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Separations, Volume 9, Issue 7

2022 July - 29 articles

Cover Story: Rooibos tea (Aspalathus linearis) is a leguminous shrub endemic to the western parts of the Cape region in South Africa and a well-known herbal tea that is enjoyed worldwide. Due to its increased use, there is a possible risk of its interaction with conventional pharmaceuticals if administered simultaneously. In addition, the gap in the provision of conclusive quality evidence for rooibos tea stems from the lack of accurate analytical methods. In our continued quest to explore the quality of botanical ingredients, this study reexamined the phenolic profile of rooibos tea, mainly the regioisomers and diastereomers, via developing and validating a robust and economical approach that potentially aids in the identification and quantification of chemical markers which can serve as guidelines for the analysis of rooibos tea samples for quality assurance. View this paper
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Articles (29)

  • Article
  • Open Access
14 Citations
4,490 Views
14 Pages

Recovery of Rare Metals from Superalloy Scraps by an Ultrasonic Leaching Method with a Two-Stage Separation Process

  • Long Wang,
  • Sujun Lu,
  • Jiayuan Fan,
  • Yutian Ma and ,
  • Juan Zhang,
  • Shiyang Wang,
  • Xiaoyao Pei,
  • Yuan Sun,
  • Guozhi Lv and
  • Tingan Zhang
  • + 5 authors+ 0 author

Superalloy scraps are deemed as potential unconventional sources of rare metals. In this study, an ultrasonic leaching method with a two-stage separation process was proposed. A series of Eh-pH diagrams for rare metals was constructed, and the result...

(This article belongs to the Special Issue Efficient and Green Recovery of Metal Minerals)
  • Article
  • Open Access
7 Citations
5,934 Views
11 Pages

A comparison between the classical gas chromatography (GC) technique with supercritical fluid chromatography (SFC) technology was performed using an essential oil of Citrus limon (lemon) as a model, considering its wide use in the cosmetic world. For...

(This article belongs to the Special Issue Early Career Stars in Separation Analysis of Natural Products and Pharmaceuticals)
  • Article
  • Open Access
33 Citations
6,795 Views
20 Pages

Zostera marina L.: Supercritical CO2-Extraction and Mass Spectrometric Characterization of Chemical Constituents Recovered from Seagrass

  • Mayya P. Razgonova,
  • Lyudmila A. Tekutyeva,
  • Anna B. Podvolotskaya,
  • Varvara D. Stepochkina and ,
  • Alexander M. Zakharenko and
  • Kirill Golokhvast
  • + 1 author+ 0 author

Three types of Zostera marina L. collection were extracted using the supercritical CO2-extraction method. For the purposes of supercritical CO2-extraction, old seagrass ejection on the surf edge, fresh seagrass ejection on the surf edge and seagrass...

(This article belongs to the Section Advanced Separation Science in Biomedical Research and Clinical Applications)
  • Article
  • Open Access
22 Citations
8,548 Views
15 Pages

Amaranth Oilseed Composition and Cosmetic Applications

  • Bouchra Sayed-Ahmad,
  • Martine Urrutigoïty,
  • Akram Hijazi,
  • Zeinab Saad and ,
  • Muriel Cerny,
  • Philippe Evon,
  • Thierry Talou and
  • Othmane Merah
  • + 3 authors+ 0 author

Amaranth (Amaranthus cruentus) is a possible alternative to high-nutritional-value crops. Amaranth seeds are considered to be one of the few sources of phytosqualene (up to 8%). The use of squalene and its hydrogenated form squalane in skincare formu...

(This article belongs to the Special Issue Food Quality and Safety: Advances in Analytical Methods and Applications)
  • Article
  • Open Access
22 Citations
4,617 Views
16 Pages

Fabrication of High-Performance Nanofiltration Membrane Using Polydopamine and Carbon Nitride as the Interlayer

  • Lei Ma,
  • Qiuyan Bi,
  • Yuanhui Tang,
  • Chao Zhang and ,
  • Fuju Qi,
  • Hao Zhang,
  • Yifan Gao and
  • Shiai Xu
  • + 3 authors+ 0 author

In order to recover lithium from brine with a high Mg2+/Li+ ratio, a positively charged nanofiltration (NF) membrane was prepared by depositing polydopamine (PDA)-coated graphitic carbon nitride (g-C3N4) as the interlayer (PDA-g-C3N4) and the interfa...

(This article belongs to the Section Materials in Separation Science)
  • Article
  • Open Access
24 Citations
6,233 Views
11 Pages

Comparison of Fenton and Ozone Oxidation for Pretreatment of Petrochemical Wastewater: COD Removal and Biodegradability Improvement Mechanism

  • Siyu Cheng,
  • Xiaomeng Ran,
  • Gengbo Ren,
  • Zizhang Wei and ,
  • Zhimin Wang,
  • Tiantong Rao,
  • Ruixuan Li and
  • Xiaodong Ma
  • + 3 authors+ 0 author

Cost-effective pretreatment of highly concentrated and bio-refractory petrochemical wastewater to improve biodegradability is of significant importance, but remains challenging. This study compared the pretreatment of petrochemical wastewater by two...

(This article belongs to the Section Environmental Separations)
  • Review
  • Open Access
115 Citations
23,727 Views
17 Pages

Single Cell Protein Production Using Different Fruit Waste: A Review

  • Punniamoorthy Thiviya,
  • Ashoka Gamage,
  • Ranganathan Kapilan,
  • Othmane Merah and
  • Terrence Madhujith

The single cell protein (SCP) technique has become a popular technology in recent days, which addresses two major issues: increasing world protein deficiency with increasing world population and the generation of substantial industrial wastes with an...

(This article belongs to the Special Issue Food Quality and Safety: Advances in Analytical Methods and Applications)
  • Article
  • Open Access
13 Citations
5,973 Views
12 Pages

Validation, Optimization and Hepatoprotective Effects of Boeravinone B and Caffeic Acid Compounds from Boerhavia diffusa Linn

  • Kamal Y. Thajudeen,
  • Abdulrhman Alsayari,
  • Shehla Nasar Mir Najib Ullah,
  • Shahana Salam and ,
  • Muhammed Elayadeth-Meethal and
  • Ilyas Uoorakkottil
  • + 1 author+ 0 author

Boerhavia diffusa, also known as Punarnava, is a plant of the Nyctaginaceae family that has been utilized in traditional medicine to cure a variety of ailments. The goal of this study was to use response surface methodology (RSM) to optimize the maxi...

(This article belongs to the Special Issue Advances in Chromatographic Analysis of Bioactive Compounds)
  • Article
  • Open Access
1 Citations
3,230 Views
9 Pages

A reliable chromatographic strategy is crucial for the extraction of target compounds from natural sources as it is related to the preparation efficiency, as well as the purity of the compounds. In this study, medium-pressure normal-phase liquid chro...

(This article belongs to the Collection State of the Art in Separation Science)
  • Review
  • Open Access
16 Citations
8,820 Views
22 Pages

Microsamples are collections usually less than 50 µL, although all devices that we have captured as part of this review do not fit within this definition (as some can perform collections of up to 600 µL); however, they are considered microsamples tha...

(This article belongs to the Section Advanced Separation Science in Biomedical Research and Clinical Applications)
  • Article
  • Open Access
18 Citations
4,061 Views
13 Pages

CO2 Capture over Activated Carbon Derived from Pulverized Semi-Coke

  • Jieying Jing,
  • Zemin Zhao,
  • Xuewei Zhang,
  • Jie Feng and
  • Wenying Li

Pulverized semi-coke was employed as raw material to prepare activated carbon via steam activation and evaluated as a CO2 adsorbent. The effects of the preparation parameters including demineralization, activation temperature, activation time and ste...

(This article belongs to the Section Environmental Separations)
  • Article
  • Open Access
8 Citations
3,303 Views
16 Pages

The aim of this study was to investigate the correlation between solid materials and micropollutants, aiming to enhance the removal of the latter during the application of the ozonation process. For that purpose, two solid materials (SiO2 and Al2O3)...

(This article belongs to the Section Environmental Separations)
  • Article
  • Open Access
8 Citations
5,187 Views
12 Pages

Screening and Estimation of Bioactive Compounds of Azanza garckeana (Jakjak) Fruit Using GC-MS, UV–Visible Spectroscopy, and HPLC Analysis

  • Abdalrhaman M. Salih,
  • Fahad Al-Qurainy,
  • Mohamed Tarroum,
  • Hassan O. Shaikhaldein and
  • Abdulrahman Hashimi

Azanza garckeana (F. Hoffm). Exell and Hillc. is an important food and medicinal plant that has been used in tropical Africa. Therefore, this study aimed to investigate the nutritional value of jakjak fruit using different analytical techniques. The...

(This article belongs to the Section Analysis of Food and Beverages)
  • Article
  • Open Access
11 Citations
3,246 Views
12 Pages

Advanced Treatment of Palm Oil Mill Effluent Using Thermally Activated Persulfate Oxidation

  • Mohammed J. K. Bashir,
  • Ong Sue Sheen,
  • Choon Aun Ng,
  • Mohammed Shadi S. Abujazar and ,
  • Motasem Y. D. Alazaiza and
  • Salim S. Abu Amr
  • + 1 author+ 0 author

Advanced treatment of biologically processed palm oil mill effluent (BIOTPOME), which possesses a potential danger to the water sources is required to meet the Malaysian discharge standard, as BIOTPOME contains high level of chemical oxygen demand (C...

(This article belongs to the Section Environmental Separations)
  • Review
  • Open Access
37 Citations
6,503 Views
32 Pages

Ionic Liquid-Assisted DLLME and SPME for the Determination of Contaminants in Food Samples

  • Lirong Nie,
  • Chaochao Cai,
  • Runpeng Guo,
  • Shun Yao and ,
  • Zhi Zhu,
  • Yanchen Hong and
  • Dong Guo
  • + 2 authors+ 0 author

Developing effective and green methods for food analysis and separation has become an urgent issue regarding the ever-increasing concern of food quality and safety. Ionic liquids (ILs) are a new chemical medium and soft functional material developed...

(This article belongs to the Section Purification Technology)
  • Article
  • Open Access
14 Citations
9,005 Views
13 Pages

In this study, a needle–cylinder electrostatic precipitator with a water cooling system was designed to enhance the harvest of atmospheric water in wet flue gas. The effects of flow rate, temperature and particles on the collection of fog dropl...

(This article belongs to the Section Environmental Separations)
  • Article
  • Open Access
6 Citations
3,006 Views
19 Pages

The deposited particulate material within a fibrous filter affects the pressure drop which develops through three different stages. The implementation of a time-adjustable matrix is intended to cause detachment of particle structures from fibers with...

  • Article
  • Open Access
11 Citations
4,530 Views
16 Pages

Analysis of Major Polyphenolic Compounds of Cydonia oblonga Miller (Quince) Fruit Extract by UPLC-MS/MS and Its Effect on Adipogenesis in 3T3-L1 Cells

  • Nawaz Khan,
  • Nulibiya Maihemuti,
  • Muhadaisi Nuer,
  • Kayisaier Abudurousuli and ,
  • Jimilihan Simayi,
  • Ziruo Talihati,
  • Mengyuan Han,
  • Sendaer Hailati,
  • Wenting Zhou and
  • Ainiwaer Wumaier
  • + 5 authors+ 0 author

Cydonia oblonga miller (quince) plant serves as a potential folk medicine for treating hypertension and cardiovascular diseases in China. However, to the best of our knowledge, no study has been conducted on the polyphenolic profile and anti-adipogen...

(This article belongs to the Section Analysis of Natural Products and Pharmaceuticals)
  • Article
  • Open Access
17 Citations
8,282 Views
18 Pages

Microplastics and Heavy Metals Removal from Fresh Water and Wastewater Systems Using a Membrane

  • Simphiwe Dineo Nkosi,
  • Soraya Phumzile Malinga and
  • Nonhlangabezo Mabuba

Water pollution, resulting from the degradation of plastics into microplastics, exposes humans and other living organisms to contaminated drinking water. Microplastics are capable of adsorbing toxic heavy metals which are carcinogenic and may affect...

(This article belongs to the Special Issue Separation Processes for Effective Removal of Emerging Contaminants from Water and Wastewater)
  • Article
  • Open Access
65 Citations
20,821 Views
10 Pages

Extraction and Evaluation of the Antimicrobial Activity of Polyphenols from Banana Peels Employing Different Extraction Techniques

  • Faiqa Chaudhry,
  • Muhammad Laiq Ahmad,
  • Zafar Hayat,
  • Muhammad Modassar Ali Nawaz Ranjha and ,
  • Komal Chaudhry,
  • Noureddine Elboughdiri,
  • Mufarreh Asmari and
  • Jalal Uddin
  • + 3 authors+ 0 author

Polyphenols are natural antioxidants and play a vital role in inhibiting oxidative stress induced by the body’s free radicals. Banana peels are a significant agro-industrial waste. This waste could be utilized to extract polyphenols to process...

(This article belongs to the Special Issue Isolation and Structure Elucidation of Antibacterial Compound)
  • Article
  • Open Access
4 Citations
5,547 Views
16 Pages

Protein purification is a complex and non-standardized process; the fact that proteins have different structural types making it difficult to create a standard methodology to obtain them in a pure, soluble, and homogeneous form. The present study sho...

  • Review
  • Open Access
42 Citations
19,181 Views
30 Pages

Recent Advances in Separation and Analysis of Saponins in Natural Products

  • Yi Wang,
  • Yan Ma,
  • Li Tao,
  • Xiaoyan Zhang and ,
  • Fusheng Hao,
  • Shipeng Zhao,
  • Lu Han and
  • Changcai Bai
  • + 3 authors+ 0 author

To better control the quality of saponins, ensure their biological activity and clinical therapeutic effect, and expand the development and application of saponins, this paper systematically and comprehensively reviews the separation and analytical m...

(This article belongs to the Section Purification Technology)
  • Article
  • Open Access
8 Citations
4,817 Views
18 Pages

The essential oils and polysaccharides from guava leaves have important functions. In the process of microwave extraction of plant essential oils and polysaccharides, pretreatment with lithium salts solution is helpful to increase the extraction rate...

(This article belongs to the Special Issue Novel Approach for Natural Product Separation from Plants)
  • Article
  • Open Access
15 Citations
8,724 Views
12 Pages

To verify the anti-fungus properties of the crop-harmful pseudocercospora, the essential oil (EO) of pomelo peel (PP) was extracted by a single factor combined with response surface optimization. Meanwhile, the composition and activity of EO were stu...

(This article belongs to the Special Issue Novel Approach for Natural Product Separation from Plants)
  • Article
  • Open Access
12 Citations
3,357 Views
14 Pages

Accurate Flow Regime Classification and Void Fraction Measurement in Two-Phase Flowmeters Using Frequency-Domain Feature Extraction and Neural Networks

  • Siavash Hosseini,
  • Abdullah M. Iliyasu,
  • Thangarajah Akilan,
  • Ahmed S. Salama and ,
  • Ehsan Eftekhari-Zadeh and
  • Kaoru Hirota
  • + 1 author+ 0 author

Two-phase flow is very important in many areas of science, engineering, and industry. Two-phase flow comprising gas and liquid phases is a common occurrence in oil and gas related industries. This study considers three flow regimes, including homogen...

(This article belongs to the Section Environmental Separations)
  • Article
  • Open Access
16 Citations
7,669 Views
14 Pages

Validation of an Analytical Method for the Determination of Manganese and Lead in Human Hair and Nails Using Graphite Furnace Atomic Absorption Spectrometry

  • José Ricardo Forero-Mendieta,
  • Juan David Varón-Calderón,
  • Diana Angelica Varela-Martínez,
  • Diego Alejandro Riaño-Herrera and ,
  • Rubén Darío Acosta-Velásquez and
  • John Alexander Benavides-Piracón
  • + 1 author+ 0 author

This article describes the validation of analytical methods for the determination of Manganese (Mn) and lead (Pb) by graphite furnace atomic absorption spectrometry (GFAAS) in human hair and nail samples. Method validation parameters such as linearit...

(This article belongs to the Section Materials in Separation Science)
  • Article
  • Open Access
22 Citations
5,864 Views
13 Pages

Chemical Fingerprinting Profile and Targeted Quantitative Analysis of Phenolic Compounds from Rooibos Tea (Aspalathus linearis) and Dietary Supplements Using UHPLC-PDA-MS

  • Omer I. Fantoukh,
  • Yan-Hong Wang,
  • Abidah Parveen,
  • Mohammed F. Hawwal and ,
  • Zulfiqar Ali,
  • Gadah A. Al-Hamoud,
  • Amar G. Chittiboyina,
  • Elizabeth Joubert,
  • Alvaro Viljoen and
  • Ikhlas A. Khan
  • + 5 authors+ 0 author

Aspalathus linearis (Burm.f.) R. Dahlgren, commonly known as rooibos tea, was consumed traditionally by the indigenous South African inhabitants as an herbal remedy. Beside antioxidant properties, it displays antiallergic, antispasmodic, and hypoglyc...

(This article belongs to the Section Analysis of Food and Beverages)
  • Article
  • Open Access
13 Citations
4,566 Views
21 Pages

The enantioseparation of syn- and anti-3,5-disubstituted hydantoins 5a–i was investigated on three immobilized polysaccharide-based columns (CHIRAL ART Amylose-SA, CHIRAL ART Cellulose-SB, CHIRAL ART Cellulose-SC) by high performance liquid chr...

(This article belongs to the Special Issue Advances in Chromatographic Analysis of Bioactive Compounds)
  • Article
  • Open Access
5 Citations
3,921 Views
11 Pages

Green Assessment of Chromatographic Methods Used for the Analysis of Four Methamphetamine Combinations with Commonly Abused Drugs

  • Saif A. Alharthy,
  • Muath A. Alharthi,
  • Sultan A. Almalki,
  • Sattam H. Alosaimi and ,
  • Abdullah H. Aqeel,
  • Sultan A. Altowairqi,
  • Izzeddin Alsalahat,
  • Dibya Sundar Panda,
  • Mona Y. Alsheikh and
  • Ibrahim A. Naguib
  • + 5 authors+ 0 author

Numerous agents with anxiolytic or stimulant effects have the potential to be overused, and their misuse is associated with serious side effects. In Saudi Arabia, the estimated percentage of Saudis who abuse drugs is around 7–8% and the age ran...

(This article belongs to the Section Analysis of Natural Products and Pharmaceuticals)
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Separations - ISSN 2297-8739