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Metals

Metals is an international, peer-reviewed, open access journal published monthly online by MDPI.
The Portuguese Society of Materials (SPM), and the Spanish Materials Society (SOCIEMAT) are affiliated with Metals and their members receive discounts on the article processing charges.
Quartile Ranking JCR - Q2 (Metallurgy and Metallurgical Engineering)

All Articles (14,440)

Continuous cooling transformation (CCT) diagrams for two thermo-mechanically controlled processed (TMCP) steels were produced using a modified Johnson–Mehl–Avrami–Kolmogorov (JMAK) model, which accounted for the simultaneous transformation of multiple phases under non-isothermal conditions. A basin hopping algorithm was used to sequentially optimize the model parameters for each phase. Samples were prepared using a dilatometer which replicated the deformation and cooling rates experienced during TMCP. Scanning electron microscopy (SEM) and electron back-scattered diffraction (EBSD) were used to identify and quantify the phases present in each steel. CCT diagrams illustrating the start and stop temperatures of each phase were constructed for both steel samples. Through inclusion of the stop temperatures of each phase transformation, the utility of the CCT diagrams were expanded. This was done by introducing the possibility of applying the Scheil additive principle with respect to the beginning and end of each phase transformation. With this modification, the CCT diagrams are now more appropriately suited to predict the phase transformations that occur on the ROT, where non-continuous cooling occurs.

16 December 2025

Dilatometer processing routes for X70 (bottom-time axis) and X80 (top-time axis) samples. The X70 samples were held for 5 s with 0.25 strain (0.1/s) at 1050 °C and 850 °C. No strain was applied to the X80 samples.

Central segregation, a typical internal defect in continuous casting slabs, significantly deteriorates the mechanical properties of steel products. However, traditional manual defect evaluation methods rely heavily on experience, are highly subjective and inefficient, making it difficult to meet the quality assessment requirements of today’s high-end steel materials. In this study, an approach which combines an unsupervised image enhancement algorithm and Otsu algorithm analysis was proposed to achieve automatic recognition and quantitative features extracting of central segregation in continuous casting slabs. The challenges posed by insufficient brightness and low contrast in central segregation images were addressed using unsupervised image enhancement algorithms. Following this enhancement, batch objective quantification of the segregation images was conducted through Otsu processing. Comparative experimental results showed that the enhanced images yielded an average Dice Similarity Coefficient of 0.965 for segregation recognition, representing a 38% improvement over unprocessed images, with consistent accuracy gains across complex segregation scenarios. This intelligent detection method eliminates the need for manually labeling a training set, substantially improves the consistency of segregation quantification and reduces the time cost significantly. Consequently, multiple parameters can be employed to quantify segregation characteristics, offering a more comprehensive and precise approach than current simplified rating methods. This advancement holds promise for enhancing quality control in steel processing and advancing Artificial Intelligence-driven technological progress within the metallurgical sector.

16 December 2025

Simplex-centroid mixture design (SCMD) is applied to change the combination of Na2SiO3, KF, NaOH and NaAlO2 to examine the influences of electrolyte components and their interactions on the thickness and corrosion resistance of micro-arc oxidation (MAO) coating of AZ91D magnesium alloy. The results indicate that the obtained regression equations are very significant (p-value < 0.01) and have high prediction accuracy (R2 = 0.9893, 0.9989). Pareto analysis shows that the interactions effect between Na2SiO3, KF and NaAlO2 on the coating thickness and corrosion resistance are 70.03% and 92.35%, respectively, which quantitatively confirms that there are interactions among electrolytes. The analysis of response surface methodology (RSM) demonstrates that the optimum formula is high concentration of Na2SiO3, high concentration of KF and low concentration of NaAlO2. When Na2SiO3 is compounded with NaAlO2, the two will react to form aluminosilicate colloids, resulting in increased viscosity of the electrolyte, and the coating corrosion resistance is poor. When the main salt of electrolyte is single Na2SiO3 or NaAlO2, the corrosion resistance is better. KF can significantly improve the coating thickness and corrosion resistance. Pearson correlation coefficient (PCC) reveals that there is a remarkable relationship between thickness and the corrosion resistance in acidic media (r = 0.88927), which was determined by the corrosion mechanism of the latter.

16 December 2025

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16 December 2025

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Metals - ISSN 2075-4701