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Molecules, Volume 2, Issue 10 (October 1997) – 18 articles , Pages 152-157, Articles M27-M39

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Open AccessBook Review
Comprehensive Polymer Science. By S. L. Aggarwal
Molecules 1997, 2(10), 157; https://doi.org/10.3390/21000157 - 31 Oct 1997
Viewed by 3148
Abstract
This final supplement to the excellent series of Comprehensive Polymer Science books is fully up to the high standard set by the originals.[...] Full article
Open AccessBook Review
Advances in Chemistry of Insect Control, Vol 3. By G.G. Briggs
Molecules 1997, 2(10), 156; https://doi.org/10.3390/21000156 - 31 Oct 1997
Viewed by 2943
Abstract
This monograph contains 18 lectures given by the experts in their field at the Symposium Advances in the Chemistry of Insect Control", held at Queens, College Cambridge, on 18-21 July 1993.[...] Full article
Open AccessBook Review
Online Searching: A Scientist's Perspective. Damon D. Ridley
Molecules 1997, 2(10), 155; https://doi.org/10.3390/21000155 - 31 Oct 1997
Viewed by 3823
Abstract
In order to be of any use computer software must be either easy to use or be supported by very well written manuals. Unfortunately, STN (previously CAS-Online) is neither.[...] Full article
Open AccessBook Review
Guidebook on Molecular Modeling in Drug Design. By N. C. Cohen
Molecules 1997, 2(10), 154; https://doi.org/10.3390/21000154 - 31 Oct 1997
Viewed by 3155
Abstract
This book is intended as a "guide for advanced students and chemists entering the field of molecular modeling".[...] Full article
Open AccessBook Review
Alkaloids: Chemical & Biological Perspectives. Vol. 10. By S.W. Pelletier
Molecules 1997, 2(10), 153; https://doi.org/10.3390/21000153 - 31 Oct 1997
Viewed by 2958
Abstract
This volume provides four excellent reviews refereed at least by one expert in the field.[...] Full article
Open AccessBook Review
Purification of Laboratory Chemicals, Fourth Edition. By W. L. F. Armarego
by R. Read
Molecules 1997, 2(10), 152; https://doi.org/10.3390/21000152 - 31 Oct 1997
Cited by 3 | Viewed by 3564
Open AccessShort Note
5-Methoxy-7,7-dimethyl-1,9(E),11-dodecatrien-3-one
Molecules 1997, 2(10), M39; https://doi.org/10.3390/M39 - 31 Oct 1997
Cited by 1 | Viewed by 1826
Abstract
Although the title compound has already been prepared in four steps [1] or three steps [2] from D-galactose, this selective tosylation consists of only a two step synthesis avoiding the preparation of several intermediates and affording much higher overall yields. Moreover, NMR spectral [...] Read more.
Although the title compound has already been prepared in four steps [1] or three steps [2] from D-galactose, this selective tosylation consists of only a two step synthesis avoiding the preparation of several intermediates and affording much higher overall yields. Moreover, NMR spectral data of the title compound have not yet been published.[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
Open AccessShort Note
5-Methoxy-7,7-dimethyl-1,9(E),11-dodecatrien-3-ol
Molecules 1997, 2(10), M37; https://doi.org/10.3390/M37 - 31 Oct 1997
Viewed by 1768
Abstract
To a stirred solution of the diene aldehyde [1] in dry THF under Ar at -78 ƒC, vinylmagnesium bromide in THF was added via a syringe.[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
Open AccessShort Note
3-Methoxy-5,5-dimethyl-7(E),9-decadiena
Molecules 1997, 2(10), M36; https://doi.org/10.3390/M36 - 31 Oct 1997
Cited by 1 | Viewed by 1858
Abstract
Using the Collins oxidation procedure previously described [1], the title aldehyde was prepared from the diene alcohol [2] as a colorless oil in 76% yield.[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
Open AccessShort Note
3-Methoxy-5,5-dimethyl-7(E),9-decadien-1-o1
Molecules 1997, 2(10), M35; https://doi.org/10.3390/M35 - 31 Oct 1997
Cited by 1 | Viewed by 1807
Abstract
To a slurry of LAH (65 mg, 1.7 mmol) in ether (4 ml) at 0 ƒC under Ar, the diene ester [1] (487 mg, 1.7 mmol) in ether (5 ml) was added dropwise.[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
Open AccessShort Note
tert-Butyl-3-methoxy-5,5-dimethyl-7(E),9-decadienoate
Molecules 1997, 2(10), M34; https://doi.org/10.3390/M34 - 31 Oct 1997
Cited by 1 | Viewed by 1770
Abstract
The diastereomeric alcohols [1], either separately or as a mixture, were converted under acidic Peterson olefination conditions to the title E-diene.[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
Open AccessShort Note
tert-Butyl-3-methoxy-5,5-dimethyl-7-hydroxy-8-trimethylsilyl-9-decenoate
Molecules 1997, 2(10), M33; https://doi.org/10.3390/M33 - 31 Oct 1997
Cited by 1 | Viewed by 1728
Abstract
The crude aldehyde, tert-butyl-3-methoxy-5,5-dimethyl-7-oxo-heptanoate [1] was treated with pinacol E-1-trimethylsilyl-1-propene-3-boronate [2] in petroleum ether at room temperature to provide a 50% yield of the diastereomeric boronic esters, which were simultaneously cleaved to the alcohols and readily separated by flash chromatography.[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
Open AccessShort Note
tert-Butyl-3-methoxy-5,5-dimethyl-7-oxo-heptanoate
Molecules 1997, 2(10), M32; https://doi.org/10.3390/M32 - 31 Oct 1997
Cited by 2 | Viewed by 1740
Abstract
Hydroboration of tert-butyl-3-methoxy-5,5-dimethyl-6-heptenoate [1] with either BH3…THF or BH3…Me2S provided the terminal alcohol tert-butyl-3-methoxy-5,5-dimethyl-7-hydroxy-heptanoate, in unoptimized, nonreproducable and disappointingly low 30% yield [2].[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
Open AccessShort Note
tert-Butyl-3-methoxy-5,5-dimethyl-7-hydroxy-heptanoate
Molecules 1997, 2(10), M31; https://doi.org/10.3390/M31 - 31 Oct 1997
Cited by 1 | Viewed by 1711
Abstract
Hydroboration of tert-butyl-3-methoxy-5,5-dimethyl-6-heptenoate [1] with either BH3ÖTHF or BH3ÖMe2S provided the terminal alcohol title compound, in unoptimized, nonreproducable and disappointingly low 30% yield.[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
Open AccessShort Note
tert-Butyl-3-methoxy-5,5-dimethyl-6-heptenoate
Molecules 1997, 2(10), M30; https://doi.org/10.3390/M30 - 31 Oct 1997
Cited by 2 | Viewed by 1724
Abstract
Preparation of the title compound from the hydroxy ester [1] proved difficult to impossible with almost all protecting groups under a variety of reaction conditions.[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
Open AccessShort Note
tert-Butyl-3-hydroxy-5,5-dimethyl-6-heptenoate
Molecules 1997, 2(10), M29; https://doi.org/10.3390/M29 - 31 Oct 1997
Cited by 1 | Viewed by 1702
Abstract
As part of our continuing studies of stereocontrol during the intramolecular Diels-Alder (IMDA) reaction leading to medium rings [1-3], we have targeted poitediol [4] as a structure of interest accessible through this technology.[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
Open AccessShort Note
2-Hydroxy-3-bromo-5-nitrophenylbis(5-methylfur-2-yl)methane
Molecules 1997, 2(10), M27; https://doi.org/10.3390/M27 - 31 Oct 1997
Viewed by 2489
Abstract
See also [1, 2].[...] Full article
(This article belongs to the Section Medicinal Chemistry)
Open AccessShort Note
2-Bromophenylbis(5-methylfur-2-yl)methane
Molecules 1997, 2(10), M28; https://doi.org/10.3390/M28 - 01 Oct 1997
Viewed by 2068
Abstract
See also [1,2]. To the solution of 2-bromobenzaldehyde (18.5 g, 100 mmol) and sylvan (20 ml, 250 mmol) in 100 ml of benzene 5 ml of Me3SiCl was added at room temperature.[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
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