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Separations, Volume 9, Issue 1

January 2022 - 20 articles

Cover Story: Natural phenols and phenolic acids are widespread in the plant kingdom, and the dietary sources include fruits and beverages derived from them. These compounds have been widely investigated for their beneficial effects on human health, and several analytical methods have been developed for their determination in these matrices. The GC-MS method presented here involves the derivatization of aromatic carboxylic acids and phenols with ethyl chloroformate; it is particularly advantageous as it can be carried out in aqueous media at room temperature, allowing excellent separation of many different phenolic compounds. This method has been used for the analysis of commercial fruit juices particularly rich in phenolic compounds. Among them, the richest in free aromatic carboxylic acids and phenols are those containing cranberry. View this paper
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Articles (20)

  • Feature Paper
  • Article
  • Open Access
7 Citations
3,753 Views
21 Pages

Steam and Pressure Management for the Conversion of Steelworks Arising Gases to H2 with CO2 Capture by Stepwise Technology

  • Francesco Sebastiani,
  • Leonie Lucking,
  • Marija Sarić,
  • Jebin James,
  • Jurriaan Boon,
  • H. J. A. Eric van Dijk,
  • Paul Cobden and
  • Johannis A. Z. Pieterse

Steel production is a main source of CO2 emissions globally. These emissions must be drastically reduced to meet climate change mitigation goals. STEPWISE is a Sorption Enhanced Reactive Process (SERP) technology that converts steel works arising gas...

  • Article
  • Open Access
14 Citations
3,422 Views
13 Pages

Distribution and Estrogenic Risk of Alkylphenolic Compounds, Hormones and Drugs Contained in Water and Natural Surface Sediments, Morelos, Mexico

  • José Gustavo Ronderos-Lara,
  • Hugo Saldarriaga-Noreña,
  • Mario Alfonso Murillo-Tovar,
  • Laura Alvarez,
  • Josefina Vergara-Sánchez,
  • Victor Barba and
  • Jorge Antonio Guerrero-Alvarez

This study evaluated the distribution and potential estrogenic risk of the presence of bisphenol A (BPA), 4-nonylphenol (4NP), naproxen (NPX), ibuprofen (IBU), 17-β-estradiol (E2) and 17-α-ethinylestradiol (EE2) in water and sediments of t...

  • Review
  • Open Access
35 Citations
7,717 Views
33 Pages

Novel Applications of Microextraction Techniques Focused on Biological and Forensic Analyses

  • Cristian D’Ovidio,
  • Martina Bonelli,
  • Enrica Rosato,
  • Angela Tartaglia,
  • Halil İbrahim Ulusoy,
  • Victoria Samanidou,
  • Kenneth G. Furton,
  • Abuzar Kabir,
  • Imran Ali and
  • Fabio Savini
  • + 2 authors

In recent years, major attention has been focused on microextraction procedures that allow high recovery of target analytes, regardless of the complexity of the sample matrices. The most used techniques included liquid-liquid extraction (LLE), solid-...

  • Review
  • Open Access
23 Citations
9,753 Views
21 Pages

Hypericum spp.—An Overview of the Extraction Methods and Analysis of Compounds

  • Valentin Ion,
  • Irina Ielciu,
  • Anca-Gabriela Cârje,
  • Daniela Lucia Muntean,
  • Gianina Crişan and
  • Ramona Păltinean

The Hypericum genus contains one of the few genera of flowering plants that contains a species with authorization for marketing as a traditional medicine, H. perforatum. Due to the fact that this is a large genus, comprising numerous species, a large...

  • Article
  • Open Access
3 Citations
4,037 Views
14 Pages

Targeted UHPLC-ESI-MS/MS Analysis of Selected Neurotransmitters, Tryptophan and Its Metabolite Kynurenine in Tau Transgenic Rat Brain Tissue: A Pivotal Study

  • Juraj Piestansky,
  • Andrea Forgacsova,
  • Dominika Olesova,
  • Jaroslav Galba,
  • Peter Mikus,
  • Petra Majerova and
  • Andrej Kovac

Neurotransmitters (NT) are widely distributed in the central nervous system. These molecules are important for many physiological processes and the function of the immune system. Imbalance of NT are linked to numerous neurological disorders and disea...

  • Article
  • Open Access
2 Citations
2,859 Views
10 Pages

Sensitivity Increase in Headspace Analysis of Hydrocarbons in Water by Using Online Selective Elimination of Gas Extractant

  • Oleg V. Rodinkov,
  • Alexey Y. Pisarev,
  • Leonid N. Moskvin,
  • Aleksandra S. Bugaichenko and
  • Pavel N. Nesterenko

In this study, a novel approach in headspace gas chromatographic analysis using the selective absorption of the gas extractant during concentration of the analytes was developed. The carbon dioxide used as the gas extractant was removed from the samp...

  • Review
  • Open Access
12 Citations
4,883 Views
23 Pages

State of the Art in Separation Processes for Alternative Working Fluids in Clean and Efficient Power Generation

  • Odi Fawwaz Alrebei,
  • Abdulkarem I. Amhamed,
  • Muftah H. El-Naas,
  • Mahmoud Hayajnh,
  • Yasmeen A. Orabi,
  • Ward Fawaz,
  • Ahmad S. Al-tawaha and
  • Agustin Valera Medina

Gas turbines must now comply with much stricter emission control regulations. In fact, to combat the greenhouse effect, regulatory authorities have drastically reduced allowable emission levels. For example, in less than 12 years, the United States&r...

  • Article
  • Open Access
4 Citations
3,736 Views
15 Pages

Escherichia coli are common pathogens, whereas E. coli O157:H7 is the most notorious E. coli strain, owing to its high virulence that can cause serious adverse effects and death. E. coli contains abundant peroxidases. Thus, the presence of E. coli ca...

  • Communication
  • Open Access
2 Citations
4,240 Views
11 Pages

The former St. Antony’s Lead Works site, now the central part of an urban recreational park (Walker Riverside Park) in the east end of Newcastle upon Tyne (England, UK), has been assessed based on the Pb concentration in topsoil according to re...

  • Article
  • Open Access
2 Citations
3,621 Views
15 Pages

A Novel and Green Method for Turning Food Waste into Environmentally-Friendly Organic Deicing Salts: Enhanced VFA Production through AnMBR

  • Qiuhong Xiang,
  • Kunlun Yang,
  • Ziwen Chen,
  • Manman Li,
  • Yuanqi Zhang,
  • Xiaorui Wang,
  • Yingying Jiang,
  • Peng Gu and
  • Hengfeng Miao

In order to improve the production efficiency of volatile fatty acids (VFAs) by anaerobic fermentation of food waste and reduce the cost for the production of organic deicing salt (ODS), ceramic microfiltration (MF) membrane separation was applied in...

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Separations - ISSN 2297-8739