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  • Feature Paper
  • Article
  • Open Access
4 Citations
3,168 Views
12 Pages

Effect of Cu on Nitriding of α-Fe

  • Andreas Leineweber,
  • Max Fischer,
  • Stefan Kante and
  • Stefan Martin

3 April 2022

Nitriding of Fe-1 wt.% Cu and Fe-5 wt.% Cu alloys at 813 K leads to the formation of predominantly the γ′-iron nitride phase (γ′-Fe4N) when using nitriding conditions, which lead to pronounced formation of ε-iron nitri...

  • Review
  • Open Access
26 Citations
10,182 Views
46 Pages

27 October 2023

Gas nitriding, as a surface modification technology to improve the wear resistance of workpiece surfaces, is widely used in wind turbine gears, pressure vessel gears, high-precision die casting abrasives, and other areas. However, the gas nitriding t...

  • Article
  • Open Access
8 Citations
4,093 Views
10 Pages

20 January 2021

Decarburization is generally avoided as it is reckoned to be a process detrimental to material surface properties. Based on the idea of duplex surface engineering, i.e., nitriding the case-hardened or through-hardened bearing steels for enhanced surf...

  • Feature Paper
  • Article
  • Open Access
14 Citations
3,188 Views
12 Pages

The Stability of the Layer Nitrided in Low-Pressure Nitriding Process

  • Emilia Wołowiec-Korecka,
  • Jerzy Michalski and
  • Bartłomiej Januszewicz

21 January 2023

The kinetics of the nitrided layer thickness growth and its structure depend on the nitrogen flux from the atmosphere to the nitrided surface. A nitrogen flux to the surface is more significant than a diffusion flux into the substrate, during forming...

  • Article
  • Open Access
8 Citations
3,853 Views
12 Pages

Optimization of Pre-Heat Treatment for Nitriding

  • Matthias Steinbacher and
  • Stefanie Hoja

15 December 2021

To achieve a core strength that meets the requirements during service life, components to be nitrided are subjected to a pre-heat treatment. Since a higher strength prior to nitriding also has a positive effect on the achievable strength in the nitri...

  • Article
  • Open Access
14 Citations
3,153 Views
15 Pages

7 May 2019

Nitrided layers on 6082 aluminum alloy substrates and 1060 aluminum substrates are formed at atmospheric pressure using thermal nitrogen plasma, which only takes seconds to form a millimeter-level layer. The nitrided layers are composed of aluminum n...

  • Article
  • Open Access
9 Citations
7,763 Views
11 Pages

Structural Characterization of Fine γ′-Fe4N Nitrides Formed by Active Screen Plasma Nitriding

  • Jaroslaw Jan Jasinski,
  • Lukasz Kurpaska,
  • Tadeusz Fraczek,
  • Malgorzata Lubas and
  • Maciej Sitarz

9 December 2020

The paper presents the structural characterization of γ′-Fe4N nitrides produced by active screen plasma nitriding (ASPN) processes. Experiments were performed on the Fe-Armco model material at 693, 773, and 853 K for 6 h. Investigation of the propert...

  • Article
  • Open Access
5 Citations
1,923 Views
11 Pages

29 October 2024

Aluminum-modified plasma nitriding was developed in this research by the addition of a few FeAl particles around samples of 42CrMo middle carbon alloy steel during plasma nitriding. The goal of this study was to enhance nitriding efficiency and the c...

  • Article
  • Open Access
3 Citations
1,631 Views
14 Pages

The Impact of Heating Rate on the Kinetics of the Nitriding Process for 52100 Steel

  • Tadeusz Frączek,
  • Rafał Prusak,
  • Jerzy Michalski,
  • Zbigniew Skuza and
  • Marzena Ogórek

16 October 2023

The aim of this study was to determine the impact of the heating rate of steel balls made of AISI 52100 alloy steel on the kinetics and efficiency of the gas nitriding process when carried out using a chemical reactor with precise thermo-gravimetric...

  • Article
  • Open Access
23 Citations
5,956 Views
22 Pages

Evolution of Microstructure and Hardness of the Nitrided Zone during Plasma Nitriding of High-Alloy Tool Steel

  • Pierre Landgraf,
  • Tim Bergelt,
  • Lisa-Marie Rymer,
  • Christian Kipp,
  • Thomas Grund,
  • Günter Bräuer and
  • Thomas Lampke

19 May 2022

Plasma nitriding is widely used in various industrial applications to improve surface hardness and wear properties. Especially for tool steels, it is also used to improve the support and adhesion of diamond-like carbon (DLC) coatings. The properties...

  • Article
  • Open Access
1,087 Views
23 Pages

29 June 2025

When nitriding 38CrMoAl steel, there are areas that need to be protected, as the process may interfere with subsequent steps. The large-scale demand for anti-nitriding coatings has driven the investigation and development of more effective anti-nitri...

  • Article
  • Open Access
14 Citations
11,847 Views
23 Pages

Design, Control and in Situ Visualization of Gas Nitriding Processes

  • Jerzy Ratajski,
  • Roman Olik,
  • Tomasz Suszko,
  • Jerzy Dobrodziej and
  • Jerzy Michalski

28 December 2009

The article presents a complex system of design, in situ visualization and control of the commonly used surface treatment process: the gas nitriding process. In the computer design conception, analytical mathematical models and artificial intelligenc...

  • Article
  • Open Access
14 Citations
6,404 Views
11 Pages

11 January 2022

Potential-controlled nitriding is an effective technique for enhancing the life of steel molds and dies by improving their surface hardness and toughness against fatigue damage. In this study, the effect of the nitriding potential on the microstructu...

  • Article
  • Open Access
10 Citations
3,164 Views
14 Pages

Nitriding of 316L Steel in a Glow Discharge Plasma

  • Tadeusz Frączek,
  • Rafał Prusak,
  • Marzena Ogórek and
  • Zbigniew Skuza

24 April 2022

The article presents the results of the research on the nitriding process of 316L austenitic steel and the change in surface properties resulting from this process used in medicine, orthopedics, and in fuel cells. The processes were carried out with...

  • Article
  • Open Access
10 Citations
2,645 Views
11 Pages

Cyclic Fatigue of Dental NiTi Instruments after Plasma Nitriding

  • Michal Bumbalek,
  • Zdenek Joska,
  • Zdenek Pokorny,
  • Josef Sedlak,
  • Jozef Majerik,
  • Vlastimil Neumann and
  • Karel Klima

23 April 2021

This study investigated the possibility of nitride NiTi instruments using low-temperature plasma nitriding technology in a standard industrial device. Changes in the properties and fatigue life of used NiTi instruments before and after low-temperatur...

  • Article
  • Open Access
1 Citations
1,619 Views
17 Pages

Modeling of Plasma Nitriding of Austenitic Stainless Steel through a Mask

  • Paulius Andriūnas,
  • Reda Čerapaitė-Trušinskienė and
  • Arvaidas Galdikas

9 August 2024

In this work, 2D simulations of stainless steel nitriding through a mask were performed with two configurations: with and without lateral adsorption under the mask, depending on the strength of the mask adhesion. The stress-induced diffusion and trap...

  • Feature Paper
  • Article
  • Open Access
7 Citations
2,742 Views
16 Pages

Duplex Treatment of AISI 420 Steel by RF-ICP Nitriding and CrAlN Coating Deposition: The Role of Nitriding Duration

  • Dmitrii Vladimirovich Sidelev,
  • Ekaterina Dmitrievna Voronina and
  • Egor Borisovich Kashkarov

9 November 2022

The duplex treatment of AISI 420 steel samples by nitriding in a radiofrequency inductively coupled plasma (RF-ICP) discharge of Ar + N2 + H2 atmosphere followed by CrAlN coating deposition was performed in this study. The influence of plasma nitridi...

  • Communication
  • Open Access
2 Citations
1,951 Views
7 Pages

13 July 2022

In this study, Ti/Cu multilayer film was deposited by magnetron sputtering and then nitrided at 800 and 900 °C in N2. The microstructure and wear performance were studied. The deposited Ti/Cu multilayer film mainly consisted of Ti and Cu phases....

  • Article
  • Open Access
4 Citations
1,396 Views
14 Pages

Kinetics of Iron Nitride Layer Growth during the Nitriding of AISI 1085 Non-Alloy Steel and AISI 52100 Alloy Steel

  • Tadeusz Frączek,
  • Rafał Prusak,
  • Jerzy Michalski and
  • Magdalena Kowalewska-Groszkowska

20 September 2024

This paper presents a comparison of two-component ammonia-based inlet atmospheres diluted with either hydrogen (NH3/H2) or nitrogen (NH3/N2). Taking advantage of the features of inlet atmospheres diluted with nitrogen and hydrogen, four two-stage pro...

  • Article
  • Open Access
1 Citations
1,066 Views
12 Pages

Comprehensive Study of Electrolytic Plasma Nitriding of Austenitic Stainless Steels

  • Bauyrzhan Rakhadilov,
  • Zarina Satbayeva,
  • Almasbek Maulit,
  • Rauan Kozhanova,
  • Rinat Kurmangaliyev and
  • Anuar Rustemov

13 May 2025

The study investigates the spectral, structural, and phase changes occurring in austenitic steel 12Kh18N10T during cathodic electrolytic plasma nitriding (EPN) in a Na2CO3–CO(NH2)2–NH4Cl electrolyte at 550 °C for 10 min. Emission spec...

  • Article
  • Open Access
13 Citations
2,428 Views
13 Pages

Electrolytic Plasma Nitriding of Medium-Carbon Steel 45 for Performance Enhancement

  • Zarina Satbayeva,
  • Almasbek Maulit,
  • Nurlybek Ispulov,
  • Daryn Baizhan,
  • Bauyrzhan Rakhadilov and
  • Rinat Kusainov

15 October 2024

This article analyzes the effect of electrolytic plasma nitriding on the performance of medium-carbon steel 45 under increased mechanical loads and in aggressive environments. Nitrided samples in carbamide electrolytes, both with and without the addi...

  • Article
  • Open Access
80 Citations
9,701 Views
16 Pages

9 January 2015

A high power direct diode laser, emitting in the range of near infrared radiation at wavelength 808–940 nm, was applied to produce a titanium matrix composite on a surface layer of titanium alloy Ti6Al4V by laser surface gas nitriding. The nitrided s...

  • Article
  • Open Access
2 Citations
3,560 Views
22 Pages

Diffusion Nitride Surface Layers on Aluminum Substrates Produced by Hybrid Method Using Gas Nitriding

  • Michał Tacikowski,
  • Jacek Słoma,
  • Rafał Jakieła,
  • Szymon Marciniak,
  • Ryszard Diduszko and
  • Tadeusz Wierzchoń

29 April 2024

While gas nitriding of steel is currently used in industry, nitriding of aluminum alloys remains an open challenge. The main obstacle is aluminum’s high susceptibility to passivation. The oxide film provides an effective barrier to nitrogen dif...

  • Article
  • Open Access
5 Citations
3,792 Views
12 Pages

Gradient Microstructure in a Gear Steel Produced by Pressurized Gas Nitriding

  • Ran Yang,
  • Guilin Wu,
  • Xiaodan Zhang,
  • Wantang Fu,
  • Niels Hansen and
  • Xiaoxu Huang

19 November 2019

A tempered martensitic gear steel (18CrNiMo7-6) sample was nitrided on two sides using a 5 atm pressurized gas at 530 °C for five hours. The nitrided sample was characterized by means of microhardness, X-ray diffraction, scanning electron microsc...

  • Article
  • Open Access
2 Citations
1,089 Views
20 Pages

Innovative Short Process of Preparation and Nitriding of Porous 316L Stainless Steel

  • Chunheng Liu,
  • Fang Zhang,
  • Lei Zhang,
  • Jun Peng,
  • Hongtao Chang and
  • Yongbin Wang

30 March 2025

Porous 316L stainless steel has a low density and high specific surface area, and is easy to process due to the large number of pores within it, making it ideal for applications such as piping in the chemical and food industries, as a medical tool, o...

  • Article
  • Open Access
1 Citations
1,202 Views
27 Pages

Control of the Nitriding Process of AISI 52100 Steel in the NH3/N2 Atmosphere

  • Jerzy Michalski,
  • Tadeusz Frączek,
  • Rafał Prusak,
  • Agata Dudek,
  • Magdalena Kowalewska-Groszkowska and
  • Maciej Major

26 June 2025

This paper proposes a mathematical description of nitriding atmospheres obtained from a one-component ammonia ingoing atmosphere and a two-component ammonia inlet nitrogen-diluted atmosphere. The Fe-N phase equilibrium diagrams of the nitriding atmos...

  • Article
  • Open Access
4 Citations
2,290 Views
18 Pages

Nitriding has long been used to engineer the surfaces of engineering steels to improve their surface and subsurface properties. The role of the surface compound layer (γ′-Fe4N and/or ε-Fe2-3N) in improving the tribological and cor...

  • Article
  • Open Access
21 Citations
3,571 Views
9 Pages

Application of Active-Screen Plasma Nitriding to an Austenitic Stainless Steel Small-Diameter Thin Pipe

  • Kenzo Sumiya,
  • Shinkichi Tokuyama,
  • Akio Nishimoto,
  • Junichi Fukui and
  • Atsushi Nishiyama

22 February 2021

Low-temperature active-screen plasma nitriding (ASPN) was applied in this study to improve the bending rigidity and corrosion resistance of a small-diameter thin pipe composed of austenitic stainless steel (SUS 304). The inner and outer diameters of...

  • Article
  • Open Access
19 Citations
4,190 Views
20 Pages

Corrosion Behavior of Nitrided Layer of Ti6Al4V Titanium Alloy by Hollow Cathodic Plasma Source Nitriding

  • Lei Zhang,
  • Minghao Shao,
  • Zhehao Zhang,
  • Xuening Yi,
  • Jiwen Yan,
  • Zelong Zhou,
  • Dazhen Fang,
  • Yongyong He and
  • Yang Li

7 April 2023

Ti6Al4V titanium alloys, with high specific strength and good biological compatibility with the human body, are ideal materials for medical surgical implants. However, Ti6Al4V titanium alloys are prone to corrosion in the human environment, which aff...

  • Article
  • Open Access
6 Citations
6,590 Views
7 Pages

17 November 2016

Surface mechanical attrition treatment (SMAT) is an effective method to accelerate the nitriding process of metallic materials. In this work, a novel technique named surface nano-alloying (SNA) was developed on the basis of surface mechanical attriti...

  • Article
  • Open Access
3 Citations
3,435 Views
17 Pages

Resistance of Aluminide Coatings on Austenitic Stainless Steel in a Nitriding Atmosphere

  • Karolina Wierzbowska,
  • Agnieszka Elżbieta Kochmańska and
  • Paweł Kochmański

27 December 2021

A new slurry cementation method was used to produce silicide-aluminide protective coatings on austenitic stainless steel 1.4541. The slurry cementation processes were carried out at temperatures of 800 and 1000 °C for 2 h with and without an addi...

  • Article
  • Open Access
5 Citations
2,570 Views
18 Pages

The Effects of Modifying the Activity of Nitriding Media by Diluting Ammonia with Nitrogen

  • Mihai Ovidiu Cojocaru,
  • Mihai Branzei,
  • Andrei Mihai Ghinea and
  • Leontin Nicolae Druga

7 May 2021

This paper discusses the issue of the effects of modifying the activity of nitriding media by diluting ammonia with nitrogen and the concomitant variation in the degree of ammonia dissociation on the layer’s growth kinetics and their phase compositio...

  • Article
  • Open Access
39 Citations
4,995 Views
12 Pages

Tribological Behavior of Titanium Alloy Treated by Nitriding and Surface Texturing Composite Technology

  • Jiajie Kang,
  • Mingzheng Wang,
  • Wen Yue,
  • Zhiqiang Fu,
  • Lina Zhu,
  • Dingshun She and
  • Chengbiao Wang

18 January 2019

This study experimentally investigated the effect of surface textures on the tribological mechanism of nitrided titanium alloy (Ti–6Al–4V). The titanium alloy samples were nitrided at various temperatures ranging from 750 to 950 °C fo...

  • Article
  • Open Access
5 Citations
2,582 Views
15 Pages

The Effectiveness of Active Screen Method in Ion Nitriding Grade 5 Titanium Alloy

  • Tadeusz Frączek,
  • Rafał Prusak,
  • Marzena Ogórek and
  • Zbigniew Skuza

15 July 2021

The study assessed the effect of ion nitriding on the properties of the surface layer of Grade 5 titanium alloy used, among others, in medicine. Titanium and its alloys have low hardness and insufficient wear resistance in conditions of friction whic...

  • Article
  • Open Access
2 Citations
2,196 Views
10 Pages

Surface Modification of Chromium–Nickel Steel by Electrolytic Plasma Nitriding Method

  • Zarina Satbayeva,
  • Bauyrzhan Rakhadilov,
  • Zhangabay Turar,
  • Nurbol Berdimuratov,
  • Daryn Baizhan and
  • Almasbek Maulit

26 August 2024

Electrolytic plasma nitriding is an attractive chemical heat treatment used to improve the surface properties of steel by implementing nitrogen saturation. This method is widely applied to steel and iron-based alloys operating under various operating...

  • Article
  • Open Access
16 Citations
4,273 Views
16 Pages

High-Efficient Gas Nitridation of AISI 316L Austenitic Stainless Steel by a Novel Critical Temperature Nitriding Process

  • Daodong Tang,
  • Chengsong Zhang,
  • Haoting Zhan,
  • Wenao Huang,
  • Zongkai Ding,
  • Dazhi Chen and
  • Guodong Cui

28 September 2023

To improve the surface properties of austenitic stainless steels, a thick S-phase layer was prepared by using a novel critical temperature nitriding (CTN) process. The properties of the thick S-phase layer were optimized by controlling the process pa...

  • Review
  • Open Access
60 Citations
8,879 Views
22 Pages

Laser-Sustained Plasma (LSP) Nitriding of Titanium: A Review

  • Amar M. Kamat,
  • Stephen M. Copley,
  • Albert E. Segall and
  • Judith A. Todd

26 April 2019

Titanium and its alloys possess several attractive properties that include a high strength-to-weight ratio, biocompatibility, and good corrosion resistance. However, due to their poor wear resistance, titanium components need to undergo surface harde...

  • Article
  • Open Access
18 Citations
3,735 Views
16 Pages

Effects of Initial Microstructure on the Low-Temperature Plasma Nitriding of Ferritic Stainless Steel

  • Lingze Li,
  • Ruiliang Liu,
  • Quanli Liu,
  • Zhaojie Wu,
  • Xianglong Meng and
  • Yulan Fang

27 September 2022

AISI 430 ferritic stainless steel with different initial microstructures was low-temperature plasma nitrided to improve its hardness and wear resistance in the present investigation. The microstructure and properties of the low-temperature nitrided l...

  • Article
  • Open Access
34 Citations
6,490 Views
12 Pages

7 June 2020

High-entropy alloys (HEAs) were fabricated by powder metallurgy using gas-atomized powder and spark plasma sintering (SPS) followed by surface modification (plasma nitriding) of the sintered sample. Plasma nitriding forms nitride and induces solid-so...

  • Article
  • Open Access
545 Views
16 Pages

Nitriding of Commercially Pure (CP) Titanium Grade 2 by the Active Screen Method

  • Tadeusz Frączek,
  • Milena Pilarska,
  • Zbigniew Skuza and
  • Rafał Prusak

16 October 2025

This paper addresses the formation of nitrided layers on CP Titanium Grade 2 substrates under direct current (DC) glow discharge conditions. In the preliminary research, the parameters for glow discharge plasma nitriding were selected, and the thresh...

  • Review
  • Open Access
7 Citations
3,905 Views
13 Pages

Nitriding Treatments in Nickel–Chromium-Based Superalloy INCONEL 718: A Review

  • Oriana Palma Calabokis,
  • Yamid E. Nuñez de la Rosa,
  • Vladimir Ballesteros-Ballesteros and
  • Edward Andrés Gil González

6 August 2024

This literature review focuses on the nitriding treatments of nickel-based superalloy UNS N07718, also called INCONEL 718. This alloy was selected due to the relevance of this alloy in the aerospace and oil and gas industries. The referenced studies...

  • Article
  • Open Access
22 Citations
5,088 Views
13 Pages

The Effect of Plasma Nitriding on the Fatigue Behavior of the Ti-6Al-4V Alloy

  • Michele C. B. de Castro,
  • Antônio A. Couto,
  • Gisele F. C. Almeida,
  • Marcos Massi,
  • Nelson B. de Lima,
  • Argemiro da Silva Sobrinho,
  • Mariano Castagnet,
  • Gleicy L. Xavier and
  • Rene R. Oliveira

9 February 2019

The Ti-6Al-4V alloy is widely used in the manufacture of components that must have low density and high corrosion resistance and fatigue strength. The fatigue strength can be improved by surface modification. The aim of this study was to determine th...

  • Article
  • Open Access
28 Citations
6,123 Views
15 Pages

Effect of Plasma Nitriding on the Creep and Tensile Properties of the Ti-6Al-4V Alloy

  • Gisele F. C. Almeida,
  • Antônio A. Couto,
  • Danieli A. P. Reis,
  • Marcos Massi,
  • Argemiro S. Da Silva Sobrinho and
  • Nelson B. De Lima

7 August 2018

This work aimed to enhance the creep resistance of Ti-6Al-4V alloy treated by plasma nitriding. The nitriding was performed on specimens with a Widmanstätten microstructure for four hours at 690 °C under a gas atmosphere containing Ar:N2:H2...

  • Article
  • Open Access
11 Citations
3,327 Views
18 Pages

17 November 2021

Low-temperature nitriding allows to improve surface hardening of austenitic stainless steels, maintaining or even increasing their corrosion resistance. The treatment conditions to be used in order to avoid the precipitation of large amounts of nitri...

  • Article
  • Open Access
1 Citations
1,918 Views
13 Pages

27 June 2023

Preparing protecting coatings on the surface of Zr claddings has been regarded as one of the accident tolerant fuel (ATF) strategies. In this study, a series of nitride-modified layers were in situ grown by hollow cathode plasma nitriding on the surf...

  • Article
  • Open Access
4 Citations
1,608 Views
13 Pages

22 February 2025

The organizational development of 316L austenitic stainless steel was examined in this work under various levels of compression deformation (0, 10%, 20%, 30%, 40%, and 50%) and thoroughly investigated at multiple scales using SEM and EBSD techniques....

  • Article
  • Open Access
2 Citations
2,332 Views
20 Pages

21 December 2024

Heat treatment technology changes all the mechanical properties of metallic materials. The influence of induction hardening, nitriding and boronising on the change in the microhardness, impact toughness, microstructure and coefficient of friction of...

  • Article
  • Open Access
24 Citations
7,679 Views
9 Pages

21 March 2017

The effects of gas nitriding temperature on the cross section morphology, element nitrogen distribution, and surface layer compositions of a cold rolled and pre-strained high manganese austenitic TWIP steel 25Mn-3Cr-3Al-0.3C-0.01N and the correspondi...

  • Article
  • Open Access
18 Citations
4,388 Views
15 Pages

10 June 2020

In order to improve the extensive application of 304 steel in various industrial fields, dimples with different diameter and spacing arrayed on the surface of 304 steel were prepared by laser etching. Then the nitriding treatment was applied on the t...

  • Article
  • Open Access
762 Views
22 Pages

Features of Structural–Phase Changes and Tribological Behavior of Tool Steel After Vacuum and Plasma Electrolytic Nitriding

  • Marina A. Volosova,
  • Sergei A. Kusmanov,
  • Tatiana L. Mukhacheva,
  • Ivan V. Tambovskiy,
  • Artem O. Komarov,
  • Andrey E. Smirnov,
  • Svetlana F. Katerzhina,
  • Igor V. Suminov and
  • Sergey N. Grigoriev

Nitriding is one of the technologies used to improve the performance properties of tool steels. In addition to traditional gas nitriding, technologies aimed at increasing the productivity and/or efficiency of processing have found application in indu...

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