Fibers

In this research, poly(ε-caprolactone) (PCL) was melt-mixed with sepiolite nanoclays in a twin-screw extruder. In a subsequent step, the extruded films were drawn in the solid state to highly oriented nanocomposite films or tapes. A twin-screw extruder equipped with a Sultzer mixer for improved mixing in combination with a bench top drawing unit was used to prepare oriented nanocomposite tapes of different sepiolite loading and draw ratios. In order to study the influence of the solidification step on the drawability of the materials, different cooling procedures were applied prior to drawing. Optical microscopy images showed that slow or fast solidification using different chill rolls settings (open or closed) for the cast films resulted in different morphological conditions for subsequent drawing. The addition of sepiolite nanofillers led to nucleation and faster crystallization kinetics and oriented tapes which deformed by homogenous deformation rather than necking. The addition of sepiolite significantly improved the mechanical properties of both undrawn and drawn PCL tapes and Young’s modulus (1.5 GPa) and tensile strength (360 MPa) for composites based on 4 wt% sepiolite were among the highest ever reported for PCL nanocomposites. Interestingly, samples cooled with open chill rolls (slow crystallization) showed the highest modulus while solidification with closed rolls (fast crystallization) showed the highest tensile strength after drawing. Full article

Curauá is a bromeliad of Amazonian origin, present in some states in the northern region of Brazil and in other countries in South America. Its natural fibers have several technological advantages for application in composite materials. The objective of this research was to investigate the potential of using the fiber of Curauá as a reinforcement element in mortars for wall covering. Mortars were made with a 1:1:6 ratio (cement:lime:sand) in relation to their mass, evaluating the effect of adding 1%, 2% and 3% of Curauá fiber natural and fiber treated in NaOH solution in relation to the mass of cement, compared to the reference mixture (0%). Technological properties such as consistency, water retention and incorporated air content, compressive strength, water absorption and durability in wetting and drying cycles were evaluated. The results showed that the addition of the Curauá fiber causes an improvement in the mechanical properties of mortars, and at levels of addition 3% or more, it causes problems of workability and incorporation of air into the dough, thus, the fiber addition in 2% presented better results for application in coating mortars, in relation a Brazilian norm, even improving the durability of external coatings. Full article

Fibre-reinforced cementitious matrix (FRCM) composites have been effectively used during the last ten years for the strengthening of existing concrete and masonry structures. These composite materials are made of medium- and high-strength fibre meshes embedded in inorganic matrices. Synthetic fibres are the ones that are currently the most used; however, natural fibres, such as basalt fibres, have recently been receiving growing attention. This work presents an extensive experimental study on the mechanical characterisation of a primed basalt fibre bidirectional grid. Fifty monotonic tensile tests on basalt grid strips were performed by varying different parameters, such as the dimension of the specimens, the clamping system, the measurement system and the test rate. Some of the tests were carried out using a video-extensometer to measure each specimen’s strain. The aim of the study was to find the most suitable setup for the tensile characterisation of basalt textiles, in particular, to prevent slippage of the samples at the gripping area and fully exploit the tensile capacity of the grid. Full article

Expanded clay concrete (ECC) is a promising structural material for buildings due to its light weight and heat- and sound-insulating properties. Adding basalt fibers (BFs) in ECC reduces its brittleness and enhances its mechanical properties. The heat treatment (HT) of BF-reinforced ECC can significantly accelerate the strength growth during cast-in-situ construction, which allows the reduction of the turnover of the formwork and the construction period, as well as leading to lower construction costs. This paper presents an HT technology for load-bearing structures, containing a BF-reinforced ECC mix and using infrared rays for cast-in-situ construction. The issue of the strength growth of BF-reinforced ECC during HT has been studied. Microsilica and fly ash were added to the ECC mix to obtain a compressive strength of more than 20 MPa. Four different mixes of ECC with chopped BFs in the ratios of 1:0, 1:0.0045, 1:0.009 and 1:0.012 by weight of cement were studied. Test specimens were heated by infrared rays for 7, 9, 11, 13, 16 and 24 h. Then, the heat-treated specimens were tested for compressive strength after 0.5, 4, 12 and 24 h cooling periods. The analysis and evaluation of the experimental data were carried out based on probability theory and mathematical statistics. Mathematical models are proposed for forecasting the strength growth of BF-reinforced ECC during cast-in-situ construction. Full article

Ultra-high molecular weight polyethylene (UHMWPE) Dyneema^® SK-76 fibers are widely used in personnel protection systems. Transverse ballistic impact onto these fibers results in complex multiaxial deformation modes such as axial tension, axial compression, transverse compression, and transverse shear. Previous experimental studies on single fibers have shown a degradation of tensile failure strain due to the presence of such multi-axial deformation modes. In this work, we study the presence and effects of such multi-axial stress-states on Dyneema^® SK-76 yarns via transverse loading experiments. Quasi-static transverse loading experiments are conducted on Dyneema^® SK-76 single yarn at different starting angles (5°, 10°, 15°, and 25°) and via four different indenter geometries: round (radius of curvature (ROC) = 3.8 mm), 200-micron, 20-micron, and razor blade (ROC $~$2 micron). Additionally, transverse loading experiments were also conducted for a 0.30 cal. fragment simulating projectile (FSP) and compared to other indenters. Experimental results show that for the round, 200-micron indenter, and FSP geometry the yarn fails in tension with no degradation in axial failure strain compared to the uniaxial tensile failure strain of SK-76 yarn (2.58%). Whereas for the 20-micron indenter and razor blade, fibers fail progressively in transverse shear followed by progressive strength degradation of the yarn. Strength degradation of yarn occurs at relatively low strains of 0.6–0.7% with eventual failure of the yarn at approximately ~1.8% and ~1.5% strain for the 20-micron indenter and razor blade, respectively. Breaking angles (range of 10°–30°) are observed to have little effect on the failure strain for all indenter geometries. Full article

Processing parameters in electrospinning allow us to control the properties of fibers on a molecular level and are able to tailor them for specific applications. In this study, we investigate how relative humidity (RH) affects the mechanical properties of electrospun polyvinylidene fluoride (PVDF). The mechanical properties of single fibers were carried out using a specialized tensile stage. The results from tensile tests were additionally correlated with high-resolution imaging showing the behavior of individual fibers under tensile stress. The mechanical characteristic is strongly dependent on the crystallinity, chain orientation, and fiber diameter of electrospun PVDF fibers. Our results show the importance of controlling RH during electrospinning as the mechanical properties are significantly affected. At low RH = 30% PVDF fibers are 400% stiffer than their counterparts prepared at high RH = 60%. Moreover, the vast differences in the strain at failure were observed, namely 310% compared to 75% for 60% and 30% RH, respectively. Our results prove that humidity is a crucial parameter in electrospinning able to control the mechanical properties of polymer fibers. Full article

The ever-increasing demand for environmentally friendly biocomposites for use in various engineering applications requires a strong understanding of these materials properties, especially in automotive applications. This study focused on investigating how the stacking sequence and fibre orientation impacts the damping properties of hybrid flax/carbon fibre-reinforced composites. Different hybrid carbon fibre/flax fibre-reinforced composites using epoxy resin as the matrix were manufactured using vacuum-assisted resin infusion moulding technique. Each composite material was then tested for tensile properties using a universal testing machine, and the damping experiment was conducted using an impulse hammer and a Laser Doppler Vibrometer. The tensile study found out that adding a flax layer to the external layers of carbon fibre laminate reduced Young’s modulus by 28% for one layer and 45% for two layers. It was noted that when the fibre orientation of the internal layer of [C/F2/C]s was replaced with two ±45° layers, this had a very little effect on Young’s modulus but reduced the ultimate tensile strength by 61%. This experimental study also showed that the most important layer when it comes to damping properties is the external layers. By adding an external flax layer into an epoxy/carbon fibre-reinforced composite considerably enhanced its damping ratio by 53.6% and by adding two layers increased it by 94%. The results indicated a high potential for the automotive semi-structural applications to improve damping properties of the vehicle. Full article

A petrol adulteration sensor based on a rectangular shaped hollow-core photonic crystal fiber is proposed and numerically analyzed in the terahertz regime. The performance of the proposed sensor was evaluated when it is employed to characterize different kerosene mixtures. In this research, the adulterated fuel sample is filled in the rectangular hollow channel and the electromagnetic signal of the terahertz band is also driven through the same channel. The received signal after the interaction of fuel with the terahertz signal will advise the refractive index of the fuel oil inside the core, which will also bear the information of how much extrinsic component is present in the fuel. The finite element method based simulation shows that the proposed sensor can reach a high relative sensitivity of 89% and presents low confinement losses at 2.8 THz. The reported sensing structure is easily realizable with the conventional manufacturing techniques. Consequently, this proposed fiber may be treated as an essential part of real-life applications of petrol adulteration measurements. Full article

Recent decades have seen substantial interest in the use of natural fibers in continuous fiber reinforced composites, such as flax, jute and hemp. Considering potential applications, it is of particular interest how natural fiber composites compare to synthetic fiber composites, such as glass and carbon, and if natural fibers can replace synthetic fibers in existing applications. Many studies have made direct comparisons between natural and synthetic fiber composites via material coupon testing; however, few studies have made such direct comparisons of full structural members. This study presents compression tests of geometrically identical structural channel sections fabricated from fiber-epoxy composites of flax, jute, hemp, glass and carbon. Glass fiber composites demonstrated superior tension material coupon properties to natural fiber composites. However, for the same fiber mass, structural compression properties of natural fiber composite channels were generally equivalent to, or in some cases superior to, glass fiber composite channels. This indicates there is substantial potential for natural fibers to replace glass fibers in structural compression members. Carbon fiber composites were far superior to all other composites, indicating little potential for replacement with natural fibers. Full article

The use of sugarcane residues in mortar and concrete is believed to contribute to a reduction of costs and environmental problems, such as the reduction of mining of natural aggregates and incorrect disposal of the sugarcane residues. Bagasse fiber has a high water retention rate and thus may be considered as a countermeasure for urban heat islands. Because of these properties, bagasse fiber and bagasse sand were added into the preparation of the interlocking concrete blocks. An investigation of the flexural strength and the contribution of the sugarcane residues against an urban heat island was made. The results showed that, by adding 2.0% of bagasse fiber and 5.0% of bagasse sand in concrete, the flexural strength and the water retention content increased in comparison to the control composite. Moreover, the surface temperature and the water evaporation rate of the blocks were smaller in comparison to the control composite. Full article

A new method of Brillouin spectra post-processing, which could be applied in modern distributed optical sensors: Brillouin optical time domain analyzers/reflectometers (BOTDA/BOTDR), has been demonstrated. It operates by means of the correlation analysis performed with special technique («backward-correlation»). It does not need any additional data for time or space averaging and operates with the single spectrum only. We have simulated the method accuracy dependence on signal-to-noise ratio (SNR) and other parameters. It is shown that the new method produces better results at low SNRs than conventional technique, based on finding of Brillouin spectrum maximum, do. These results are in a good agreement with the experiment. Finally, we have estimated the performance of the new method for its application in polarization-BOTDA set-up for a polarization maintaining (PM) fiber modal birefringence distributed study. Full article

The aim of this research was to determine the optimum twist equation for ring-spun yarns. The yarn twist can be calculated by different equations. With the research, we tried to find the appropriate equation to determine the yarn twist, which is determined by the values of yarn strength and hairiness. In the research, yarns from long staple combed cotton rovings and of different fineness (10 tex, 11.8 tex, 20 tex and 29.4 tex) were analyzed. The yarn twist was calculated using the equations of Koechlin and Laetsch. The analyzed yarns were produced in the spinning mill on the laboratory ring spinning machine Spinntester. In the second part of the investigation, yarn strength and hairiness were analyzed as a function of yarn twist. The results showed that Laetsch’s equation is suitable for determining the twist for yarns with a fineness of 10 tex, 11.8 tex, 20 tex and 29.4 tex, since, in this case, the calculated number of yarn threads is higher and thus the strength and elongation at break are also higher. The yarn hairiness is higher in analyzed samples for yarns with the twist calculated according to the Koechlin’s equation. Full article

Woven jute fabric was used as a reinforcing material for making two types of composite, named Jute/PR and Jute/Epoxy, with two different matrixes of polyester resin and epoxy, respectively, by hand layup techniques. Five different doses of gamma radiation from 100 to 500 krad were used to investigate the effects of the mechanical properties of the composites and the jute fabrics. Though gamma radiation improved the mechanical properties, such as the tensile strength (TS) and Young’s modulus (Y), and decreased the elongation at break % (Eb%) of the composites, it deteriorated all these properties for jute fabrics. The highest values of TS and Y and the lowest value of Eb% were found to be 39.44 Mpa, 1218.33 Mpa, and 7.68% for the Jute/PR; and 48.83 Mpa, 1459.67 Mpa, and 3.68% for the Jute/Epoxy composites, respectively, at a 300 krad gamma radiation dose. A further increase in dose altered all these properties; thus, 300 krad was found to be the optimum dose for both of the composites. Between the two composites, gamma radiation influenced the Jute/PR composite more than the Jute/Epoxy composite. Full article

In this paper, a sol-gel N-propyl-trimethoxy-silane coating filled with different amount of multi-wall carbon nanotubes (MWCNTs) was investigated in order to improve the aluminum corrosion resistance. The nanocomposite coating was applied, by drop casting, on AA6061 aluminum alloy substrate. The morphological analysis highlighted that a uniform sol-gel coating was obtained with 0.4 wt.% CNT. Lower or higher nanotube contents lead to the formation of heterogeneities or agglomeration in the coating, respectively. Furthermore, all nanocomposite coatings exhibited effective adhesion to the substrate. In particular, the pull-off strength ranged in 0.82–1.17 MPa. Corrosion protection of the aluminum alloy in NaCl 3.5 wt.% electrolyte (seawater) was significantly improved after CNT addition to the base coating. The stability in electrochemical impedance was observed during three days of immersion in the sodium chloride solution. AS3-CNT2 and AS3-CNT4 batches showed advanced electrochemical stability during immersion tests. Furthermore, interesting results were evidenced in potentiodynamic polarization curves where a decrease of the corrosion current of at least two order of magnitude was observed. Moreover, the breakdown potential was shifted toward noble values. Best results were observed on AS3-CNT6 specimen which exhibited a passivation current density of approximately 1.0 × 10⁻⁵ mA/cm² and a breaking potential of 0.620 V/AgAgCl_sat. Full article

This study presents a non-linear cracked-hinge model for the post-cracking response of fiber-reinforced cementitious composites loaded in bending. The proposed displacement-based model follows a meso-mechanical approach, which makes it possible to consider explicitly the random distribution and orientation of the reinforcing fibers. Moreover, the model allows for considering two different fiber typologies whereas the cement matrix is modelled as a homogeneous material. The proposed mechanical model combines a fracture-based, stress-crack opening relationship for the cementitious matrix with generalized laws aimed to capture the crack-bridging effect played by the reinforcing fibers. These laws are derived by considering both the fiber-to-matrix bond mechanism and fiber anchoring action possibly due to hooked ends. The paper includes a numerical implementation of the proposed theory, which is validated against experimental results dealing with fiber-reinforced cement composites reinforced with different short fibers. The excellent theory vs. experiment matching demonstrates the high technical potential of the presented model, obtained at a reasonable computational cost. Full article

Polyacrylonitrile (PAN) nanofibers, prepared by electrospinning, are often used as a precursor for carbon nanofibers. The thermal carbonization process necessitates a preceding oxidative stabilization, which is usually performed thermally, i.e., by carefully heating the electrospun nanofibers in an oven. One of the typical problems occurring during this process is a strong deformation of the fiber morphologies—the fibers become thicker and shorter, and show partly undesired conglutinations. This problem can be solved by stretching the nanofiber mat during thermal treatment, which, on the other hand, can lead to breakage of the nanofiber mat. In a previous study, we have shown that the electrospinning of PAN on aluminum foils and the subsequent stabilization of this substrate is a simple method for retaining the fiber morphology without breaking the nanofiber mat. Here, we report on the impact of different aluminum foils on the physical and chemical properties of stabilized PAN nanofibers mats, and on the following incipient carbonization process at a temperature of max. 600 °C, i.e., below the melting temperature of aluminum. Full article

This study presents a method for predicting the local fiber orientation of veneers made from peeled Douglas-fir logs based on the knowledge of the tree branch characteristics (location, radius, insertion angle, azimuth angle, and living branch ratio). This model is based on the Rankine oval theory approach and focuses on the local deviation of the fiber orientation in the vicinity of knots. The local fiber orientation was measured online during the peeling process with an in-house-developed scanner based on the tracheid effect. Two logs from the same tree were peeled, and their ribbons were scanned. The knot locations and fiber orientation were deduced from the scanner data. The first objective was to compare the fiber orientation model with measurements to enhance and validate the model for French Douglas-fir. The second objective was to link data measurable on logs to veneer quality. Full article

The use of fiber-reinforced polymer (FRP) composite materials are continuously growing in civil infrastructure due to their high strength, low weight, and manufacturing flexibility. However, FRP is characterized by sudden failure and lacks ductility. When used in construction, gradual failure of FRP components is desired to avoid catastrophic structural collapse. Due to its mechanical orthotropy, the behavior of FRP relies significantly on fiber orientation and stacking sequence. In this paper, a novel multi-angled glass fiber reinforced polymer (GFRP) composite laminate showing pseudo ductile behavior is produced using 3D-printing. This is accomplished by varying fiber orientation angles, stacking sequence, and thickness of lamina. Single-angled GFRP composite specimens were 3D-printed with different fiber orientation angles of 0°, 12°, 24°, 30°, 45°, and 90° using continuous and fused filament techniques. The tension test results of the single-angled specimens were then used to aid the design of multi-angled laminate for potential progressive failure behavior. A 3D finite element (FE) model was developed to predict the response of the experimental results and to provide insight into the failure mechanism of the multi-angled laminate. The experimental observations and the FE simulations show the possibility of producing pseudo ductile FRP-by-design composite using 3D-printing technology, which leads the way to fabricate next-generation composites for civil infrastructure. Full article

One of the challenges of the century is to reach compatibility between the required resistance and the usage of lightweight building materials that may negatively affect the mechanical properties. Natural fibers nowadays are used as enhancers in the industrial field. Hence, the fibers contribute by giving an ideal solution to improve mechanical proprieties of the structural elements such as tensile and impact strength. In previous studies, the use of natural fibers as reinforcement in construction materials has increased. Natural fibers have a lot of characteristics such as being strong, lightweight, inexpensive, and eco-friendly. This paper aims to investigate the performance of banana fiber bars (BFB) as reinforced material. Through this study, the development and characterization of natural fibers-based composite beams were observed. After the beams were designed, several types of finite element analysis were conducted using ‘ANSYS’ nonlinear finite element program under one-point loading. Results show good correlations between experimental and predicted results. Full article