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Journal Description
Journal of Composites Science
Journal of Composites Science
is an international, peer-reviewed, open access journal on the science and technology of composites, published monthly online by MDPI.
- Open Access— free for readers, with article processing charges (APC) paid by authors or their institutions.
- High Visibility: indexed within Scopus, ESCI (Web of Science), Inspec, CAPlus / SciFinder, and other databases.
- Journal Rank: JCR - Q2 (Materials Science, Composites) / CiteScore - Q1 (Engineering (miscellaneous))
- Rapid Publication: manuscripts are peer-reviewed and a first decision is provided to authors approximately 16.2 days after submission; acceptance to publication is undertaken in 3.5 days (median values for papers published in this journal in the first half of 2025).
- Recognition of Reviewers: reviewers who provide timely, thorough peer-review reports receive vouchers entitling them to a discount on the APC of their next publication in any MDPI journal, in appreciation of the work done.
Impact Factor:
3.7 (2024);
5-Year Impact Factor:
3.9 (2024)
Latest Articles
A Unified Three-Dimensional Micromechanical Framework for Coupled Inelasticity and Damage Evolution in Diverse Composite Materials
J. Compos. Sci. 2025, 9(12), 677; https://doi.org/10.3390/jcs9120677 - 5 Dec 2025
Abstract
This study introduces a comprehensive three-dimensional micromechanical framework to capture the nonlinear mechanical behavior of diverse composite materials, including coupled elastic degradation, inelastic strain evolution, and phenomenological failure in their constituents. The primary objective is to integrate a generalized elastic degradation–inelasticity (EDI) model
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This study introduces a comprehensive three-dimensional micromechanical framework to capture the nonlinear mechanical behavior of diverse composite materials, including coupled elastic degradation, inelastic strain evolution, and phenomenological failure in their constituents. The primary objective is to integrate a generalized elastic degradation–inelasticity (EDI) model into the parametric high-fidelity generalized method of cells (PHFGMC) micromechanical approach, enabling accurate prediction of nonlinear responses and failure mechanisms in multi-phase composites. To achieve this, a unified three-dimensional orthotropic EDI modeling formulation is developed and implemented in the PHFGMC. Grounded in continuum mechanics, the EDI employs scalar field variables to quantify material damage and defines an energy potential function. Thermodynamic forces are specified along three principal directions, decomposed into tensile and compressive components, with shear failure accounted for across the respective planes. Inelastic strain evolution is modeled using incremental anisotropic plasticity theory, coupling damage and inelasticity to maintain generality and flexibility for diverse phase behaviors. The proposed model offers a general, unified framework for modeling damage and inelasticity, which can be calibrated to operate in either coupled or decoupled modes. The PHFGMC micromechanics framework then derives the overall (macroscopic) nonlinear and damage responses of the multi-phase composite. A failure criterion can be applied for ultimate strength evaluation, and a crack-band type theory can be used for post-ultimate degradation. The method is applicable to different types of composites, including polymer matrix composites (PMCs) and ceramic matrix composites (CMCs). Applications demonstrate predictions of monotonic and cyclic loading responses for PMCs and CMCs, incorporating inelasticity and coupled damage mechanisms (such as crack closure and tension–compression asymmetry). The proposed framework is validated through comparisons with experimental and numerical results from the literature.
Full article
(This article belongs to the Topic Numerical Simulation of Composite Material Performance)
Open AccessArticle
Quasi-Static Axial Crushing Behaviour of Rectangular Foam-Filled CFRP-Aluminium Hybrid Composite Tubes
by
Tabrej Khan, Harri Junaedi and Tamer A. Sebaey
J. Compos. Sci. 2025, 9(12), 676; https://doi.org/10.3390/jcs9120676 - 5 Dec 2025
Abstract
This study investigates the quasi-static axial crushing behaviour of carbon fibre-reinforced polymer (CFRP) tubes with variations incorporating polyurethane foam (PU) and aluminium tubes. Six different composite configurations were fabricated, including a baseline hollow CFRP tube and hybrid structures with foam and aluminium reinforcements.
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This study investigates the quasi-static axial crushing behaviour of carbon fibre-reinforced polymer (CFRP) tubes with variations incorporating polyurethane foam (PU) and aluminium tubes. Six different composite configurations were fabricated, including a baseline hollow CFRP tube and hybrid structures with foam and aluminium reinforcements. The mechanical response was evaluated through load–displacement behaviour and energy absorption. Visual inspection of the failure modes revealed distinct fracture mechanisms influenced by the type of reinforcement. The results indicate that incorporating aluminium significantly enhances load-bearing capacity, energy absorption, and crushing efficiency, with the sample containing four aluminium secondary tubes exhibiting the highest specific energy absorption. Meanwhile, foam-filled samples improved load-bearing capacity while mitigating brittle failure. These findings suggest that CFRP hybrid structures with aluminium and foam reinforcements offer promising solutions for lightweight Crashworthiness applications in the automotive and aerospace industries.
Full article
(This article belongs to the Section Carbon Composites)
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Open AccessArticle
Highly Effective Injection Composites with Fly Ash and Microsilica for Soil Stabilization
by
Yasin Onuralp Özkılıç, Alexey N. Beskopylny, Ceyhun Aksoylu, Sergey A. Stel’makh, Evgenii M. Shcherban’, Emrah Madenci, Diana M. Shakhalieva, Andrei Chernil’nik and Alexey Kosykh
J. Compos. Sci. 2025, 9(12), 675; https://doi.org/10.3390/jcs9120675 - 4 Dec 2025
Abstract
Injection composites based on mineral binders are widely used for soil stabilization, using jet grouting technology to solve various geotechnical problems. Cement, which contains toxic components and worsens the ecology of the environment, is typically the main mineral component used to manufacture injection
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Injection composites based on mineral binders are widely used for soil stabilization, using jet grouting technology to solve various geotechnical problems. Cement, which contains toxic components and worsens the ecology of the environment, is typically the main mineral component used to manufacture injection composites. Reducing cement consumption in the production of building materials is currently of great importance. This study developed highly effective, environmentally friendly injection composites for soil stabilization based on three mineral components: Portland cement, fly ash (FA), and microsilica (MS). FA was introduced into the composites as a partial Portland cement substitute, in amounts ranging from 5 to 50% in 5% increments. The properties of fresh and hardened composites, including the density, flow rate, water separation, compressive strength at 7 and 28 days, and the structure and phase composition of the composites, were studied. The inclusion of FA in the composition of composites contributes to a decrease in density by 16.9%, from 1.89 g/cm3 to 1.57 g/cm3, and cone spread by 9%, from 30.1 cm to 27.4 cm, and an increase in water bleeding by 91.4%, from 3.5% to 6.7%, respectively. Based on the results of the experimental studies, the most effective dosage of FA was determined, which amounted to 20%. An increase in compressive strength was recorded for composites at the age of 7 days of 8.3%, from 33.6 MPa to 36.4 MPa, and for compressive strength at the age of 28 days of 9.4%, from 41.3 MPa to 45.2 MPa, respectively. SEM and XRD analysis results show that including FA and MS promotes the formation of additional calcium hydrosilicates (CSH) and the development of a compact and organized composite structure. The developed composites with FA contents of up to 50% exhibit the required properties and can be used for their intended purpose in real-world construction for soil stabilization.
Full article
(This article belongs to the Section Composites Applications)
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Open AccessArticle
Upcycling Oyster Shell Waste into Sustainable Polypropylene Biocomposites: Synthesis and Characterization
by
Zahira Benaichouba, Bel Abbes Bachir Bouiadjra, Mohamed Mokhtar Bouziane, Mokhtar Khaldi, Manoj Kumar Singh and Sathish Kumar Palaniappan
J. Compos. Sci. 2025, 9(12), 674; https://doi.org/10.3390/jcs9120674 - 4 Dec 2025
Abstract
There is a growing interest in the application of natural and waste-derived biofillers for reinforcing thermoplastic polymers, as their utilization helps to reduce the carbon footprint and therefore enhances sustainable development. The aim of this study is to synthesize and characterize a biocomposite
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There is a growing interest in the application of natural and waste-derived biofillers for reinforcing thermoplastic polymers, as their utilization helps to reduce the carbon footprint and therefore enhances sustainable development. The aim of this study is to synthesize and characterize a biocomposite based on PP reinforced with OS particles derived from biomass in order to reduce plastic shrinkage after injection molding and to assess their viability as environmentally sustainable materials. The addition of OS particles (10 wt.% and 30 wt.%) significantly reduces the crystallinity of the PP, thereby improving its rigidity, its tensile strength, and its thermal stability. DSC analysis and TGA validated superior thermal properties, whereas mechanical and dynamic mechanical assessments indicated augmented stiffness and energy storage capacity with increasing filler content. The utilization of OS waste, abundant in CaCO3, facilitates a circular economy model, minimizing environmental impact and enhancing waste valorization. The findings underscore the viability of PP/OS biocomposites as sustainable substitutes for traditional mineral-filled polymers in engineering applications.
Full article
(This article belongs to the Section Biocomposites)
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Open AccessArticle
Additive Manufacturing of Graphene Oxide/Sodium Alginate–Cotton Microfiber Composite Hydrogels: Structure, Properties, and Adsorption Performance
by
Nickolly B. V. Serafim, Caroline M. B. de Araujo, Margarida S. C. A. Brito, Yaidelin A. Manrique, Cláudia G. Silva, Marcos G. Ghislandi, Jose L. Sanchez-Salvador, Angeles Blanco, Jorge V. F. L. Cavalcanti, Maurício A. da Motta Sobrinho and Alexandre F. P. Ferreira
J. Compos. Sci. 2025, 9(12), 673; https://doi.org/10.3390/jcs9120673 - 4 Dec 2025
Abstract
The high use and improper disposal of chloroquine (CQ) during the COVID-19 pandemic have significantly increased its presence in water bodies, representing an environmental risk. Adsorption is one of the most-used treatments to remove recalcitrant compounds, although there is still a lack of
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The high use and improper disposal of chloroquine (CQ) during the COVID-19 pandemic have significantly increased its presence in water bodies, representing an environmental risk. Adsorption is one of the most-used treatments to remove recalcitrant compounds, although there is still a lack of efficient biosorbents. This work aimed to develop an efficient biosorbent using additive manufacturing (AM) to synthesize bionanocomposite hydrogels based on cellulose fibers, sodium alginate (SA), and graphene oxide (GO) for CQ adsorption. The hydrogels were characterized by mechanical, morphological, and physicochemical techniques. Results show that increasing GO content and reducing water contributed to higher yield stress, which is important for maintaining shape fidelity during the printing. SEM images evidenced thin GO layers interacting with the polymer matrix and cellulose fibers, resulting in 3D disordered porous microstructures. The adsorption capacity of the 3D-printed hydrogel samples for aqueous CQ was analyzed by evaluating the pH effect, contact time, and the adsorption equilibrium isotherms, showing notorious potential for CQ removal, with maximum adsorption capacity of ~25 mg∙g−1 at 25 °C. Results show that the tested formulations were stable for producing hydrogels and efficient on chloroquine adsorption, revealing their potential as novel adsorbents for removing emerging organic pollutants from water.
Full article
(This article belongs to the Special Issue Advanced Composite Materials: Design, Implementation and Characterization)
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Open AccessArticle
A Unified Framework for Free Vibration Analysis of Variable-Angle Tow Composite Shells with Spatially Varying Curvature
by
Domenico Andrea Iannotta, Gaetano Giunta and Marco Montemurro
J. Compos. Sci. 2025, 9(12), 672; https://doi.org/10.3390/jcs9120672 - 4 Dec 2025
Abstract
The combination of variable-angle tow composites with shell geometries presents significant potential in various engineering and technical applications, particularly with regard to structural performance. Nevertheless, the numerical modeling of these structures can be challenging, as the larger number of unknowns significantly increases computational
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The combination of variable-angle tow composites with shell geometries presents significant potential in various engineering and technical applications, particularly with regard to structural performance. Nevertheless, the numerical modeling of these structures can be challenging, as the larger number of unknowns significantly increases computational effort. The Carrera’s unified formulation has demonstrated promising results in the analysis of plates and shells reinforced with curvilinear fibers, offering an effective balance between numerical accuracy and the number of variables. This paper extends the unified formulation to more complex variable-angle tow shell structures characterized by variable curvature radii within their physical domain. The governing equations of the dynamic problem are derived using a displacement-based variational method, and the results are validated through comparisons with reference solutions from Abaqus 3D models. The First-Order Shear Deformation Theory (FSDT) is presented for a broader comparison of the proposed models. The maximum percentage error in terms of frequency shift observed for the FSDT model is , whereas the corresponding error for the most refined model is only . Across all examined cases, the computed fundamental frequencies and mode shapes closely match the reference results, demonstrating the reliability and effectiveness of the proposed method.
Full article
(This article belongs to the Special Issue Feature Papers in Journal of Composites Science in 2025)
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Open AccessArticle
Early Hydration Behaviours and Kinetics of Portland Cement Composites Incorporating Low-Calcium Circulating Fluidized Bed Fly Ash
by
Chun-Ran Wu, Zhen-Po Xiao, Jing-Jie Wei, Shi-Cong Kou and Meng-Xiong Tang
J. Compos. Sci. 2025, 9(12), 671; https://doi.org/10.3390/jcs9120671 - 4 Dec 2025
Abstract
Low-calcium circulating fluidized bed fly ash (LCFA) exhibits obvious potential as a supplementary cementitious material (SCM) due to its minimal impact on concrete volume stability. However, its early hydration behavior remains unclear. This study investigates the hydration characteristics of cementitious composites incorporating varying
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Low-calcium circulating fluidized bed fly ash (LCFA) exhibits obvious potential as a supplementary cementitious material (SCM) due to its minimal impact on concrete volume stability. However, its early hydration behavior remains unclear. This study investigates the hydration characteristics of cementitious composites incorporating varying LCFA dosages. Setting time, hydration heat, pore solution ion concentrations (Ca2+ and SO42−), and XRD analysis were employed. Hydration kinetics were described using the Krstulovic–Dabic model, with corresponding kinetic parameters calculated. The results demonstrate that LCFA inhibits the formation of calcium hydroxide (CH) and C-S-H precipitation while delaying sulfate depletion. Consequently, LCFA incorporation significantly extends both initial and final setting times. Hydration kinetics were effectively described by the Krstulovic–Dabic model, identifying three distinct stages of nucleation and crystal growth (NG), interactions at phase boundaries (I), and diffusion (D). Increasing the LCFA dosage reduced the rate constant for the NG process (KNG′) but increased the rate constants processes of I (KI′) and D (KD′). Furthermore, LCFA increased transition points of NG → I (α1) and I → D (α2).
Full article
(This article belongs to the Special Issue High-Performance Composite Materials in Construction)
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Open AccessArticle
Facile Synthesis of Cellulose Whisker from Cotton Linter as Filler for the Polymer Electrolyte Membrane (PEM) of Fuel Cells
by
Ronaldo P. Parreño, Jr., Reynaldo A. Badua, Jr., Jowin L. Rama and Apollo Victor O. Bawagan
J. Compos. Sci. 2025, 9(12), 670; https://doi.org/10.3390/jcs9120670 - 3 Dec 2025
Abstract
Hybrid membranes are promising alternatives for various applications, combining a continuous polymer phase with a dispersed filler phase to achieve synergistic functional benefits. The ideal fillers should possess well-defined structures and unique properties for multi-functionality, as well as being sourced from renewable, biodegradable
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Hybrid membranes are promising alternatives for various applications, combining a continuous polymer phase with a dispersed filler phase to achieve synergistic functional benefits. The ideal fillers should possess well-defined structures and unique properties for multi-functionality, as well as being sourced from renewable, biodegradable materials for sustainability purposes. This study explored the potential of using cellulose-based renewable materials as fillers for hybrid polymer electrolyte membranes (PEMs) in fuel cells. Cellulose whiskers (CWs), known for their high crystallinity and elastic modulus, were effectively synthesized via optimized sequential alkali treatment and acid hydrolysis. Subsequent functionalization with citric acid was performed to enhance their reinforcing properties and overall performance. Initial characterization using ATR-FTIR and XRD confirmed the CWs’ structural composition, high crystallinity, and the presence of reactive groups (sulfate and hydroxyl). The functionalization process introduced new carbonyl groups (C=O), which was verified by ATR-FTIR, while maintaining high hydrophilicity. Morphological analysis revealed that the crosslinked CWs created a denser and more compact microstructure within the membrane, leading to a significant enhancement in mechanical strength. The modifications to the cellulose whiskers not only improved structural integrity but also boosted the membrane’s ion exchange capacity (IEC) and proton conductivity compared to membranes with unmodified CWs. Initial experiments demonstrated CWs’ compatibility as a filler in a polysulfone (PSU) matrix, forming hybrid membranes suitable for fuel cell applications.
Full article
(This article belongs to the Section Polymer Composites)
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Open AccessArticle
Observations from Processing Thick Continuous Fiber Polyphenylene Sulfide (PPS) Laminates with and Without Carbon Black
by
Benjamin N. Dwyer, David F. Erb, Jr., William B. Yori, Danny H. Pham, Scott M. Nelson, Quest O. Teichman, Jonathan R. Roy, Robert J. Hart and Andrew Q. Smail
J. Compos. Sci. 2025, 9(12), 669; https://doi.org/10.3390/jcs9120669 - 3 Dec 2025
Abstract
During the manufacturing and development of a proof-of-concept prototype of a continuous fiber polyphenylene sulfide (PPS) composite vehicle component, unexpected results were observed in thick laminates of an E-glass-fiber-reinforced PPS matrix, which utilized carbon black as a colorant (GF/PPS+CB). Extensive interlaminar macrocracking, transverse
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During the manufacturing and development of a proof-of-concept prototype of a continuous fiber polyphenylene sulfide (PPS) composite vehicle component, unexpected results were observed in thick laminates of an E-glass-fiber-reinforced PPS matrix, which utilized carbon black as a colorant (GF/PPS+CB). Extensive interlaminar macrocracking, transverse intralaminar microcracking, and micro-/macrovoids were observed in GF/PPS+CB laminates after compression forming. When processed under identical conditions, no micro-/macrocracking or voids were present in GF/PPS laminates and carbon fiber/PPS laminates without carbon black colorant. These observations prompted further investigation into the influence of processing conditions, presence of colorant, mold design (open and closed molds), and geometry (flat and curved) on the development of matrix defects in thick continuous fiber-reinforced PPS laminates.
Full article
(This article belongs to the Special Issue Advances in Continuous Fiber Reinforced Thermoplastic Composites)
Open AccessArticle
Evaluation of Sasa kurilensis Biomass-Derived Hard Carbon as a Promising Anode Material for Sodium-Ion Batteries
by
Polina A. Marmaza, Oleg O. Shichalin, Zlata E. Priimak, Alina I. Seroshtan, Nikita P. Ivanov, Grigory P. Lakienko, Alexei S. Korenevskiy, Sergey A. Syubaev, Vitaly Yu. Mayorov, Maria A. Ushkova, Eduard A. Tokar, Roman I. Korneikov, Vadim V. Efremov, Alexy V. Ognev, Eugeniy K. Papynov and Ivan G. Tananaev
J. Compos. Sci. 2025, 9(12), 668; https://doi.org/10.3390/jcs9120668 - 3 Dec 2025
Abstract
The depletion of global lithium reserves, coupled with the necessity for environmentally sustainable and economically accessible energy storage systems, has driven the development of sodium-ion batteries (SIBs) as a promising alternative to lithium-ion technologies. Among various anode materials for SIBs, hard carbon exhibits
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The depletion of global lithium reserves, coupled with the necessity for environmentally sustainable and economically accessible energy storage systems, has driven the development of sodium-ion batteries (SIBs) as a promising alternative to lithium-ion technologies. Among various anode materials for SIBs, hard carbon exhibits obvious advantages and significant commercial potential owing to its high energy density, low operating potential, and stable capacity retention during prolonged cycling. Biomass represents the most attractive source of non-graphitizable carbon from a practical standpoint, being readily available, renewable, and low-cost. However, the complex internal structure of biomass precursors creates significant challenges for precise control of microstructure and properties of the resulting hard carbon materials, requiring further research and optimization of synthesis methodologies. This work reports the synthesis of hard carbon from Sasa kurilensis via pyrolysis at 900 °C and investigates the effect of alkaline pretreatment on the structural and electrochemical characteristics of the anode material for SIBs. Sasa kurilensis is employed for the first time as a source for non-graphitizable carbon synthesis, whose unique natural vascular structure forms optimal hierarchical porosity for sodium-ion intercalation upon thermal treatment. The materials were characterized by X-ray diffraction, infrared and Raman spectroscopy, scanning electron microscopy, X-ray microtomography and low-temperature nitrogen adsorption–desorption. Electrochemical properties were evaluated by galvanostatic cycling in the potential range of 0.02–2 V at a current density of 25 mAhg−1 in half-cells with sodium metal counter electrodes. The unmodified sample demonstrated a discharge capacity of 160 mAhg−1 by the 6th cycle, with an initial capacity of 77 mAhg−1. The alkaline-treated material exhibited lower discharge capacity (114 mAhg−1) and initial Coulombic efficiency (40%) due to increased specific surface area, leading to excessive electrolyte decomposition.
Full article
(This article belongs to the Special Issue Composite Materials for Energy Management, Storage or Transportation)
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Open AccessReview
Advances in the Stabilization of Eutectic Salts as Phase Change Materials (PCMs) for Enhanced Thermal Performance: A Critical Review
by
Elmer Marcial Cervantes Ramírez, Danna Trejo Arroyo, Julio César Cruz Argüello, Blandy Berenice Pamplona Solís and Javier Rodrigo Nahuat Sansores
J. Compos. Sci. 2025, 9(12), 667; https://doi.org/10.3390/jcs9120667 - 3 Dec 2025
Abstract
Inorganic phase change materials (PCMs) can be employed in passive thermal regulation systems as building envelopes to decrease energy consumption. Nonetheless, they present a manifold of issues, such as leakage, incongruent melting, crystallization, and supercooling, which limit their performance and durability. A widely
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Inorganic phase change materials (PCMs) can be employed in passive thermal regulation systems as building envelopes to decrease energy consumption. Nonetheless, they present a manifold of issues, such as leakage, incongruent melting, crystallization, and supercooling, which limit their performance and durability. A widely explored approach to address these shortcomings is the development of eutectic salts and their stabilization through techniques such as the use of porous substrates and encapsulation, in addition to combining them with the incorporation of carbon derivatives as fillers and nucleating agents to enhance thermal performance and durability during charge and discharge cycles. In this study, a critical review is developed via analysis and discussions of different methods for incorporating inorganic PCMs. The focus is mainly on eutectic salts and the challenges associated with their application, the generation of new eutectic salts, stabilization methods, and use cases where the incorporation of fillers, the use of porous substrates, and the implementation of nucleating agents have contributed to improving thermal performance, reducing the degree of supercooling, and minimizing PCM leakage during phase transitions.
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(This article belongs to the Section Composites Applications)
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Open AccessArticle
Preparation and Characterization of Polyethylene-Based Composites with Iron-Manganese “Core-Shell” Nanoparticles
by
Gleb Yu. Yurkov, Alexander V. Kozinkin, Anna V. Maksimova, Valeriy G. Vlasenko, Stanislav P. Kubrin, Vladislav E. Kirillov and Vitaliy I. Solodilov
J. Compos. Sci. 2025, 9(12), 666; https://doi.org/10.3390/jcs9120666 - 3 Dec 2025
Abstract
Composite materials based on low-density polyethylene (LDPE) embedded with iron-manganese nanoparticles with compositions Fe0.9Mn0.1 and Fe0.8Mn0.2 were prepared and investigated. The newly created composites were characterized using transmission electron microscopy (TEM), X-ray diffraction (XRD), X-ray absorption near-edge
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Composite materials based on low-density polyethylene (LDPE) embedded with iron-manganese nanoparticles with compositions Fe0.9Mn0.1 and Fe0.8Mn0.2 were prepared and investigated. The newly created composites were characterized using transmission electron microscopy (TEM), X-ray diffraction (XRD), X-ray absorption near-edge structure (XANES), extended X-ray absorption fine structure (EXAFS), and Mössbauer spectroscopy. The composition, electronic, and atomic structure of the nanoparticles were established. The study confirms that the nanoparticles possess a ‘core-shell’ structure, the nature of which depends on the manganese content. The nanoparticles of Fe0.8Mn0.2 in LDPE exhibit a three-layered structure: a metallic α-Fe core is coated with an intermediate oxidized layer structurally close to Fe2O3, while the outermost shell consists of manganese oxide (Mn2O3). In contrast, nanoparticles with lower Mn content Fe0.9Mn0.1 show a predominantly fully oxidized structure. This structural evolution is consistent with thermodynamic principles, where manganese, having a higher oxide formation enthalpy, migrates to the surface. The core–shell architecture is promising for applications requiring stable magnetic components or tailored catalytic interfaces within a polymer matrix.
Full article
(This article belongs to the Special Issue Advanced Composite Materials: Design, Implementation and Characterization)
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Open AccessArticle
Defect Visualization in the Bridge Underpass Arch Structure: A Photogrammetry Assessment Using UAV-Captured Imagery
by
Muhammad Ali Musarat, Carl James Debono, Vijay Prakash, Ruben Paul Borg, Dylan Seychell, Gabriel Hili, Jiangpeng Shu and Wei Ding
J. Compos. Sci. 2025, 9(12), 665; https://doi.org/10.3390/jcs9120665 - 2 Dec 2025
Abstract
Concrete structures develop several defects as the structure ages. One of the common concerns in structural integrity is the formation of cracks, which demands regular inspection with precision. In this study, a bridge underpass arch structure was inspected with the help of an
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Concrete structures develop several defects as the structure ages. One of the common concerns in structural integrity is the formation of cracks, which demands regular inspection with precision. In this study, a bridge underpass arch structure was inspected with the help of an Unmanned Aerial Vehicle (UAV) in a coastal region of the Mediterranean Sea, where 2D captured images were transferred into a 3D model for better visualisation from a Structural Health Monitoring (SHM) perspective. The images with cracks were manually annotated, using the VGG tool, by an expert. Using the 3DF Zephyr software, from sparse to dense point clouds, and 3D mesh to orthophoto, all 3D models were constructed from the annotated and unannotated images of the structure. The 3D model achieved a Ground Sampling Distance of 0.0046 m/pixel, with an image alignment of 60%. The Bundle Adjustment Mean Reprojection Error confirmed satisfactory internal model accuracy. The final assessment through the orthophoto, where a resolution of 4531 × 2433 pixels was achieved, revealed that the images were of sufficient quality to capture the details and the defects present, and better visualisation could be made. This output demonstrates that UAV-based photogrammetry is time- and cost-efficient and surpasses the traditional visual inspection of confined structures.
Full article
(This article belongs to the Special Issue Structural Design, Health Monitoring and Performance Evaluation of Composite Materials)
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Open AccessArticle
Effect of High Carbon Nanotube Content on Electromagnetic Shielding and Mechanical Properties of Cementitious Mortars
by
Ivan Vrdoljak, Ivana Miličević, Oliver Romić and Robert Bušić
J. Compos. Sci. 2025, 9(12), 664; https://doi.org/10.3390/jcs9120664 - 2 Dec 2025
Abstract
The increasing exposure to non-ionizing electromagnetic (EM) radiation driven by urbanization and digitalization has encouraged the development of building materials with EM shielding properties. This study investigates the potential of enhancing the electromagnetic shielding properties of cement mortars by incorporating multi-walled carbon nanotubes
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The increasing exposure to non-ionizing electromagnetic (EM) radiation driven by urbanization and digitalization has encouraged the development of building materials with EM shielding properties. This study investigates the potential of enhancing the electromagnetic shielding properties of cement mortars by incorporating multi-walled carbon nanotubes (MWCNT) in various dosages (1%, 3%, 6%, 9% and 10% by binder mass). The microstructural and mechanical effects of MWCNT addition, as well as their efficiency in reducing EM transmission in the frequency range of 1.5–10 GHz (covering LTE, 5G, WiFi, and radar systems), were analyzed. S21 measurements were performed using a modified coaxial transmission line method with a vector network analyzer. Results show that increasing the MWCNT content enhances EM shielding effectiveness but simultaneously affects the mortar’s microstructure and mechanical properties. Higher MWCNT levels achieved the best EM shielding, with an improvement of up to 27.66 dB compared to ordinary mortar in the navigation radar frequency range. These findings confirm the potential of MWCNT-modified mortars for protecting buildings and sensitive infrastructure—such a hospitals, communication hubs, data centers and military facilities—from EM radiation.
Full article
(This article belongs to the Special Issue Novel Cement and Concrete Materials)
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Open AccessArticle
Bifunctionalized Microspheres via Pickering Emulsion Polymerization for Removal of Diclofenac from Aqueous Solution
by
Xiaoyi Gou, Zia Ahmad, Zaijin You and Zhou Ren
J. Compos. Sci. 2025, 9(12), 663; https://doi.org/10.3390/jcs9120663 - 2 Dec 2025
Abstract
The removal of water pollutants with high selectivity and efficiency is still a huge challenge owing to the complex composition of contaminated water. The preparation, modification of Pickering emulsion microspheres, and their application in the adsorption and removal of non-steroidal anti-inflammatory drugs (diclofenac)
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The removal of water pollutants with high selectivity and efficiency is still a huge challenge owing to the complex composition of contaminated water. The preparation, modification of Pickering emulsion microspheres, and their application in the adsorption and removal of non-steroidal anti-inflammatory drugs (diclofenac) in water were studied. Poly(2-(diethylamino)ethyl methacrylate-divinylbenzene), (P(DEAEMA-DVB)) microspheres were prepared by Pickering emulsion polymerization. The P(DEAEMA-DVB) polymer was modified with glycidyl trimethylammonium chloride (GTAC) and phenyl glycidyl ether (PGE) to prepare the adsorbent poly(quaternized and phenyl-functionalized) (P(QP-DVB)) with a substantial quantity of quaternary ammonium functional groups. The non-steroidal anti-inflammatory drugs in aqueous solution was mainly adsorbed by the anion exchange interaction with quaternary ammonium species. The adsorption kinetics coincided with the pseudo-second-order kinetic model, and the adsorption isotherm conformed to the Langmuir isotherm model. The optimized P(QP-DVB) particles exhibited well-defined spherical morphology and a uniform particle size distribution ranging from 15 to 30 µm. Nitrogen adsorption/desorption characterization revealed a high specific surface area of 674 m2 g−1 and a pore size distribution from 2 to 25 nm. In addition, the aforementioned microsphere underwent chemical regeneration and exhibits good reusability, thereby reducing both the economic costs and environmental impacts.
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(This article belongs to the Section Composites Applications)
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Open AccessArticle
Rheological and Thermo-Mechanical Characterisation of Sustainable Polypropylene Composites Reinforced with Micronised Rice Husk
by
Inês Santos, Tatiana Zhiltsova, José Martinho Oliveira, Sara P. Magalhães da Silva and Mónica S. A. Oliveira
J. Compos. Sci. 2025, 9(12), 662; https://doi.org/10.3390/jcs9120662 - 2 Dec 2025
Abstract
The growing demand for sustainable materials in construction and sanitation has increased interest in natural fibre-reinforced polymer composites. Rice husk, an abundant agricultural by-product, offers a promising alternative as a reinforcing filler in polypropylene (PP) composites. This study aims to assess the suitability
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The growing demand for sustainable materials in construction and sanitation has increased interest in natural fibre-reinforced polymer composites. Rice husk, an abundant agricultural by-product, offers a promising alternative as a reinforcing filler in polypropylene (PP) composites. This study aims to assess the suitability of PP composites reinforced with micronised rice husk particles for application in sanitary components. Two formulations containing 20% and 30% rice husk were developed and characterised. Comprehensive analysis included morphological, thermal, rheological, mechanical, hygroscopic, and tribological testing. Results showed that particles incorporation enhanced thermal stability and crystallinity due to a nucleating effect, with the 30% composite showing higher crystallinity. Thermogravimetric analysis showed that although the T5% decreased from 374.1 °C for neat PP to 309.2 °C and 296.2 °C for the 20% and 30% composites, respectively, the DTG peak temperatures increased by 15.9 °C and 17.6 °C, indicating a delayed main decomposition stage of PP matrix and enhanced overall thermal stability. Rheological behaviour revealed increased viscosity and pseudoplasticity at higher particle content Mechanical characterisation showed an increase in Young’s modulus from 1021 MPa for neat PP to 1065 MPa (+4%) and 1125 MPa (+10%) for PP_Rice_20% and PP_Rice_30%, respectively. In contrast, the nominal strain at break dropped sharply from 238% (PP) to 30% (PP_Rice_20%) and 16% (PP_Rice_30%). Shrinkage decreased from 1.31% (PP) to approximately 1.05% in both composites, indicating improved dimensional stability. However, water absorption rose from 0.015% (PP) to 0.111% (PP_Rice_20%) and 0.144% (PP_Rice_30%), accompanied by an increase in surface roughness (Sa from 0.34 µm to 0.78 µm and 1.06 µm, respectively). The composite with 20% rice husk demonstrated better filler dispersion, reduced water uptake, and smoother surfaces, making it more suitable for injection-moulded components intended for use in humid environments. Overall, the study supports the use of agricultural residues in high-performance biocomposites, contributing to circular economy strategies and the development of more sustainable polymer-based materials for technical applications.
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(This article belongs to the Special Issue Mechanical Properties of Composite Materials and Joints)
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Open AccessArticle
Impact of Chemical Treatment on Banana-Fibre-Reinforced Carbon–Kevlar Hybrid Composites: Short-Beam Shear Strength, Vibrational, and Acoustic Properties
by
Kanchan B. M., Kulmani Mehar and Yogeesha Pai
J. Compos. Sci. 2025, 9(12), 661; https://doi.org/10.3390/jcs9120661 - 2 Dec 2025
Abstract
This study evaluates the effect of chemical treatments on the short-beam shear strength, vibrational, and acoustic performance of banana-fibre-reinforced carbon–Kevlar hybrid composites. Banana fibres were treated with 5% NaOH and 0.5% KMnO4 to improve fibre surface characteristics and interfacial bonding within a
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This study evaluates the effect of chemical treatments on the short-beam shear strength, vibrational, and acoustic performance of banana-fibre-reinforced carbon–Kevlar hybrid composites. Banana fibres were treated with 5% NaOH and 0.5% KMnO4 to improve fibre surface characteristics and interfacial bonding within a sandwich laminate of carbon–Kevlar intraply skins and banana fibre core fabricated by hand lay-up and compression moulding. Short-beam shear strength (SBSS) increased from 14.27 MPa in untreated composites to 17.65 MPa and 19.52 MPa with KMnO4 and NaOH treatments, respectively, due to enhanced fibrematrix adhesion and removal of surface impurities. Vibrational analysis showed untreated composites had low stiffness (7780.23 N/m) and damping ratio (0.00716), whereas NaOH treatment increased stiffness (9480.51 N/m) and natural frequency (28.68 Hz), improving rigidity and moderate damping. KMnO4 treatment yielded the highest damping ratio (0.0557) with reduced stiffness, favouring vibration energy dissipation. Acoustic tests revealed KMnO4-treated composites have superior sound transmission loss across low to middle frequencies, peaking at 15.6 dB at 63 Hz, indicating effective acoustic insulation linked to better mechanical damping. Scanning electron microscopy confirmed enhanced fibre impregnation and fewer defects after treatments. These findings highlight the significant role of chemical surface modification in optimising structural integrity, vibration control, and acoustic insulation in sustainable banana fibre/carbon–Kevlar hybrids. The improved multifunctional properties suggest promising applications in aerospace, automotive, and structural fields requiring lightweight, durable, and sound-mitigating materials.
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(This article belongs to the Section Polymer Composites)
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Open AccessArticle
Evaluation of the Influence of Temperature on the Mechanical Properties of Biocomposites
by
Darius Albrektas and Daiva Sajek
J. Compos. Sci. 2025, 9(12), 660; https://doi.org/10.3390/jcs9120660 - 2 Dec 2025
Abstract
Environmentally friendly or “green” materials are receiving growing attention due to their sustainability and low energy requirements during production. One such material is mycelium, which can be described as a particle board where fungal hyphae act as a natural adhesive instead of synthetic
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Environmentally friendly or “green” materials are receiving growing attention due to their sustainability and low energy requirements during production. One such material is mycelium, which can be described as a particle board where fungal hyphae act as a natural adhesive instead of synthetic binders. This biodegradable and low-energy material is commonly used in packaging and interior design. However, its relatively weak mechanical properties limit its use in load-bearing or structural applications. To mitigate the main drawback of mycelium—its poor mechanical performance—an original mycelium–wood biocomposite with unique properties was developed. Using an original methodology and equipment, it was determined that its dynamic modulus of elasticity and coefficient of damping depend not only on the wood-to-mycelium ratio within the biocomposite, but also on the orientation of the wooden lamella embedded in it. Subsequently, the influence of ambient temperature on the viscoelastic properties of samples with different “configurations” was assessed. The samples were conditioned for 24 h at temperatures ranging from –20 °C to +40 °C. Results showed that temperature had a lesser effect on the biocomposite compared to natural wood. As temperature increased, the MOEd of samples with 37% wood decreased by about 3–4%, while that of samples with 11% wood remained nearly unchanged. The coefficient of damping increased by 20–30% across all cases.
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(This article belongs to the Section Biocomposites)
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Vibration Energy Harvesting Characteristics of Pyramid Sandwich Beams Under Periodic Elastic Constraints
by
Weimin Xiao, Junjuan Zhao, Jingkai Nie, Shuai Jiang, Zhenkun Guo and Lei Shi
J. Compos. Sci. 2025, 9(12), 659; https://doi.org/10.3390/jcs9120659 - 1 Dec 2025
Abstract
Vibration energy harvesting from ambient mechanical sources offers a sustainable alternative to batteries for powering low-power electronics in remote environments, yet challenges persist in achieving broadband efficiency, low-frequency operation, and concurrent vibration suppression. Here, we introduce a pyramidal piezoelectric sandwich beam (PPSB) with
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Vibration energy harvesting from ambient mechanical sources offers a sustainable alternative to batteries for powering low-power electronics in remote environments, yet challenges persist in achieving broadband efficiency, low-frequency operation, and concurrent vibration suppression. Here, we introduce a pyramidal piezoelectric sandwich beam (PPSB) with periodic elastic constraints, leveraging homogenized lattice truss cores for enhanced electromechanical coupling. Using Lagrange equations, we derive the coupled dynamics, validated against finite element simulations with resonant frequency errors below 3%. Compared to equivalent-stiffness uniform beams, the PPSB exhibits 3.42-fold higher voltage and 11.68-fold greater power output, attributed to optimized strain distribution and resonance amplification. Parametric analyses reveal trade-offs: increasing core thickness or spring stiffness elevates resonant frequencies but reduces voltage peaks due to stiffness–strain imbalances; conversely, a larger beam length, truss radius or tilt angle will reduce the natural frequency while increasing the output through inertia and shear enhancement. Piezoelectric constants and load resistance minimally affect mechanics but optimize electrical impedance matching. This single-phase, geometrically tunable design bridges gaps in multifunctional metamaterials, enabling self-powered sensors with vibration attenuation for aerospace, civil infrastructure, and biomedical applications, paving the way for energy-autonomous systems.
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(This article belongs to the Section Composites Modelling and Characterization)
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Influence of Drill Geometry on Adhesion Layer Formation and Tool Wear During Drilling of AFRP/Al7075-T6 Stacked Composites for Aircraft Industry Applications
by
Jebaratnam Joy Mathavan, Choo Then Xiang, Muhammad Hafiz Hassan and Gérald Franz
J. Compos. Sci. 2025, 9(12), 658; https://doi.org/10.3390/jcs9120658 - 1 Dec 2025
Abstract
Aramid Fiber Reinforced Plastic (AFRP) and aluminum alloy Al7075-T6 are widely used in the aerospace industry because they offer a high strength-to-weight ratio and reliable structural performance. However, drilling through stacked AFRP and Al7075-T6 materials in a single operation presents considerable challenges due
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Aramid Fiber Reinforced Plastic (AFRP) and aluminum alloy Al7075-T6 are widely used in the aerospace industry because they offer a high strength-to-weight ratio and reliable structural performance. However, drilling through stacked AFRP and Al7075-T6 materials in a single operation presents considerable challenges due to the differences in their mechanical and thermal properties. In this study, three types of customized twist drill bits were designed and fabricated to evaluate their effectiveness in single-shot drilling of these stacked materials. The drill geometries included the W-point design, the tapered web design, and the burnishing design. Each drill bit was tested using its own optimized drilling parameters to produce a total of one hundred holes. The aim was to determine which drill geometry provided the best overall performance in terms of tool wear and hole quality. After the drilling experiments, the tool tips were examined using a Scanning Electron Microscope (SEM) to observe wear characteristics and analyze elemental composition. The analysis revealed that aluminum adhered to the cutting lips of all drill bits. The percentage of adhesion layer, known as percentage of adhesion layer (PAL), was calculated to assess the severity of material adhesion. In addition, the morphology of the produced chips and dust was analyzed to support the PAL results. The findings showed that the drill bit with the lowest PAL value demonstrated superior wear resistance, a longer tool life, and the ability to produce holes of higher quality when drilling AFRP and Al7075-T6 stacked materials.
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(This article belongs to the Section Composites Manufacturing and Processing)
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