ/cm, with surface and core energies reaching 343.33 J and 215.18 J, respectively. The optimal toughness is attributed to the formation of acicular ferrite and a high fraction of high-angle grain boundaries (up to 48.7%), which effectively inhibit crack propagation. These findings provide a practical basis for selecting heat input to balance welding efficiency and mechanical performance in marine steel fabrication.
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Open AccessReview
A Review of Experimental and Simulation Methods for Rolling Contact Fatigue
by
Minghui Wang, Hao Su, Zhigang Yan, Chen Chen, Chunlei Zheng, Bo Lv and Fucheng Zhang
Metals 2026, 16(2), 168; https://doi.org/10.3390/met16020168 (registering DOI) - 31 Jan 2026
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Rolling contact fatigue and wear of wheel–rail systems are critical factors affecting the safety of high-speed railways and have long been key research topics in materials science. This paper reviews the theoretical foundations of wheel–rail rolling contact fatigue, introduces representative experimental methods for
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Rolling contact fatigue and wear of wheel–rail systems are critical factors affecting the safety of high-speed railways and have long been key research topics in materials science. This paper reviews the theoretical foundations of wheel–rail rolling contact fatigue, introduces representative experimental methods for studying rolling contact fatigue, and discusses the stress–strain problems in wheel–rail contact. Additionally, it provides a detailed overview of the emerging computational simulation approach for rolling contact fatigue wear, summarizes commonly used simulation software and their respective characteristics, and analyzes material factors influencing rolling contact fatigue simulations in wheel–rail steels. Finally, based on the classification of rolling contact fatigue algorithms, various measures are proposed to enhance rapid and accurate detection and evaluation.
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The Influence of Annealing on Microstructure Evolution and Mechanical Properties of 442 Ferritic Stainless Steel
by
Yufeng Li, Changbo Wang, Yang Hui, Chen Chen, Xuefeng Lu, Jie Sheng and Xingchang Tang
Metals 2026, 16(2), 167; https://doi.org/10.3390/met16020167 - 30 Jan 2026
Abstract
The microstructure evolution law and the changes in mechanical properties of 442 ferritic stainless steel after annealing treatment at different temperatures are systematically investigated. The results show that, as the annealing temperature increases, the cold-rolled 442 ferritic stainless steel successively undergoes the process
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The microstructure evolution law and the changes in mechanical properties of 442 ferritic stainless steel after annealing treatment at different temperatures are systematically investigated. The results show that, as the annealing temperature increases, the cold-rolled 442 ferritic stainless steel successively undergoes the process of recovery, recrystallization and grain growth, with the microstructure gradually changing from a fibrous to recrystallized structure, and the secondary phases, such as the Nb(C, N) phase, σ phase and Laves phase, precipitate. In terms of mechanical properties, the tensile strength, yield strength and Vickers hardness gradually decrease, while the elongation after fracture gradually increases. When the annealing temperature reaches 800 °C, the material exhibits the optimal comprehensive mechanical properties. The yield strength, tensile strength and elongation reach 371 MPa, 534 MPa and 31%, respectively, and the hardness is 175 HV. The fracture mode of the sample is mainly ductile fracture. EBSD analysis indicates that the strong Brass {110}<112> texture existing in the cold-rolled state gradually weakens with the annealing process, and the {111}<110>texture strengthens, thereby reducing the influence of unfavorable textures. The research results provide theoretical basis and data support for microstructure regulation and performance optimization of 442 ferritic stainless steel.
Full article
(This article belongs to the Special Issue Advances in High-Strength Low-Alloy Steels (2nd Edition))
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Hydrogen-Induced Crack Evolution and Microstructural Adaptation in Zirconium Alloy: An In Situ EBSD Tensile Study
by
Changxing Cui, Bo Li, Huanzheng Sun, Hui Wang, Shuo Sun, Guannan Zhao, Zheng Feng and Wen Zhang
Metals 2026, 16(2), 166; https://doi.org/10.3390/met16020166 - 30 Jan 2026
Abstract
The performance of Zr-2.5Nb alloy pressure tubes in nuclear reactors is critically dependent on the behavior of precipitated hydrides. In this study, a hydrogen-charged Zr-2.5Nb alloy pressure tube was subjected to in situ tensile testing combined with electron backscatter diffraction to elucidate microcrack
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The performance of Zr-2.5Nb alloy pressure tubes in nuclear reactors is critically dependent on the behavior of precipitated hydrides. In this study, a hydrogen-charged Zr-2.5Nb alloy pressure tube was subjected to in situ tensile testing combined with electron backscatter diffraction to elucidate microcrack evolution and microstructural adaptation. Initially, longitudinal hydride–hydride interface cracks nucleated at non-coherent interfaces of two types of hydrides due to the inherent brittleness. Subsequently, stress redistribution by a small proportion of hydride–hydride interface cracks resulted in the emergence of microcracks at the transverse hydride–matrix interfaces, accompanied by partial hydride phase transformation. Finally, under high strain conditions, increased dislocation movement in the matrix triggered a single slip system, leading to the formation of numerous low-angle grain boundaries. As strain further increased, multiple slip systems were activated, and longitudinal matrix–matrix interface cracks began to nucleate at certain grain boundary locations.
Full article
(This article belongs to the Section Crystallography and Applications of Metallic Materials)
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Synergistic Effects in Separation of Cobalt(II) and Lithium(I) from Chloride Solutions by Cyphos IL-101 and TBP
by
Beata Pospiech
Metals 2026, 16(2), 165; https://doi.org/10.3390/met16020165 - 30 Jan 2026
Abstract
This work reports on the extraction and separation of Co(II) and Li(I) ions from chloride solutions using a synergistic mixture, namely Cyphos IL 101 (trihexyl(tetradecyl)phosphonium chloride[R4PCl] and TBP (tributylphosphate). This system has not been described up to now. The aim of
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This work reports on the extraction and separation of Co(II) and Li(I) ions from chloride solutions using a synergistic mixture, namely Cyphos IL 101 (trihexyl(tetradecyl)phosphonium chloride[R4PCl] and TBP (tributylphosphate). This system has not been described up to now. The aim of this research was to compare the extraction efficiency (%E) and the extraction selectivity of Co(II) over Li(I) (SCo/Li) using single extractants and their equimolar mixture. Co(II) extraction with Cyphos IL 101 and TBP depends strongly on hydrochloric acid concentration in the aqueous phase. The separation coefficient of the studied metal ions was determined depending on the hydrochloric acid concentrations in the aqueous phase. The significance of the work is in the examination of the re-extraction of cobalt(II) from the organic phase after extraction. For this purpose, inorganic acids were investigated as the stripping agents, i.e., HCl (hydrochloric acid), H2SO4 (sulfuric acid) and HNO3 (nitric acid). Finally, optimal conditions for the separation of Co(II) and Li(I) were established by using a synergistic mixture. A highly selective and effective solvent extraction of cobalt(II) over lithium(I) from 5 mol∙dm−3 hydrochloric acid has been achieved with the synergistic mixture of 0.1 mol∙dm−3 Cyphos IL 101 and 0.1 mol∙dm−3 TBP in kerosene. The selectivity coefficients of Co(II) over Li(I) (CCo/Li) in the solvent extraction with 0.1 mol∙dm−3 Cyphos IL 101, 0.1 mol∙dm−3 TBP, and with their equimolar mixture were found to be equal: 73.1, 3.7 and 225.5, respectively. Efficient Co(II) stripping was achieved using 0.5 mol∙dm−3 sulfuric acid.
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(This article belongs to the Section Extractive Metallurgy)
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Open AccessArticle
Research on the Edge Crack Suppression Mechanism of Magnesium Alloy Plates Processed by Lattice Severe Deformation Rolling
by
Guang Feng, Zhongxiang Li and Kai Huang
Metals 2026, 16(2), 164; https://doi.org/10.3390/met16020164 - 29 Jan 2026
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Edge cracking severely limits the rolling yield of magnesium alloy plates. A novel lattice severe deformation rolling (LSDR) process using corrugated rolls is proposed to suppress edge cracking. Numerical simulations, rolling experiments, and microstructural analyses were conducted, with results compared to conventional flat
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Edge cracking severely limits the rolling yield of magnesium alloy plates. A novel lattice severe deformation rolling (LSDR) process using corrugated rolls is proposed to suppress edge cracking. Numerical simulations, rolling experiments, and microstructural analyses were conducted, with results compared to conventional flat rolling (FR), to elucidate the suppression mechanism. LSDR induces a multi-peak stress distribution and restricts metal flow, thereby reducing additional stresses responsible for edge cracking. Deformation heat generated in local severe deformation zones compensates for thermal loss, alleviates the temperature gradient between the plate edge and center, and enhances overall plasticity. According to the Cockcroft–Latham fracture criterion, LSDR effectively limits damage growth and confines damage within a single lattice, suppressing crack propagation, whereas FR produces damage values far exceeding the critical value of 0.43. Furthermore, fine grains formed in severe deformation zones, together with dislocation entanglement induced by twinning, impede crack propagation. This work demonstrates the effectiveness of LSDR and provides a new approach for mitigating edge cracking in rolled metal plates.
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Physics-Informed Machine Learning for Predicting Carburizing Process Outcomes in 20Cr2Ni4 Steel: A Cascade Modeling Approach
by
Chuansheng Liang, Peng Cheng and Chenxi Shao
Metals 2026, 16(2), 163; https://doi.org/10.3390/met16020163 - 29 Jan 2026
Abstract
Carburizing process optimization requires accurate prediction of multiple interrelated outcomes, yet existing models either oversimplify the physics or require prohibitively large datasets. Here, we present a physics-informed machine learning (PIML) cascade model for vacuum carburizing of 20Cr2Ni4 gear steel that predicts surface carbon
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Carburizing process optimization requires accurate prediction of multiple interrelated outcomes, yet existing models either oversimplify the physics or require prohibitively large datasets. Here, we present a physics-informed machine learning (PIML) cascade model for vacuum carburizing of 20Cr2Ni4 gear steel that predicts surface carbon content, maximum hardness, and effective case depth through a three-stage sequential architecture. The model integrates Fick’s diffusion law and empirical carbon–hardness relationships with ensemble learning using physics-derived features to reduce data requirements while maintaining interpretability. Validation against experimental data yields coefficient of determination values of 0.968 (surface carbon, RMSE = 0.0023 wt%), 0.963 (maximum hardness, RMSE = 1.27 HV), and 0.999 (case depth, RMSE = 0.0053 mm) on physics-augmented test data; leave-one-out cross-validation (LOOCV) on original experimental data yields = 0.87–0.95, representing true generalization capability. Feature importance analysis reveals that physics-derived features collectively account for over 70% of the prediction power, with the characteristic diffusion length ( ) contributing 42.2%, followed by temperature-related features (22.4%) and time-related features (14.8%). Compared to pure physics-based and data-driven approaches, the proposed framework achieves superior accuracy for case depth prediction while preserving physical consistency. The methodology demonstrates potential for adaptation to other vacuum-carburizing applications with similar Cr-Ni steel compositions, although extension to fundamentally different processes (e.g., gas carburizing and nitriding) would require process-specific recalibration.
Full article
Open AccessReview
Large Language Models for High-Entropy Alloys: Literature Mining, Design Orchestration, and Evaluation Standards
by
Yutong Guo and Chao Yang
Metals 2026, 16(2), 162; https://doi.org/10.3390/met16020162 - 29 Jan 2026
Abstract
High-entropy alloys (HEAs) present a fundamental design paradox: their exceptional properties arise from complex, high-dimensional composition–process–microstructure–property (CPMP) relationships, yet the knowledge needed to navigate this space is fragmented across a vast and unstructured literature. Large language models (LLMs) offer a transformative interface to
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High-entropy alloys (HEAs) present a fundamental design paradox: their exceptional properties arise from complex, high-dimensional composition–process–microstructure–property (CPMP) relationships, yet the knowledge needed to navigate this space is fragmented across a vast and unstructured literature. Large language models (LLMs) offer a transformative interface to this complexity. By extracting structured facts from text, they can convert dispersed and heterogeneous evidence (i.e., findings scattered across many studies and reported with inconsistent test protocols or characterization standards) into queryable knowledge graphs. Through code generation and tool composition, they can automate simulation pipelines, surrogate model construction, and inverse design workflows. This review analyzes how LLMs can augment key stages of HEA research—from intelligent literature mining and multimodal data integration (using LLMs to automatically extract and structure data from texts and to combine information across text, images, and other data sources) to model-driven design and closed-loop experimentation—illustrated by emerging case studies. We propose concrete evaluation protocols that measure direct scientific utility, including knowledge-graph completeness, workflow setup efficiency, and experimental validation hit rates. We also confront practical limitations: data sparsity and noise, model hallucination, domain bias (where models may exhibit superior predictive performance for specific, well-represented alloy systems over others due to imbalances in training data), and the imperative for reproducible infrastructure. We argue that domain-specialized LLMs, embedded within grounded, verifiable research systems, can not only accelerate HEA discovery but also standardize the representation, sharing, and reuse of community knowledge.
Full article
(This article belongs to the Special Issue Advances in High-Entropy Alloys’ Microstructure, Properties and Preparation)
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A State-of-the-Art Review on Metallic Hysteretic Dampers: Design, Materials, Advanced Modeling, and Future Challenges
by
Álvaro Gómez, Rodrigo Valle, Flavia Bustos and Víctor Tuninetti
Metals 2026, 16(2), 161; https://doi.org/10.3390/met16020161 - 29 Jan 2026
Abstract
Metallic seismic dampers are an effective tool for reducing structural damage during seismic events. While previous reviews have often focused on cataloging device types, this review presents a deep analysis of the underlying science governing their performance. Particular emphasis is placed on advanced
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Metallic seismic dampers are an effective tool for reducing structural damage during seismic events. While previous reviews have often focused on cataloging device types, this review presents a deep analysis of the underlying science governing their performance. Particular emphasis is placed on advanced computational methods, such as non-linear kinematic hardening (e.g., Chaboche) and micromechanical damage models (e.g., GTN), which are essential for accurately predicting low-cycle fatigue and fracture. Furthermore, advances in materials science are analyzed, ranging from low-yield-strength (LYS) steels to self-centering shape memory alloys (SMAs). Finally, the influence of manufacturing processes (including additive manufacturing) is explored, and critical future challenges in design, modeling, and long-term durability are identified. This analysis provides a foundational resource for researchers seeking to advance beyond simple phenomenological design toward physics-based prediction of damper performance.
Full article
(This article belongs to the Special Issue Advanced Structural Metals: Integrating Mechanics, Processing, and Performance Characterization)
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Open AccessArticle
Effects of the Scrap Steel Ratio and Bottom-Blowing Process Parameters on the Fluid Flow Characteristics in a Physical Model of a Steelmaking Converter
by
Fei Yuan, Xuan Liu, Anjun Xu and Xueying Li
Metals 2026, 16(2), 160; https://doi.org/10.3390/met16020160 - 29 Jan 2026
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The amount of scrap steel and selection of blowing process parameters are known to influence the fluid flow characteristics of the melt pool in converter steelmaking. However, few studies have considered the effects of scrap steel and blowing process parameters together. In this
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The amount of scrap steel and selection of blowing process parameters are known to influence the fluid flow characteristics of the melt pool in converter steelmaking. However, few studies have considered the effects of scrap steel and blowing process parameters together. In this study, a physical model of a converter is established to investigate the influences of the amount of scrap steel and bottom-blowing process parameters on the fluid flow characteristics of the melt pool. Particle image velocimetry is used to measure the velocity distribution in the melt pool, and the stimulus–response method is used to measure the mixing time of the melt pool under different operating conditions. The results show that increasing the scrap steel ratio worsens the dynamic conditions of the melt pool. The best of the explored combinations is achieved at a scrap steel ratio of 20% and with six nozzles. The mixing time decreases as the gas flow rate increases, but the rate of decrease also decreases. Based on the results, the mixing time can be predicted from the gas flow rate and the number of nozzles. A relationship between the stirring power and mixing time of a converter using the bottom-blowing process is established.
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Open AccessArticle
Hydrogen-Induced Delayed Fracture Susceptibility in Ti–Nb–V Microalloyed Press-Hardened Steel Compared to Ti-Microalloyed Reference
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Renzo Valentini, Leonardo Bertini, Fabio D’Aiuto, Michele Maria Tedesco and Hardy Mohrbacher
Metals 2026, 16(2), 159; https://doi.org/10.3390/met16020159 - 28 Jan 2026
Abstract
In alignment with the European Union’s 2050 carbon-neutrality targets, the automotive industry is intensifying efforts to adopt lightweight materials that ensure structural integrity without compromising safety. Press-hardened steels (PHS), offering a combination of ultra-high strength and formability, are at the forefront of these
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In alignment with the European Union’s 2050 carbon-neutrality targets, the automotive industry is intensifying efforts to adopt lightweight materials that ensure structural integrity without compromising safety. Press-hardened steels (PHS), offering a combination of ultra-high strength and formability, are at the forefront of these developments. Standard PHS grades rely on Ti–B microalloying; however, further alloying with Nb and V has been proposed to enhance hydrogen embrittlement resistance via microstructural refinement and hydrogen trapping. This study investigates hydrogen transport and mechanical degradation in a Ti–Nb–V microalloyed PHS compared to a conventional Ti-only 22MnB5 grade. Electrochemical permeation, thermal desorption, and mechanical testing were employed to characterize hydrogen diffusivity, solubility, and trapping mechanisms. The Ti–Nb–V variant demonstrated lower hydrogen diffusivity, higher solubility, and improved resistance to delayed fracture, attributable to the presence of fine NbTiV precipitates.
Full article
(This article belongs to the Special Issue Microstructure and Mechanical Behavior of High-Strength Steel)
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A Numerical Simulation on the Melting Behavior of Ferrochrome Alloy in Molten Steel
by
Yuanhao Hai, Mengke Liu, Guojun Ma, Xiang Zhang and Dingli Zheng
Metals 2026, 16(2), 158; https://doi.org/10.3390/met16020158 - 28 Jan 2026
Abstract
Ferrochrome alloy is a crucial additive in steelmaking, significantly enhancing the strength, hardness, and corrosion resistance of steel; investigating the melting behavior of ferrochrome alloy could provide a theoretical foundation for producing stainless steel with improved properties. To gain insight into the melting
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Ferrochrome alloy is a crucial additive in steelmaking, significantly enhancing the strength, hardness, and corrosion resistance of steel; investigating the melting behavior of ferrochrome alloy could provide a theoretical foundation for producing stainless steel with improved properties. To gain insight into the melting behavior and mechanism of ferrochrome alloy in molten steel, this paper employed a numerical simulation with ANSYS Fluent software to investigate the effects of bath temperature, bath chromium content, bath carbon content, alloy chromium content, alloy carbon content, alloy size, and alloy preheating temperature on the melting behavior of ferrochromium alloy. The results showed that when the ferrochrome alloy is immersed into the molten bath, a solidified layer formed on the surface of the alloy, and as immersion time increased, the thickness of the solidified layer initially increased and then decreased; subsequent to the complete melting of the solidified layer, the alloy body began to melt. The center temperature of the alloy remained the lowest throughout the melting process and raised with increasing immersion time. Additionally, as the bath temperature and bath carbon content increased, the formation time of the solidified layer on the surface of the alloy shortened, its maximum thickness decreased, the alloy’s melting rate accelerated from 0.49 × 10−4 m/s to 1.22 × 10−4 m/s, and the complete melting time decreased from 134.7 s to 41 s. Conversely, increasing the bath chromium content raised the melting point of the solidified layer, prolonged the time required for remelting, slowed the alloy’s melting rate from 2.47 × 10−4 m/s to 0.91 × 10−4 m/s, and increased the complete melting time from 67.6 s to 75.2 s. As the alloy carbon content and preheating temperature increased, the alloy chromium content and size decreased, the formation time of the solidified layer shortened, its maximum thickness initially increased and then decreased, the melting rate of the alloy accelerated from 0.47 × 10−4 m/s to 1.97 × 10−4 m/s, and the complete melting time reduced from 165.8 s to 18.1 s.
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(This article belongs to the Section Computation and Simulation on Metals)
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The Coupling Relationship of Dynamic Recrystallization and Lamellar Globularization of the BT25y Alloy During High-Temperature Deformation
by
Xuemei Yang, Xiaojing Zong, Cheng Wang, Yueyu Sun, Jiayuan Wang, Boshi Zheng, Juncheng Fang, Xuewei Yan and Xiaonan Shi
Metals 2026, 16(2), 157; https://doi.org/10.3390/met16020157 - 28 Jan 2026
Abstract
In the aerospace field, the BT25y titanium alloy is recommended as a candidate material for manufacturing compressor discs and rotor blades of aircraft engines. The influence of hot deformation parameters on the microstructural evolution, recrystallization softening, and globularization mechanism of the BT25y alloy
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In the aerospace field, the BT25y titanium alloy is recommended as a candidate material for manufacturing compressor discs and rotor blades of aircraft engines. The influence of hot deformation parameters on the microstructural evolution, recrystallization softening, and globularization mechanism of the BT25y alloy with an initial lamellar structure was studied. Furthermore, the coupling relationship between dynamic recrystallization and lamellar globularization was explored by means of EBSD, SEM, and TEM techniques. The experiment results indicate that the characteristics of initial lamellar α, α/α sub-grain boundaries within α lamellae, and the α/β phase boundary show significant variations due to the formation of equiaxed α grains during hot deformation. As the strain rate increases, the recrystallization mechanism of α phase gradually shifts from CDRX softening characterized by sub-grain evolution and lamellae fracture, to DDRX softening characterized by grain boundary arching and sub-grain boundary bridging. As the deformation temperature increases, the intense thermal activation promotes the accumulation of distortion storage energy, providing enhanced driving force for the occurrence of dynamic recrystallization. The research results will contribute to a deeper understanding of the relationship between dynamic recrystallization and lamellar globularization, providing theoretical guidance for the deformation process optimization and mechanical property control of the BT25y alloy.
Full article
(This article belongs to the Special Issue Advances in Metal Forming and Plasticity)
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Open AccessReview
Separation Strategies for Indium Recovery: Exploring Solvent Extraction, Ion-Exchange, and Membrane Methods
by
Ewa Rudnik
Metals 2026, 16(2), 156; https://doi.org/10.3390/met16020156 - 27 Jan 2026
Abstract
Indium is a strategically important metal, essential for the production of transparent conductive oxides, flat panel displays, thin-film photovoltaics, and advanced optoelectronic devices. Due to its limited natural abundance and its occurrence in trace amounts alongside other metals in both primary and secondary
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Indium is a strategically important metal, essential for the production of transparent conductive oxides, flat panel displays, thin-film photovoltaics, and advanced optoelectronic devices. Due to its limited natural abundance and its occurrence in trace amounts alongside other metals in both primary and secondary sources, the recovery of indium through efficient separation techniques has gained increasing attention. This review discusses three major separation strategies for indium recovery: solvent extraction, ion-exchange, and membrane processes, applied to both synthetic solutions and real leachates. D2EHPA has demonstrated its applicability as an effective agent for indium separation, not only in solvent extraction but also as an impregnating agent in polymer resins and membranes. While solvent extraction achieves high recovery rates, ion-exchange resins and membrane-based methods offer significant advantages in terms of reusability, reduced chemical consumption, and minimal environmental impact. The selective separation of indium from impurities such as Fe3+ and Sn2+ remains a key consideration, which can be addressed by optimizing feed solution conditions or adjusting the selective stripping stages. A comparative overview of these methods is provided, focusing on separation efficiency, operational conditions, and potential integration into close-loop systems. The article highlights recent innovations and outlines the challenges involved in achieving sustainable indium recovery, in line with circular economy principles.
Full article
(This article belongs to the Special Issue Cutting-Edge Innovations in Metal Recovery from Electronic Waste: Challenges, Techniques and Future Horizons)
Open AccessArticle
Effect of the Welding Electrode Geometry on the Peak Load, Energy Absorption, Fracture Type, and Microstructure of Resistance Spot-Welded Dissimilar Ultra-High Strength MS1500 and SPFC590 Steels
by
Mehmet Okan Görtan and Ümit Türkmen
Metals 2026, 16(2), 155; https://doi.org/10.3390/met16020155 - 27 Jan 2026
Abstract
In the present study, the effects of electrode geometry and welding current on the tensile-shear strength, failure energy, fracture type, and joint microstructure were investigated during the RSW of ultra-high-strength MS1500 steel to high-strength low-alloy SPFC590 steel, both 1.2 mm in thickness. Three
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In the present study, the effects of electrode geometry and welding current on the tensile-shear strength, failure energy, fracture type, and joint microstructure were investigated during the RSW of ultra-high-strength MS1500 steel to high-strength low-alloy SPFC590 steel, both 1.2 mm in thickness. Three electrode geometries—designated as G0-6 mm, G0-8 mm, and A0—recommended for 1.2 mm sheets according to ISO 5821 were examined. It was found that in the G0-6 mm electrode geometry, which has the smallest contact area, excessive expulsion occurred at lower current levels compared to the other geometries. Consequently, this configuration resulted in lower maximum tensile-shear strength and failure energy values. The highest mechanical performance was achieved with the G0-8 mm electrode geometry, where the tensile-shear strength and failure energy were measured as 19.42 kN and 43.81 J, respectively. For the A0 electrode, although the maximum tensile-shear strength (19.68 kN) was comparable to that of the G0-8 mm geometry, the failure energy was approximately 7% lower (40.94 J). For all electrode geometries corresponding to maximum mechanical strength, a pull-out failure mode was observed, where the nugget region of the SPFC590 steel detached from the base metal and remained adhered to the ultra-high-strength MS1500 sheet.
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(This article belongs to the Special Issue Advances in Welding Processes of Metallic Materials—2nd Edition)
Open AccessArticle
Accelerated Optimization of Superalloys by Integrating Thermodynamic Calculation Data with Machine Learning Models: A Reference Alloy Approach
by
Yubing Pei, Zhenhuan Gao, Junjie Wu, Liping Nie, Song Lu, Jiaxin Tan, Ziyun Wu, Longfei Li and Xiufang Gong
Metals 2026, 16(2), 154; https://doi.org/10.3390/met16020154 - 27 Jan 2026
Abstract
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The multi-objective optimization of multicomponent superalloys has long been impeded by not only the complex interactions among multiple elements but also the low efficiency and high cost of traditional trial-and-error methods. To address this issue, this study proposed a thermodynamic calculation data-driven optimization
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The multi-objective optimization of multicomponent superalloys has long been impeded by not only the complex interactions among multiple elements but also the low efficiency and high cost of traditional trial-and-error methods. To address this issue, this study proposed a thermodynamic calculation data-driven optimization framework that integrates machine learning (ML) and multi-objective screening based on domain knowledge. The core of this methodology involves introducing a commercial reference alloy and rapidly generating a large-scale thermodynamic dataset through ML models. After training, the ML models were verified to be more efficient at predicting phase transition temperatures and γ′ volume fractions than the CALPHAD methods. Focusing on the mechanical properties, critical strength indices, including solid solution strengthening, precipitation strengthening, and creep resistance based on the calculated γ/γ′ two-phase compositions, were compared with the reference alloy and set as the critical screen criteria. Optimal alloys were selected from the 388,000 candidates. Compared with the reference alloy, two new alloys were experimentally verified to have superior or comparable compressive yield strength and creep resistance at 900 °C at the expense of oxidation resistance and density, while maintaining comparable cost. This work demonstrates the significant potential of combining high-throughput thermodynamic data with intelligent multi-objective optimization to accelerate the development of new alloys with tailored property profiles.
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Open AccessEditorial
Metallic Functional Materials: Development and Applications
by
Changlong Tan, Kun Zhang and Yan Feng
Metals 2026, 16(2), 153; https://doi.org/10.3390/met16020153 - 27 Jan 2026
Abstract
Metallic functional materials have become a strategic focus in contemporary material research, driven by the rising demand for intelligent, adaptive, and high-performance systems across energy conversion, aerospace actuation, biomedical devices, and next-generation flexible or micro-electromechanical technologies [...]
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(This article belongs to the Special Issue Metallic Functional Materials: Development and Applications)
Open AccessArticle
High-Temperature Mechanical Properties and Friction-Wear Performance of CrAlN Coatings Prepared by Arc Ion Plating via Mo Doping
by
Rongjun Yang, Lingxin Zhou, Songjie Zhou, Hongwu Liu, Weilin Chen, Weizhou Li and Minming Jiang
Metals 2026, 16(2), 152; https://doi.org/10.3390/met16020152 - 27 Jan 2026
Abstract
CrAlN coatings are widely used for surface protection because of their excellent properties. Alloying with additional elements has been shown to effectively modify mechanical and tribological behavior of these coatings. In this study, CrAlMoxN coatings (x = 0–18.83 at%) were prepared
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CrAlN coatings are widely used for surface protection because of their excellent properties. Alloying with additional elements has been shown to effectively modify mechanical and tribological behavior of these coatings. In this study, CrAlMoxN coatings (x = 0–18.83 at%) were prepared by an arc ion plating technology, corresponding to CrAlN and Mo-doped variants CrAlMoN-1, CrAlMoN-2 and CrAlMoN-3, respectively). The effects of Mo incorporation on the microstructure, mechanical properties, and friction-wear performance at both room and high temperature were systematically investigated. Results indicate that Mo dissolves into the CrAlN lattice to form a solid-solution structure, which induces lattice expansion as confirmed by the shift of XRD peaks toward lower angles. Furthermore, a moderate addition of Mo substantially improves the hardness, toughness, and crack propagation resistance of the coatings. All four coatings exhibit friction coefficients of approximately 0.5 at room temperature. However, at 600 °C, the CrAlMoN-2 coating demonstrates a much more stable friction coefficient curve and achieves the lowest average friction coefficient of 0.75, together with a wear rate of 3.94 × 10−6 mm3/N·m, indicating greatly improved high-temperature tribological performance.
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(This article belongs to the Section Corrosion and Protection)
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