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Journal Description

Minerals

Minerals is an international, peer-reviewed, open access journal of natural mineral systems, mineral resources, mining, and mineral processing, and is published monthly online by MDPI.

Open Access— free for readers, with article processing charges (APC) paid by authors or their institutions.
High Visibility: indexed within Scopus, SCIE (Web of Science), GEOBASE, GeoRef, CaPlus / SciFinder, Inspec, Astrophysics Data System, AGRIS, and other databases.
Journal Rank: JCR - Q2 (Mining and Mineral Processing) / CiteScore - Q1 (Geology)
Rapid Publication: manuscripts are peer-reviewed and a first decision is provided to authors approximately 17.7 days after submission; acceptance to publication is undertaken in 2.6 days (median values for papers published in this journal in the second half of 2025).
Recognition of Reviewers: reviewers who provide timely, thorough peer-review reports receive vouchers entitling them to a discount on the APC of their next publication in any MDPI journal, in appreciation of the work done.
Companion journal: Mining
Journal Cluster of Geotechnical Engineering and Geology: Minerals, GeoHazards, Mining, Geotechnics, Glacies and Stratigraphy and Sedimentology.

Impact Factor: 2.2 (2024); 5-Year Impact Factor: 2.5 (2024)

Imprint Information Journal Flyer Open Access ISSN: 2075-163X

Latest Articles

11 pages, 524 KB

Open AccessArticle

Geochemical and Radiological Assessment of a Region with Phosphate Deposits, Democratic Republic of the Congo

by Bruno O. Deko, Ruben K. Koy, Fernando P. Carvalho, John Poté and Emmanuel K. Atibu

Minerals 2026, 16(4), 359; https://doi.org/10.3390/min16040359 (registering DOI) - 28 Mar 2026

Four areas in the Kongo Central Province, western Democratic Republic of the Congo, with unexploited phosphate deposits were investigated to assess the composition of phosphatic materials and to evaluate pollution hazards, including radiological hazards arising from naturally occurring radionuclides. In those areas, phosphate [...] Read more.

Four areas in the Kongo Central Province, western Democratic Republic of the Congo, with unexploited phosphate deposits were investigated to assess the composition of phosphatic materials and to evaluate pollution hazards, including radiological hazards arising from naturally occurring radionuclides. In those areas, phosphate rocks were sampled and analyzed for P₂O₅ content (by ED-XRF), and for the naturally occurring radionuclides ²³⁸U, ²²⁶Ra, ²³²Th, ⁴⁰K (by gamma-ray spectrometry). Phosphate rocks displayed P₂O₅ content ranging from 1.06 to 24.42% (dry weight) and exceptionally high ²³⁸U and ²²⁶Ra activity concentrations (up to 3069 and 2273 Bq kg⁻¹, respectively), significantly exceeding global averages in soils. Radiological hazard indices, including the radium equivalent (RaEq), annual effective dose and lifetime cancer risk, confirmed potential health risks associated with phosphate-rich rocks. With the upcoming development of phosphate deposits in DRC, such phosphate materials might become future sources of both geochemical contamination and radiological exposure, emphasizing the need for suitable radiation monitoring and waste management plans prior to and during mineral resource exploitation. Full article

(This article belongs to the Special Issue Radionuclides and Radiation Exposure in Minerals Extraction, Processing and Applications)

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26 pages, 1830 KB

Open AccessReview

Use of Mining Waste Classification in the Context of a Circular Economy—A Review

by Bruno Lemière and Richard Lord

Minerals 2026, 16(4), 358; https://doi.org/10.3390/min16040358 (registering DOI) - 28 Mar 2026

The beneficial use of mining waste aligns with circular economy thinking: saving primary resources can extend their lifetime and maintain availability, reduce the volume of legacy mining waste and its environmental impacts, and develop a resource beneficiation industry that is less energy and [...] Read more.

The beneficial use of mining waste aligns with circular economy thinking: saving primary resources can extend their lifetime and maintain availability, reduce the volume of legacy mining waste and its environmental impacts, and develop a resource beneficiation industry that is less energy and water intensive; mining lower grades at larger scale inevitably requires more beneficial reuse. Existing classifications applicable to different types of mine waste were reviewed. These include factors such as the mode of origin during the mining operation, grain size, chemical composition and stability. The result shows that these factors also largely control their civil engineering applications, suitability for end use sectors and potential hazards. Long-term liabilities related to chemical stability were identified as the most difficult challenge. When developing a reuse project, either by the end users or by the mine operator, it is likely that resource screening covering a comprehensive range of factors will be required, as none of the existing schemes individually cover all of the aspects needed to fully assess suitability for beneficial use. In conclusion, there is a need for a systematic and structured approach to classification of mining waste to facilitate reuse as raw materials, such as that presented in our review. Full article

(This article belongs to the Section Environmental Mineralogy and Biogeochemistry)

23 pages, 12467 KB

Open AccessArticle

Key Ore-Controlling Factors and Genetic Model of the Tamusu Super-Large Sandstone-Type Uranium Deposit, Bayingobi Basin

by Chao Lu, Zhongyue Zhang, Yangquan Jiao, Zhao Li, Xiaoyi Yuwen, Yinan Zhuang, Chengyuan Jin, Chengcheng Zhang, Weihui Zhong and Qilin Wang

Minerals 2026, 16(4), 357; https://doi.org/10.3390/min16040357 - 27 Mar 2026

Tamusu, the only identified super-large sandstone-hosted uranium deposit in the Bayingobi Basin, provides an important natural laboratory for evaluating ore-controlling factors and genetic models of sandstone-type uranium mineralization. Based on core descriptions from more than 200 boreholes, log facies analysis and geochemical environmental [...] Read more.

Tamusu, the only identified super-large sandstone-hosted uranium deposit in the Bayingobi Basin, provides an important natural laboratory for evaluating ore-controlling factors and genetic models of sandstone-type uranium mineralization. Based on core descriptions from more than 200 boreholes, log facies analysis and geochemical environmental proxies, this study constrains the sedimentary–mineralization architecture and key controlling factors of the deposit. Uranium orebodies are mainly hosted in the upper member of the Lower Cretaceous Bayingobi Formation (Sq2) within a gravity flow-dominated fan-delta–lacustrine system. Braided distributary channel sands on the fan-delta plain and subaqueous distributary channel sands on the delta front constitute the principal uranium reservoirs, controlling both the migration pathways and storage space for U-bearing fluids. Mineralization is jointly governed by fan-delta architecture, interlayer oxidation zonation and reducing agents. The interlayer oxidation zone displays a north-thick–south-thin geometry, and uranium orebodies are concentrated at redox transition positions, with grades of 0.01–0.33 wt%. The metallogenic evolution can be summarized in three stages: syndepositional uranium pre-enrichment, interlayer oxidation mineralization, and a late hydrothermal/diagenetic overprint that mainly modified reservoir properties, favored ore preservation, and did not contribute to the primary uranium budget. Accordingly, a genetic model of “fan-delta architecture + interlayer oxidation control + late overprint and preservation” is proposed to guide exploration in the Bayingobi Basin and analogous sandstone-type uranium systems. Full article

(This article belongs to the Special Issue Genesis of Uranium Deposit: Geology, Geochemistry, and Geochronology)

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18 pages, 1636 KB

Open AccessArticle

Microwave-Assisted Alkaline Leaching of Aluminum from Coal Fly Ash Using Amorphous Graphite: Experimental Study and Kinetic Analysis

by Nursaule Baatarbek, Lyazzat Mussapyrova, Aisulu Batkal, Bagdatgul Milikhat, Roza Abdulkarimova, Almagul Niyazbaeva, Timur Osserov and Kaster Kamunur

Minerals 2026, 16(4), 356; https://doi.org/10.3390/min16040356 - 27 Mar 2026

This study investigated the extraction of aluminum from aluminum silicate-rich coal ash from the ash-slag waste of the Almaty CHP-2 power station using microwave-assisted alkaline leaching. The high chemical stability of the quartz and mullite phases in the ash leads to high energy [...] Read more.

This study investigated the extraction of aluminum from aluminum silicate-rich coal ash from the ash-slag waste of the Almaty CHP-2 power station using microwave-assisted alkaline leaching. The high chemical stability of the quartz and mullite phases in the ash leads to high energy consumption during conventional acid–base treatment. To improve the kinetic parameters of the leaching process, amorphous graphite was therefore used as an active additive, which effectively absorbs microwave energy. The experiments were conducted in the temperature range of 50–200 °C, in 1–6 M NaOH solution, and over a period of 5–30 min. The amount of amorphous graphite varied between 5 and 20 wt%. The proportion of amorphous graphite varied between 5 and 20 wt%. Upon microwave irradiation, the graphite-free ash reached a temperature of 200 °C within approximately 12 min, whereas this temperature was reached in the system with 15% amorphous graphite after only 8–9 min. At low alkali concentrations (1–2 M NaOH), the aluminum transfer into solution in the graphite-free system was approximately 18%–35%. With increasing NaOH concentrations to 3–4 M, the aluminum removal efficiency increased to 38%–58%. Under the same temperature conditions, the leaching process was significantly accelerated by the addition of amorphous graphite; thus, at temperatures near 200 °C and in a 5–6 M NaOH solution, 70%–72% of aluminum was removed. The leaching kinetics were analyzed using the shrinking core model. The results showed that the apparent activation energy of the reaction decreased from 54 kJ/mol to 32 kJ/mol in the presence of graphite. These results suggest that microwave-assisted alkaline leaching in the presence of amorphous graphite is an energy-efficient and promising method for aluminum recovery from coal ash. Full article

(This article belongs to the Section Mineral Processing and Extractive Metallurgy)

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13 pages, 1804 KB

Open AccessArticle

Microfluidic Pre-Concentration of Metals from Fine Flotation Tailings

by Olesya Tyumentseva, Kaster Kamunur, Lyazzat Mussapyrova, Aisulu Batkal, Luisa Beisembayeva and Rashid Nadirov

Minerals 2026, 16(4), 355; https://doi.org/10.3390/min16040355 - 27 Mar 2026

The large volumes of fine flotation tailings constitute a persistent challenge for the conventional treatment of minerals due to their wide particle size distribution and their low metal contents. In this work, the potential of passive inertial microfluidics for the selective redistribution of [...] Read more.

The large volumes of fine flotation tailings constitute a persistent challenge for the conventional treatment of minerals due to their wide particle size distribution and their low metal contents. In this work, the potential of passive inertial microfluidics for the selective redistribution of mineral particles from actual copper flotation tailings is studied. A suspension of tailings was treated in a rectangular microfluidic channel in a laminar regime, without an external magnetic field or sheath flux. The solid fractions obtained were characterized in terms of particle size distribution, phase composition and element content. The microfluidic treatment induced a systematic distribution of the particles between the output fractions. The central fraction was enriched with coarser particles, the median particle size increasing from about 15 µm in the feed to about 20 µm, and had high concentrations of Cu, Fe, Ag and Zn, with enrichment factors reaching 2.0 to 2.7 depending on the element. On the other hand, the lateral fraction was mainly composed of finer particles (D50 ≈ 13 µm) and depleted in metalliferous phases. The elemental mass balance confirmed that the observed enrichment results from selective redistribution rather than from a loss of material. These results indicate that the separation of the particles cannot be explained solely by size effects and are consistent with a preferential migration of the denser and metal-rich particles towards stable inertial focusing trajectories. Full article

(This article belongs to the Section Mineral Processing and Extractive Metallurgy)

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21 pages, 12142 KB

Open AccessArticle

Systematic Mineralogical and Geochemical Analyses of Magnetite in the Xinqiao Cu-S Polymetallic Deposit, Eastern China

by Lei Shi, Yinan Liu, Xiao Xin and Yu Fan

Minerals 2026, 16(4), 354; https://doi.org/10.3390/min16040354 - 27 Mar 2026

The Xinqiao Cu-S polymetallic deposit is located in the Tongling ore concentration area of the Middle-Lower Yangtze River metallogenic belt. The orebodies consist of skarn orebodies and stratiform sulfide orebodies, but the genetic link between them remains controversial. In this study, magnetite was [...] Read more.

The Xinqiao Cu-S polymetallic deposit is located in the Tongling ore concentration area of the Middle-Lower Yangtze River metallogenic belt. The orebodies consist of skarn orebodies and stratiform sulfide orebodies, but the genetic link between them remains controversial. In this study, magnetite was used as a proxy to systematically constrain the hydrothermal evolution from the intrusion to the contact zone and further to the stratiform orebodies. A representative drill hole (E603) was logged, and samples were systematically collected from the Jitou pluton outward to the contact zone. Composite samples from the 8–28 m interval were crushed and prepared as resin mounts for integrated TIMA automated mineralogy, BSE textural observation, and in situ LA-ICP-MS trace element analysis. Five types of magnetite (Mt1 to Mt5) were systematically identified. Mt1 occurs as inclusions within feldspar in the quartz monzodiorite. It exhibits typical magmatic magnetite characteristics and contains grid-like ilmenite exsolution, indicating crystallization during the late magmatic stage. Mt2 is distributed in the interstices of magmatic minerals, commonly showing hematitization and replacement of ilmenite exsolution lamellae by titanite. Its trace element geochemistry displays magmatic–hydrothermal transitional features. Mt3–Mt5 in the skarn and stratiform orebodies are paragenetic with retrograde alteration minerals (e.g., epidote, chlorite, and actinolite) and sulfides, and are characterized by low Ti, Al, and V contents and high Mg, Mn, and Sn contents, indicating a hydrothermal origin. From Mt3 to Mt5, (Ti + V) and (Al + Mn) decrease, while Zn and Mn increase, accompanied by a decrease in the (Si + Al)/(Mg + Mn) ratio. This reflects a trend of decreasing fluid temperature and progressively enhanced wall-rock buffering. The Mg-in-magnetite geothermometer yields relatively consistent results for Mt1–Mt3, but anomalously high temperatures for Mt4–Mt5. This suggests that the elevated Mg activity in the fluid, caused by reaction with carbonate wall rocks, can significantly influence the calculated temperatures. Therefore, this geothermometer should be used cautiously for magnetite in the outer skarn zone and interpreted in combination with other temperature constraints. The textures, paragenetic mineral assemblages, and trace element characteristics of magnetite collectively reveal a continuous mineralization process linking the skarn and stratiform orebodies at Xinqiao, providing robust mineralogical and geochemical evidence for the contribution of Yanshanian magmatic–hydrothermal activity to the stratiform mineralization. Full article

(This article belongs to the Special Issue Magmatic–Hydrothermal Process and the Genesis of Related Mineral Deposits)

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17 pages, 3950 KB

Open AccessArticle

Triaxial Creep Behavior of Gangue–Gypsum Cemented Backfill and Applicability Verification of the Burgers Model

by Jingduo Liu, Xinguo Zhang, Jingjing Jiao, Zhongying Zhang, Pengkun Wang and Youpeng Li

Minerals 2026, 16(4), 353; https://doi.org/10.3390/min16040353 - 26 Mar 2026

Gangue backfilling has become an important technique for promoting environmentally friendly and low-carbon coal mining. The long-term creep behavior of cemented backfill plays a critical role in maintaining stope stability and controlling surface subsidence during long-term service. Although considerable research has been conducted [...] Read more.

Gangue backfilling has become an important technique for promoting environmentally friendly and low-carbon coal mining. The long-term creep behavior of cemented backfill plays a critical role in maintaining stope stability and controlling surface subsidence during long-term service. Although considerable research has been conducted on cemented tailings backfill, systematic investigations on the triaxial creep evolution, long-term strength characteristics, confining pressure effects, and the applicability of the classical Burgers model for gangue–gypsum cemented backfill under engineering-relevant confining pressures remain limited. In this study, the experimental scheme was designed based on field monitoring data from practical backfill mining operations, which indicate that the in situ backfill generally remains stable without significant deformation or instability under normal working conditions. Multi-stage loading triaxial creep tests were conducted on gangue–gypsum cemented backfill under confining pressures of 1, 2, 3, and 4 MPa. The creep deformation characteristics were analyzed using Chen’s superposition method, while the long-term strength was computed via inflection point method of isochronous stress–strain curves. The parameters of the Burgers creep model were identified using the Levenberg–Marquardt optimization algorithm, and numerical verification was performed using FLAC3D. Our findings demonstrate that the creep deformation process of the backfill consists of three typical stages: instantaneous deformation, attenuated creep, and steady-state creep, and no accelerated creep was observed within the applied stress range. The absolute creep strain surges nonlinearly with increasing stress level (S_L), whereas higher confining pressure significantly suppresses the creep response of the material. Within the investigated stress range, the backfill exhibits mainly linear viscoelastic behavior, and its critical long-term strength is not less than 0.9 times the failure deviatoric stress (qf). Although confining pressure enhances the long-term strength, the strengthening effect weakens as the confining pressure increases. Model fitting outcomes imply that Burgers model precisely describes the creep behavior of gangue–gypsum cemented backfill under all test conditions, with correlation coefficients (R²) exceeding 0.97. The identified parameters show systematic variation with S_L, reflecting stiffness degradation and viscous evolution during loading. Numerical simulation results agree well with the experimental data, providing theoretical guidance for mixture proportion optimization, long-term stability evaluation, and stope support parameter design in gangue backfill mining engineering. Full article

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22 pages, 954 KB

Open AccessReview

Geodynamic Evolution of the Dibaya Granitic–Migmatitic Complex, Kanyiki–Kapangu Area (Kasaï Shield): A Synthesis of Magmatic and Metamorphic Insights

by Trésor Mulunda Bululu, Jean Paul Kapuya Bulaba Nyembwe, Nsenda Lukumwena and Alphonse Tshimanga Kambaji

Minerals 2026, 16(4), 352; https://doi.org/10.3390/min16040352 - 26 Mar 2026

The Dibaya Granitic and Migmatitic Complex (DGMC), located in the Kanyiki–Kapangu sector of the Kasaï Shield (Congo–Kasaï Craton, Democratic Republic of the Congo), represents a key exposure of Neoarchean continental crust in Central Africa. Despite its geological importance, information on its petrology, geochronology, [...] Read more.

The Dibaya Granitic and Migmatitic Complex (DGMC), located in the Kanyiki–Kapangu sector of the Kasaï Shield (Congo–Kasaï Craton, Democratic Republic of the Congo), represents a key exposure of Neoarchean continental crust in Central Africa. Despite its geological importance, information on its petrology, geochronology, geochemistry, and structural evolution remains dispersed across historical studies. This contribution presents a structured geological synthesis based exclusively on previously published cartographic, petrographic, structural, and isotopic data. No new analytical data are introduced; rather, existing datasets are systematically compiled, critically reassessed, and integrated into a coherent tectono-thermal framework. Published Rb–Sr and U–Pb ages indicate high-grade metamorphism and widespread migmatitization at ca. 2.72 Ga, followed by granitoid emplacement at ca. 2.65 Ga. Documented mineral assemblages (garnet–biotite–plagioclase–quartz ± K-feldspar ± amphibole) and the absence of reported high-pressure index minerals support high-temperature, moderate-pressure metamorphism consistent with intracrustal reworking. Reported regional geochemical characteristics suggest high-K calc-alkaline, weakly to moderately peraluminous granitoids derived predominantly from reworking of older TTG-type crust. Structural relationships, particularly along the Malafudi corridor, demonstrate strong coupling between deformation, anatexis, and magma emplacement. Collectively, this synthesis formalizes a Neoarchean intracrustal reworking model and provides a structured analytical basis for future high-resolution petrochronological and geochemical investigations. Although no new quantitative datasets are presented, this study provides the first systematic integration of dispersed geological and isotopic information for the Dibaya Complex, establishing a transparent analytical framework for future high-resolution investigations. Full article

(This article belongs to the Section Mineral Deposits)

26 pages, 8352 KB

Open AccessArticle

Efficient Leaching and Kinetic Analysis of Rare Earth Elements from Rare-Earth-Enriched Residues of Associated Rare Earth Phosphate Ores

by Jiawei Lin, Jue Kou, Chunbao Sun, Hongda Xu and Xiaojin Wen

Minerals 2026, 16(4), 351; https://doi.org/10.3390/min16040351 - 26 Mar 2026

The efficient recovery of rare earth elements from associated rare-earth-bearing phosphate ores is of paramount importance for expanding the supply of rare earth resources. In contrast to conventional studies that focus on extracting rare earths either from phosphate concentrates or from phosphogypsum generated [...] Read more.

The efficient recovery of rare earth elements from associated rare-earth-bearing phosphate ores is of paramount importance for expanding the supply of rare earth resources. In contrast to conventional studies that focus on extracting rare earths either from phosphate concentrates or from phosphogypsum generated during the sulfuric acid wet-process, this study takes as its subject the rare-earth-enriched residue—an intermediate product obtained after the selective leaching of phosphorus via the hydrochloric acid route—from a rare-earth-bearing phosphate ore in Zhijin, Guizhou Province. The occurrence states, leaching behavior, and kinetic mechanisms of rare earth elements within this residue were systematically elucidated. Analyses using scanning electron microscopy coupled with energy-dispersive spectroscopy (SEM–EDS) and aberration-corrected scanning transmission electron microscopy (STEM) reveal that rare earth elements are hosted in residual fluorapatite and newly formed CaF₂ through isomorphic substitution. The substitution of REE³⁺ for Ca²⁺ induces lattice contraction in CaF₂, with the interplanar spacing decreasing from 0.27 nm to 0.26 nm. Through single-factor experiments and response surface methodology (RSM) optimization, the optimal leaching conditions were determined to be a temperature of 80 °C, a leaching time of 120 min, a hydrochloric acid dosage of 160% of the theoretical requirement, a solid–liquid ratio of 1:6, and a agitation speed of 500 r·min⁻¹. Under these conditions, the leaching efficiency of rare earth elements reached as high as 92.69%. Kinetic analysis indicates that the leaching process follows the shrinking-core model, with the rate controlled by diffusion through the solid product layer. The apparent activation energy was calculated to be 37.2 kJ·mol⁻¹, characteristic of a diffusion-controlled process. Furthermore, response surface analysis of variance confirms that leaching temperature and time are the most significant factors influencing rare earth leaching. This study elucidates, from multiple perspectives, the leaching mechanism of rare earth elements from enriched residues within a hydrochloric acid system, thereby providing important theoretical support for the efficient recovery and process optimization of rare earth resources from associated phosphate ores. Full article

(This article belongs to the Special Issue Recent Advances in Separation Techniques for Critical Minerals/Metals, Circular Economy, and Sustainability)

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21 pages, 6646 KB

Open AccessArticle

Whole-Rock Element Analyses Constraining the Magmatic Evolution and Metallogenesis of the Jiaojia Fault Zone, Jiaodong Gold Province

by Jiabao Jia, Yueliang Hu, Lin Gao, Yulu Lv, Junjie Wang, Xiaomei Yang, Yan Liu, Xiaoliang Shi, Jing Lv, Yanbo Xu, Mengmeng Zhang and Wu Li

Minerals 2026, 16(4), 350; https://doi.org/10.3390/min16040350 - 26 Mar 2026

The Jiaodong Peninsula constitutes a world-class gold province in eastern China, containing more than 5000 t of identified gold resources. The Jiaojia gold deposit is one of the largest deposits within this gold province, and mineralization is primarily distributed along the northern segment [...] Read more.

The Jiaodong Peninsula constitutes a world-class gold province in eastern China, containing more than 5000 t of identified gold resources. The Jiaojia gold deposit is one of the largest deposits within this gold province, and mineralization is primarily distributed along the northern segment of the Jiaojia Fault. The structural characteristics and mineralization processes of the northern segment have been extensively documented. In contrast, the ore-forming mechanisms of the southern Jiaojia Fault remain poorly constrained, hindering further exploration targeting. We chose several gold deposits and one drill core along the Jiaojia Fault, then present whole-rock major and trace elements data to evaluate magmatic affinities and their ore-forming potential. The results show that the lithological differences in plutonic and stratigraphic units suggest that variations in petrogenesis may have exerted a fundamental control on mineralization styles. Almost all samples are characterized by enrichment in light rare earth elements, relative enrichment in Europium, and pronounced depletion in heavy rare earth elements. Alteration characteristics indicate the northern segment is dominated by advanced argillic alteration, whereas phyllic alteration is more prevalent in the southern segment. The rare earth elements discrimination plot clearly suggests differentiation from the northern and southern fault segments. Consequently, we propose that the northern segment records synorogenic arc magmatism, while the southern segment experienced both synorogenic and a subsequent intraplate extensional transitional stage. Full article

(This article belongs to the Special Issue Gold–Polymetallic Deposits in Convergent Margins)

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16 pages, 1903 KB

Open AccessArticle

Age of the Early Cretaceous Longjiang Formation in the Central Great Xing’an Range, Discovery of Its Basal Unconformity, and Implications for Tectonic Transition

by Jiameng Fan, Tao Qin, Jide Shu, Bo Zhao, Zhi Li and Jiucheng Yang

Minerals 2026, 16(4), 349; https://doi.org/10.3390/min16040349 - 26 Mar 2026

The geochronological framework of the Late Mesozoic volcanic succession in the Great Xing’an Range is crucial for understanding the tectonic regime transition in Northeast Asia. However, the ages and stratigraphic relationships of key volcanic units remain poorly constrained. This study presents zircon LA-ICP-MS [...] Read more.

The geochronological framework of the Late Mesozoic volcanic succession in the Great Xing’an Range is crucial for understanding the tectonic regime transition in Northeast Asia. However, the ages and stratigraphic relationships of key volcanic units remain poorly constrained. This study presents zircon LA-ICP-MS U–Pb geochronological data from volcanic rocks above and below the basal unconformity of the Longjiang Formation in the Zhalantun–Jalaid Banner area, central Great Xing’an Range, aiming to determine the timing of volcanic activity, constrain the formation age of the unconformity, and explore its regional tectonic implications. The volcanic–stratigraphic succession in the study area, from base to top, comprises the Baiyingaolao Formation, the basal andesitic conglomerate of the Longjiang Formation, and the Longjiang Formation andesites. Geochronological results indicate that the underlying rhyolitic tuff of the Baiyingaolao Formation yields an age of 130.0 ± 0.1 Ma. Within the andesitic conglomerate overlying the unconformity, andesitic clasts yield an age of 135.8 ± 1.1 Ma, whereas the matrix provides a youngest detrital zircon population age of 130.7 ± 1.0 Ma, constraining the maximum depositional age of the conglomerate. The overlying andesite of the Longjiang Formation gives an eruption age of 125.6 ± 0.8 Ma. These data indicate that the main phase of Longjiang Formation volcanism occurred at ~125.6 Ma, and the basal conglomerate was deposited after ~130.7 Ma. Combined with the ~130 Ma age of the underlying Baiyingaolao Formation and the presence of weathering crusts and erosional surfaces between the two formations, the sedimentary hiatus and exhumation event represented by this unconformity are precisely constrained to have occurred between ~130 Ma and 125.6 Ma. The timing of this unconformity closely coincides with the regional transition in magmatic assemblages from bimodal to andesitic compositions, suggesting that it records a significant tectonic adjustment event in the Great Xing’an Range during the middle to late Early Cretaceous. This finding provides key chronological evidence for understanding the episodic tectonic evolution of Northeast Asia during the Late Mesozoic. Full article

(This article belongs to the Section Mineral Geochemistry and Geochronology)

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23 pages, 9051 KB

Open AccessArticle

New Contributions to Mineralogical and Geochemical Knowledge of Old Preguiça Mine, Beja, Portugal

by Teresa P. Silva, Igor Morais, Sofia Soares, Ivo Rodrigues, Daniel P. S. de Oliveira and José Mirão

Minerals 2026, 16(4), 348; https://doi.org/10.3390/min16040348 - 26 Mar 2026

Abandoned mining areas provide valuable opportunities to investigate ore-forming processes, supergene mineral transformations, and the geochemical behaviour of metals. In this sense, the old Preguiça mine (Beja, Portugal), exploited for Fe–Zn–Pb, was studied providing new mineralogical and geochemical data aimed at improving the [...] Read more.

Abandoned mining areas provide valuable opportunities to investigate ore-forming processes, supergene mineral transformations, and the geochemical behaviour of metals. In this sense, the old Preguiça mine (Beja, Portugal), exploited for Fe–Zn–Pb, was studied providing new mineralogical and geochemical data aimed at improving the understanding of the secondary mineral assemblages of this deposit. A total of 70 samples collected from three accessible underground levels (first, second and third) and mine waste, complemented by 16 samples from a deeper level (fourth) previously collected, were analysed using X-ray diffraction (XRD), scanning electron microscopy (SEM), and a portable X-ray fluorescence (pXRF) equipment. Mineralogical phases are dominated by a wide range of secondary oxides, carbonates, arsenates, vanadates, silicates, phosphates and sulphates, but remnants of primary sulphides were also found. The following minerals can be emphasised: goethite, hematite, calcite, dolomite, descloizite, willemite, mimetite, cerussite, smithsonite and fraipontite. The presence of massicot in the Preguiça mine, is described for the first time. Bulk geochemical analyses show high concentrations of Fe, Ca, Zn and Pb, consistent with the observed mineralogy. The presence of vanadium- and arsenic-bearing minerals highlights the occurrence of critical raw materials, supporting the importance of reassessing other abandoned mining areas in the context of sustainable resource management and strategic raw-material planning. Full article

(This article belongs to the Special Issue Mineralogical and Geochemical Characterization of Geological Materials, 2nd Edition)

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4 pages, 152 KB

Open AccessEditorial

Editorial for Special Issue “From Clay Minerals to Ceramics: Progress and Challenges”

by Maite Garcia-Valles and Pura Alfonso

Minerals 2026, 16(4), 347; https://doi.org/10.3390/min16040347 - 26 Mar 2026

Clay has been used in the manufacture of pottery since ancient times [...] Full article

(This article belongs to the Special Issue From Clay Minerals to Ceramics: Progress and Challenges)

14 pages, 2506 KB

Open AccessArticle

Trace Elements and REEs of the Late Cretaceous Halite from Thakhek Basin, Laos and Its Paleoenvironmental Implication

by Jinyang Sha, Huijing Yin, Xize Zeng and Hua Zhang

Minerals 2026, 16(4), 346; https://doi.org/10.3390/min16040346 - 26 Mar 2026

Rare earth elements (REEs) play a critical role in provenance tracing and the environmental reconstruction of the Earth. However, systematic investigations into the geochemical behavior and fractionation mechanisms of REEs during halite crystallization in brine–salt systems remain limited. This study reports new trace [...] Read more.

Rare earth elements (REEs) play a critical role in provenance tracing and the environmental reconstruction of the Earth. However, systematic investigations into the geochemical behavior and fractionation mechanisms of REEs during halite crystallization in brine–salt systems remain limited. This study reports new trace element and REE data for Late Cretaceous halites from the Thakhek Basin, Laos. Ratios of Sr/Ba, Sr/Cu, and V/Cr indicate a marine origin for the halites, which formed under hot climatic and oscillating oxidizing–anoxic redox conditions. Both primary and secondary halites display uniform Post-Archean Australian Shale (PAAS)-normalized REE distribution patterns, characterized by relative enrichment in medium rare earth elements (MREE) and depletion in light (LREE) and heavy rare earth elements (HREE). Similar REE patterns are also observed in halites from other modern and ancient, continental and marine salt basins worldwide. These observations suggest that the influences of parent brine composition and external provenance supplies on REE fractionation are negligible, given the consistent source, salinity, and redox conditions recorded in these halites. Accordingly, REE fractionation in halite was largely controlled by crystallographic effects, with aqueous MREE preferentially incorporated into halite crystals during deposition. In addition, the relatively lower Zr/Hf ratios in secondary halites compared to primary halites further validate the utility of the Zr/Hf ratio for distinguishing authigenic halite from salt modified by diagenesis, weathering, dissolution, or recrystallization. While our results establish a fundamental REE distribution pattern for halite, further research is needed to better constrain the underlying fractionation mechanisms of REEs in evaporite minerals within brine–salt systems. Full article

(This article belongs to the Section Environmental Mineralogy and Biogeochemistry)

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32 pages, 12683 KB

Open AccessArticle

Model-Space Processing and Inversion of Magnetotelluric Data: A Multi-Model Jackknife Method

by Shaoting Feng, Dikun Yang and Lian Liu

Minerals 2026, 16(4), 345; https://doi.org/10.3390/min16040345 (registering DOI) - 25 Mar 2026

Magnetotelluric (MT) inversion models are widely used to interpret crustal conductivity structures related to fluid pathways, deformation zones, and mineralization processes; however, evaluating the reliability of inversion-derived anomalies remains challenging when datasets contain subtle station-dependent distortions or residual cultural noise. We present a [...] Read more.

Magnetotelluric (MT) inversion models are widely used to interpret crustal conductivity structures related to fluid pathways, deformation zones, and mineralization processes; however, evaluating the reliability of inversion-derived anomalies remains challenging when datasets contain subtle station-dependent distortions or residual cultural noise. We present a jackknife-inspired, model-space diagnostic framework based on leave-one-station-out (LOSO) inversion to quantify station influence and improve interpretation reliability. The workflow consists of (1) generating a LOSO inversion ensemble using identical inversion settings, (2) computing ensemble statistics and standardized perturbation metrics to identify sensitive zones, and (3) applying distribution-based diagnostics to classify station influence and guide construction of an ensemble-refined model. Synthetic experiments demonstrate that the framework distinguishes localized station-controlled artifacts from broadly supported structural responses, allowing targeted correction without altering robust features. Application to a field MT dataset acquired in a noise-affected environment shows that a mid-crustal conductive structure remains stable across the LOSO ensemble, while some shallow anomalies exhibit strong station dependence. The resulting ensemble-refined model introduces only localized modifications, demonstrating that ensemble-based model-space diagnostics provide a practical and reproducible strategy for validating MT inversion results and improving confidence in exploration-oriented conductivity interpretations. Full article

(This article belongs to the Special Issue Advances in Magnetic and Electromagnetic Techniques for Mineral Exploration: Enhancing Resource Discovery, 2nd Edition)

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21 pages, 9466 KB

Open AccessArticle

Mineralogy and In Situ Sulfur Isotope Geochemistry of Pyrite: Implications for Ore-Forming Processes of the Moshan Gold Deposit, Jiaodong Peninsula, North China

by Faqiang Zhao, Zhimin Li, Tongliang Tian, Peng Guo, Bin Li, Huaidong Luo, Yongliang Qi, Jiepeng Tian and Pengpeng Zhang

Minerals 2026, 16(4), 344; https://doi.org/10.3390/min16040344 - 24 Mar 2026

The Jiaodong gold-mineralized area is one of the most significant gold districts in China. The newly discovered Moshan gold deposit is hosted in the Late Jurassic Queshan granite, previously considered a prospecting blind zone. In this study, pyrite from the Moshan gold deposit [...] Read more.

The Jiaodong gold-mineralized area is one of the most significant gold districts in China. The newly discovered Moshan gold deposit is hosted in the Late Jurassic Queshan granite, previously considered a prospecting blind zone. In this study, pyrite from the Moshan gold deposit is examined as the primary research subject. To elucidate the ore-forming processes and genetic mechanisms of this deposit, we conducted a comprehensive mineralogical and geochemical study on pyrite, the principal gold-bearing mineral. EPMA and LA-MC-ICP-MS analyses reveal that the pyrite is slightly sulfur-deficient (average S/Fe ratio of 1.976) and exhibits trace element variations (As, Co, and Ni) strongly correlated with distinct metallogenic stages. Gold occurs in various forms, including visible inclusion gold, fracture gold, and invisible nano-particulate gold (Au⁰). The in situ sulfur isotope δ³⁴S values range from 7.11‰ to 9.40‰ (average 8.00‰), displaying high homogeneity and a positive deviation from the troilite in the Canyon Diablo iron meteorite. By integrating pyrite S-Fe relationships, Co-Ni-As systematics, and sulfur isotope characteristics, the study indicates that the Moshan gold deposit originates from a magmatic-hydrothermal source. The ore-forming materials predominantly derive from Mesozoic granite-derived magmatic-hydrothermal fluids, with a minor contribution from crustal basement materials. The depth of mineralization is interpreted as mid-shallow. These findings not only highlight the metallogenic potential of the Queshan granite and clarify the genetic relationship between the Moshan gold deposit and other regional gold deposits but also provide a novel theoretical foundation and technical support for deep gold exploration in the Jiaodong region. Full article

(This article belongs to the Section Mineral Deposits)

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17 pages, 3121 KB

Open AccessArticle

Experimental Investigation of Spatial Particle Size Distribution and Segregation in Tailings Slurry for High-Goaf Backfilling

by Qinli Zhang, Chuanyi Cheng, Peng Zhang, Daolin Wang, Bin Liu and Qiusong Chen

Minerals 2026, 16(4), 343; https://doi.org/10.3390/min16040343 - 24 Mar 2026

Tailings backfilling (TB) is widely recognized as an environmentally friendly and engineering safe technique to enhance mining efficiency. However, the heterogeneous particle distribution in TB slurry, also-named the segregation phenomenon, can significantly affect the mechanical strength of the backfill, especially under high goaf [...] Read more.

Tailings backfilling (TB) is widely recognized as an environmentally friendly and engineering safe technique to enhance mining efficiency. However, the heterogeneous particle distribution in TB slurry, also-named the segregation phenomenon, can significantly affect the mechanical strength of the backfill, especially under high goaf conditions. Therefore, elucidating the spatial distribution characteristics of particles during high-goaf filling has become a crucial research focus for improving the mechanical behavior of tailings backfill. A systematic experimental investigation was conducted in this study, incorporating the similarity principle, to analyze the migration behavior of backfill slurry particles and to clarify how the different backfill heights influence the spatial distribution of fine, medium, and coarse particles. The results indicate a clear vertical variation in PSD. Based on statistical analysis of samples collected from different backfill height experiments, coarse particle content increased progressively from the upper to lower layers (median: 16.2%, 23.6%, and 25.0%), while medium-sized particles remained relatively stable (37.0%, 37.3%, 37.0%). Fine particles dominated overall but decreased with layers (45.6%, 38.8%, 38.3%). Coarse particles tended to settle downward due to gravitational forces, whereas fine particles migrated upward. The distribution of medium-sized particles remained largely homogeneous. Fine and coarse particles were subjected to opposing driving forces. Meanwhile, particles maintained an approximately symmetrical distribution in the horizontal direction. Moreover, when the backfill height exceeded 800 mm, a notable intensification of stratification occurred, indicating a strong height-dependent transition in segregation behavior. In contrast, in the horizontal direction, the PSD showed no clear dependence on backfill height. These findings provide new insights into the mechanisms of particle segregation within backfill materials, offering a theoretical foundation and experimental support for optimizing PSD within the backfill body and elucidating the collapse mechanisms of high goafs. Full article

(This article belongs to the Special Issue Advances in Mine Backfilling Technology and Materials, 2nd Edition)

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6 pages, 153 KB

Open AccessEditorial

Editorial for Special Issue “Clay Minerals: From Paleoclimatic and Paleoenvironmental Indicators to Industrial Raw Materials”

by Elisa Laita, Javier García-Rivas and Isabel Abad

Minerals 2026, 16(4), 342; https://doi.org/10.3390/min16040342 - 24 Mar 2026

Clays and clay minerals constitute important mineral resources from both scientific and industrial perspectives [...] Full article

(This article belongs to the Special Issue Clay Minerals: From Paleoclimatic and Paleoenvironmental Indicators to Industrial Raw Materials)

33 pages, 18189 KB

Open AccessArticle

Geochronology of the Magmatic Rocks in the Duobaoshan Porphyry Cu-Mo Deposit in the Great Xing’an Range: Implication for the Metallogenic Epochs and Related Geodynamics

by Baoshan Liu, Linlin Kou, Chunpeng Zhang, Renping Han, Wanbing Song and Ri Han

Minerals 2026, 16(4), 341; https://doi.org/10.3390/min16040341 - 24 Mar 2026

The Duobaoshan porphyry copper–molybdenum deposit is located in the Great Xing’an Range, eastern segment of the Xing-Meng orogenic belt. It is the largest porphyry Cu-Mo deposit in NE China. Based on the contact relations of intrusive rocks and the results of LA-ICP-MS zircon [...] Read more.

The Duobaoshan porphyry copper–molybdenum deposit is located in the Great Xing’an Range, eastern segment of the Xing-Meng orogenic belt. It is the largest porphyry Cu-Mo deposit in NE China. Based on the contact relations of intrusive rocks and the results of LA-ICP-MS zircon U-Pb ages, we found that there were five stages of magmatism in the mining area, including the Early Ordovician (478.1 ± 3.2 Ma) granodiorite, the Middle Ordovician (462.1 ± 3.3 Ma, 459.5 ± 2.3 Ma) granodiorite porphyry, the Late Triassic (226.3 ± 0.4 Ma) oligoclase granite, the Middle Jurassic (170.1 ± 5.6 Ma) andesitic porphyrite, and the Early Cretaceous (118.1 ± 6.6 Ma) diorite. The Early and Middle Ordovician granodiorite and granodiorite porphyry are the principal host rocks for the mineralization in the deposit. However, Cu-Mo mineralization was also observed within the Late Triassic oligoclase granite, indicating that there are two stages of Cu-Mo mineralization in the Duobaoshan deposit. Combined with the previously reported Late Triassic skarn Cu mineralization occurring in the Xiaoduobaoshan deposit, and the Early Jurassic skarn Cu mineralization in the Sankuanggou and Yubaoshan deposits, we conclude that there are four metallogenetic stages in the Duobaoshan ore-concentration area. Regionally, there are five stages of Cu-Mo mineralization occurring in the northern Great Xing’an Range, including the Ordovician, Late Triassic, Early Jurassic, Late Jurassic, and Early Cretaceous. After discussing the tectonic setting for the generation of these deposits, we propose that the Duobaoshan ore-concentration area was influenced by the subduction of the Paleo-Asian Ocean, Mongol-Okhotsk, and Paleo-Pacific Plates during the Phanerozoic. Full article

(This article belongs to the Special Issue Thermal History and Preservation Mechanisms of Porphyry-Cu Deposits: Evidence from Thermochronology, Mineral and Isotopic Geochemistry)

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17 pages, 11160 KB

Open AccessArticle

Mineralogical Characteristics and Leaching Behavior of Sandstone-Hosted Uranium Ore: Implications for In Situ Recovery in the Zhenyuan Deposit, SW Ordos Basin, China

by Chunru Hou, Shihai Chen, Ying Zhang, Zhengbang Liu, Xiansheng Xie, Jinxun Deng, Yuhan Zou and Wensheng Liao

Minerals 2026, 16(4), 340; https://doi.org/10.3390/min16040340 - 24 Mar 2026

The mineralogical composition, textural characteristics, and uranium occurrence of sandstone-hosted uranium ores significantly influence the leaching performance during in situ recovery. This study investigates ore samples from the Zhenyuan uranium deposit, China, utilizing SEM, EPMA, XRD, and XRF to characterize their texture and [...] Read more.

The mineralogical composition, textural characteristics, and uranium occurrence of sandstone-hosted uranium ores significantly influence the leaching performance during in situ recovery. This study investigates ore samples from the Zhenyuan uranium deposit, China, utilizing SEM, EPMA, XRD, and XRF to characterize their texture and mineralogy. Combined with thin-section leaching tests, batch stirring experiments, and pressurized column leaching experiments, the leaching behavior of pitchblende, associated gangue minerals, and the whole rocks were evaluated. The results indicate that: Uranium mainly occurs as nano-spherical and film-like pitchblende distributed along the edges of detrital grains and Ti-oxides. Minor uranium is incorporated into Ti-oxides and dolomite lattices via isomorphic substitution or adsorbed by chlorite. Under CO₂ + O₂ leaching conditions, pitchblende was almost completely dissolved, while U-bearing Ti-oxides experienced slight corrosion. Dolomite underwent partial dissolution, providing bicarbonate ions and improving rock permeability. Pyrite dissolution was limited during the early stage of leaching. The high dolomite content, low clay abundance, favorable pore structure, and easily leachable pitchblende suggest that the Zhenyuan deposit is well suited for CO₂ + O₂ in situ recovery. Increasing CO₂ pressure is recommended to enhance dolomite dissolution and improve uranium recovery efficiency. Full article

(This article belongs to the Section Mineral Processing and Extractive Metallurgy)

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