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Metals

Metals is an international, peer-reviewed, open access journal published monthly online by MDPI.
The Spanish Materials Society (SOCIEMAT) is affiliated with Metals and their members receive discounts on the article processing charges.
Quartile Ranking JCR - Q2 (Metallurgy and Metallurgical Engineering)

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All Articles (14,742)

This study addresses the challenge of achieving efficient separation of vanadium and chromium from vanadium–chromium slag (VCS) while simultaneously tackling issues related to artificial granite waste residue (AGWR), such as its substantial stockpiling and associated air pollution. AGWR was used as a substitute calcination additive for calcium carbonate to achieve efficient separation through a calcination-leaching process. Orthogonal experiments were conducted to investigate the effects of AGWR addition amount, calcination temperature, and calcination time on the leaching behavior of vanadium and chromium. During calcination, vanadium reacts with CaO (a decomposition product of AGWR) to form acid-soluble calcium vanadate. Concurrently, chromium hydroxide decomposes into chromium oxide, which is poorly soluble in dilute acid. Subsequent leaching of the calcination product with dilute sulfuric acid leaches vanadium (V) into the solution, while chromium (Cr) remains in the residue, thus achieving separation. The experimental results showed that under the conditions of 30% AGWR addition; calcination at 850 °C for 1 h; leaching at 90 °C for 2 h with a liquid-to-solid ratio of 10:1 and a sulfuric acid concentration of 50 g·L−1; the leaching rate of vanadium reached 85.68%, whereas that of chromium was only 2.34%. These results demonstrate highly efficient separation of vanadium and chromium, offering valuable insights for resource recovery from both VCS and AGWR.

4 March 2026

Schematic diagram showing the sources of VCS and AGWR [10,21]. (a) Sources of VCS; (b) Sources of AGWR.

The seamless flatness roll is a critical inspection device in cold-rolled strip flatness control systems. Prolonged service causes cracks and scratches on the roll surface, while repeated grinding gradually removes the hardened layer, potentially rendering the roll unusable. To address the risk of thermal damage to internal sensors during the laser cladding repair of seamless flatness rolls, this study proposes a process optimization strategy using the Finite Element Method (FEM) and Response Surface Methodology (RSM). Focusing on an 820 mm roll, a regression prediction model for laser spot and internal component temperatures was constructed using a Box–Behnken design (BBD) based on an experimentally calibrated FEM model. Multi-objective optimization determined the optimal process parameters: laser power of 1.43 kW, laser radius of 3.73 mm, scanning speed of 23.45 mm/s, and overlap rate of 50.40%. Under these conditions, the average error between the predicted and experimental results was only 4.14%. The results confirm that the optimized process ensures the formation of a molten pool while maintaining internal components within safety thresholds, validating the feasibility of this non-destructive repair method.

4 March 2026

(a) Mild and (b) severe wear of seamless flatness roll surfaces.

To synergistically enhance the strength and toughness of low-alloy cast steels, a quenching–partitioning–tempering (Q-P-T) heat treatment process was specifically performed based on the “Constrained Carbon Equilibrium” thermodynamic model. The effects of partitioning temperature on microstructure and mechanical properties were examined. The Q-P(210)-T approach successfully produced an ultra-high strength cast steel (48SiNiMnCrMoAl6-4-4-3-8-14) with a tensile strength exceeding 2000 MPa and an elongation greater than 19.0%. The microstructure of this cast steel consists of tempered martensite (TM), bainite, ferrite, and retained austenite (RA). During tensile deformation, dislocations from adjacent martensite are absorbed by the film-like RA, thereby alleviating stress concentration induced by dislocations. Meanwhile, the transformation-induced plasticity (TRIP) effect of the RA significantly enhances the toughness of the cast steel. Furthermore, the ultra-high strength of the cast steel is jointly ensured by the fine crystalline strengthening of the martensite and the precipitation strengthening of the transitional carbides in the microstructure of the cast steel. This work provides a good reference for the development of high-performance cast steels.

4 March 2026

Equilibrium phase diagram of the tested steel: (a) The phase diagram calculation results showing the phase composition at different temperatures. (b) The fraction of phases at different temperatures.
  • Communication
  • Open Access

The revelation of the distribution of twin boundaries on three-dimensional (3D) grains is of critical importance for the comprehension of their influence on material properties. However, this remains a significant challenge in the field of 3D material characterization. In this study, the distribution of twin boundaries on the surfaces of 3D grains in solution-annealed 316L stainless steel was systematically and quantitatively characterized using 3D electron backscatter diffraction. The results show that the average size of twin boundaries is significantly larger than that of random boundaries (approximately 52% larger). Although the size distributions of grains, random boundaries, and twin boundaries, as well as the distributions of the total number of grain boundaries and the number of twin boundaries per grain, all conform to a lognormal distribution, the area fraction of twin boundaries on grain surfaces exhibits a typical Lorentz distribution, while their number fraction shows no clear pattern. On average, each grain possesses 9.6 boundaries, of which 1.7 are twin boundaries, and the average area coverage of twin boundaries on grain surfaces reaches 38.4%. The findings offer a 3D statistical foundation for optimizing grain boundary engineering strategies in austenitic alloys.

4 March 2026

(a) Reconstructed 3D-EBSD microstructure and (c) a representative 2D EBSD map, both colored according to the inverse pole figure (IPF) relative to the sample normal direction (Z-axis). (b) IPF color codes for grain orientation and grain boundary. Reconstructed 3D networks of (d) all grain boundaries, (e) random boundaries, and (f) twin boundaries, colored according to their misorientation angles.

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Metals - ISSN 2075-4701