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Separations, Volume 10, Issue 11

2023 November - 32 articles

Cover Story: Heavy metal pollution has risen in recent years and has become an ongoing issue for environmental organizations, being one of the most serious ecological concerns at present. Exposure to certain heavy metals has been linked to a number of disorders that are harmful to human health. Trace metal concentration in real samples is extremely low and the complexity of matrices in real samples may substantially interfere with the determination of analytes. Therefore, it is necessary to develop simple, selective, reliable, efficient, and eco-friendly sample pretreatment methods for the extraction of trace amounts of heavy metals in environmental and biological samples before determination. In this study, we developed an analytical method for the determination of trace metals in wastewater samples using a new Co-doped magnetic carbon as a sorbent. View this paper
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Articles (32)

  • Article
  • Open Access
2 Citations
3,123 Views
15 Pages

Selective H2 Evolution and CO2 Absorption in Electrolysis of Ethanolamine Aqueous Solutions

  • Satoshi Fukada,
  • Ryosuke Sakai,
  • Makoto Oya and
  • Kazunari Katayama

20 November 2023

Selective H2 evolution and CO2 absorption in several ethanolamine aqueous solutions are comparatively investigated using a new electrolysis reactor. H2 bubbles are generated from a cathode in any ethanolamine electrolyte, and its experimental gas evo...

(This article belongs to the Special Issue Advances in CO2 Adsorptive Separation for CO2 Capture)
  • Article
  • Open Access
8 Citations
2,728 Views
17 Pages

19 November 2023

The development of analytical procedures capable of simultaneous determination of two or more drugs is in crucial demand due to the availability of different formulations that are composed of different APIs. The presented study aimed to optimize and...

  • Article
  • Open Access
6 Citations
3,328 Views
12 Pages

19 November 2023

Glyphosate-based herbicides are the most widely used pesticides in the world; however, the toxicity of glyphosate (GlyP) toward humans, especially its carcinogenicity, is controversial. The aim of this work was to validate a rapid assay for measuring...

  • Article
  • Open Access
2 Citations
3,303 Views
26 Pages

Nutritional and Possible Pharmaceutical Aspects of Tree Exudates Eaten by Lemurs of Madagascar’s Dry Forests

  • Jörg U. Ganzhorn,
  • Yedidya R. Ratovonamana,
  • Melina Rother,
  • Peggy Giertz and ,
  • Curswan A. Andrews,
  • Sabine Baumann,
  • Yvonne E.-M. B. Bohr,
  • Peter M. Kappeler,
  • B. Karina Montero and
  • Irene Tomaschewski
  • + 12 authors+ 7 authors

18 November 2023

Gums produced by trees after injuries are valuable food resources for several primate species. Yet, information on the chemical characteristics of gum is scant and inconsistent. We use gums consumed by lemurs (strepsirrhine primates of Madagascar) as...

(This article belongs to the Section Analysis of Natural Products and Pharmaceuticals)
  • Article
  • Open Access
10 Citations
4,424 Views
13 Pages

Mineralogical Characteristics of Baima Vanadium Titanomagnetite during Magnetic Separation Upgrading

  • Xiang Zhong,
  • Haoran Hu,
  • Shuo Li,
  • Jian Gao and ,
  • Zhixin Shi and
  • Fuxing Zhu
  • + 1 author+ 0 author

17 November 2023

The Baima vanadium titanomagnetite deposit, located in the Panzhihua-Xichang (Panxi) metallogenic belt in China, is one of the super-large deposits in the region. The titanomagnetite upgrading process involves grinding the raw ore followed by magneti...

  • Article
  • Open Access
1 Citations
2,751 Views
11 Pages

Rapid Determination of Five Residual Solvents in Ursodeoxycholic Acid Raw Materials

  • Ran Zhou,
  • Jingyu He,
  • Yi Shi,
  • Xiaoying Gao and ,
  • Fei Wang and
  • Sijie Liu
  • + 1 author+ 0 author

17 November 2023

The chromatographic conditions were optimized using headspace gas chromatography, and a simple and rapid method was established for the simultaneous determination of five residual solvents in ursodeoxycholic acid raw materials. The corresponding qual...

(This article belongs to the Special Issue Comprehensive Separations of Complex Mixtures by Gas Chromatography/Mass Spectrometry)
  • Review
  • Open Access
10 Citations
13,421 Views
20 Pages

16 November 2023

As early as 1946, Felix Bloch and Edward Mills Purcell detected nuclear magnetic resonance signals, earning themselves the Nobel Prize in 1952. The same year saw the launch of the first commercial nuclear magnetic resonance (NMR) spectrometer. Since...

  • Article
  • Open Access
1 Citations
2,878 Views
21 Pages

Diffusion, Separation, and Buffering of Non-Steady-State VOCs Flow on Activated Carbon

  • Tianzhe Shi,
  • Tao Liu,
  • Ning Qiang,
  • Jiao He and ,
  • Zhaohai Li,
  • Yiqi Cao and
  • Xianbin Shi
  • + 2 authors+ 0 author

16 November 2023

In this study, the diffusion, separation, and buffering of volatile organic compounds emitted in a non-steady state on activated carbon were studied. Ethanol and xylene, which have large differences in adsorption capacity and diffusion rate, were sel...

  • Article
  • Open Access
15 Citations
10,420 Views
18 Pages

Synthesis of Polyaluminum Chloride Coagulant from Waste Aluminum Foil and Utilization in Petroleum Wastewater Treatment

  • Hanan H. Youssef,
  • Sherif A. Younis,
  • Esraa M. El-Fawal,
  • Hager R. Ali and ,
  • Yasser M. Moustafa and
  • Gehad G. Mohamed
  • + 1 author+ 0 author

15 November 2023

This work investigates the potential synthesis of cost-effective polyaluminum chloride (PACl) coagulant from waste household aluminum foil and utilization for treating petroleum wastewater (PWW), especially dissolved organic compounds (DOC, like octa...

(This article belongs to the Section Materials in Separation Science)
  • Review
  • Open Access
20 Citations
8,325 Views
18 Pages

Nanostructure-Based Oil–Water Separation: Mechanism and Status

  • Bao Wang,
  • Shaotong Feng,
  • Caihua Wang,
  • Xiaoyan Liu and ,
  • Lei Chen and
  • Dayun Yan
  • + 1 author+ 0 author

15 November 2023

Flexible and effective methods for oil–water separation are crucial for reducing pollutant emissions and safeguarding water and fuel resources. In recent years, there has been growing interest in fundamental research and engineering application...

(This article belongs to the Special Issue Advanced Oil–Water Separation Technology)
  • Article
  • Open Access
2 Citations
3,146 Views
17 Pages

Fenton Oxidation Combined with Iron–Carbon Micro-Electrolysis for Treating Leachate Generated from Thermally Treated Sludge

  • Xiaoqing Dong,
  • Hui Liu,
  • Ji Li,
  • Ruiqi Gan and ,
  • Quanze Liu and
  • Xiaolei Zhang
  • + 1 author+ 0 author

14 November 2023

In this study, Iron–Carbon Micro-Electrolysis (ICME), Fenton oxidation, and their combination were investigated to treat the leachate obtained from a wastewater treatment plant located in southern China. The results show that the Fenton-ICME pr...

(This article belongs to the Collection Feature Paper Collection in Section 'Materials in Separation Science')
  • Article
  • Open Access
6 Citations
4,162 Views
12 Pages

Simultaneous Quantification Method of Flavonoids in Jeju Native Citrus from Different Harvest Times Using a High-Performance Liquid Chromatography–Diode Array Detector (HPLC–DAD)

  • Hyejin Hyeon,
  • Ho Bong Hyun,
  • Sung Chun Kim,
  • Boram Go and ,
  • Seon-A Yoon,
  • Yong-Hwan Jung and
  • Young-Min Ham
  • + 2 authors+ 0 author

11 November 2023

In Jeju-native Citrus, flavonoids are the main contributors to the various types of biological activity, such as antioxidant, antitumor, and anti-inflammatory activity. Thus, we developed simultaneous quantification methods for the analysis of ten bi...

(This article belongs to the Section Analysis of Food and Beverages)
  • Article
  • Open Access
12 Citations
6,428 Views
16 Pages

10 November 2023

Understanding the VOC profile released during the early post-mortem period is essential for applications in training human remains detection dogs and urban search and rescue operations (USAR) to rapidly locate living and deceased victims. Human cadav...

(This article belongs to the Section Forensic Science and Toxicology)
  • Review
  • Open Access
164 Citations
19,191 Views
26 Pages

Advancements in Adsorption Techniques for Sustainable Water Purification: A Focus on Lead Removal

  • Amal M. Badran,
  • Uthumporn Utra,
  • Nor Shariffa Yussof and
  • Mohammed J. K. Bashir

10 November 2023

The long-term sustainability of the global water supply, with a paramount emphasis on cleanliness and safety, stands as a formidable challenge in our modern era. In response to this pressing issue, adsorption techniques have emerged as pivotal and wi...

(This article belongs to the Collection Feature Paper Collection in Section 'Materials in Separation Science')
  • Article
  • Open Access
12 Citations
4,140 Views
14 Pages

Analysis of Polycyclic Aromatic Hydrocarbons Using Magnetic Three-Dimensional Graphene Solid-Phase Extraction Coupled with Gas Chromatography–Mass Spectrometry

  • Hassan Sereshti,
  • Mahsa Karimi,
  • Sajad Karami,
  • Shokouh Mahpishanian and ,
  • Mehdi Esmaeili Bidhendi,
  • Shahabaldin Rezania,
  • Amin Mojiri,
  • Hesam Kamyab and
  • Hamid Rashidi Nodeh
  • + 4 authors+ 0 author

10 November 2023

In this study, a composite material consisting of three-dimensional graphene aerogel and iron oxide nanoparticles (3DG/Fe3O4) was created and utilized for the purpose of magnetic solid-phase extraction (MSPE) of thirteen polycyclic aromatic hydrocarb...

(This article belongs to the Section Environmental Separations)
  • Article
  • Open Access
10 Citations
4,685 Views
18 Pages

Enhancing Trace Metal Extraction from Wastewater: Magnetic Activated Carbon as a High-Performance Sorbent for Inductively Coupled Plasma Optical Emission Spectrometry Analysis

  • Sergio J. Abellán-Martín,
  • David Villalgordo-Hernández,
  • Miguel Ángel Aguirre,
  • Enrique V. Ramos-Fernández and ,
  • Javier Narciso and
  • Antonio Canals
  • + 1 author+ 0 author

10 November 2023

A new fast, sensitive, and environmentally friendly analytical method has been developed for the simultaneous determination of Ba, Be, Cd, Cr, Cu, Fe, Hg, Mn, Ni, Pb, and Zn in wastewater samples using inductively coupled plasma optical emission spec...

(This article belongs to the Topic Analysis and Separations of Trace Elements in the Environment)
  • Article
  • Open Access
8 Citations
2,937 Views
17 Pages

A Study on the Removal Characteristics and Mechanism of Phosphorus from Simulated Wastewater Using a Novel Modified Red-Mud-Based Adsorption Material

  • Wenbao Liu,
  • Qin Zhang,
  • Yanbai Shen,
  • Weichao Li and ,
  • Sikai Zhao,
  • Qiang Zhao and
  • Yiqun Zhang
  • + 2 authors+ 0 author

10 November 2023

In this work, a common third-generation environmentally friendly quaternary ammonium salt disinfectant, dimethyl dioctadecyl ammonium chloride (DDAC), was used as the modifier to achieve one-step rapid preparation of the modified red-mud-based adsorp...

(This article belongs to the Section Separation Science in Energies)
  • Article
  • Open Access
10 Citations
5,999 Views
19 Pages

9 November 2023

Kazakhstan ranks as the 12th largest oil producer globally and boasts a diverse range of crude oils. This research introduces a method for distinguishing between the different types of crude oils based on biomarker analysis of 28 crude oils from West...

(This article belongs to the Topic Oil, Gas and Water Separation Research)
  • Article
  • Open Access
10 Citations
3,003 Views
13 Pages

9 November 2023

The solvothermal synthesis technique was employed to successfully fabricate a series of rare earth doped SnO2-Sb electrodes on the TNTs array substrate, serving as anode material for electrocatalytic degradation of phenol. The electrode doped with ra...

(This article belongs to the Section Environmental Separations)
  • Article
  • Open Access
15 Citations
4,202 Views
18 Pages

Adsorption Properties and Mechanism of Copper Ions from Wastewater by Lessonia nigrescens and Lessonia nigrescens Residue

  • Haoran Chen,
  • Rui Zhang,
  • Xiaohan Qu,
  • Yuan Yuan and ,
  • Bo Zhu,
  • Shichao Zhao and
  • Tengyao Jiang
  • + 2 authors+ 0 author

5 November 2023

Given the advantages of readily availability, low cost, convenient operation, and large adsorption capacity, brown seaweed has been studied extensively as a biosorbent for heavy metal remediation from aqueous media. Herein, raw Lessonia nigrescens an...

(This article belongs to the Special Issue Advanced Functional Materials for Wastewater Treatment and Purification)
  • Article
  • Open Access
6 Citations
7,093 Views
25 Pages

Evaluation of CO2 Adsorption Parameters in Fluidised Zeolite 13X Beds Using Non-Linear Multivariate Optimisation

  • Alessio Caravella,
  • Giuseppe Prenesti,
  • Salvatore De Luca,
  • Maria Turano and ,
  • Flaviano Testa and
  • Rossella Girimonte
  • + 1 author+ 0 author

3 November 2023

This work is part of a research project aimed at studying potential sorbents for CO2 capture. The main parameters characterising the adsorption process of zeolite 13X were derived with the aim of overcoming the limits of experimental analysis and thu...

(This article belongs to the Special Issue Advances in CO2 Adsorptive Separation for CO2 Capture)
  • Article
  • Open Access
3 Citations
2,904 Views
14 Pages

Examination of Volatile Signatures of Fusarium Bulb Rot in Garlic Using Proton-Transfer-Reaction Time-of-Flight Mass Spectrometry and Solid-Phase Microextraction Gas Chromatography/Mass Spectrometry

  • Alessandro Infantino,
  • Cosimo Taiti,
  • Alessandro Grottoli,
  • Stefano Mancuso and ,
  • Corrado Costa and
  • Stefania Garzoli
  • + 1 author+ 0 author

31 October 2023

Fusarium bulb rot, caused by Fusarium proliferatum, is a worldwide disease of garlic, both in the open field and during storage. Early diagnosis of the disease during storage is difficult due to the morphology of the bulbs and cloves. Volatile organi...

(This article belongs to the Special Issue Application of Chromatography in Analytical Chemistry)
  • Article
  • Open Access
1 Citations
2,632 Views
21 Pages

31 October 2023

A chemical recognition algorithm is an integral part of any autonomous microscale gas chromatography (µGC) system for automated chemical analysis. For a multi-detector µGC system, the chemical analysis must account for the retention time...

(This article belongs to the Section Chromatographic Separations)
  • Article
  • Open Access
6 Citations
3,789 Views
21 Pages

Purification, Characterization, and Ferrous Oxidation Kinetics of Iron Oxidase from Acidithiobacillus ferridurans

  • Yuandong Liu,
  • Jiayu He,
  • Xiangdong Shangguan,
  • Run Liu and ,
  • Xiaofeng Zeng,
  • Wissal Belqadi,
  • Kan Wang,
  • Yan Tong,
  • Runlan Yu and
  • Guanzhou Qiu
  • + 8 authors+ 3 authors

31 October 2023

Iron oxidase was proposed to be the initial electron acceptor from the ferrous ion in the iron oxidation of the Acidithiobacillus genus for metal bioextraction; however, its most fundamental property of direct ferrous oxidation kinetics remains undet...

  • Article
  • Open Access
6 Citations
3,842 Views
13 Pages

Analysis of Volatile Components and Antibacterial Activity of Silver Wormwood Essential Oils from Different Habitats by E-Nose Combined with GC-MS

  • Yiqin Yang,
  • Dongyun Guo,
  • Shujie Yang,
  • Huiquan Hu and ,
  • Xiaorong Luo and
  • Na Wan
  • + 1 author+ 0 author

31 October 2023

Electronic nose (E-nose) combined with gas chromatography–mass spectrometry (GC-MS) was used to analyze the volatile components of silver wormwood from different habitats, and the antibacterial activity of essential oils was also studied, to pr...

(This article belongs to the Section Analysis of Natural Products and Pharmaceuticals)
  • Article
  • Open Access
7 Citations
3,944 Views
22 Pages

LC/MS-Based Profiling of Hedyotis aspera Whole-Plant Methanolic Extract and Evaluation of Its Nephroprotective Potential against Gentamicin-Induced Nephrotoxicity in Rats Supported by In Silico Studies

  • Dsnbk Prasanth,
  • Lingareddygari Siva Sanker Reddy,
  • Tharani Dasari,
  • Pamula Reddy Bhavanam and ,
  • Sheikh F. Ahmad,
  • Rahul Nalluri and
  • Praveen Kumar Pasala
  • + 2 authors+ 0 author

30 October 2023

Many high-altitude plants, such as Hedyotis aspera, need to be explored for their possible medicinal value. The current study explored the protective effect of Hedyotis aspera methanolic extract whole plant (HAME) against gentamicin-induced nephrotox...

(This article belongs to the Special Issue Advanced Research on Extraction and Analysis of Plant Extracts)
  • Article
  • Open Access
9 Citations
6,467 Views
15 Pages

29 October 2023

The synthesis of 14 hydrazone compounds derived from pyridoxal, pyridine-4-carbaldehyde, and quinoline-2-carbaldehyde using two methods, conventional method in deep eutectic solvents (DESs) and effective combination of ultrasound and DESs, is present...

(This article belongs to the Section Purification Technology)
  • Article
  • Open Access
5 Citations
3,218 Views
14 Pages

Design Methodology for a Low-Shear Rotating Swirler

  • Zheng Si,
  • Yipeng Ji,
  • Jiaqing Chen,
  • Xiujun Wang and ,
  • Hong Du,
  • Jian Zhang,
  • Hai Yu,
  • Qiang Ren and
  • Zhao Hua
  • + 4 authors+ 0 author

28 October 2023

The tubular dynamic hydrocyclone (TDH) holds great potential for the pre-deoiling of offshore oil platforms. However, the shear and turbulence in the flow field can cause the oil droplets, the dispersed phase in water, to break up when the swirling f...

(This article belongs to the Special Issue Advanced Oil–Water Separation Technology)
  • Article
  • Open Access
8 Citations
2,948 Views
14 Pages

27 October 2023

Industrial wastewater usually contains a large amount of organic and inorganic pollutants, and many microorganisms. However, the types of microorganism present in industrial wastewater are still unclear. The aim of this study was to analyze the physi...

  • Article
  • Open Access
4 Citations
3,260 Views
15 Pages

Metabolic Stability of Eight Airborne OrganoPhosphate Flame Retardants (OPFRs) in Human Liver, Skin Microsomes and Human Hepatocytes

  • Stefano Di Bona,
  • Emanuele Artino,
  • Francesca Buiarelli,
  • Patrizia Di Filippo and ,
  • Roberta Galarini,
  • Stefano Lorenzetti,
  • Franco Lucarelli,
  • Gabriele Cruciani and
  • Laura Goracci
  • + 4 authors+ 0 author

25 October 2023

The waste of electrical and electronic equipment (WEEE) is generally considered a secondary raw material for the recovery of valuable components. However, emerging issues regarding the impact of suspended particles arising from WEEE recycling operati...

(This article belongs to the Section Chromatographic Separations)
  • Article
  • Open Access
11 Citations
4,491 Views
14 Pages

Untargeted Screening of Per- and Polyfluoroalkyl Substances (PFASs) in Airborne Particulate of Three Italian E-Waste Recycling Facilities

  • Carolina Barola,
  • Elisabetta Bucaletti,
  • Simone Moretti,
  • Francesca Buiarelli and ,
  • Giulia Simonetti,
  • Franco Lucarelli,
  • Laura Goracci,
  • Stefano Lorenzetti,
  • Patrizia Di Filippo and
  • Roberta Galarini
  • + 7 authors+ 2 authors

25 October 2023

Poly- and perfluorinated alkyl substances (PFASs) are widely used in the electrical and electronic appliance industry to the point that waste of electrical and electronic equipment (WEEE), also known as e-waste, creates significant potential for PFAS...

(This article belongs to the Section Chromatographic Separations)
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Separations - ISSN 2297-8739