Journal of Manufacturing and Materials Processing

Ti-6Al-4V titanium is considered a difficult-to-cut material used in critical applications in the aerospace industry requiring high reliability levels. An appropriate selection of cutting conditions can improve the machinability of this alloy and the surface integrity of the machined surface, including the generation of compressive residual stresses. In this paper, orthogonal cutting tests of Ti-6Al-4V titanium were performed using coated and uncoated tungsten carbide tools. Suitable design of experiments (DOE) was used to investigate the influence of the cutting conditions (cutting speed V_c, uncut chip thickness h, tool rake angle γ_n, and the cutting edge radius r_n) on the forces, chip compression ratio, and residual stresses. Due to the time consumed and the high cost of the residual stress measurements, they were only measured for selected cutting conditions of the DOE. Then, the machine learning method based on mathematical regression analysis was applied to predict the residual stresses for other cutting conditions of the DOE. Finally, the optimal cutting conditions that minimize the machining outcomes were determined. The results showed that when increasing the compressive residual stresses at the machined surface by 40%, the rake angle should be increased from negative (−6°) to positive (5°), the cutting edge radius should be doubled (from 16 µm to 30 µm), and the cutting speed should be reduced by 67% (from 60 to 20 m/min). Full article

Fused filament fabrication (FFF) is a widely used additive manufacturing process that can produce parts from thermoplastics. Its ease of operation and wide variety of materials make it a popular choice for manufacturing. To leverage such benefits, the commonly used thermoplastics (e.g., PLA and ABS) are impregnated with nanoparticles, short or continuous fibers, and other additives. The addition of graphene nanoplatelets to PLA makes for a high-quality filament possessing enhanced mechanical, electrical, and thermal properties. Even with the advancement in materials, the optimisation of the process parameter remains the most complex aspect for FFF. Therefore, this study investigates the influence of two under-researched and overlooked processing parameters (material extrusion rates and line widths) on commercially available graphene-enhanced PLA (GPLA). Nine different material extrusion rates (70% to 150%) and five different line widths (0.2 mm to 1 mm) were used to manufacture GPLA specimens using a low-cost, desktop-based 3D printer, as per British and international standards. The study analyses the influence of these two processing parameters on mass, dimensional accuracy, surface texture, and mechanical properties of GPLA specimens. A non-destructive test has also been conducted and correlated with three-point flexural test to establish its applicability in evaluating flexural properties of GPLA. The results how that small line widths provide more accuracy with longer print times whereas large line widths offer more strength with shorter printing times. Increase in material extrusion rates adversely affect the surface finish and hardness but positively influence the flexural strength of GPLA specimens. The study shows that the manipulation of material extrusion rates and line widths can help designers in understanding the limitations of the default printing settings (100% material extrusion rate and 0.4 mm line width) on most desktop 3D printers and identifying the optimal combination to achieve desired properties using the FFF process. Full article

The shape and size of processed materials play a crucial role in the solid conveying characteristics of single-screw extruders. Thus, the increasing amount of plastic regrind leads to new challenges in screw extrusion. This work investigates the conveying behavior of three distinctly different material shapes in an axially as well as a helically grooved solid conveying zone. A uniform virgin polypropylene (PP) granule, an irregularly plate-shaped PP regrind and a powdery polyethylene (PE) are processed at screw speeds up to 1350 rpm. Thereby, frictionally engaged conveying in the grooves is visualized for the utilized powder. Similarly, the virgin granule is subject to forced conveying by interlocking in the grooves. The experimentally determined throughput is furthermore compared to analytical calculations which assume a so-called nut–screw conveying. It is found that these calculations perfectly predict the throughput when processing the virgin granule and the powder in a helically grooved barrel. In contrast, the analytical calculation significantly underestimates the throughput for the regrind. This underestimation is expected to be mainly caused by its plate shape and a difference in bulk density. The actual bulk density in the extruder is probably significantly higher due to both orientation and compaction effects compared to the measured bulk density that is used for the analytical calculation. Additionally, the regrind exhibits a fluctuating throughput due to the non-constant bulk density, which results from an irregular regrind shape and a broad size distribution. Full article

Although industry 4.0 has gained increased attention in the industry, academic, and governmental fields, there is a lack of information about the relationship between this digital transformation and sustainable development. This work explores the concept of sustainability applied in industry 4.0 and the main advantages that this revolution incorporates into society. To this end, a conscientiously documented investigation was conducted by reviewing actual case studies or scenarios where sustainability was applied in different manufacturing industries, enterprises, or research fields worldwide. A critical and descriptive analysis of the information was performed to identify the main tools and procedures that can be implemented in the industry to address the triple bottom line perspective of industry 4.0, and the results are presented in this document. From the analysis, it was observed that currently, I4.0 has been mainly adopted to improve efficiency and cost reduction in manufacturing companies. However, since only a few enterprises embrace the social paradigm of I4.0, a significant gap in understanding and unbalance is visualized. Therefore, we conclude that there is a lack of information on social benefits and the barriers that must be overcome from the social perspective. On the other hand, this work highlights the importance of adopting industry 4.0 as a positive way to improve the performance of emerging technologies, such as fuel cells, solar cells, and wind turbines, while producing products or services with high efficiency and profitability incomes. For practitioners, this work can provide insightful information about the real implications of I4.0 from a sustainability perspective in our daily life and the possible strategies to improve sustainable development. Full article

Surface properties of injection molded parts have a strong effect on the visual and haptic perception of the parts by customers. Especially for injection molded automotive interior parts, grained surfaces can often be found. In conventional tooling, graining requires separate process steps. This makes the realization of grained injection molded prototype parts very complex. By additive manufacturing of injection molds in prototype tooling, it is possible to print micro structures into the mold surface in one printing operation. An injection mold with four different graining structures varying in depth and distance was designed and additively manufactured. The specification regarding the surface graining was analyzed by means of roughness measurements of the CAD model, injection mold and injection molded parts. Results show the feasibility of highly controllable additive surface graining. Full article

In this contribution, the influence of the reaction injection moulding process on the thermomechanical material behaviour of aliphatic hexamethylene diisocyanate (HDI) based fast curing polyurethane is demonstrated. Uniaxial tensile tests, temperature-frequency dependent dynamic mechanical thermal analysis (DMTA) and Differential Scanning Calorimetry (DSC) are used to show the differences in properties for ten different sets of process parameters. The mould and resin components temperature, the mass flow during the filling process and the residence time during the reaction process of the polyurethane are varied in several stages. Further experiments to determine the molar mass of the molecular chain between two crosslinking points of the polyurethane are used to explain the process influences on the thermomechanical properties. Thus, a direct correlation between manufacturing and material properties is shown. In addition, the mutual effect of the different parameters and their overall influence on the material behaviour is presented. Full article

AlSi10Mg is the most widely additively manufactured and commercialized aluminum alloy and has been used in this study to analyze the effect of heat treatment on its microstructure and mechanical properties. Although research indicates AlSi10Mg parts produced by selective laser melting have characteristically very fine microstructures, there is a need for more intensive study to comprehend the effect of heat treatment on the mechanical properties of this alloy by analyzing its microstructure. In this study, AlSi10Mg specimens heat-treated at varying temperatures were analyzed by optical and electron microscopes. Micro-indentation hardness and tensile tests were performed to evaluate mechanical properties while considering the specimen build orientation. Observation shows that it is nearly impossible to completely dissolve the evolved second phase silicon-rich particles, which may have significant effects on the mechanical characteristics. Electron microscopy images show the evolution of iron-rich particles in the Al matrix, which may have a significant influence on the mechanical properties of the alloy. Full article

The thermal load that occurs during grinding can be reduced with the aid of an optimized metalworking fluid (MWF) supply. In previous work, mainly the free jet was considered for the determination of the conditions required for an optimized MWF supply. An investigation of the interaction area between the MWF and the grinding wheel has not yet been carried out due to the lack of suitable measurement techniques. In the presented work, both the free jet and the interaction area are analyzed with the aid of new metrological analysis and evaluation methods based on high-speed records (shadowgraphy and shadogram imaging velocimetry) in order to assess the free jet geometry and velocities, as well as the velocity distribution and the MWF amount in the interaction area. Using this approach, the following main results were derived: (1) The free jet velocity remains approximately constant in a defined free jet cross-section even at high distances from the nozzle outlet. (2) The velocity distribution in the interaction area is mainly influenced by the flow rate. (3) A new image parameter (black pixel fraction) was derived for the evaluation of the MWF supply to the contact zone. Full article

Welded joints show a comparably low fatigue strength compared to the base material. Thus, different post-weld treatment methods are used to enhance the fatigue strength of welded joints. A promising method to enhance the fatigue strength of metallic components is the deep rolling process, but this has rarely been applied to welds. For the qualification of the deep rolling process as an effective post-weld treatment method, knowledge about its influence on the surface and subsurface properties at the fatigue critical weld toe is necessary. Here, geometrical and metallurgical inhomogeneities lead to complex contact states between deep rolling tools and weld toes. Thus, for a first analysis of the local deformation behavior during deep rolling of welded joints, experimentally and numerically generated deep rolling single tracks are compared. Cyclic strain-controlled tests to determine the material behavior were carried out for the numerical analyses using finite element simulation. The presented study shows that it is possible to describe the local deformation of welded joints during deep rolling using finite element simulation. A correct depiction of material behavior is crucial for such an analysis. It was shown that certain irregularities in material behavior lead to lower coincidences between simulation and experiment, especially for the investigated welds, where only low differences in hardness between base material, heat-affected zone, and filler material were found. Full article

A pair of punch and die was often fabricated using subtractive manufacturing processes such as milling and other machining processes. However, additive manufacturing could be used to perform the same processes. This study explored this possibility. In particular, this study fabricated a pair of T-shaped punch and die made of AISI316L austenitic stainless steel using an additive manufacturing process called plasma-assisted 3D printing. Accordingly, T-shaped negative and positive 2D patterns were screen-printed onto the mirror-polished surfaces of the substrates made of AISI316L austenitic stainless steel. The printed film worked like a mask to prevent the printed substrate surfaces from nitriding. In order to form a thick nitrided layer, the unprinted substrate surfaces were selectively nitrided at 673 K for 14.4 ks. The un-nitrided segments of the substrates were uniformly removed by sand-blasting that involved shooting silica particles on the substrate’s surfaces. As a result, the substrates printed with negative and positive T-shaped patterns were transformed into the punch head and die cavity. In order to see the efficacy of the fabricated punch and die pair, this pair was used for piercing the electrical steel sheets under a controlled clearance. Scanning Electron Microscopy with Energy Dispersive X-ray (SEM-EDX) was used to measure surface topography after piercing. In addition, SEM and a 3D profilometer were used to measure the punch and die profiles after piercing. The abovementioned measurement results showed that the fabricated punch and die exhibited highly accurate piercing behavior. Thus, the plasma-assisted 3D printing was useful for punch and die fabrication. Full article

Austenitic high-manganese steels (HMnS) offer very high wear resistance under dynamic loading due to their high work hardening capacity. However, resistance to static abrasive loading is limited. Various approaches to increasing abrasion resistance are known from traditionally manufactured metallurgical components. These confirm the high potential for surface protection applications. In this work, the powder of the Hadfield HMnS X120Mn12 is prepared and processed by high-velocity oxy-fuel (HVOF) spraying and spark-plasma sintering (SPS). A good correlation was observed between the results of the HVOF and SPS specimen. Different surface conditions of the coatings and the sintered specimens were prepared by machining. Compared to the polished state, turning and diamond smoothing can increase the surface hardness from 220 HV to over 700 HV significantly. Regardless of the surface finish condition, similar good wear resistance can be demonstrated due to strong work hardening under sliding and reciprocating wear loading. In contrast, the finish machining process clearly influences abrasion resistance in the scratch test with the best results for the diamond smoothed condition. Especially against the background of current trends toward alternative coating systems, the presented results offer a promising approach for the development of HMnS in the field of coating technology. Full article

We investigated the temperature increase caused by heat generation from plastic deformation during β-processed forging in a near-β titanium alloy, Ti-17 alloy (Ti-5Al-2Sn-2Zr-4Cr-4Mo, wt%), by inserting thermocouples into large workpieces (100 mm in diameter and 50 mm in height). The workpiece was initially heated and held at 1193 K (920 °C) in the single-β region. It was subsequently forged between hot dies in surrounding heaters at a compression percentage of 75% at strain rates of 0.05 and 0.5 s⁻¹ at 1023–1123 K in the (α + β) region. At 0.05 s⁻¹, the temperature logarithmically increased by 39 K in 28 s for 1023 K; it increased by 30 K in 28 s for 1073 K. However, at 0.5 s⁻¹, the material temperature increased, in 3 s, beyond or close to the β-transus temperature during forging at 1023 and 1073 K. In addition, as the forging temperature decreased, the increase in material temperature moderated, resulting in a difference of 27 K in the last forging stage, between the conditions of 1023 and 1073 K. This would reduce the temperature difference effect on microstructure formation during β-processed forging. Full article

The present paper proposes a combined tribo-mechanical methodology for assessing friction under conditions representative of metal cutting, without resorting to machining process monitoring. The purpose is to withdraw the size effect’s contribution due to tool edge radius to the well-known overestimation of the friction coefficient. Comparative numerical analysis of several tribological tests led us to conclude that the ring compression test is one of the most suitable for reproducing the frictional conditions at the chip–tool interface. Two distinct metallic alloys were selected to demonstrate the application of the proposed methodology (UNS L51120 lead alloy and 18Ni300 maraging steel in conventional and additively manufactured conditions). The results help to better explain the influences of process parameters on the friction coefficient value under high temperature and high strain rate conditions. Results showed a typical increase in the coefficient of friction of up to 20% due to both temperature and strain rate parameters for 18Ni300. The results are of interest because they allow considering potential sources of error in the numerical simulation of metal cutting when the same friction coefficient value is considered for a wide range of cutting parameters. Full article

Process variables of bioprinting (including extrusion pressure, nozzle size, and bioink composition) can affect the shape fidelity and cell viability of printed constructs. Reported studies show that increasing extrusion pressure or decreasing nozzle size would decrease cell viability in printed constructs. However, a smaller nozzle size is often necessary for printing constructs of higher shape fidelity, and a higher extrusion pressure is usually needed to extrude bioink through nozzles with a smaller diameter. Because values of printing process variables that increase shape fidelity can be detrimental to cell viability, the optimum combination of variables regarding both shape fidelity and cell viability must be determined for specific bioink compositions. This paper reports a designed experimental investigation (full factorial design with three variables and two levels) on bioprinting by applying layer-by-layer photo-crosslinking and using the alginate-methylcellulose-GelMA bioink containing algae cells. The study investigates both the main effects and interaction effects of extrusion pressure, nozzle size, and bioink composition on the shape fidelity and cell viability of printed constructs. Results show that, as extrusion pressure changed from its low level to its high level, shape fidelity and cell viability decreased. As nozzle size changed from its low level to its high level, shape fidelity decreased while cell viability increased. As bioink composition changed from its low level (with more methylcellulose content in the bioink) to its high level (with less methylcellulose content in the bioink), shape fidelity and cell viability increased. Full article

Heat generation is a critical issue in grinding. If the grinding point generates significant heat, dimensional and shape accuracy may decrease due to thermal deformation, and the machined surface may deteriorate due to grinding burn. Therefore, monitoring the temperature during grinding is important to obtain ideal machining results. In this research, we develop a new method to measure the grinding surface and grinding wheel surface temperature during in-process machining. The proposed method measures the temperature of the grinding surface through small holes in a rotating grinding wheel. Using this method, we measured the temperature of the grinding surface during the dry grinding of carbon fiber reinforced plastics (CFRP). Temperature of the grinding surface was measured every 1/4 rotation of the grinding wheel at any depth of cut, assuming precision grinding, rough grinding, and high-efficiency grinding. The measurement value changed depending on the temperature measurement position of the infrared thermometer from numerical analysis of the grinding surface temperature. We also found that when the cut depth was small, the temperature, including the surface of the workpiece before machining, was measured at a specific temperature measurement position. The newly developed temperature measurement method was capable of in-process measurement of the grinding surface temperature and of detecting temperature rise when the grinding wheel was clogged. Full article

Surface finishing is challenging in the context of additively manufactured components with complex geometries. Magnetic abrasive finishing (MAF) is a promising surface finishing technology that can refine the surface quality of components with complex shapes produced by additive manufacturing. However, there is insufficient study regarding the impact of MAF on microstructure–property relationships for additively manufactured builds, which is critical for evaluating mechanical performance. In this work, we studied the effects of different combinations of MAF and heat treatment steps on the microstructure–property relationships of Inconel 718 superalloys made by laser powder bed fusion (LPBF). The application of MAF was found to significantly reduce the surface roughness and refine the grain size of aged alloys. Moreover, MAF was able to increase the alloy elongation, which could be further influenced by the sequence of MAF and different heat treatment steps. The highest elongation could be achieved when MAF was performed between homogenization and aging processes. This work indicates that an effective combination of surface finishing and heat treatment is critical for the improvement of alloy performance. Furthermore, it demonstrates a promising solution for improving the performance of LPBF Inconel 718 by integrating MAF and heat treatment, which provides new perspectives on the post-processing optimization of additively manufactured alloys. Full article

Acoustic emission (AE) signals collected from different locations might provide various sensitivities to tool wear condition. Studies for tool wear monitoring using AE signals from sensors on workpieces has been reported in a number of papers. However, it is not feasible to implement in the production line. To study the feasibility of AE signals obtained from sensors on spindles to monitor tool wear in micro-milling, AE signals obtained from the spindle housing and workpiece were collected simultaneously and analyzed in this study for micro tool wear monitoring. In analyzing both signals on tool wear monitoring in micro-cutting, a feature selection algorithm and hidden Markov model (HMM) were also developed to verify the effect of both signals on the monitoring system performance. The results show that the frequency responses of signals collected from workpiece and spindle are different. Based on the signal feature/tool wear analysis, the results indicate that the AE signals obtained from the spindle housing have a lower sensitivity to the micro tool wear than AE signals obtained from the workpiece. However, the analysis of performance for the tool wear monitoring system demonstrates that a 100% classification rate could be obtained by using spindle AE signal features with a frequency span of 16 kHz. This suggests that AE signals collected on spindles might provide a promising solution to monitor the wear of the micro-mill in micro-milling with proper selection of the feature bandwidth and other parameters. Full article

High quality and long product life are two fundamental requirements for all circuit carriers, including molded interconnect devices (MID), to find application in various fields, such as automotive, sensor technology, medical technology, and communication technology. When developing a MID for a certain application, not only the design, but also the choice of material as well as the process parameters need to be carefully considered. A well-established method to evaluate the lifetime of such MID, respective of their conductor tracks, is the thermal shock test, which induces thermomechanical stresses upon cycling. Even though this method has numerous advantages, one major disadvantage is its long testing time, which impedes rapid developments. Addressing this disadvantage, this study focuses on the laser direct structuring of thermoplastic LCP Vectra E840i LDS substrates and the subsequent electroless metallization of the commonly used layer system Cu/Ni/Au to force differences in the conductor tracks’ structure and composition. Performing standardized thermal shock tests alongside with flexural fatigue tests, using a customized setup, allows comparison of both methods. Moreover, corresponding thermomechanical simulations provide a direct correlation. The flexural fatigue tests induce equivalent or even higher mechanical stresses at a much higher cycling rate, thus drastically shorten the testing time. Full article

Metal additive-manufacturing technologies enable the production of complex geometries. However, high manufacturing costs hinder these technologies being employed in some industries. In this sense, a hybrid strategy is presented in this paper, to achieve the best of additive and subtractive technologies, offering economic advantages. AlSi10Mg aluminium powder was deposited on AW-6082 pre-machined substrates and mechanical and thermal properties of these specimens were evaluated considering the application of a stress relief heat treatment. The results were especially good in the compressive mechanical properties and in the thermal properties: compressive properties were improved by up to 27%, and the specific heat capacity and coefficient of thermal expansion were reduced by up to 38%, compared to additively manufactured AlSi10Mg. Therefore, hybrid manufacturing can be a profitable solution (i) in thermal management applications, (ii) when compressive loads are presented, or (iii) to repair damaged parts, providing a circular economy, as presented in a case study of this paper. Full article