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Materials, Volume 9, Issue 11

2016 November - 95 articles

Cover Story: Multi-scale analysis of concrete requires validation and determination of input parameters at all scales. This paper presents techniques for making, testing and modelling micro-cubes of cement paste. The micro-cubes are made by precision cutting, grinding and micro-dicing. The microstructure is determined by X-ray tomography. Mechanical testing of the micro-cubes is performed by nano-indentation and the modelling is done by a lattice fracture model. View the paper
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Articles (95)

  • Article
  • Open Access
64 Citations
7,008 Views
14 Pages

Fabrication of Al/Mg/Al Composites via Accumulative Roll Bonding and Their Mechanical Properties

  • Jinfeng Nie,
  • Mingxing Liu,
  • Fang Wang,
  • Yonghao Zhao,
  • Yusheng Li,
  • Yang Cao and
  • Yuntian Zhu

23 November 2016

Al(1060)/Mg(AZ31)/Al(1060) multilayered composite was successfully produced using an accumulative roll bonding (ARB) process for up to four cycles at an elevated temperature (400 °C). The microstructure evolution of the composites and the bonding cha...

  • Article
  • Open Access
44 Citations
7,388 Views
15 Pages

The Effect of Curing Temperature on the Properties of Cement Pastes Modified with TiO2 Nanoparticles

  • Karine Pimenta Teixeira,
  • Isadora Perdigão Rocha,
  • Leticia De Sá Carneiro,
  • Jessica Flores,
  • Edward A. Dauer and
  • Ali Ghahremaninezhad

23 November 2016

This paper investigates the effect of curing temperature on the hydration, microstructure, compressive strength, and transport of cement pastes modified with TiO2 nanoparticles. These characteristics of cement pastes were studied using non-evaporable...

  • Article
  • Open Access
4,631 Views
8 Pages

Recording Characteristics, Microstructure, and Crystallization Kinetics of Ge/GeCu Recording Film Used for Write-Once Blu-Ray Disc

  • Sin-Liang Ou,
  • Feng-Min Lai,
  • Wei-Kai Wang,
  • Shih-Yung Huang,
  • An-Cheng Sun,
  • Ching-Ho Tien,
  • Zhi-Jia Xu,
  • Chin-Yen Yeh and
  • Kuo-Sheng Kao

23 November 2016

A Ge67Cu33 (16 nm) layer and a Ge (3 nm)/Ge67Cu33 (16 nm) bilayer were grown by sputtering at room temperature and used as the recording films for write-once blue laser media. In comparison to the crystallization temperature of Ge in a GeCu film (380...

  • Article
  • Open Access
13 Citations
6,110 Views
11 Pages

Effects of BMP-2 Delivery in Calcium Phosphate Bone Graft Materials with Different Compositions on Bone Regeneration

  • Jin-Chul Park,
  • Eun-Bin Bae,
  • Se-Eun Kim,
  • So-Yun Kim,
  • Kyung-Hee Choi,
  • Jae-Won Choi,
  • Ji-Hyeon Bae,
  • Jae-Jun Ryu and
  • Jung-Bo Huh

23 November 2016

This study was undertaken to investigate the effect of loading rhBMP-2 onto biphasic calcium phosphate (BCP) and calcium pyrophosphate (CPP) on bone regeneration, and to examine the efficacies of BCP and CPP as rhBMP-2 carriers. Specimens were divide...

  • Article
  • Open Access
61 Citations
8,552 Views
16 Pages

Protein-Mediated Precipitation of Calcium Carbonate

  • Izabela Polowczyk,
  • Anna Bastrzyk and
  • Marta Fiedot

22 November 2016

Calcium carbonate is an important component in exoskeletons of many organisms. The synthesis of calcium carbonate was performed by mixing dimethyl carbonate and an aqueous solution of calcium chloride dihydrate. The precipitation product was characte...

  • Article
  • Open Access
16 Citations
7,188 Views
13 Pages

Laboratory Testing of Silica Sol Grout in Coal Measure Mudstones

  • Dongjiang Pan,
  • Nong Zhang,
  • Zhengzheng Xie,
  • Xiaowei Feng and
  • Yong Kong

22 November 2016

The effectiveness of silica sol grout on mudstones is reported in this paper. Using X-ray diffraction (XRD), the study investigates how the silica sol grout modifies mudstone mineralogy. Micropore sizes and mechanical properties of the mudstone befor...

  • Article
  • Open Access
29 Citations
7,869 Views
12 Pages

Targeted Magnetic Nanoparticles for Mechanical Lysis of Tumor Cells by Low-Amplitude Alternating Magnetic Field

  • Adi Vegerhof,
  • Eran A. Barnoy,
  • Menachem Motiei,
  • Dror Malka,
  • Yossef Danan,
  • Zeev Zalevsky and
  • Rachela Popovtzer

22 November 2016

Currently available cancer therapies can cause damage to healthy tissue. We developed a unique method for specific mechanical lysis of cancer cells using superparamagnetic iron oxide nanoparticle rotation under a weak alternating magnetic field. Iron...

  • Article
  • Open Access
29 Citations
6,824 Views
14 Pages

22 November 2016

Perforated wooden panels are typically utilized as a resonant sound absorbing material in indoor noise control. In this paper, the absorption properties of wooden panels perforated with tiny holes of 1–3 mm diameter were studied both experimentally a...

  • Article
  • Open Access
31 Citations
5,842 Views
18 Pages

A Bayesian Approach for Sensor Optimisation in Impact Identification

  • Vincenzo Mallardo,
  • Zahra Sharif Khodaei and
  • Ferri M. H. Aliabadi

22 November 2016

This paper presents a Bayesian approach for optimizing the position of sensors aimed at impact identification in composite structures under operational conditions. The uncertainty in the sensor data has been represented by statistical distributions o...

  • Article
  • Open Access
16 Citations
5,361 Views
15 Pages

Prediction of Three-Dimensional Downward Flame Spread Characteristics over Poly(methyl methacrylate) Slabs in Different Pressure Environments

  • Kun Zhao,
  • Xiao-Dong Zhou,
  • Xue-Qiang Liu,
  • Lei Lu,
  • Zhi-Bo Wu,
  • Fei Peng,
  • Xiao-Yu Ju and
  • Li-Zhong Yang

22 November 2016

The present study is aimed at predicting downward flame spread characteristics over poly(methyl methacrylate) (PMMA) with different sample dimensions in different pressure environments. Three-dimensional (3-D) downward flame spread experiments on fre...

  • Article
  • Open Access
79 Citations
10,567 Views
22 Pages

The Effect of Acceptor and Donor Doping on Oxygen Vacancy Concentrations in Lead Zirconate Titanate (PZT)

  • Christoph Slouka,
  • Theresa Kainz,
  • Edvinas Navickas,
  • Gregor Walch,
  • Herbert Hutter,
  • Klaus Reichmann and
  • Jürgen Fleig

22 November 2016

The different properties of acceptor-doped (hard) and donor-doped (soft) lead zirconate titanate (PZT) ceramics are often attributed to different amounts of oxygen vacancies introduced by the dopant. Acceptor doping is believed to cause high oxygen v...

  • Article
  • Open Access
15 Citations
7,448 Views
21 Pages

Efficient Solar-Induced Photoelectrochemical Response Using Coupling Semiconductor TiO2-ZnO Nanorod Film

  • Nur Azimah Abd Samad,
  • Chin Wei Lai,
  • Kung Shiuh Lau and
  • Sharifah Bee Abd Hamid

22 November 2016

Efficient solar driven photoelectrochemical (PEC) response by enhancing charge separation has attracted great interest in the hydrogen generation application. The formation of one-dimensional ZnO nanorod structure without bundling is essential for hi...

  • Article
  • Open Access
22 Citations
7,229 Views
19 Pages

22 November 2016

Halloysite nanotubes-thermoplastic polyurethane (HNTs-TPU) nanocomposites are attractive products due to increasing demands for specialized materials. This study attempts to optimize the parameters for injection just before marketing. The study shows...

  • Article
  • Open Access
21 Citations
8,999 Views
12 Pages

Friction and Wear Reduction of Eccentric Journal Bearing Made of Sn-Based Babbitt for Ore Cone Crusher

  • Auezhan Amanov,
  • Byungmin Ahn,
  • Moon Gu Lee,
  • Yongho Jeon and
  • Young-Sik Pyun

22 November 2016

An anti-friction Babbitt alloy-coated bearing made by a casting process is a journal bearing, which is used in an ore cone crusher eccentric. The main purpose of the Babbitt coated eccentric is to provide a low friction to support and guide a rotatin...

  • Article
  • Open Access
23 Citations
7,760 Views
12 Pages

In Vitro and In Vivo Study of a Novel Porcine Collagen Membrane for Guided Bone Regeneration

  • Eisner Salamanca,
  • Chi-Yang Tsai,
  • Yu-Hwa Pan,
  • Yu-Te Lin,
  • Haw-Ming Huang,
  • Nai-Chia Teng,
  • Che-Tong Lin,
  • Sheng-Wei Feng and
  • Wei-Jen Chang

22 November 2016

For years, in order to improve bone regeneration and prevent the need of a second stage surgery to remove non-resorbable membranes, biological absorbable membranes have gradually been developed and applied in guided tissue regeneration (GTR). The pre...

  • Article
  • Open Access
3 Citations
6,941 Views
15 Pages

21 November 2016

A 3D finite element model constructed to predict the intensity-dependent refractive index profile induced by femtosecond laser radiation is presented. A fiber core irradiated by a pulsed laser is modeled as a cylinder subject to predefined boundary c...

  • Article
  • Open Access
5 Citations
5,419 Views
18 Pages

18 November 2016

This article presents a combined use of a retarder (d-gluconic acid) and an alkaline activator (sodium hydroxide) in a binder system based on ground granulated blast-furnace slag. The properties of the retarder are extending the dormant hydration per...

  • Feature Paper
  • Communication
  • Open Access
42 Citations
7,897 Views
9 Pages

Energy Storage Characteristics of BiFeO3/BaTiO3 Bi-Layers Integrated on Si

  • Menglin Liu,
  • Hanfei Zhu,
  • Yunxiang Zhang,
  • Caihong Xue and
  • Jun Ouyang

18 November 2016

BiFeO3/BaTiO3 bi-layer thick films (~1 μm) were deposited on Pt/Ti/SiO2/(100) Si substrates with LaNiO3 buffer layers at 500 °C via a rf magnetron sputtering process. X-ray diffraction (XRD) analysis revealed that both BiFeO3 and BaTiO3 layers have a...

  • Article
  • Open Access
23 Citations
7,361 Views
16 Pages

18 November 2016

Metal/fluoropolymer composites represent a new category of energetic structural materials that release energy through exothermic chemical reactions initiated under shock loading conditions. This paper describes an experiment designed to study the rea...

  • Feature Paper
  • Article
  • Open Access
8 Citations
6,686 Views
15 Pages

Molecular Weight Cut-Off and Structural Analysis of Vacuum-Assisted Titania Membranes for Water Processing

  • Siti Nurehan Abd Jalil,
  • David K. Wang,
  • Christelle Yacou,
  • Julius Motuzas,
  • Simon Smart and
  • João C. Diniz da Costa

18 November 2016

This work investigates the structural formation and analyses of titania membranes (TM) prepared using different vacuum exposure times for molecular weight (MW) cut-off performance and oil/water separation. Titania membranes were synthesized via a sol...

  • Article
  • Open Access
32 Citations
5,837 Views
13 Pages

Characterization and Bioactivity Evaluation of (Polyetheretherketone/Polyglycolicacid)-Hydroyapatite Scaffolds for Tissue Regeneration

  • Cijun Shuai,
  • Chenying Shuai,
  • Ping Wu,
  • Fulai Yuan,
  • Pei Feng,
  • Youwen Yang,
  • Wang Guo,
  • Xiaohan Fan,
  • Ting Su and
  • Chengde Gao
  • + 1 author

18 November 2016

Bioactivity and biocompatibility are crucial for tissue engineering scaffolds. In this study, hydroxyapatite (HAP) was incorporated into polyetheretherketone/polyglycolicacid (PEEK/PGA) hybrid to improve its biological properties, and the composite s...

  • Article
  • Open Access
8 Citations
5,240 Views
14 Pages

18 November 2016

In this study, methane–ethylene jet diffusion flames modulated by acoustic excitation in an atmospheric environment were used to investigate the effects of acoustic excitation frequency and mixed fuel on nanomaterial formation. Acoustic output power...

  • Article
  • Open Access
29 Citations
5,642 Views
15 Pages

17 November 2016

Microencapsulated rejuvenator has been attracted much attention for self-healing bitumen. The diffusion coefficient is one of the key parameters to estimate the feasibility of rejuvenator to age bitumen. The objective of this research was to evaluate...

  • Article
  • Open Access
35 Citations
6,315 Views
23 Pages

Feasibility of Using Unbound Mixed Recycled Aggregates from CDW over Expansive Clay Subgrade in Unpaved Rural Roads

  • Isaac Del Rey,
  • Jesús Ayuso,
  • Adela P. Galvín,
  • José R. Jiménez and
  • Auxi Barbudo

17 November 2016

Social awareness aims to increase practical skills, such as sustainable development, which seeks to increase the use of different types of waste in construction activities. Although insufficient attention is sometimes given to these actions, it is es...

  • Article
  • Open Access
30 Citations
9,870 Views
17 Pages

Freckle Defect Formation near the Casting Interfaces of Directionally Solidified Superalloys

  • Jianping Hong,
  • Dexin Ma,
  • Jun Wang,
  • Fu Wang,
  • Baode Sun,
  • Anping Dong,
  • Fei Li and
  • Andreas Bührig-Polaczek

16 November 2016

Freckle defects usually appear on the surface of castings and industrial ingots during the directional solidification process and most of them are located near the interface between the shell mold and superalloys. Ceramic cores create more interfaces...

  • Article
  • Open Access
12 Citations
6,425 Views
20 Pages

Separation of Hydrogen from Carbon Dioxide through Porous Ceramics

  • Taro Shimonosono,
  • Hikari Imada,
  • Hikaru Maeda and
  • Yoshihiro Hirata

16 November 2016

The gas permeability of α-alumina, yttria-stabilized zirconia (YSZ), and silicon carbide porous ceramics toward H2, CO2, and H2–CO2 mixtures were investigated at room temperature. The permeation of H2 and CO2 single gases occurred above a critical pr...

  • Article
  • Open Access
43 Citations
7,425 Views
14 Pages

Comparison of Electrochemical Methods for the Evaluation of Cast AZ91 Magnesium Alloy

  • Jakub Tkacz,
  • Jozef Minda,
  • Stanislava Fintová and
  • Jaromír Wasserbauer

15 November 2016

Linear polarization is a potentiodynamic method used for electrochemical characterization of materials. Obtained values of corrosion potential and corrosion current density offer information about material behavior in corrosion environments from the...

  • Article
  • Open Access
61 Citations
9,270 Views
16 Pages

15 November 2016

In this work, a ZnO-layered double hydroxide@graphitic carbon nitride composite (ZnO-LDH@C3N4) was synthesized via co-precipitation method with solvothermal treatment. The structure and morphology of ZnO-LDH@C3N4 composite were characterized using X-...

  • Article
  • Open Access
8 Citations
6,092 Views
13 Pages

15 November 2016

Tissue-like phantoms are widely used as a model for mimicking the optical properties of live tissue. This paper presents the results of a diffusion reflection method and fluorescence lifetime imaging microscopy measurements of fluorescein-conjugated...

  • Communication
  • Open Access
8 Citations
4,021 Views
10 Pages

15 November 2016

Iron-based materials proved being a viable candidate material for biodegradable implants. Magnetron sputtering combined with UV-lithography offers the possibility to fabricate structured, freestanding foils of iron-based alloys and even composites wi...

  • Article
  • Open Access
9 Citations
5,296 Views
12 Pages

Metamaterial Behavior of Polymer Nanocomposites Based on Polypropylene/Multi-Walled Carbon Nanotubes Fabricated by Means of Ultrasound-Assisted Extrusion

  • Juan C. Pérez-Medina,
  • Miguel A. Waldo-Mendoza,
  • Víctor J. Cruz-Delgado,
  • Zoe V. Quiñones-Jurado,
  • Pablo González-Morones,
  • Ronald F. Ziolo,
  • Juan G. Martínez-Colunga,
  • Florentino Soriano-Corral and
  • Carlos A. Avila-Orta

14 November 2016

Metamaterial behavior of polymer nanocomposites (NCs) based on isotactic polypropylene (iPP) and multi-walled carbon nanotubes (MWCNTs) was investigated based on the observation of a negative dielectric constant (ε′). It is demonstrated that as the d...

  • Article
  • Open Access
31 Citations
5,678 Views
17 Pages

14 November 2016

(Bi,Sr)FeO3−δ (BSF) cathode materials doped with either Co, Ni or Mn are synthesized by an ethylene diamine tetra-acetic acid (EDTA)-citrate complexing method, and the effects of the doping level on the mixed electronic-ionic conductivity at various...

  • Article
  • Open Access
41 Citations
10,205 Views
19 Pages

Oxygen Evolution at Manganite Perovskite Ruddlesden-Popper Type Particles: Trends of Activity on Structure, Valence and Covalence

  • Majid Ebrahimizadeh Abrishami,
  • Marcel Risch,
  • Julius Scholz,
  • Vladimir Roddatis,
  • Norbert Osterthun and
  • Christian Jooss

14 November 2016

An improved understanding of the correlation between the electronic properties of Mn-O bonds, activity and stability of electro-catalysts for the oxygen evolution reaction (OER) is of great importance for an improved catalyst design. Here, an in-dept...

  • Article
  • Open Access
55 Citations
7,699 Views
12 Pages

14 November 2016

The main problem with cement composites is that they have structural defects, including cracks, holes, and a disordered morphology, which significantly affects their strength and durability. Therefore, the construction of cement composites with defec...

  • Article
  • Open Access
12 Citations
4,679 Views
12 Pages

12 November 2016

This study aimed to evaluate the bonding strength and thermal properties of demineralized dentin with and without EDC treatment. Sound human molars were randomly divided into seven treatment groups (n = 20): control, 80% ethanol, and five EDC ethanol...

  • Article
  • Open Access
35 Citations
5,427 Views
14 Pages

12 November 2016

This study presents a novel monitoring method for hole-edge corrosion damage in plate structures based on Lamb wave tomographic imaging techniques. An experimental procedure with a cross-hole layout using 16 piezoelectric transducers (PZTs) was desig...

  • Article
  • Open Access
9 Citations
4,441 Views
12 Pages

11 November 2016

The dielectric constants of nylon fabrics saturated with aqueous NaCl solutions, Fabric-Superdielectric Materials (F-SDM), were measured to be >105 even at the shortest discharge times (>0.001 s) for which reliable data could be obtained using...

  • Article
  • Open Access
26 Citations
7,111 Views
9 Pages

A Filmy Black-Phosphorus Polyimide Saturable Absorber for Q-Switched Operation in an Erbium-Doped Fiber Laser

  • Tianxian Feng,
  • Dong Mao,
  • Xiaoqi Cui,
  • Mingkun Li,
  • Kun Song,
  • Biqiang Jiang,
  • Hua Lu and
  • Wangmin Quan

11 November 2016

We demonstrate an erbium-doped fiber laser passively Q-switched by a black-phosphorus polyimide film. The multi-layer black-phosphorus (BP) nanosheets were prepared via a liquid exfoliation approach exploiting N-methylpyrrolidone as the dispersion li...

  • Article
  • Open Access
20 Citations
5,261 Views
13 Pages

Influence of Sintering Temperature on the Microstructure and Mechanical Properties of In Situ Reinforced Titanium Composites by Inductive Hot Pressing

  • Cristina Arévalo,
  • Isabel Montealegre-Meléndez,
  • Enrique Ariza,
  • Michael Kitzmantel,
  • Cristina Rubio-Escudero and
  • Erich Neubauer

11 November 2016

This research is focused on the influence of processing temperature on titanium matrix composites reinforced through Ti, Al, and B4C reactions. In order to investigate the effect of Ti-Al based intermetallic compounds on the properties of the composi...

  • Article
  • Open Access
29 Citations
6,390 Views
11 Pages

10 November 2016

Four porous carbon samples denoted as LSC-1, LSC-2, LCS-3, and LSC-4 were prepared by carbonization of loofah sponge pretreated by ZnCl2 activation, immersion in N,N-dimethylformamide (DMF), DMF-assisted solvothermal and melamine-assisted hydrotherma...

  • Review
  • Open Access
158 Citations
17,870 Views
47 Pages

Inkjet Printing of Functional Materials for Optical and Photonic Applications

  • Jorge Alamán,
  • Raquel Alicante,
  • Jose Ignacio Peña and
  • Carlos Sánchez-Somolinos

10 November 2016

Inkjet printing, traditionally used in graphics, has been widely investigated as a valuable tool in the preparation of functional surfaces and devices. This review focuses on the use of inkjet printing technology for the manufacturing of different op...

  • Article
  • Open Access
27 Citations
6,595 Views
10 Pages

10 November 2016

Cu–Ag thin films with various atomic ratios were prepared using a co-sputtering technique, followed by rapid thermal annealing at various temperatures. The films’ structural, mechanical, and electrical properties were then characterized using X-ray d...

  • Article
  • Open Access
49 Citations
8,401 Views
17 Pages

Prediction of the Vickers Microhardness and Ultimate Tensile Strength of AA5754 H111 Friction Stir Welding Butt Joints Using Artificial Neural Network

  • Luigi Alberto Ciro De Filippis,
  • Livia Maria Serio,
  • Francesco Facchini,
  • Giovanni Mummolo and
  • Antonio Domenico Ludovico

10 November 2016

A simulation model was developed for the monitoring, controlling and optimization of the Friction Stir Welding (FSW) process. This approach, using the FSW technique, allows identifying the correlation between the process parameters (input variable) a...

  • Article
  • Open Access
3 Citations
5,118 Views
10 Pages

10 November 2016

Regioselective modification of d-glucosamine (2-amino-2-deoxy-d-glucopyranose, GA) through C-1 and C-2 positions to synthesized thermo-responsive D-Glucosamine-poly(N-iso-propylacrylamide) (PNIPAM) via atom transfer radical polymerization (ATRP) was...

  • Review
  • Open Access
28 Citations
9,474 Views
17 Pages

Additive Manufacturing of Biomedical Constructs with Biomimetic Structural Organizations

  • Xiao Li,
  • Jiankang He,
  • Weijie Zhang,
  • Nan Jiang and
  • Dichen Li

9 November 2016

Additive manufacturing (AM), sometimes called three-dimensional (3D) printing, has attracted a lot of research interest and is presenting unprecedented opportunities in biomedical fields, because this technology enables the fabrication of biomedical...

  • Article
  • Open Access
1 Citations
4,592 Views
9 Pages

8 November 2016

A pressure-induced phase transition of Mg2Sr intermetallics from the low-pressure C14-type phase to an orthorhombic phase (space group Cmcm, Z = 4) at a high pressure of 21.0 GPa was firstly predicted using first-principles calculations combined with...

  • Review
  • Open Access
92 Citations
11,754 Views
13 Pages

Influence of Electrode Design and Contacting Layers on Performance of Electrolyte Supported SOFC/SOEC Single Cells

  • Mihails Kusnezoff,
  • Nikolai Trofimenko,
  • Martin Müller and
  • Alexander Michaelis

8 November 2016

The solid oxide cell is a basis for highly efficient and reversible electrochemical energy conversion. A single cell based on a planar electrolyte substrate as support (ESC) is often utilized for SOFC/SOEC stack manufacturing and fulfills necessary r...

  • Article
  • Open Access
16 Citations
5,357 Views
7 Pages

The Microwave-Assisted Green Synthesis of TiC Powders

  • Hui Wang,
  • Wencheng Zhu,
  • Yanchun Liu,
  • Lingke Zeng and
  • Luyi Sun

8 November 2016

Titanium carbide (TiC) is an important engineering material and has found widespread applications. Currently, TiC is typically synthesized through carbothermal reduction, requiring a high temperature (ca. 1700–2300 °C) and long reaction time (ca. 10–...

  • Article
  • Open Access
26 Citations
4,777 Views
23 Pages

Microstructural Effects of Sulphate Attack in Sustainable Grouts for Micropiles

  • José Marcos Ortega Álvarez,
  • María Dolores Esteban Pérez,
  • Raúl Rubén Rodríguez Escribano,
  • José Luís Pastor Navarro and
  • Isidro Sánchez Martín

8 November 2016

Nowadays, the use of micropiles has undergone a great development. In general, they are made with cement grout, reinforced with steel tubing. In Spain, these grouts are prepared using OPC, although the standards do not forbid the use of other cements...

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Materials - ISSN 1996-1944