1,431 Results Found

Metal Additive Manufacturing and Laser Powder Bed Fusion (LPBF), in particular, have come forth in recent years as an outstanding innovative manufacturing approach. The LPBF process is notably characterized by very high solidification and cooling rat...

Scanning electron microscopy is widespread in field of material science and research, especially because of its high surface sensitivity due to the increased interactions of electrons with the target material’s atoms compared to X-ray-oriented...

For the precise determination of orientations in polycrystalline materials, electron backscatter diffraction (EBSD) requires a consistent calibration of the diffraction geometry in the scanning electron microscope (SEM). In the present paper, the var...

Microstructures of a series of La-Mg-Ni-based superlattice metal hydride alloys produced by a novel method of interaction of a LaNi₅ alloy and Mg vapor were studied using a combination of X-ray energy dispersive spectroscopy and electron backscatter...

In recent decades, the automotive industry has faced challenges around improving energy efficiency, reducing pollutant emissions, increasing occupant safety, and reducing production costs. To solve these challenges, it is necessary to reduce the weig...

The Al₅Fe₂ intermetallic rouses interest due to its rapid formation at the interface between iron/steel and aluminum by reactive interdiffusion. Only in the last few years have the differently ordered states of that intermetallic been elucidated (&et...

It is, in general, essential to investigate correlations between the microstructure and properties of materials. Plastic deformation often localizes within thin layers. As a result, many material properties within such layers are very different from...

Additive manufacturing (AM) methods like powder bed fusion–laser beam (PBF-LB) enable complex geometry production. However, understanding and predicting the microstructural properties of AM parts remain challenging due to the inherent non-homog...

Residual stress/strain and microstructure used in additively manufactured material are strongly dependent on process parameter combination. With the aim to better understand and correlate process parameters used in electron beam melting (EBM) of Ti-6...

Electron backscatter diffraction (EBSD) has been used for more than 30 years for analyzing the structure of minerals and artificial substances. In recent times, EBSD has been widely applied for investigation of irradiated nuclear fuel and matrices fo...

The characteristics of texture and microstructure of lean duplex stainless steels with low Ni content produced through hot rolling followed by annealing were investigated locally with electron backscatter diffraction and globally with neutron diffrac...

Embrittlement induced by high-temperature tempering was investigated in two quenched-and-tempered offshore steels. Electron backscattering diffraction and analysis of Kernel average misorientation were applied to study the coalescence of martensite;...

The grain boundaries of three Laves phase-related body-center-cubic (bcc) solid-solution, metal hydride (MH) alloys with different phase abundances were closely examined by scanning electron microscopy (SEM), transmission electron microscopy (TEM), a...

Sub-micro dislocation cellular structures formed during rapid solidification break the strength–ductility trade-off in laser powder bed fusion (LPBF)-processed 316L stainless steel through high-density dislocations and segregated elements or pr...

The effect of equal channel angular pressing (ECAP) through the route Bc and aging treatment on the grain structure and properties of the Cu–1Cr–0.2Si alloy was investigated. Microstructure was detected by scanning electron microscopy (SE...

Low-angle grain boundaries (LAGBs) accommodate residual stress through the rearrangement and accumulation of dislocations during cold rolling. This study presents an electron wind force-based annealing approach to recover cold-rolling induced residua...

Additive manufacturing, particularly selective laser melting, presents exciting possibilities for fabricating components from high-temperature nickel-based superalloys. Controlling microstructural features and minimizing defects in fabricated specime...

The evolutions of the microstructure and its effect on the mechanical and electrical conductivity properties of Cu1.5Cr0.1Si alloy after equal channel angle pressing (ECAP)-C path deformation and aging treatment have been investigated using scanning...

This study investigated the susceptible sites for pit nucleation in a transformation-induced plasticity (TRIP) Fe₃₉Mn₂₀Co₂₀Cr₁₅Si₅Al₁ (at.%) high-entropy alloy (HEA) in 3.5 wt.% NaCl solution. The investigation involved a constant-load stress corrosi...

The formation and growth kinetics of the reverted austenite during tempering in 13Cr supermartensitic stainless steel were investigated by a combination X-ray diffraction (XRD), transmission electron microscopy (TEM) and electron backscatter diffract...

The growth of $\alpha$-quartz-based piezoelectric thin films opens the door to higher-frequency electromechanical devices than those available through top-down approaches. We report on the growth of SiO${}_2$/GeO${}_2$ thin films by pulsed laser deposition and their...

The effect of welding speed on microstructure, mechanical properties, and corrosion properties of laser-assisted welded joints of a twinning-induced plasticity (TWIP) steel was investigated by using X-ray diffraction (XRD), scanning electron microsco...

Accurate phase fraction analysis is an essential element of the microstructural characterization of alloys and often serves as a basis to quantify effects such as heat treatment or mechanical deformation. Additive manufacturing (AM) of metals, due to...

A microstructure evolution of the thermomechanically processed 3Mn-1.5Al type steel and mechanical stability of retained austenite were investigated during interrupted tensile tests. The microstructural details were revealed using scanning electron m...

In this article we discuss the effect of different test parameters on the analysis of retained austenite in TRIP590, TRIP780 and X90 steels, by means of Electron Backscattered Diffraction (EBSD) and X-ray Diffraction (XRD), respectively. By analyzing...

The “gold dust defect” (GDD) appears at the surface of ferritic stainless steels (FSS) and degrades their appearance. Previous research showed that this defect might be related to intergranular corrosion and that the addition of aluminium...

Iron hollow sphere filled aluminum matrix syntactic foams (AMSFs) were produced by low pressure, inert gas assisted infiltration. The microstructure of the produced AMSFs was investigated by light and electron microscopy, extended by energy dispersiv...

Yellow cuboid diamonds are commonly found in diamondiferous alluvial placers of the Northeastern Siberian platform. The internal structure of these diamonds have been studied by optical microscopy, X-Ray topography (XRT) and electron backscatter diff...

Understanding the effects of wheel-rail contact on the microstructure of rails is an important issue for railway management. The impact of wheel-rail contact and surface preparation on the microstructure of rails is studied using a rolling contact be...

Yttria-stabilized zirconia (YSZ) coatings with typical pyramid columnar and dense layered structure were prepared by plasma spray-physical vapor deposition (PS-PVD). The evolution behavior of microstructure and crystallography of the coatings before...

Electron backscatter diffraction (EBSD) is an excellent tool for characterizing the crystallographic orientation aspects of the microstructure of polycrystalline material. In some additively manufactured materials, the material may undergo a phase tr...

It has been reported that a multiphase microstructure with bainite, martensite, and retained austenite obtained by austempering, or quenching and tempering of spring steel containing Si, Mn, and Cr exhibits high strength and ductility. However, littl...

Pure shear tests of textured magnesium AZ31B sheet samples were carried out using a 5 kN Kammrath & Weiss in situ tension-compression stage in a scanning electron microscope in combination with real-time electron backscatter diffraction lattice o...

A type of advanced γ-TiAl-based alloy called β-solidifying γ-TiAl has elicited remarkable research interest in the last few decadesbecause of its excellent workability and homogeneous microstructures. Thermomechanical treatments are...

Graphene films were grown by chemical vapor deposition on Cu foil. The obtained samples were characterized by Raman spectroscopy, ellipsometry, X-ray photoelectron spectroscopy and electron back-scatter diffraction. We discuss the time-dependent chan...

Microstructure optimization of Al-Zn-Mg-Cu-Zr aluminum alloys, particularly through recrystallization inhibition, for improved strength and corrosion resistance properties has been an important consideration in alloy development for aerospace applica...

Bi₆Fe₂Ti₃O₁₈ (BFTO) ceramics were synthesized via a solid-state reaction route using stoichiometric amounts of Bi₂O₃, TiO₂, and Fe₂O₃ powders. A thermal analysis of the powder mixture was conducted to optimize the heat treatment parameters. Energy-di...

The transformation mechanism of reverted austenite and the amount of reverted austenite during the tempering process in supermartensitic stainless steel have been investigated by X-ray diffraction (XRD), electron backscattered diffraction (EBSD), and...

The paper presents new data on the internal structure of super-deep (sublithospheric) diamonds from Saõ-Luiz river placers (Brazil) and from alluvial placers of the northeastern Siberian platform (Yakutia). The sublithospheric origin of these...

The FeCoNiCrAl_0.1 high entropy alloys (HEAs) and pure copper (Cu) composite plates were successfully fabricated by the explosive welding technique using two different gap distances. The interfacial microstructure, elemental distribution, grain struct...

In this study, the grain boundary character and texture of 50% and 90% cold-rolled FePd alloy was investigated during recrystallization at 700 °C. Electron backscatter diffraction (EBSD) measurements were performed on the rolling direction to normal...

Laser shock peening (LSP) is an innovative technique that is used to enhance the fatigue strength of structural materials via the generation of significant residual stress. The present work was undertaken to evaluate the degree of plastic strain intr...

A novel approach for the correlation of local martensite tetragonality determined by electron backscatter diffraction and carbon distribution by atom probe tomography (APT) is presented. The two methods are correlated by site-specific sample preparat...

The present work was undertaken to shed additional light on the globular-α microstructure produced during FSP of Ti-6Al-4V. To this end, the electron backscatter diffraction (EBSD) technique was employed to characterize the crystallographic asp...

The severe sliding abrasion of single-phase metallic materials is a complex issue with a gaining importance in industrial applications. Different materials with different lattice structures react distinctly to stresses, as the material reaction to we...

We have investigated the impact of the process parameters for the selective laser melting (SLM) of the stainless steel AISI 316L on its microstructure and mechanical properties. Properly selected SLM process parameters produce tailored material prope...

The development of metal nanocomposites reinforced by carbon nanotubes (CNTs) remains a focus of the scientific community due to the growing need to produce lightweight advanced materials with unique mechanical properties. However, for the successful...

Small objects of an alloy tool steel were built by selective laser melting at different scan speeds, and their microstructures were analyzed using electron backscatter diffraction (EBSD). To present an explicit correlation with the local thermal cycl...

This paper reports on an investigation of crystallographic texture of as-built and heat-treated Ti6Al4V (ELI) produced by direct metal laser sintering (DMLS). The texture analyses were conducted using electron backscatter diffraction (EBSD). The &bet...

The microstructure of austempered ductile iron was investigated by electron backscatter diffraction technique. The results show that the orientation relationship between acicular bainitic ferrite and austenite is Greninger–Troiano relationship. A sin...