C, Volume 9, Issue 3
2023 September - 27 articles
Cover Story: In this work, a statistical evaluation of the main parameters influencing the synthesis of graphite oxides (GrO) using the Tour method is carried out. A screening experimental design is carried out, using temperature, time and the amounts of KMnO4 and H2O2 as variables. Specific surface area (SSA), porosity and carbon content (%C) are chosen as responses, since they are decisive characteristics in adsorption-related applications. After statistical evaluation of all the results (obtained using the Brunauer–Emmett–Teller method, Elemental Analysis, Scanning Electron Microscopy, X-Ray Diffraction and Raman), it is concluded that temperature is the most influential factor. Higher temperatures result in more exfoliated GrO, with higher SSA, smaller crystal size and lower %C. View this paper - Issues are regarded as officially published after their release is announced to the table of contents alert mailing list .
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