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Molecules, Volume 2, Issue 10 (October 1997), Pages 152-157, Articles M27-M39

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Open AccessBook Review Comprehensive Polymer Science. By S. L. Aggarwal
Molecules 1997, 2(10), 157; https://doi.org/10.3390/21000157
Received: 17 September 1997 / Published: 31 October 1997
Viewed by 2637 | PDF Full-text (3 KB) | HTML Full-text | XML Full-text
Abstract
This final supplement to the excellent series of Comprehensive Polymer Science books is fully up to the high standard set by the originals.[...] Full article
Open AccessBook Review Advances in Chemistry of Insect Control, Vol 3. By G.G. Briggs
Molecules 1997, 2(10), 156; https://doi.org/10.3390/21000156
Received: 17 September 1997 / Published: 31 October 1997
Viewed by 2531 | PDF Full-text (3 KB) | HTML Full-text | XML Full-text
Abstract
This monograph contains 18 lectures given by the experts in their field at the Symposium Advances in the Chemistry of Insect Control", held at Queens, College Cambridge, on 18-21 July 1993.[...] Full article
Open AccessBook Review Online Searching: A Scientist's Perspective. Damon D. Ridley
Molecules 1997, 2(10), 155; https://doi.org/10.3390/21000155
Received: 17 September 1997 / Published: 31 October 1997
Viewed by 3435 | PDF Full-text (4 KB) | HTML Full-text | XML Full-text
Abstract
In order to be of any use computer software must be either easy to use or be supported by very well written manuals. Unfortunately, STN (previously CAS-Online) is neither.[...] Full article
Open AccessBook Review Guidebook on Molecular Modeling in Drug Design. By N. C. Cohen
Molecules 1997, 2(10), 154; https://doi.org/10.3390/21000154
Received: 17 September 1997 / Published: 31 October 1997
Viewed by 2714 | PDF Full-text (3 KB) | HTML Full-text | XML Full-text
Abstract
This book is intended as a "guide for advanced students and chemists entering the field of molecular modeling".[...] Full article
Open AccessBook Review Alkaloids: Chemical & Biological Perspectives. Vol. 10. By S.W. Pelletier
Molecules 1997, 2(10), 153; https://doi.org/10.3390/21000153
Received: 17 September 1997 / Published: 31 October 1997
Viewed by 2549 | PDF Full-text (3 KB) | HTML Full-text | XML Full-text
Abstract
This volume provides four excellent reviews refereed at least by one expert in the field.[...] Full article
Open AccessBook Review Purification of Laboratory Chemicals, Fourth Edition. By W. L. F. Armarego
Molecules 1997, 2(10), 152; https://doi.org/10.3390/21000152
Published: 31 October 1997
Cited by 2 | Viewed by 2971 | PDF Full-text (4 KB) | HTML Full-text | XML Full-text
Open AccessShort Note 5-Methoxy-7,7-dimethyl-1,9(E),11-dodecatrien-3-one
Molecules 1997, 2(10), M39; https://doi.org/10.3390/M39
Received: 29 September 1997 / Published: 31 October 1997
Cited by 1 | Viewed by 1696 | Supplementary Files
Abstract
Although the title compound has already been prepared in four steps [1] or three steps [2] from D-galactose, this selective tosylation consists of only a two step synthesis avoiding the preparation of several intermediates and affording much higher overall yields. Moreover, NMR spectral
[...] Read more.
Although the title compound has already been prepared in four steps [1] or three steps [2] from D-galactose, this selective tosylation consists of only a two step synthesis avoiding the preparation of several intermediates and affording much higher overall yields. Moreover, NMR spectral data of the title compound have not yet been published.[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
Open AccessShort Note 5-Methoxy-7,7-dimethyl-1,9(E),11-dodecatrien-3-ol
Molecules 1997, 2(10), M37; https://doi.org/10.3390/M37
Received: 29 September 1997 / Published: 31 October 1997
Viewed by 1638 | Supplementary Files
Abstract
To a stirred solution of the diene aldehyde [1] in dry THF under Ar at -78 ƒC, vinylmagnesium bromide in THF was added via a syringe.[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
Open AccessShort Note 3-Methoxy-5,5-dimethyl-7(E),9-decadiena
Molecules 1997, 2(10), M36; https://doi.org/10.3390/M36
Received: 29 September 1997 / Published: 31 October 1997
Cited by 1 | Viewed by 1726 | Supplementary Files
Abstract
Using the Collins oxidation procedure previously described [1], the title aldehyde was prepared from the diene alcohol [2] as a colorless oil in 76% yield.[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
Open AccessShort Note 3-Methoxy-5,5-dimethyl-7(E),9-decadien-1-o1
Molecules 1997, 2(10), M35; https://doi.org/10.3390/M35
Received: 29 September 1997 / Published: 31 October 1997
Cited by 1 | Viewed by 1689 | Supplementary Files
Abstract
To a slurry of LAH (65 mg, 1.7 mmol) in ether (4 ml) at 0 ƒC under Ar, the diene ester [1] (487 mg, 1.7 mmol) in ether (5 ml) was added dropwise.[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
Open AccessShort Note tert-Butyl-3-methoxy-5,5-dimethyl-7(E),9-decadienoate
Molecules 1997, 2(10), M34; https://doi.org/10.3390/M34
Received: 29 September 1997 / Published: 31 October 1997
Cited by 1 | Viewed by 1646 | Supplementary Files
Abstract
The diastereomeric alcohols [1], either separately or as a mixture, were converted under acidic Peterson olefination conditions to the title E-diene.[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
Open AccessShort Note tert-Butyl-3-methoxy-5,5-dimethyl-7-hydroxy-8-trimethylsilyl-9-decenoate
Molecules 1997, 2(10), M33; https://doi.org/10.3390/M33
Received: 29 September 1997 / Published: 31 October 1997
Cited by 1 | Viewed by 1593 | Supplementary Files
Abstract
The crude aldehyde, tert-butyl-3-methoxy-5,5-dimethyl-7-oxo-heptanoate [1] was treated with pinacol E-1-trimethylsilyl-1-propene-3-boronate [2] in petroleum ether at room temperature to provide a 50% yield of the diastereomeric boronic esters, which were simultaneously cleaved to the alcohols and readily separated by flash chromatography.[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
Open AccessShort Note tert-Butyl-3-methoxy-5,5-dimethyl-7-oxo-heptanoate
Molecules 1997, 2(10), M32; https://doi.org/10.3390/M32
Received: 29 September 1997 / Published: 31 October 1997
Cited by 2 | Viewed by 1624 | Supplementary Files
Abstract
Hydroboration of tert-butyl-3-methoxy-5,5-dimethyl-6-heptenoate [1] with either BH3…THF or BH3…Me2S provided the terminal alcohol tert-butyl-3-methoxy-5,5-dimethyl-7-hydroxy-heptanoate, in unoptimized, nonreproducable and disappointingly low 30% yield [2].[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
Open AccessShort Note tert-Butyl-3-methoxy-5,5-dimethyl-7-hydroxy-heptanoate
Molecules 1997, 2(10), M31; https://doi.org/10.3390/M31
Received: 29 September 1997 / Published: 31 October 1997
Cited by 1 | Viewed by 1596 | Supplementary Files
Abstract
Hydroboration of tert-butyl-3-methoxy-5,5-dimethyl-6-heptenoate [1] with either BH3ÖTHF or BH3ÖMe2S provided the terminal alcohol title compound, in unoptimized, nonreproducable and disappointingly low 30% yield.[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
Open AccessShort Note tert-Butyl-3-methoxy-5,5-dimethyl-6-heptenoate
Molecules 1997, 2(10), M30; https://doi.org/10.3390/M30
Received: 29 September 1997 / Published: 31 October 1997
Cited by 2 | Viewed by 1584 | Supplementary Files
Abstract
Preparation of the title compound from the hydroxy ester [1] proved difficult to impossible with almost all protecting groups under a variety of reaction conditions.[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
Open AccessShort Note tert-Butyl-3-hydroxy-5,5-dimethyl-6-heptenoate
Molecules 1997, 2(10), M29; https://doi.org/10.3390/M29
Received: 29 September 1997 / Published: 31 October 1997
Cited by 1 | Viewed by 1578 | Supplementary Files
Abstract
As part of our continuing studies of stereocontrol during the intramolecular Diels-Alder (IMDA) reaction leading to medium rings [1-3], we have targeted poitediol [4] as a structure of interest accessible through this technology.[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
Open AccessShort Note 2-Hydroxy-3-bromo-5-nitrophenylbis(5-methylfur-2-yl)methane
Molecules 1997, 2(10), M27; https://doi.org/10.3390/M27
Received: 22 September 1997 / Published: 31 October 1997
Viewed by 2345 | Supplementary Files
Abstract
See also [1, 2].[...] Full article
(This article belongs to the Section Medicinal Chemistry)
Open AccessShort Note 2-Bromophenylbis(5-methylfur-2-yl)methane
Molecules 1997, 2(10), M28; https://doi.org/10.3390/M28
Received: 22 September 1997 / Published: 1 October 1997
Viewed by 1963 | PDF Full-text (79 KB) | HTML Full-text | XML Full-text | Supplementary Files
Abstract
See also [1,2]. To the solution of 2-bromobenzaldehyde (18.5 g, 100 mmol) and sylvan (20 ml, 250 mmol) in 100 ml of benzene 5 ml of Me3SiCl was added at room temperature.[...] Full article
(This article belongs to the Section Molbank Section of Molecules, 1997-2001)
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