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Separations, Volume 10, Issue 2

2023 February - 82 articles

Cover Story: Nowadays, in order to reduce pollution, it is essential to find a second life for waste. In this work, a sorbent has been prepared starting from wastepaper to which graphene oxide and Fe2O3 have been added. Using a carbothermal reaction, a nanocomposite sorbent based on rG-activated carbon-Fe3O4 was obtained to be used as a sorbent in the magnetic dispersive solid-phase extraction of antibiotics from human plasma. The morphological and structural features of the prepared “rG-AC-Fe3O4” samples were investigated via thermal analysis, X-ray diffraction, Raman spectroscopy, and scanning electron microscopy. Parameters affecting magnetic dispersive solid-phase extraction were optimized one variable at a time (OVAT). Finally, a UHPLC-PDA method was developed and applied for the determination of antibiotics. View this paper
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Articles (82)

  • Article
  • Open Access
3 Citations
3,452 Views
14 Pages

20 February 2023

The isomeric metabolites τ- and π-methylhistidine (formerly referred to as 3- and 1-methylhistidine) are known biomarkers for muscle protein breakdown and meat protein intake, frequently used in studies involving humans and animals. In the pre...

  • Review
  • Open Access
14 Citations
5,482 Views
27 Pages

19 February 2023

The present work deals with the continuous flow systems based on renewable resource biosorbents towards the green removal of various categories of chemical pollutants from aqueous media. The opening discussions are focused on: (a) renewable resources...

  • Review
  • Open Access
8 Citations
4,228 Views
23 Pages

Contaminant Cocktails of High Concern in Honey: Challenges, QuEChERS Extraction and Levels

  • Mariana Lamas,
  • Francisca Rodrigues,
  • Maria Helena Amaral,
  • Cristina Delerue-Matos and
  • Virgínia Cruz Fernandes

18 February 2023

Environmental pollution is a crucial problem in our society, having nowadays a better understanding of its consequences, which include the increase of contaminant cocktails present in the environment. The contamination of honeybees can occur through...

  • Article
  • Open Access
7 Citations
4,150 Views
13 Pages

Chemical Profiling of Significant Antioxidant and Phytotoxic Microwave-Extracted Essential Oil from Araucaria heterophylla Resin

  • Ahmed M. Abd-ElGawad,
  • Ibrahim Saleh,
  • Mohamed H. Abd El-Razek,
  • Asmaa S. Abd Elkarim,
  • Yasser A. El-Amier,
  • Tarik A. Mohamed,
  • Abd El-Nasser G. El Gendy,
  • Sherif M. Afifi,
  • Tuba Esatbeyoglu and
  • Abdelsamed I. Elshamy

18 February 2023

Due to the various hazards of using synthetic chemical compounds in pharmaceutics, agriculture, and industry, scientists and researchers do their best to explore and assess new green natural compounds from natural resources with potent activity. The...

  • Article
  • Open Access
2 Citations
2,149 Views
11 Pages

18 February 2023

The direct use of nanosorbents for water purification is limited due to their aggregation and the lack of techniques for their recovery from natural waters. To overcome these problems, the affixation of nanomaterials onto bulk, non-mobile supports ha...

  • Review
  • Open Access
7 Citations
4,220 Views
16 Pages

Condensed Phase Membrane Introduction Mass Spectrometry: A Direct Alternative to Fully Exploit the Mass Spectrometry Potential in Environmental Sample Analysis

  • Veronica Termopoli,
  • Maurizio Piergiovanni,
  • Davide Ballabio,
  • Viviana Consonni,
  • Emmanuel Cruz Muñoz and
  • Fabio Gosetti

17 February 2023

Membrane introduction mass spectrometry (MIMS) is a direct mass spectrometry technique used to monitor online chemical systems or quickly quantify trace levels of different groups of compounds in complex matrices without extensive sample preparation...

  • Article
  • Open Access
12 Citations
3,383 Views
14 Pages

A Validated, Stability-Indicating, Eco-Friendly HPTLC Method for the Determination of Cinnarizine

  • Mohammed H. Alqarni,
  • Faiyaz Shakeel,
  • Ahmed I. Foudah,
  • Tariq M. Aljarba,
  • Wael A. Mahdi,
  • Fatma M. Abdel Bar,
  • Sultan Alshehri and
  • Prawez Alam

17 February 2023

The eco-friendly high-performance thin-layer chromatographic (HPTLC) approaches for measuring cinnarizine (CIN) are scant in reported databases. As a result, the current work has developed and validated an eco-friendly HPTLC technique for assessing C...

  • Article
  • Open Access
16 Citations
3,931 Views
15 Pages

Effect of Hydrothermal Conditions on Kenaf-Based Carbon Quantum Dots Properties and Photocatalytic Degradation

  • Nabilah Saafie,
  • Nonni Soraya Sambudi,
  • Mohd Dzul Hakim Wirzal and
  • Suriati Sufian

17 February 2023

The development of biomass-based CQD is highly attentive to enhancing photocatalytic performance, especially in secondary or ternary heterogeneous photocatalysts by allowing for smooth electron-hole separation and migration. In this study, kenaf-base...

  • Article
  • Open Access
7 Citations
3,405 Views
13 Pages

Green Automated Solid Phase Extraction to Measure Levofloxacin in Human Serum via Liquid Chromatography with Fluorescence Detection for Pharmacokinetic Study

  • Hager Ebrahim,
  • Heba Sonbol,
  • Monika Malak,
  • Ahmed Ali,
  • Yasmine Aboulella,
  • Ghada Hadad,
  • Walaa Zarad,
  • Samy Emara and
  • Lamyaa Bazan

17 February 2023

A simple, selective, rapid, sensitive and less costly green automated solid phase extraction bio-analytical high-performance liquid chromatographic-based technique with fluorescence detection (Aut-SPE-BA-HPLC-FL) for the quantification of levofloxaci...

  • Article
  • Open Access
2 Citations
2,694 Views
16 Pages

16 February 2023

In this study, the formation of natural gas liquid in gas distribution lines, particularly at regional stations, service boxes, customer installations, and gas meters, was investigated. The study aims to address the problems associated with natural g...

  • Article
  • Open Access
9 Citations
6,903 Views
15 Pages

Surfactant-Enhanced Extraction of Lutein from Marigold Petals using an Aqueous Two-Phase System

  • Neha Maheshwari,
  • Raj Kumar Arya,
  • George D. Verros,
  • Pradip B. Dhamole and
  • Ashwin Kannan

15 February 2023

The extraction of lutein from marigold petals using a surfactant-based aqueous two-phase system is reported. In this work, the effectiveness of the hydrophilic-lipophilic balance of surfactants on extraction performance for the extraction of lutein f...

  • Article
  • Open Access
5 Citations
2,727 Views
15 Pages

15 February 2023

In recent years, high permeability membranes (HPMs) have attracted wide attention in seawater reverse osmosis (SWRO) desalination. However, the limitation of hydrodynamics and mass transfer characteristics for conventional spiral wound modules defeat...

  • Review
  • Open Access
47 Citations
10,669 Views
26 Pages

Potential of Advanced Oxidation as Pretreatment for Microplastics Biodegradation

  • Kristina Bule Možar,
  • Martina Miloloža,
  • Viktorija Martinjak,
  • Matija Cvetnić,
  • Hrvoje Kušić,
  • Tomislav Bolanča,
  • Dajana Kučić Grgić and
  • Šime Ukić

15 February 2023

In the last two decades, microplastics (MP) have been identified as an emerging environmental pollutant. Due to their small size, MP particles may easily enter the food chain, where they can have adverse effects on organisms and the environment in ge...

  • Article
  • Open Access
7 Citations
3,207 Views
13 Pages

15 February 2023

The Scutellaria baicalensisCoptis chinensis pair is an herbal combination used for the treatment of various heat-related diseases. During the extraction process, two herbs can mutually influence the extraction efficiency of the chemical consti...

  • Article
  • Open Access
5 Citations
2,791 Views
14 Pages

Influence of Chemical Pretreatment on the Adsorption of N2 and O2 in Ca-Clinoptilolite

  • Miguel Ángel Hernández,
  • Gabriela I. Hernández,
  • Roberto Ignacio Portillo,
  • Ma de los Ángeles Velasco,
  • Juana Deisy Santamaría-Juárez,
  • Efraín Rubio and
  • Vitalii Petranovskii

15 February 2023

N2 and O2 adsorption isotherms in chemically modified clinoptilolite-Ca zeolites were experimentally estimated by inverse adsorption chromatography. Natural zeolites (CLINA) were chemically treated with HCl at different concentrations (H1-H4). The ad...

  • Article
  • Open Access
1 Citations
2,443 Views
15 Pages

14 February 2023

The flexibility of membrane contactors (MCs) is highlighted for a reverse osmosis (RO) desalination plant. MCs are applied as pre-treatment for the oxygen removal and the pH reduction of seawater, also as post-treatment for the pH increase of the RO...

  • Article
  • Open Access
7 Citations
6,273 Views
15 Pages

Effect of Extraction Methods on Essential Oil Composition: A Case Study of Irish Bog Myrtle-Myrica gale L.

  • Shipra Nagar,
  • Maria Pigott,
  • Sophie Whyms,
  • Apolline Berlemont and
  • Helen Sheridan

14 February 2023

Myrica gale is an aromatic peatland shrub that has reported traditional use as an insect repellent. Different extraction methodologies were used in this study to isolate the essential oil of Myrica gale L., including Clevenger hydrodistillation (CH)...

  • Article
  • Open Access
7 Citations
2,658 Views
12 Pages

Application of Encapsulated Quorum Quenching Strain Acinetobacter pittii HITSZ001 to a Membrane Bioreactor for Biofouling Control

  • Yongmei Wang,
  • Xiaochi Feng,
  • Wenqian Wang,
  • Hongtao Shi,
  • Zijie Xiao,
  • Chenyi Jiang,
  • Yujie Xu,
  • Xin Zhang and
  • Nanqi Ren

13 February 2023

Quorum quenching (QQ) is a novel anti-biofouling strategy for membrane bioreactors (MBRs) used in wastewater treatment. However, actual operation of QQ-MBR systems for wastewater treatment needs to be systematically studied to evaluate the comprehens...

  • Review
  • Open Access
11 Citations
8,502 Views
22 Pages

13 February 2023

Loquat is an evergreen tree belonging to the genus Loquat in Rosaceae. It is widely used in the processing of food and medicine. Based on the literature findings, the anti-tumor, antibacterial, anti-inflammatory and anti-oxidation activities of the e...

  • Review
  • Open Access
15 Citations
3,199 Views
32 Pages

Advancements in Clay Materials for Trace Level Determination and Remediation of Phenols from Wastewater: A Review

  • Zakariyya Uba Zango,
  • Muhammad Nur’Hafiz Rozaini,
  • Noor Hana Hanif Abu Bakar,
  • Muttaqa Uba Zango,
  • Maje Alhaji Haruna,
  • John Ojur Dennis,
  • Ahmed Alsadig,
  • Khalid Hassan Ibnaouf,
  • Osamah A. Aldaghri and
  • Ismael Abdalla Wadi

10 February 2023

The wide spread of phenols and their toxicity in the environment pose a severe threat to the existence and sustainability of living organisms. Rapid detection of these pollutants in wastewaters has attracted the attention of researchers from various...

  • Article
  • Open Access
8 Citations
3,444 Views
17 Pages

10 February 2023

In this project, a prompt, efficient, and effective method for Cd2+ ions extraction from different food and water samples using magnetic dispersion-based solid phase extraction by functionalized iron oxide nanoparticles was proposed. Iron oxide nanop...

  • Article
  • Open Access
5 Citations
3,170 Views
18 Pages

For years, researchers have focused on the determination of metal ions at trace levels in environmental and food samples using analytical methods that employ techniques with low cost acquisition and maintenance and without microwave-assisted acid dig...

  • Article
  • Open Access
11 Citations
4,178 Views
17 Pages

Combined Effects of Polyamide Microplastics and Hydrochemical Factors on the Transport of Bisphenol A in Groundwater

  • Zhou Cheng,
  • Xuanhao Lin,
  • Ming Wu,
  • Guoping Lu,
  • Yanru Hao,
  • Cehui Mo,
  • Qusheng Li,
  • Jianfeng Wu,
  • Jichun Wu and
  • Bill X. Hu

Polyamide (PA) and bisphenol A (BPA) are selected as typical microplastic and endocrine-disrupting chemicals in this study. The adsorption of BPA on the surface of PA and the effect of PA on the transport behavior of BPA in groundwater are systematic...

  • Review
  • Open Access
48 Citations
16,009 Views
25 Pages

In recent years, the scientific community has turned its attention to the further study and application of green chemistry as well as to sustainable development in reducing the consumption of raw materials, solvents, and energy. The application of gr...

  • Article
  • Open Access
7 Citations
4,068 Views
12 Pages

The fixed dose combination of valsartan (VAL) and hydrochlorothiazide (HCTZ) is the most commonly prescribed medicine for the effective treatment of hypertension. In this study, a simple sensitive and accurate liquid chromatography-tandem mass spectr...

  • Article
  • Open Access
19 Citations
3,579 Views
14 Pages

Sustainable Microwave-Assisted Extraction of Santalin from Red Sandal Wood Powder (Ptrecarpus santalinus) for Bio-Coloration of Mordanted Silk Fabric

  • Samra Barkaat,
  • Maria Mehboob,
  • Shahid Adeel,
  • Fazal-ur-Rehman,
  • Nimra Amin,
  • Noman Habib and
  • Mozhgan Hosseinnezhad

The coloring behavior of santalin, a natural reddish-brown dye derived from sandalwood, has been investigated in this work for the dyeing of silk fabrics while being heated in MW radiation. Microwave (MW) radiation up to 5 min has been employed to is...

  • Article
  • Open Access
2,658 Views
15 Pages

Just Suspended Speed Simulation in Torus Reactor Using Multiple Non-Linear Regression Model

  • Houssem Eddine Sayah,
  • Ali Alouache,
  • Mohamed Annad,
  • Abdelouahab Lefkir,
  • L’hadi Nouri,
  • Ammar Selatnia and
  • Mohammed Messaoudi

In the chemical and water treatment industries, it is necessary to achieve maximum contact between the solid and liquid phase, thus promoting the mass and heat transfer, to obtain a homogeneous solution. Increasing stirring speed is the most recommen...

  • Article
  • Open Access
3 Citations
2,554 Views
15 Pages

Investigation of Imidazolium-Based Ionic Liquids as Additives for the Separation of Urinary Biogenic Amines via Capillary Electrophoresis

  • Natalia Kaczmarczyk,
  • Natalia Treder,
  • Piotr Kowalski,
  • Alina Plenis,
  • Anna Roszkowska,
  • Tomasz Bączek and
  • Ilona Olędzka

Ionic liquids (ILs), such as imidazoles, can be used to prevent the sorption of analytes onto the walls of the capillary. Prior works have confirmed that coating the capillary wall with a cationic layer can increase its surface stability, thereby imp...

  • Article
  • Open Access
6 Citations
2,693 Views
15 Pages

Preparation of Fe3O4-Reduced Graphene-Activated Carbon from Wastepaper in the Dispersive Solid-Phase Extraction and UHPLC-PDA Determination of Antibiotics in Human Plasma

  • Pantaleone Bruni,
  • Pasquale Avino,
  • Vincenzo Ferrone,
  • Serena Pilato,
  • Nadia Barbacane,
  • Valentino Canale,
  • Giuseppe Carlucci and
  • Stefania Ferrari

In this work, a sorbent was prepared from wastepaper samples enriched with iron oxide particles and graphene oxide and used in the solid phase extraction of antibiotics. The precursor underwent a carbothermal reduction to promote the formation of par...

  • Article
  • Open Access
5 Citations
2,667 Views
11 Pages

Ballota saxatilis from Jordan: Evaluation of Essential Oil Composition and Phytochemical Profiling of Crude Extracts and Their In-Vitro Antioxidant Activity

  • Nezar Al-Bataineh,
  • Faisal K. Algethami,
  • Hala I. Al-Jaber,
  • Abdulrahman G. Alhamzani,
  • Rand M. Bataineh,
  • Yousef Al-Dalahmeh,
  • Tareq T. Bataineh,
  • Sultan T. Abu-Orabi and
  • Mahmoud A. Al-Qudah

The chemical composition of essential oil extracted from the aerial parts of Ballota saxatilis Sieber ex C.Presl from Jordan has been elucidated by gas chromatography–mass spectrometry (GC-MS). Additionally, aqueous methanol (BsA), Butanol (BsB...

  • Communication
  • Open Access
1 Citations
1,751 Views
12 Pages

Removal of Ni(II) from Aqueous Solution by Novel Lycopersicon esculentum Peel and Brassica botrytis Leaves Adsorbents

  • Israf Ud Din,
  • Qadeer Ullah Shah,
  • Syed Tasleem,
  • Abdul Naeem,
  • Abdulrahman I. Alharthi and
  • Mshari Ayad Alotaibi

The current work reports adsorption of Ni(II) using Brassica botrytis leaves (BBL), Brassica botrytis leaves-activated carbon (BBL-AC), Lycopersicon esculentum peel (LEP) and Lycopersicon esculentum peel-activated carbon (LEP-AC). The adsorption of N...

  • Review
  • Open Access
15 Citations
5,644 Views
45 Pages

The extraction of useful minerals or geological materials from the Earth’s crust, most typically from various sources, is crucial to a country’s development and progress. Mineral-rich countries use these resources to transform their econo...

  • Article
  • Open Access
6 Citations
3,715 Views
15 Pages

β-Diketone-Driven Deep Eutectic Solvent for Ultra-Efficient Natural Stable Lithium-7 Isotope Separation

  • Zexing Xie,
  • Meiying Xie,
  • Tingting Tang,
  • Fan Yang,
  • Liyan Xue and
  • Zhengming Jiang

6Li and 7Li are strategic resources. Because Li+ ions have no outermost electrons and the radii of 6Li and 7Li differ by only one neutron, the separation of the naturally stable isotopes of Li, especially by solvent extraction, is recognized as a dif...

  • Article
  • Open Access
11 Citations
6,814 Views
13 Pages

A Preliminary Cytotoxicity Study of Fagonia arabica against Breast (MCF-7), Oral (KB-3-1), and Lung Cancer (A-549) Cell Lines: A Study Supported by Molecular Marker Analysis Using Dual Staining Dyes

  • Ismail A. Walbi,
  • Ali Mohamed Alshabi,
  • Saad Ahmed Alkahtani,
  • Ibrahim Ahmed Shaikh,
  • Basel A. Abdel-Wahab,
  • Masood Medleri Khateeb,
  • Mohammed Shafiuddin Habeeb,
  • Mohamed A. A. Orabi,
  • Arun K. Shettar and
  • Joy H. Hoskeri

Aim: The objective of this research is to present a phytochemical profile of Fagonia arabica and to investigate the cytotoxic potential of its extracts against breast, oral, and lung cancer cell lines using MTT assay and dual staining-based mechanist...

  • Article
  • Open Access
4 Citations
2,714 Views
20 Pages

Synthesis and Characterization of Mesoporous Silica Modified with Purpald and Its Application in the Preconcentration of Cu2+ and Cd2+ from Aqueous Samples through Solid-Phase Extraction

  • Marcos Henrique Pereira Wondracek,
  • Alexandre de Oliveira Jorgetto,
  • Adrielli Cristina Peres da Silva,
  • José Fabián Schneider,
  • Valber de Albuquerque Pedrosa,
  • Margarida Juri Saeki and
  • Gustavo Rocha de Castro

The synthesis of an organofunctionalized mesoporous silica was accomplished by a two-step process involving (1) the co-condensation of a silylant agent at the surface of silica, followed by (2) the immobilization of Purpald (ligand) at the organic te...

  • Conference Report
  • Open Access
2 Citations
8,475 Views
93 Pages

Proceedings of APCE-CECE-ITP-IUPAC 2022

  • František Foret,
  • Doo Soo Chung,
  • Jana Lavická,
  • Jan Přikryl,
  • Haengdo Lee and
  • Iveta Drobníková

In a demonstration of modern analytical chemistry at its best, the International Interdisciplinary Conference of Chemical Analysis, APCE-CECE-ITP-IUPAC 2022 was held after two years of COVID-19-related delays in Siem Reap, Cambodia. The quadruple mee...

  • Article
  • Open Access
2 Citations
3,132 Views
12 Pages

Antioxidant-Activity-Guided Purification and Separation of Octocrylene from Saussurea heteromalla

  • Saboon,
  • Yamin Bibi,
  • Samha Al Ayoubi,
  • Tayyiba Afzal,
  • Sobia Gilani,
  • Khafsa Malik,
  • Abdul Qayyum,
  • Mubashar Hussain and
  • Sunjeet Kumar

Plants have been a source of medicine since ancient times, and such traditional medications are widely practiced nowadays. Saussurea heteromalla is widely used in traditional medicine in the Himalayan region for the treatment of different ailments. H...

  • Article
  • Open Access
5 Citations
2,883 Views
12 Pages

Coriander (Coriandrum sativum L.) is among the most widely used medicinal and aromatic plants. It is well known for its multiple health benefits, most of which are correlated with its phenolic composition. Four phenolic compounds were identified in t...

  • Review
  • Open Access
6 Citations
5,429 Views
28 Pages

Identification and Isolation Techniques for Plant Growth Inhibitors in Rice

  • Nguyen Thi Hai Anh,
  • La Hoang Anh,
  • Nguyen Phuong Mai,
  • Nguyen Van Quan and
  • Tran Dang Xuan

Plant growth inhibitors (PGIs) in rice (Oryza sativa), or rice allelochemicals, are secondary metabolites that are either exudated by rice plants to cope with natural competitors or produced during the decomposition of rice by-products in the paddy f...

  • Article
  • Open Access
31 Citations
5,019 Views
18 Pages

Extraction, Characterization, and Antioxidant Activity of Polysaccharides from Ajwa Seed and Flesh

  • Manel Dhahri,
  • Salim Sioud,
  • Shuruq Alsuhaymi,
  • Fatimah Almulhim,
  • Ali Haneef,
  • Abdelhamid Saoudi,
  • Mariusz Jaremko and
  • Abdul-Hamid M. Emwas

The date palm has been cultivated in dry and hot areas of the planet for much of human history. In the Kingdom of Saudi Arabia, dates are the main crop used as a source of food. Among several species of date fruits, the Ajwa AL-Madinah date is unique...

  • Article
  • Open Access
1 Citations
2,444 Views
16 Pages

Synthesis and Characterization of Electrospun Sorbent for the Solid-Phase Extraction of Fluoroquinolones in Human Plasma and Their UHPLC-PDA Determination

  • Vincenzo Ferrone,
  • Giuseppe Carlucci,
  • Pantaleone Bruni,
  • Lisa Marinelli,
  • Pasquale Avino,
  • Edoardo Milanetti,
  • Serena Pilato,
  • Leonardo Sbrascini,
  • Pietro Di Profio and
  • Stefania Ferrari

In this work we investigated the synthesis and the characterization of electrospun polyacrylonitrile (PAN) and polymethyl methacrylate (PMMA) stabilized in air, made in a 5:1 ratio, used as sorbent for the solid-phase extraction of fluoroquinolones i...

  • Article
  • Open Access
4 Citations
2,682 Views
13 Pages

Pattern Recognition of Phytoconstituents and Bioactivities of Date Pit Extracts from Different Cultivars Grown in the Qassim Area

  • Elham Amin,
  • Enas I. A. Mohamed,
  • Amani Salem Alenezi,
  • Maemonh Ali Aldwesh,
  • Mohamed Sebak,
  • Ibrahim A. Naguib,
  • Sarah I. Bukhari,
  • Khulud Bukhari,
  • Mohamed A. Zaki and
  • Naglaa Afifi

A huge number of date varieties grow annually throughout the world. The genetic variation between different date varieties is reflected in their variable sensory characters and phytochemical contents. Date pits are considered a waste product of the d...

  • Article
  • Open Access
18 Citations
4,380 Views
14 Pages

Spectroscopic Tracking of the Characteristics of Microplastic-Derived Dissolved Organic Matter

  • Mengna Yuan,
  • Huiqing Xiang,
  • Yang Tong,
  • Kanggen Zhou,
  • Changhong Peng and
  • Wei Chen

Microplastic-derived dissolved organic matter (MP-DOM) has received increasing attention in recent years. In this study, the fluorescence excitation-emission matrix (EEM) combined with parallel factor analysis (PARAFAC) was used to track the leaching...

  • Article
  • Open Access
8 Citations
3,623 Views
15 Pages

Cytotoxic, Scolicidal, and Insecticidal Activities of Lavandula stoechas Essential Oil

  • Abdel-Azeem S. Abdel-Baki,
  • Shawky M. Aboelhadid,
  • Saleh Al-Quraishy,
  • Ahmed O. Hassan,
  • Dimitra Daferera,
  • Atalay Sokmen and
  • Asmaa A. Kamel

Essential oils (EOs) have recently attracted more interest due to their insecticidal activities, low harmfulness, and rapid degradation in the environment. Therefore, Lavandula steochas (L. steochas) essential oil was assessed for its chemical c...

  • Article
  • Open Access
13 Citations
8,695 Views
10 Pages

Determination of Sodium, Potassium, and Magnesium as Sulfate Salts in Oral Preparations Using Ion Chromatography and Conductivity Detection

  • Suresh Reddy Yelampalli,
  • Kumaraswamy Gandla,
  • Konatham Teja Kumar Reddy,
  • Adel Ehab Ibrahim and
  • Sami El Deeb

An ion chromatography technique with conductivity detection was selected as an analytical tool for the simultaneous indirect determination of sodium sulfate, potassium sulfate, and magnesium sulfate via their respective cations. The method was develo...

  • Article
  • Open Access
6 Citations
4,812 Views
15 Pages

Greener Stability-Indicating HPLC Approach for the Determination of Curcumin in In-House Developed Nanoemulsion and Curcuma longa L. Extract

  • Nazrul Haq,
  • Faiyaz Shakeel,
  • Mohammed M. Ghoneim,
  • Syed Mohammed Basheeruddin Asdaq,
  • Prawez Alam,
  • Saleh A. Alanazi and
  • Sultan Alshehri

Despite the fact that several analytical methodologies have been reported for the determination of curcumin (CCM) in a wide range of sample matrices, the greener liquid chromatographic approaches to determine CCM are scarce in the literature. Therefo...

  • Article
  • Open Access
8 Citations
3,647 Views
11 Pages

Synthesis, Characterization and Application of Novel Cationic Surfactants as Antibacterial Agents

  • Shaban R. M. Sayed,
  • Abdelrahman O. Ezzat,
  • Mohamed Taha Yassin and
  • Ashraf M. M. Abdelbacki

It is of great necessity to develop new antimicrobial agents to overcome the accelerated increment in drug-resistant bacteria. The main aim of this work is to manufacture two cationic surfactants, QHETA-9 and QHETA-14, based on quaternary hexamethyle...

  • Article
  • Open Access
4 Citations
5,616 Views
15 Pages

Durian Waste Husks as an Adsorbent in Improving Soaking Water during the Retting Process of Piper nigrum L. (Pepper Berries)

  • Muhammad Hazwan Hamzah,
  • Ainaa Syaheera Amran,
  • Adila Fazliyana Aili Hamzah,
  • Mohd Zuhair Mohd Nor,
  • Rosnah Shamsudin,
  • Hasfalina Che Man and
  • Wan Aizuddin Wan Razali

The potential of raw durian husk and NaOH-modified durian husk as an adsorbent, using different doses, 0.5 g, 1.0 g, 1.5 g, and 2.0 g, is investigated to improve soaking water of pepper berries during the retting process. The surface area and the por...

  • Article
  • Open Access
11 Citations
5,625 Views
15 Pages

Vanadium titanomagnetite (VTM) is an important mineral for developing titanium resources, but the comprehensive recovery of ilmenite separation is extremely poor, resulting in the low-efficiency utilization of titanium resources. Here, the separation...

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Separations - ISSN 2297-8739