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Lubricants, Volume 13, Issue 6 (June 2025) – 16 articles

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25 pages, 10039 KiB  
Article
Microstructure, Mechanical Strength, and Tribological Behavior of B4C/WS2-Hybrid-Reinforced B319 Aluminum Matrix Composites
by Ufuk Tasci
Lubricants 2025, 13(6), 247; https://doi.org/10.3390/lubricants13060247 (registering DOI) - 29 May 2025
Abstract
Hybrid B319 aluminum matrix composites reinforced with 10 wt% B4C and varying WS2 contents were fabricated to improve mechanical and tribological performance. The composite containing 2 wt% WS2 showed the best overall results, with a 29% increase in microhardness [...] Read more.
Hybrid B319 aluminum matrix composites reinforced with 10 wt% B4C and varying WS2 contents were fabricated to improve mechanical and tribological performance. The composite containing 2 wt% WS2 showed the best overall results, with a 29% increase in microhardness (104.3 HV) and a 20% improvement in transverse rupture strength (196.3 MPa) compared to unreinforced B319. Additionally, the friction coefficient dropped by 64% (from 0.497 to 0.178), and the specific wear rate was reduced to 4.34 × 10−6 mm3/N·m. Microstructural analyses confirmed homogeneous reinforcement distribution and adequate interfacial bonding. These enhancements are attributed to the dual action of B4C-induced strengthening and WS2-mediated tribo-film formation, offering a promising solution for lightweight, wear-resistant components in engineering applications. Full article
26 pages, 7153 KiB  
Article
Dynamic Precision and Reliability of Multi-Link Linkages with Translational Pair Clearance
by Quanzhi Zuo, Mingyang Cai, Yuyang Lian, Jianuo Zhu and Shuai Jiang
Lubricants 2025, 13(6), 246; https://doi.org/10.3390/lubricants13060246 - 29 May 2025
Abstract
This study investigates the dynamic behavior and reliability of planar multi-link linkages with clearance in translational pairs. Using the Lagrange multiplier method, a dynamic model that accounts for clearance effects is developed. Furthermore, a reliability model is established by combining the first-order second-moment [...] Read more.
This study investigates the dynamic behavior and reliability of planar multi-link linkages with clearance in translational pairs. Using the Lagrange multiplier method, a dynamic model that accounts for clearance effects is developed. Furthermore, a reliability model is established by combining the first-order second-moment method with the stress-strength interference theory. Numerical simulations were performed to evaluate the impact of varying clearance sizes and driving speeds on motion errors and system reliability. This study also explores the nonlinear dynamics of the end-effector. The results indicate that increased clearance and higher driving speeds lead to certain changes in motion errors and operational reliability. Phase diagrams and Poincaré maps reveal directional differences in dynamic stability: chaotic motion along the X-direction and periodic oscillations along the Y-direction. These findings provide valuable insights for optimizing mechanism design and enhancing operational reliability. Full article
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14 pages, 4846 KiB  
Article
Study of Corrosion, Power Consumption, and Wear Characteristics of Herringbone-Grooved Fan Bearings in High-Temperature and High-Humidity Environments
by Jim-Chwen Yeh, Yu-Chang Lee, Chun-Hsiang Huang, Ming-Yuan Li and Chin-Chung Wei
Lubricants 2025, 13(6), 245; https://doi.org/10.3390/lubricants13060245 - 28 May 2025
Abstract
Fans are essential electronic components for heat dissipation in electronic systems, with fan bearings being critical parts that determine fan performance and lifespan. This paper investigates the corrosion, wear, power consumption, temperature, and vibration characteristics of a newly designed and manufactured powder metallurgy [...] Read more.
Fans are essential electronic components for heat dissipation in electronic systems, with fan bearings being critical parts that determine fan performance and lifespan. This paper investigates the corrosion, wear, power consumption, temperature, and vibration characteristics of a newly designed and manufactured powder metallurgy bearing with herringbone oil grooves for fans under high-humidity and high-temperature conditions. Corrosion experiments on iron–copper powder metallurgy bearings show that a higher environmental temperature and humidity result in greater corrosion current and reduced corrosion resistance. Bearings operated under high humidity (85% RH) and a high temperature (80 °C) for 0, 3, and 8 days, respectively, revealed that wear and corrosion occur simultaneously. The longer the operating time, the more significant the wear and corrosion. After 3 and 8 days, the lubricating oil flow in the oil grooves decreased by 9.8% and 51.5%, respectively. When bearings subjected to varying degrees of corrosion were tested under the same standard operating conditions, it was found that the bearings corroded for 3 and 8 days, resulting in a significant increase in the number of wear debris particles, higher RMS vibration values, and a power consumption increase of 6.9% and 7.8%, respectively. The percentage of iron elements on the surface gradually decreased, with the copper elements being the primary wear particles during the wear process. However, due to the increased clearance between the rotating shaft and the bearing caused by wear, the fan temperature slightly decreased with increased surface wear. Full article
(This article belongs to the Special Issue Recent Advances in Tribological Properties of Machine Tools)
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18 pages, 7950 KiB  
Article
Combined Effects of DLC Coating and Surface Texturing on Seizure and Friction in Reciprocating Sliding
by Slawomir Wos, Waldemar Koszela, Andrzej Dzierwa and Pawel Pawlus
Lubricants 2025, 13(6), 244; https://doi.org/10.3390/lubricants13060244 - 28 May 2025
Abstract
Surface texturing is designed to improve the functional properties of machine elements by generating dimples on the surface contacted. Friction and wear resistance can also be improved by creating diamond-like carbon (DLC) coatings. These two techniques were combined to extend the lifetime of [...] Read more.
Surface texturing is designed to improve the functional properties of machine elements by generating dimples on the surface contacted. Friction and wear resistance can also be improved by creating diamond-like carbon (DLC) coatings. These two techniques were combined to extend the lifetime of the elements and minimise friction in reciprocating conformal sliding contact. This work is functionally important for assemblies operating under high normal loads. Experiments were carried out in initially lubricated reciprocating sliding contact using an Optimol SRV 5 tribotester in the flat-on-flat configuration. The disc samples were untextured, laser textured, and DLC-coated untextured and textured. The combination of DLC coating and surface texturing caused an enhancement of the tribological performance of the sliding pair compared to that of untextured discs with and without DLC coating and textured discs without DLC coating. The DLC coating of the untextured disc caused a growth in the lifetime of a friction pair by a factor of 2.4. Seizure resistance also increased due to surface texturing of the steel disc for pit area ratios of 9 and 13%. Combining surface texturing with pit area ratios of 3 and 9% and DLC coating led to a decrease in the coefficients of friction of sliding pairs compared to only textured and coated discs. The DLC coating caused a decrease in the wear of the disc sample and reduction in wear levels of the counter samples in comparison to those of textured discs without DLC coatings. Full article
(This article belongs to the Special Issue Tribology of Textured Surfaces)
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28 pages, 11569 KiB  
Article
Optimization of Micro-Texture Parameters for Machine Tool Guide Rail Combination Based on Response Surface Methodology and Research on Its Anti-Friction and Lubrication Performance
by Youzheng Cui, Bingyang Yan, Minli Zheng, Haijing Mu, Chengxin Liu, Dongyang Wang, Xinmiao Li, Qingwei Li, Hui Jiang, Fengjuan Wang and Qingming Hu
Lubricants 2025, 13(6), 243; https://doi.org/10.3390/lubricants13060243 - 27 May 2025
Abstract
In the process of heavy-duty cutting, the reciprocating motion of the sliding guide pair surface is prone to local wear, which seriously affects the overall machining accuracy and service life of the machine tool. This study proposes a biomimetic micro-texture design scheme combining [...] Read more.
In the process of heavy-duty cutting, the reciprocating motion of the sliding guide pair surface is prone to local wear, which seriously affects the overall machining accuracy and service life of the machine tool. This study proposes a biomimetic micro-texture design scheme combining elliptical grooves and shell-shaped grooves on the surface of carp as biomimetic prototypes to enhance the oil film bearing capacity, drag reduction, and wear resistance of guide rail pairs. Based on Fluent fluid simulation research, it has been shown that this texture has a better dynamic pressure lubrication effect. We used response surface methodology to optimize the texture design parameters and further verify the accuracy of the optimal parameters with the NSGA-II genetic algorithm. The results show that under lubricated conditions, the load-bearing pressure of the combined micro-textured guide rail pair increased by 53.79%, the friction coefficient decreased by 39.04%, and the temperature decreased by 15.83%. This texture can still significantly improve drag reduction and wear resistance in a low-oil state. Full article
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20 pages, 10062 KiB  
Article
Experimental Study on Vibration Characteristics of Journal Bearing-Rotor System Under Base Roll and Pitch Motions
by Fangcheng Xu, Jiyu Wang, Kaidi Zhu, Guilong Wang, Jingwei Yi and Zhongliang Xie
Lubricants 2025, 13(6), 242; https://doi.org/10.3390/lubricants13060242 - 27 May 2025
Viewed by 121
Abstract
Currently, there is limited experimental research on the stability of journal bearing-rotor systems under base motion, and the influence of rocking motion on the stability of such systems remains unclear. This study develops an experimental test rig for a journal bearing-rotor system and [...] Read more.
Currently, there is limited experimental research on the stability of journal bearing-rotor systems under base motion, and the influence of rocking motion on the stability of such systems remains unclear. This study develops an experimental test rig for a journal bearing-rotor system and employs a six-degrees-of-freedom shaking table to apply complex alternating loads, with the aim of investigating the effects of rocking amplitude and frequency on the vibration characteristics of the shaft system. The experimental results show that, under the excitation of base roll and pitch motions, the critical speed of the sliding bearing-rotor system remains nearly unchanged, while the resonance amplitude increases significantly, and the instability speed occurs earlier. In addition, base rocking motion not only induces periodic and uniform changes in the vibration amplitude of the shaft system but also demonstrates a strong positive correlation between the amplitude of system vibration and the amplitude of base rocking. Full article
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16 pages, 4930 KiB  
Article
Trade-Off for CFRP Quality Using High-Frequency Ultrasonic-Assisted Drilling Under Lubricant Absence
by Khaled Hamdy and Saood Ali
Lubricants 2025, 13(6), 241; https://doi.org/10.3390/lubricants13060241 - 26 May 2025
Viewed by 65
Abstract
Carbon fiber reinforced polymers (CFRPs) are significantly vital for industries. However, the drilling process of a CFRP is considered a challenge due to its nature, which causes delamination, fiber pull-out, peel-up, high friction, and a decrease in cutting tool life. Wet drilling is [...] Read more.
Carbon fiber reinforced polymers (CFRPs) are significantly vital for industries. However, the drilling process of a CFRP is considered a challenge due to its nature, which causes delamination, fiber pull-out, peel-up, high friction, and a decrease in cutting tool life. Wet drilling is necessary for minimizing defects, and lubricants are very costly. In the current work, ultrasonic-assisted drilling (UAD) with a longitudinal vibration of 39.7 kHz was applied to the drill bit in the feed direction, used for CFRPs, and compared with conventional drilling (CD). Low spindle speeds under 5000 rpm were applied with different feed rates. The morphology, delamination factor, and cutting forces were investigated through the specific input machining parameters for CD and UAD. SEM was applied to study the morphology of the hole entrance and exit as well as the burr heights of evacuated chips. UAD with 39.7 kHz succeeded in minimizing the surface roughness by 50% compared with the surface roughness resulting from CD and could drill high-precision holes for CFRPs with a trade-off concept, besides achieving near-zero delamination (K ≃ 1) in the absence of a lubricant, which is being extended for industrial application. Full article
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17 pages, 2429 KiB  
Article
Experimental Investigation on Cutting Forces in Sustainable Hard Milling of Hardox 500 Steel Under Al2O3/MoS2 Hybrid Nanofluid MQCL Environment
by Tran The Long
Lubricants 2025, 13(6), 240; https://doi.org/10.3390/lubricants13060240 - 26 May 2025
Viewed by 124
Abstract
Hardox 500 is a special low-alloy, martensitic steel possessing extraordinary wear resistance, high hardness, and high ductility; thus, it has been widely used in many industrial applications. Nevertheless, this type of steel has a low machinability and is grouped among the difficult-to-machine materials. [...] Read more.
Hardox 500 is a special low-alloy, martensitic steel possessing extraordinary wear resistance, high hardness, and high ductility; thus, it has been widely used in many industrial applications. Nevertheless, this type of steel has a low machinability and is grouped among the difficult-to-machine materials. Hence, this paper’s objective was to study its hard milling performance under minimum quantity cooling lubrication (MQCL) conditions using an Al2O3/MoS2 hybrid nano cutting oil. The Box–Behnken response surface methodology was used to investigate the effects of the nanoparticle concentration (NC), cutting speed (v), and feed rate (f) on the total cutting force F and cutting force coefficient Fy/Fz. The obtained results indicate that the cutting efficiency of Hardox 500 steel was improved thanks to the enhancement in cooling lubrication from the MQCL using the Al2O3/MoS2 hybrid nano cutting oil. The applicability of vegetable oil and coated carbide inserts is thus extended to the hard milling of difficult-to-cut materials. Moreover, the provision of the appropriate ranges and optimal set of investigated variables obtained in this paper will be useful guides for technologists and further studies. Concretely, NC = 0.5–0.7%, v = 110–115 m/min, and f = 0.08–0.10 mm/tooth are the optimal set for the total cutting force F, while NC = 0.5%, v = 138–140 m/min, and f = 0.08–0.09 mm/tooth are suggested for the cutting force coefficient Fy/Fz. Full article
(This article belongs to the Special Issue Recent Advances in Tribological Properties of Machine Tools)
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18 pages, 5787 KiB  
Article
Use of Advanced Piston Ring Coatings on Agricultural Engines
by Xiaochao He, Bang Liu, Eduardo Tomanik, Grzegorz Koszalka and Anna Orlova
Lubricants 2025, 13(6), 239; https://doi.org/10.3390/lubricants13060239 - 26 May 2025
Viewed by 307
Abstract
The use of combustion engines on agricultural vehicles will persist much longer than on-road vehicles. Introducing new technologies in agricultural engines is crucial to mitigating emissions while accounting for customer cost-sensitivity, harsh operation conditions, and typically sub-optimal maintenance. This work describes the use [...] Read more.
The use of combustion engines on agricultural vehicles will persist much longer than on-road vehicles. Introducing new technologies in agricultural engines is crucial to mitigating emissions while accounting for customer cost-sensitivity, harsh operation conditions, and typically sub-optimal maintenance. This work describes the use of CrN and tetrahedral amorphous carbon (ta-C) DLC-coated rings in small agricultural diesel engines. Compared with the gas nitride rings, the CrN and the ta-C DLC coatings exhibited, respectively, 74% and 86% lower wear in rig tests. The DLC also presented a very low coefficient of friction and high resistance to scuffing. A similar wear trend was observed on durability engine tests, where the CrN top ring showed an 80% lower wear rate than the GNS used in a similar engine. Wear on the DLC oil ring was below the measurement capability. Liner radial wear was measured on the piston ring reversal points in four angular positions, and except for one position, was lower than 3 µm. At the end of the test, engine performance and emissions are nearly identical to those at the test’s start, demonstrating that the use of advanced tribological solutions can significantly contribute to emissions mitigation in agricultural engines. Full article
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15 pages, 5949 KiB  
Article
The Influence of Graphite Orientation on the Current-Carrying Friction Performance of Copper–Graphite Composite Materials
by Zhenghai Yang, Wenbo Li, Yingjian Song, Xiaomeng Zheng and Yongzhen Zhang
Lubricants 2025, 13(6), 238; https://doi.org/10.3390/lubricants13060238 - 26 May 2025
Viewed by 132
Abstract
In response to the need to optimize the performance of copper–graphite current-carrying friction materials, spark plasma sintering (SPS) technology was used to prepare copper–graphite composite materials with different graphite orientations. A self-made current-carrying friction testing machine was used to study the effect of [...] Read more.
In response to the need to optimize the performance of copper–graphite current-carrying friction materials, spark plasma sintering (SPS) technology was used to prepare copper–graphite composite materials with different graphite orientations. A self-made current-carrying friction testing machine was used to study the effect of graphite orientation on the current-carrying friction performance of copper–graphite composites. The results showed that as the graphite orientation increased, the current-carrying friction performance of the copper–graphite composites initially improved and then deteriorated. The performance was optimal when the graphite orientation of the 7.5 wt% graphite–copper composite was 90°, primarily constrained by the wear rate. The main wear mechanism was furrowing, and graphite enrichment occurred on the worn surface, where the graphite content on the wear surface was higher than that in the bulk material. The degree of enrichment varied under different wear mechanisms. The graphite content near the entry region of the friction surface was significantly lower than that near the exit region. Full article
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22 pages, 7683 KiB  
Article
Surface Characterization of Cylinder Liner–Piston Ring Friction Pairs Under Different Temperature and Load by Power Spectral Density Method
by Xiaori Liu, Xiaofei Cao, Xuan Ma and Menghan Li
Lubricants 2025, 13(6), 237; https://doi.org/10.3390/lubricants13060237 - 25 May 2025
Viewed by 171
Abstract
Piston ring–cylinder liner is one of the most important friction pairs in internal combustion engines. The surfaces of the piston ring and the cylinder liner are affected by high temperature and high pressure, and the influence mechanism of temperature and pressure on their [...] Read more.
Piston ring–cylinder liner is one of the most important friction pairs in internal combustion engines. The surfaces of the piston ring and the cylinder liner are affected by high temperature and high pressure, and the influence mechanism of temperature and pressure on their microscopic morphology parameters is yet to be revealed. In this paper, high temperature friction and wear experiments on the piston ring and cylinder liner are carried out to obtain the microscopic morphology of the cylinder liner and piston ring at different temperatures and pressures, and their changes under different temperatures and pressures are investigated by using two methods, namely, fractal dimension and three-dimensional surface roughness characterization. The results show that, as the temperature increases, the texture patterns on the cylinder liner’s friction surface become simpler, with the fractal dimension showing a decreasing trend while the roughness shows an increasing trend. Compared to the condition at 80 °C, the surface roughness (Sa) of the cylinder liner increased by approximately 58.43% at 190 °C, while that of the piston ring increased by about 96.5%. With increasing pressure, both the fractal dimension and the roughness of the friction surface first decrease and then increase. Full article
(This article belongs to the Special Issue Thermal Hydrodynamic Lubrication)
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17 pages, 3922 KiB  
Article
Effect of Post-Aging on Laser-Boronized Surface of 18Ni-300 Maraging Steel with Hypoeutectic Structure
by Jelena Škamat, Olegas Černašėjus, Kęstutis Bučelis and Oleksandr Kapustynskyi
Lubricants 2025, 13(6), 236; https://doi.org/10.3390/lubricants13060236 - 25 May 2025
Viewed by 146
Abstract
Laser-boronized parts manufactured by a selective laser melting process from 18Ni to 300 maraging steel are investigated in this study. Two main issues are addressed, namely (i) the possibility to restore the hardness of the heat-affected zone (HAZ) formed during laser processing and [...] Read more.
Laser-boronized parts manufactured by a selective laser melting process from 18Ni to 300 maraging steel are investigated in this study. Two main issues are addressed, namely (i) the possibility to restore the hardness of the heat-affected zone (HAZ) formed during laser processing and (ii) the effect of re-aging on the hardness and wear resistance of the laser-boronized layer with a hypoeutectic structure. Optical microscopy, scanning electron microscopy, energy-dispersive spectroscopy, X-ray diffraction analysis, microhardness measurements, the “ball-on-plate” dry sliding test, and the two-body dry abrasive wear test were employed to answer the questions. The results confirmed that HAZ is formed with the dissolution of intermetallides formed before and undergo full (near the molten pool) or partial (at some distance from the molten pool) iron–base matrix recrystallization. The hardness of HAZ (350–550 HK0.05) has been restored after re-aging to the 550–600 HK0.05 level. Moreover, a certain positive effect of re-aging on the laser-boronized layer with a hardness of ~470–750 HK0.2 is established, associated with structural transformations induced by aging in the iron-based solid solution phase. The hardness increased by ~9–25%. The wear resistance of the hardest boronized samples (~750 HK0.2) under dry sliding and dry abrasive wear conditions was ~5.8 times and 3.7 times higher than that of the aged control sample, while re-aging provided further improvement of these characteristics. The presented results provide insights into the effectiveness of laser-boronized layers having a hypoeutectic structure in terms of increasing the wear resistance of maraging steel. Full article
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33 pages, 7667 KiB  
Article
Development of a Non-Uniform Heat Source Model for Accurate Prediction of Wheel Tread Temperature on Long Downhill Ramps
by Jinyu Zhang, Jingxian Ding and Jianyong Zuo
Lubricants 2025, 13(6), 235; https://doi.org/10.3390/lubricants13060235 - 24 May 2025
Viewed by 102
Abstract
Accurately simulating the thermal behavior of wheel–brake shoe friction on long downhill ramps is challenging due to the complexity of modeling appropriate heat source models. This study investigates heat generation during the frictional braking process of freight train wheels and brake shoes under [...] Read more.
Accurately simulating the thermal behavior of wheel–brake shoe friction on long downhill ramps is challenging due to the complexity of modeling appropriate heat source models. This study investigates heat generation during the frictional braking process of freight train wheels and brake shoes under long-slope conditions. Four heat source models—constant, modified Gaussian, sinusoidal, and parabolic distributions—were developed based on energy conservation principles and validated through experimental data. A thermomechanical coupled finite element model was established, incorporating a moving heat source to analyze the effects of different models on wheel tread temperature distribution and its evolution over time. The results show that all four models effectively simulate frictional heat generation, with computed temperatures, deviating by only 6.0–8.2% from experimental measurements, confirming their accuracy and reliability. Among the models, the modified Gaussian distribution heat source, with its significantly higher peak local heat flux (2.82 times that of the constant model) and rapid attenuation, offers the most precise simulation of the non-uniform temperature distribution in the contact region. This leads to a 40% increase in the temperature gradient variation rate and effectively reproduces the “hot spot” effect. The new non-uniform heat source model accurately captures local temperature dynamics and predicts frictional heat transfer and thermal damage trends. The modified Gaussian distribution model outperforms others in simulating local temperature peaks, offering support for optimizing braking system models and improving thermal damage prediction. Future research will refine this model by incorporating factors like material wear, environmental conditions, and dynamic contact characteristics. Full article
(This article belongs to the Special Issue Tribology in Railway Engineering)
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16 pages, 4064 KiB  
Article
The Importance of Fiber Orientation for the Performance of High-Performance Polymer-Based Hybrid Materials in Sliding Contact with Steel
by Alois K. Schlarb, Miaozi Huang, Yao Xu, Chi Hua and Leyu Lin
Lubricants 2025, 13(6), 234; https://doi.org/10.3390/lubricants13060234 - 24 May 2025
Viewed by 180
Abstract
The properties of composite materials depend not only on the composition but also on the distribution and orientation of the fillers, i.e., on the internal material architecture. Using the example of two differently composed PEEK-based hybrid materials, the influence of fiber orientation on [...] Read more.
The properties of composite materials depend not only on the composition but also on the distribution and orientation of the fillers, i.e., on the internal material architecture. Using the example of two differently composed PEEK-based hybrid materials, the influence of fiber orientation on the tribological behavior of these materials in sliding contact with steel was investigated. The tribological performance of these composites was assessed using a pin-on-disc (PoD) tribometer, testing in a pv range from 0.25 to 32 MPa·m/s. The findings indicate that the printed specimens exhibit a high degree of fiber orientation aligned parallel to the printing paths. Conversely, the injection-molded samples display a three-layered structure across the thickness, with fibers in the skin layers aligned parallel to the injection direction but perpendicular to it in the core. These variations in morphology are evident in both the mechanical properties and the tribological behavior. To describe the influence of the fiber orientation on tribological properties, a model is proposed that allows the prediction of tribological properties for any fiber orientation. Although fiber orientation appears to be the dominant factor in tribological behavior, there is also a clear influence of additional fillers. Full article
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13 pages, 13643 KiB  
Article
Effect of Quenching Temperature on Microstructure and Wear Resistant Properties of Mo2FeB2 Cermet Coating
by Hao Zhang, Yongqi Hu and Yang Zhang
Lubricants 2025, 13(6), 233; https://doi.org/10.3390/lubricants13060233 - 23 May 2025
Viewed by 156
Abstract
H13 steel, a widely used material in hot work tooling, faces premature failure due to insufficient hardness and wear resistance. To address this limitation, Mo2FeB2 cermet coatings were fabricated on H13 alloy steel via plasma spray welding, and subsequently quenched [...] Read more.
H13 steel, a widely used material in hot work tooling, faces premature failure due to insufficient hardness and wear resistance. To address this limitation, Mo2FeB2 cermet coatings were fabricated on H13 alloy steel via plasma spray welding, and subsequently quenched at 850 °C, 1000 °C, and 1150 °C. The effects of the quenching temperature on the microstructure and wear resistance were investigated using optical microscopy (OM) for cross-sectional morphology, scanning electron microscopy (SEM) for microstructural and wear surface analyses, energy-dispersive spectroscopy (EDS) for elemental composition analysis, and X-ray diffraction (XRD) for phase identification. The coating primarily consisted of α-Fe, Mo2FeB2, (Mo,Fe,Cr)3B2, and Fe23(B,C)6 phases. Increasing the temperature to 1150 °C increased the Mo2FeB2 hard phase and elevated microhardness by 32.04% (from 827 HV0.5 to 1092 HV0.5). Wear resistance improved by 46.38% (mass loss reduced from 6.9 mg to 3.7 mg). The main wear mechanism was identified as abrasive wear due to the spalling of hard phase particles. These results demonstrate that optimizing quenching temperature enhances the hardness and wear resistance in Mo2FeB2 coatings, offering a viable strategy to extend H13 steel service life in high-temperature industrial applications. Full article
(This article belongs to the Special Issue Wear-Resistant Coatings and Film Materials)
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27 pages, 5523 KiB  
Review
Tribological Aspects of Graphene and Its Derivatives
by Çağla Gizem Acar and Audrius Žunda
Lubricants 2025, 13(6), 232; https://doi.org/10.3390/lubricants13060232 - 22 May 2025
Viewed by 262
Abstract
Tribology is the branch of science and engineering that focuses on understanding friction, wear, and lubrication, which is essential for saving energy, improving performance, reducing vibration, and creating eco-friendly lubricants and wear resistance. Over the past decade, nanomaterials have captured the immense interest [...] Read more.
Tribology is the branch of science and engineering that focuses on understanding friction, wear, and lubrication, which is essential for saving energy, improving performance, reducing vibration, and creating eco-friendly lubricants and wear resistance. Over the past decade, nanomaterials have captured the immense interest of tribology science. This review aimed to analyze how graphene and its derivatives can be incorporated into lubricants to enhance their properties, particularly in mitigating friction and wear. This is due to graphene’s excellent specific properties, such as a low friction coefficient, mechanical strength, high thermal and electrical conductivity, biocompatibility, high load-carrying capacity, wear resistance, and chemical stability. This study briefly introduces graphite, graphene, and graphene oxide, as well as presents graphene as a material for tribological applications. Among other things, the environmentally friendly possibilities of chemical reduction of reduced graphene oxide are analyzed here, as well as the macro-, micro-, and nano-tribological examination of graphene and its derivatives. Despite what is already known about graphene in tribology, further research is needed to gain a deeper understanding of development regarding integration with different materials, long-term performance, eco-friendly synthesis using green reducing agents, and comprehending how these approaches may affect systems at various scales. Full article
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