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Separations, Volume 9, Issue 9

2022 September - 34 articles

Cover Story: H2S is a toxic impurity gas that occurs in various industrial products. It is harmful to both humans and the environment. Nowadays, more and more industrial processes prefer H2S levels below 1 ppm. Therefore, H2S removal, especially trace H2S removal from industrial gases is of vital importance. Zeolite is widely used in H2S adsorption as it has a large specific surface area and unique structure. This paper reviews the current status and issues of zeolite-based adsorbents used to remove H2S from industrial gases. Particular attention is paid to the adsorption mechanism and the measures regarding how to enhance the adsorption performance. In addition, the studies of hydrogen sulfide removal by molecular simulation are also reviewed here. Based on these studies, we attempt to shed light on new perspectives for further research. View this paper
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Articles (34)

  • Article
  • Open Access
33 Citations
5,518 Views
26 Pages

Multiprotein Inhibitory Effect of Dietary Polyphenol Rutin from Whole Green Jackfruit Flour Targeting Different Stages of Diabetes Mellitus: Defining a Bio-Computational Stratagem

  • Tejaswini Maradesha,
  • Shashank M. Patil,
  • Bhaskar Phanindra,
  • Raghu Ram Achar,
  • Ekaterina Silina,
  • Victor Stupin and
  • Ramith Ramu

19 September 2022

The anti-diabetic potential of whole unripe jackfruit (peel with pulp, flake, and seed) was investigated using inhibitory assays for α-glucosidase, α-amylase, aldose reductase, and glycation at multiple stages. Using activity-guided repea...

  • Article
  • Open Access
5 Citations
4,331 Views
15 Pages

Research on the Removal of Levamisole Residues in Bovine, Ovine, Caprine, Porcine and Poultry Tissues

  • Viviana Carmen Ciucă,
  • Carmen Otilia Rusănescu and
  • Victor Viorel Safta

14 September 2022

In this paper, we set the waiting time for the elimination of levamisole residues at a safe level from tissues (muscles and organs) from animals treated with levamisole 10%—oral solution. We studied the depletion of levamisole residues by high...

  • Article
  • Open Access
4 Citations
3,517 Views
19 Pages

Exploring the Antioxidant and Bioinsecticidal Activity of Spontaneous Flora Vegetal Extracts for Plant Protection and Prevention of Soil Contamination

  • Gabriel Mihăiță Daraban,
  • Lăcrămioara Rusu,
  • Rodica Mihaela Dinica,
  • Mihaela Roşca,
  • Marinela Badeanu,
  • Maria Daniela Ionica Mihaila and
  • Daniela Suteu

13 September 2022

The purpose of this article was to evaluate the application of different plant extracts with bioinsecticidal action and antioxidant activity for plants and soil protection, by substitution of the application of synthetically formulated pesticides wit...

  • Article
  • Open Access
13 Citations
3,797 Views
11 Pages

13 September 2022

Spent lithium-ion batteries (LIBs) contain a large number of valuable metals and will be an important strategic resource in the future. Therefore, recycling is extremely important. In this work, acetic acid and hydrogen peroxide were used as leaching...

  • Article
  • Open Access
4 Citations
3,379 Views
14 Pages

Influence of Geographical Location of Spirulina (Arthrospira platensis) on the Recovery of Bioactive Compounds Assisted by Pulsed Electric Fields

  • Francesc Ramon-Mascarell,
  • Francisco J. Martí-Quijal,
  • Juan Manuel Castagnini,
  • Yuthana Phimolsiripol,
  • Warintorn Ruksiriwanich,
  • Muhammad Shahid Riaz Rajoka,
  • Hafiza Mahreen Mehwish and
  • Francisco J. Barba

13 September 2022

Spirulina (Arthrospira platensis) has been consumed by humans since ancient times. It is rich in high added-value compounds such as chlorophylls, carotenoids and polyphenols. Pulsed electric fields (PEF) is an innovative non-thermal technique that im...

  • Article
  • Open Access
34 Citations
3,918 Views
21 Pages

Synthesis, Characterization, and Performance Evaluation of Hybrid Waste Sludge Biochar for COD and Color Removal from Agro-Industrial Effluent

  • Ahmad Hussaini Jagaba,
  • Shamsul Rahman Mohamed Kutty,
  • Sule Abubakar,
  • Abdullahi Haruna Birniwa,
  • Ibrahim Mohammed Lawal,
  • Ibrahim Umaru,
  • Abdullahi Kilaco Usman,
  • Nura Shehu Aliyu Yaro,
  • Nabil Al-Zaqri and
  • Fida Hussain
  • + 2 authors

13 September 2022

Agro-waste management processes are evolving through the development of novel experimental approaches to understand the mechanisms in reducing their pollution levels efficiently and economically from industrial effluents. Agro-industrial effluent (AI...

  • Review
  • Open Access
35 Citations
6,629 Views
26 Pages

Exploring the Biosorption of Methylene Blue Dye onto Agricultural Products: A Critical Review

  • Manish Kumar Sah,
  • Khaled Edbey,
  • Ashraf EL-Hashani,
  • Sanad Almshety,
  • Luisetto Mauro,
  • Taghrid S. Alomar,
  • Najla AlMasoud and
  • Ajaya Bhattarai

13 September 2022

Due to their higher specific area and, in most cases, higher adsorption capacity, nanomaterials are noteworthy and attractive adsorbents. Agricultural products that are locally available are the best option for removing methylene blue (MB) dye from a...

  • Article
  • Open Access
39 Citations
5,296 Views
11 Pages

Recovery of Bioactive Extracts from Olive Leaves Using Conventional and Microwave-Assisted Extraction with Classical and Deep Eutectic Solvents

  • Eleni Boli,
  • Nikos Prinos,
  • Vasiliki Louli,
  • Georgia Pappa,
  • Haralambos Stamatis,
  • Kostis Magoulas and
  • Epaminondas Voutsas

The recovery of phenolic compounds from olive leaves (Olea europaea L.) has received special attention due to their significant potential for applications in food, nutraceuticals, cosmetics, and pharmaceuticals. In this work, the extraction of the ph...

  • Article
  • Open Access
7 Citations
4,632 Views
10 Pages

Wound Healing Potential of Commiphora gileadensis Stems Essential Oil and Chloroform Extract

  • Hassan N. Althurwi,
  • Mohammad Ayman A. Salkini,
  • Gamal A. Soliman,
  • Mohd Nazam Ansari,
  • Elmutasim O. Ibnouf and
  • Maged S. Abdel-Kader

Essential oils (EOs) prepared from the fresh and dried stems of Commiphora gileadensis were compared qualitatively and quantitatively. Although the components were closely similar, the amount of oil decreased from 2.23 to 1.77% upon drying. Both samp...

  • Editorial
  • Open Access
2 Citations
2,464 Views
4 Pages

Novel Polymeric Membranes Preparation and Membrane Process

  • Wenzhong Ma,
  • Yakai Lin and
  • Yuanhui Tang

Polymer-based membranes have advanced or novel functions in the various membrane separation processes for liquid and gaseous mixtures, such as gas separation, pervaporation (PV), reverse osmosis (RO), nanofiltration (NF), ultrafiltration (UF), microf...

  • Article
  • Open Access
2 Citations
3,266 Views
13 Pages

High-Purity Corundum as Support for Affinity Extractions from Complex Samples

  • Jule L. Völzke,
  • Parya Hodjat Shamami,
  • Kornelia Gawlitza,
  • Ines Feldmann,
  • Annett Zimathies,
  • Klas Meyer and
  • Michael G. Weller

Nonporous corundum powder, known as an abrasive material in the industry, was functionalized covalently with protein binders to isolate and enrich specific proteins from complex matrices. The materials based on corundum were characterized by TEM, ESE...

  • Article
  • Open Access
7 Citations
2,907 Views
13 Pages

Extracellular vesicles (EVs) are 50–1000 nm membranous vesicles secreted from all cells that play important roles in many biological processes. Exosomes, a smaller-sized subset of EVs, have become of increasing interest in fundamental biochemis...

  • Article
  • Open Access
1 Citations
15,942 Views
7 Pages

False Positive Results of Phosphatidylethanol (PEth) Quantitation in Dried Blood Spots (DBS): The Influence of Alcohol Vapors

  • Anton Bashilov,
  • Sergey Osipenko,
  • Karolina Ikonnikova,
  • Oxana Kovaleva,
  • Boris Izotov,
  • Evgeny Nikolaev and
  • Yury Kostyukevich

The role of phosphatidylethanol (PEth) as an alcohol consumption marker is increasing in clinical and forensic medicine. During the COVID-19 pandemic, the role of hygiene increased, and it became common practice to use disinfectants almost everywhere...

  • Article
  • Open Access
5 Citations
2,746 Views
8 Pages

Chemical Composition of the Fixed Oil of Harconia speciosa and Modulation of the Antibiotic Activity against Non-Resistant and MDR Bacterial Strains

  • Erlânio O. de Sousa,
  • Maria do Socorro Costa,
  • Cícera Datiane M. Oliveira-Tintino,
  • Carla de Fátima A. Nonato,
  • Jacqueline C. A. Pinheiro,
  • Henrique Douglas M. Coutinho,
  • Irwin Rose A. de Menezes and
  • José Galberto M. Costa

The species Hancornia speciosa (mangabeira) has varied potential. The bark has astringent properties, latex is used for tuberculosis, ulcers, herpes, dermatoses and warts, leaf tea is used for menstrual cramps and the root decoction to treat dislocat...

  • Article
  • Open Access
7 Citations
4,327 Views
17 Pages

A Resolved Simulation Approach to Investigate the Separation Behavior in Solid Bowl Centrifuges Using Material Functions

  • Helene Katharina Baust,
  • Simon Hammerich,
  • Hartmut König,
  • Hermann Nirschl and
  • Marco Gleiß

The separation of finely dispersed particles from liquids is a basic operation in mechanical process engineering. On an industrial scale, continuously operating decanter centrifuges are often used, whose separation principle is based on the density d...

  • Article
  • Open Access
8 Citations
3,817 Views
18 Pages

Comparative Elucidation of Aroma, Key Odorants, and Fatty Acid Profiles of Ivorian Shea Butter Prepared by Three Different Extraction Methods

  • Kouame Fulbert Oussou,
  • Gamze Guclu,
  • Onur Sevindik,
  • Małgorzata Starowicz,
  • Hasim Kelebek and
  • Serkan Selli

In the present study, the volatile compounds, key odorants, and fatty acid profiles of Ivorian shea butter produced by cold press extraction (CPE), solvent extraction (SE) and traditional extraction (TE) methods were investigated for the first time....

  • Article
  • Open Access
40 Citations
8,966 Views
11 Pages

Phenolic Composition, Antioxidant and Antibacterial Activities of Extract from Flowers of Rosa damascena from Morocco

  • Mounia Chroho,
  • Aziz Bouymajane,
  • Yassine Oulad El Majdoub,
  • Francesco Cacciola,
  • Luigi Mondello,
  • Mustapha Aazza,
  • Touriya Zair and
  • Latifa Bouissane

Rosa damascena is referred to as the queen of roses due to its ornamental, flavoring, and perfuming uses, along with its recognized use in therapy. This study aimed to investigate the total phenols and flavonoids contents, the phenolic compounds, and...

  • Article
  • Open Access
4 Citations
3,759 Views
19 Pages

Camphorsulfonic acid salts are commonly used in the manufacturing production of active pharmaceutical ingredients (APIs) and have the potential to form alkyl camphorsulfonates, which can be considered as potential genotoxic impurities (PGIs). Alkyl c...

  • Article
  • Open Access
44 Citations
13,174 Views
9 Pages

Antioxidant Activity and Phenolic Content of Sonication- and Maceration-Assisted Ethanol and Acetone Extracts of Cymbopogon citratus Leaves

  • Shafeeqa Irfan,
  • Muhammad Mudassar Ali Nawaz Ranjha,
  • Muhammad Nadeem,
  • Muhammad Naeem Safdar,
  • Saqib Jabbar,
  • Shahid Mahmood,
  • Mian Anjum Murtaza,
  • Kashif Ameer and
  • Salam A. Ibrahim

Cymbopogon citratus is a medicinal and well-known aromatic plant which is usually used as a substitute for green-tea with extraordinary phytomedicinal potential. It is of great importance because it offers several promising health effects. The object...

  • Communication
  • Open Access
3 Citations
3,337 Views
9 Pages

Boosting the Liquid Chromatography Separation of Complex Bispecific Antibody Products by Using the Multi-Isocratic Elution Mode

  • Amarande Murisier,
  • Valentina D’Atri,
  • Vincent Larraillet,
  • Sebastian Pirner and
  • Davy Guillarme

In reversed-phase liquid chromatography (RPLC), the selectivity between major species and minor variants of protein biopharmaceutical products is always limited. Unfortunately, the stationary phase chemistry, type of mobile phase (organic modifier an...

  • Article
  • Open Access
12 Citations
4,496 Views
9 Pages

Speciation of Selenium in Selenium-Enriched Foods by High-Performance Liquid Chromatography-Inductively Coupled Plasma-Tandem Mass Spectrometry

  • Yue Luo,
  • Gang Chen,
  • Xiuqing Deng,
  • Hanqing Cai,
  • Xueheng Fu,
  • Fujian Xu,
  • Xiaonian Xiao,
  • Yumeng Huo and
  • Jin Luo

Herein, a method was established for the speciation of six selenium species by high performance liquid chromatography-inductively coupled plasma-tandem mass spectrometry (HPLC-ICP-MS/MS). The factors affecting separation were carefully investigated,...

  • Article
  • Open Access
3 Citations
2,883 Views
26 Pages

Impact of Phenol on Membranes during Bipolar Membrane Electrodialysis for High Salinity Pesticide Wastewater Treatment

  • Yuanhui Tang,
  • Wenwen Sun,
  • Yakai Lin,
  • Lin Wang,
  • Hedi Chen,
  • Huanhuan Wu,
  • Lixin Yu and
  • Xiaolin Wang

To achieve a cleaner production, pesticide wastewater with concentrated NaCl can be treated by using a bipolar membrane electrodialysis (BMED) and converted to NaOH and HCl, which minimizes acid and alkali consumption in a pesticide production proces...

  • Article
  • Open Access
3 Citations
2,822 Views
11 Pages

Medicago sativa (alfalfa) is a widely used animal feed. However, its quality has been difficult to control due to the lack of appropriate marker compounds. Therefore, it is very necessary to select an appropriate quality marker (Q-marker) to control...

  • Article
  • Open Access
3 Citations
2,269 Views
12 Pages

Myconoside Affects the Viability of Polarized Epithelial MDCKII Cell Line by Interacting with the Plasma Membrane and the Apical Junctional Complexes

  • Aneliya Kostadinova,
  • Galya Staneva,
  • Tanya Topouzova-Hristova,
  • Daniela Moyankova,
  • Vesela Yordanova,
  • Ralitsa Veleva,
  • Biliana Nikolova,
  • Albena Momchilova,
  • Dimitar Djilianov and
  • Rusina Hazarosova

The phenyl glycoside myconoside, extracted from Balkan endemic Haberlea rhodopensis, has a positive effect on human health, but the exact molecular mechanism of its action is still unknown. The cell membrane and its associated junctional complex are...

  • Article
  • Open Access
5 Citations
5,746 Views
10 Pages

The search for new anti-inflammatory drugs with less side effects requires simple, fast and reliable screening methods. In this context, we have developed a sensitive thin-layer chromatographic (TLC) assay on silica gel plates to detect cyclooxygenas...

  • Article
  • Open Access
8 Citations
3,103 Views
19 Pages

Optimization of Microwave-Assisted Extraction and Matrix Solid-Phase Dispersion for the Extraction of Polyphenolic Compounds from Grape Skin

  • Danijela Ašperger,
  • Marija Gavranić,
  • Barbara Prišlin,
  • Nera Rendulić,
  • Iva Šikuten,
  • Zvjezdana Marković,
  • Bruna Babić,
  • Edi Maletić,
  • Jasminka Karoglan Kontić and
  • Ivana Tomaz
  • + 1 author

Polyphenols are organic compounds that can be found in food, especially in fruits, vegetables, and their products. It was shown that their presence significantly affects the properties of food products and that the consumption of food rich in phenoli...

  • Article
  • Open Access
4 Citations
2,738 Views
16 Pages

Purification, Identification and Neuroprotective Effects of Proteins from Bombyx batryticatus in Glu-Stimulated PC12 Cells

  • Mei-Bian Hu,
  • Xiang-Long Meng,
  • Pu Wang,
  • Shuo-Sheng Zhang,
  • Chun-Jie Wu and
  • Yu-Jie Liu

Bombyx batryticatus (BB) is one of the most commonly used Traditional Chinese Medicines (TCMs) in the treatment of convulsions and epilepsy. The antiepileptic effects of total proteins from BB (BBPs) have been proven in our previous research. In this...

  • Communication
  • Open Access
1 Citations
2,205 Views
10 Pages

Synthesis and Chromatographic Determination of S-Nitrosopantetheine: Exploring Reactivity and Stability in Different Aqueous Solutions

  • Daniel Di Risola,
  • Roberto Mattioli,
  • Giulia Mazzoccanti,
  • Simone Manetto,
  • Maurizio Trovato,
  • Mario Fontana,
  • Luciana Mosca and
  • Antonio Francioso

S-nitrosothiols (RSNOs) are a group of sulfur-containing compounds biologically involved in nitric oxide (NO˙) release and signalling pathway. NO˙ plays important physiological and pharmacological activities, particularly in vasodilation an...

  • Article
  • Open Access
29 Citations
10,008 Views
22 Pages

Antioxidant Activity, Total Phenolic and Flavonoid Content and LC–MS Profiling of Leaves Extracts of Alstonia angustiloba

  • Nurhidayah Ab. Rahim,
  • Muhammad Nabil Fikri Roslan,
  • Musthahimah Muhamad and
  • Azman Seeni

Plants have a wide range of active compounds crucial in treating various diseases. Most people consume plants and herbals as an alternative medicine to improve their health and abilities. A. angustiloba extract showed antinematodal activity against B...

  • Article
  • Open Access
8 Citations
4,688 Views
14 Pages

Pipette tip solid-phase extraction facilitates the handling of low-volume samples and organic solvents in order to achieve more environmentally friendly pre-treatment sample techniques. The use of pipette tip extraction was examined for the quick and...

  • Article
  • Open Access
9 Citations
4,243 Views
12 Pages

Optimization of an Analytical Method for Indoxacarb Residues in Fourteen Medicinal Herbs Using GC–μECD, GC–MS/MS and LC–MS/MS

  • Hun-Ju Ham,
  • Syed Wasim Sardar,
  • Abd Elaziz Sulieman Ahmed Ishag,
  • Jeong-Yoon Choi and
  • Jang-Hyun Hur

Pesticide residue analysis in medicinal herbs is a challenging task because of the matrix effect and its influence on quantitative analysis despite the continuous development of several new analytical methods and instrumentations. In this study, a mo...

  • Article
  • Open Access
2 Citations
2,310 Views
15 Pages

Cuscutae Semen (CS; Chinese common name “Tusizi”) is one of the most common traditional herbal medicines used to treat liver and kidney diseases in China. Although it is most commonly used as a processed product, little progress has been...

  • Article
  • Open Access
8 Citations
3,820 Views
11 Pages

Antiproliferative Effect of Sechium edule (Jacq.) Sw., cv. Madre Negra Extracts on Breast Cancer In Vitro

  • Jorge Cadena-Iñiguez,
  • Itzen Aguiñiga-Sánchez,
  • María Teresa Uriostegui-Arias,
  • Edelmiro Santiago-Osorio,
  • Lucero del Mar Ruiz-Posadas and
  • Marcos Soto-Hernández

Sechium edule shows a wide biological diversity. Hybrids and varieties of Sechium edule have been created, producing fruits of different shapes, sizes, colors, tastes, and textures. These hybrids and varieties have been used as food and in traditiona...

  • Review
  • Open Access
25 Citations
11,091 Views
17 Pages

Review of Hydrogen Sulfide Removal from Various Industrial Gases by Zeolites

  • Tao Yu,
  • Zhuo Chen,
  • Zhendong Liu,
  • Jianhong Xu and
  • Yundong Wang

Hydrogen sulfide (H2S) removal from various industrial gases is crucial because it can cause huge damage to humans, the environment, and industrial production. Zeolite possesses huge specific surface area and well-developed pore structure, making it...

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Separations - ISSN 2297-8739