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Separations, Volume 8, Issue 4

2021 April - 19 articles

Cover Story: Perchlorate ion is considered an environmental threat due to its ability to disrupt thyroid function. Although it has been found in many environmental samples worldwide, the information on perchlorate contamination of Polish waters is very limited. In the present study, we determined the concentration of perchlorate in various types of water from Poland using ion chromatography with suppressed conductivity detection (IC-CD). Bottled, tap, river and swimming pool water samples were analyzed. Furthermore, we compared the results to the current health advisory level of perchlorate in water. To our knowledge, this is the first attempt to provide information on the perchlorate presence in Polish waters. View this paper
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Articles (19)

  • Article
  • Open Access
9 Citations
3,436 Views
17 Pages

Comparison of the Fitting Performance of Retention Models and Elution Strength Behaviour in Hydrophilic-Interaction and Reversed-Phase Liquid Chromatography

  • Ester Peris-García,
  • María José Ruiz-Angel,
  • Juan José Baeza-Baeza and
  • María Celia García-Alvarez-Coque

Hydrophilic interaction liquid chromatography (HILIC) is able to separate from polar to highly polar solutes, using similar eluents to those in the reversed-phase mode (RPLC) and a polar stationary phase, where water is adsorbed onto its surface. It...

  • Article
  • Open Access
2 Citations
4,035 Views
15 Pages

Protocol Optimization of Proteomic Analysis of Korean Ginseng (Panax ginseng Meyer)

  • Clarissa Braccia,
  • Bhakti Prinsi,
  • Mara Colzani,
  • Alessandra A. Altomare,
  • Luca Espen,
  • Yoon-Mi Lee,
  • Giancarlo Aldini and
  • Kyung-Jin Yeum

The benefits of ginseng have been mainly attributed to its triterpenoids, called ginsenosides. Recent genome sequencing of the Panax ginseng has paved the way for in-depth proteomic studies of this medicinal plant. The current study was conducted to...

  • Article
  • Open Access
14 Citations
6,411 Views
17 Pages

The fatty acid compositions, including isomer compositions, of seven seed oils containing conjugated fatty acids (CFA) were determined. Seed oils were extracted using a modified Folch extraction, converted to fatty acid methyl esters, and analyzed by...

  • Article
  • Open Access
25 Citations
4,610 Views
15 Pages

Enhanced Adsorption Capacities of Fungicides Using Peanut Shell Biochar via Successive Chemical Modification with KMnO4 and KOH

  • Yong-Gu Lee,
  • Jaegwan Shin,
  • Jinwoo Kwak,
  • Sangwon Kim,
  • Changgil Son,
  • Geon-Youb Kim,
  • Chang-Ha Lee and
  • Kangmin Chon

This study explored the effects of peanut shell biochar (PSB) on the adsorption capacities of fungicides with and without successive chemical modifications, using KMnO4 and KOH (PSBOX-A), in order to provide a valuable understanding of their adsorpti...

  • Article
  • Open Access
9 Citations
4,221 Views
20 Pages

The dissociation constant is an important physicochemical property of drug molecules that affects the pharmacokinetic and pharmacodynamic properties of drugs. In this study, the distribution coefficients of 16 active ingredients extracted from herbal...

  • Feature Paper
  • Article
  • Open Access
5 Citations
3,162 Views
11 Pages

Comparison of Adsorbents Containing Carbon Nanotubes for Express Pre-Concentration of Volatile Organic Compounds from the Air Flow

  • Oleg Rodinkov,
  • Victor Postnov,
  • Valery Spivakovskyi,
  • Andrey Vlasov,
  • Alexandra Bugaichenko,
  • Svetlana Slastina,
  • Ekaterina Znamenskaya,
  • Roman Shilov,
  • Sergey Lanin and
  • Pavel Nesterenko

New composite adsorbents including silica supports (silica, aerosilogel, and diatomite) and carbon materials (multiwall carbon nanotubes and pyrolytic carbon) have been prepared and characterized. The analytical capabilities of the produced sorbents...

  • Article
  • Open Access
4 Citations
4,320 Views
8 Pages

Monitoring of Remaining Thiophenic Compounds in Liquid Fuel Desulphurization Studies Using a Fast HPLC-UV Method

  • Vasiliki Kapsali,
  • Konstantinos Triantafyllidis,
  • Eleni Deliyanni and
  • Victoria Samanidou

Thiophenic compounds constitute a class of sulfur compounds derived by thiophene, containing at least one thiophenic ring. Their presence in fuels (crude oil, etc.) is important and can reach 3% m/m. The combustion of fuels leads to the formation of...

  • Feature Paper
  • Review
  • Open Access
23 Citations
6,516 Views
14 Pages

The Use of Ferrofluids in Analytical Sample Preparation: A Review

  • Raúl González-Martín,
  • Adrián Gutiérrez-Serpa and
  • Verónica Pino

Ferrofluids (FFs) constitute a type of tunable magnetic material, formed by magnetic nanoparticles suspended in a liquid carrier. The astonishing magnetic properties of these materials and their liquid nature have led to their extended use in differe...

  • Article
  • Open Access
4 Citations
5,869 Views
11 Pages

Niacin is a water-soluble vitamin whose deficiency causes many disorders and diseases, including pellagra and high blood cholesterol. Herein, niacin and four common impurities, isonicotinic acid (ISO), 5-ethyl-2-methylpyridine (MP), pyridine-2, 5-dic...

  • Article
  • Open Access
17 Citations
7,284 Views
12 Pages

High-Performance Thin-Layer Chromatography for Rutin, Chlorogenic Acid, Caffeic Acid, Ursolic Acid, and Stigmasterol Analysis in Periploca aphylla Extracts

  • Raha Orfali,
  • Shagufta Perveen,
  • Hanan Y. Aati,
  • Perwez Alam,
  • Omar M. Noman,
  • Javier Palacios,
  • Bayan Salem S. Al-Kurbi,
  • Areej M. Al-Taweel,
  • Afsar Khan and
  • Shabana Iqrar Khan
  • + 1 author

Periploca aphylla (PA), an interesting Saudi medicinal plant, is used in folk medicine to treat urticaria, cerebral fever, tumors, and swelling. To prove its use in folk medicine, two different extracts from the aerial parts of the plant: chloroform...

  • Article
  • Open Access
6 Citations
3,748 Views
13 Pages

Phenolic composition of green tea (Camellia sinensis) varies according to manufacturing processes that result in deglycosylation of glycosylated phenolics and condensation, epimerization, and degalloylation of flavan-3-ols (catechins). Ambiguous phen...

  • Article
  • Open Access
10 Citations
3,897 Views
9 Pages

The selective separation and recovery of specific platinum-group metals (PGMs) from metal mixtures is a significant challenge owing to the similarity of these metals in terms of chemical and physical properties. Among the typical PGMs (Pd, Pt, and Rh...

  • Article
  • Open Access
1 Citations
3,058 Views
21 Pages

The article revisits the discrete recurrence method to model the instruments of liquid–liquid partition chromatography as counter-current chromatography (CCC) and centrifugal partition chromatography (CPC). The purpose is to simplify the computation...

  • Article
  • Open Access
26 Citations
4,119 Views
19 Pages

Grafting of Acrylic Membrane Prepared from Fibers Waste for Dyes Removal: Methylene Blue and Congo Red

  • Ahmed Labena,
  • Ahmed E. Abdelhamid,
  • Shimaa Husien,
  • Tarek Youssef,
  • Ehab Azab,
  • Adil A. Gobouri and
  • Gehan Safwat

Dyes are a type of pollutant that have been discharged into water streams by various industries and had harmful effects on the environment and human health. Therefore, present work was directed to recycle acrylic fibers waste to be used as an adsorbe...

  • Article
  • Open Access
8 Citations
5,506 Views
16 Pages

A Study on the Reaction Kinetics of Anaerobic Microbes Using Batch Anaerobic Sludge Technique for Beverage Industrial Wastewater

  • Um-e-Habiba,
  • Muhammad Saleem Khan,
  • Waseem Raza,
  • Hajera Gul,
  • Maham Hussain,
  • Barizah Malik,
  • Mudassar Azam and
  • Franz Winter

In this study, a low-cost, efficient, and environmentally friendly anaerobic sludge process for the treatment of industrial beverage wastewater was investigated to analyze the effect of bacteria growth on the degradation of organic matter (chemical o...

  • Article
  • Open Access
3 Citations
5,547 Views
16 Pages

The Role of Ionic Liquid Interaction in the Separation of Fatty Acid Methyl Esters—Polyunsaturated Geometric Isomers in GC–MS

  • Emerencia Mező,
  • Anita Bufa,
  • Csilla Páger,
  • Viktória Poór,
  • Tamás Marosvölgyi,
  • Ferenc Kilár and
  • Lilla Makszin

Knowledge of the type and level of saturated and unsaturated fatty acids in food and clinical matrices is of practical importance, but the wide variety of fatty acids makes analyses very complex. The discrimination of the geometric isomers of fatty a...

  • Article
  • Open Access
15 Citations
5,158 Views
17 Pages

Potentiality of Azolla pinnata R. Br. for Phytoremediation of Polluted Freshwater with Crude Petroleum Oil

  • Aya A. Mostafa,
  • Ahmad K. Hegazy,
  • Nermen H. Mohamed,
  • Rehab M. Hafez,
  • Ehab Azab,
  • Adil A. Gobouri,
  • Hosam A. Saad,
  • Azza M. Abd-El Fattah and
  • Yasser M. Mustafa

The pollution of freshwater resources with crude petroleum oil is a major environmental issue in oil-producing countries. As a result, the remediation of polluted aquatic ecosystems using eco-friendly and cost-effective technology is receiving increa...

  • Article
  • Open Access
5 Citations
4,625 Views
12 Pages

Perchlorate Levels in Polish Water Samples of Various Origin

  • Przemysław Niziński,
  • Patrycja Wiśniewska,
  • Joanna Kończyk and
  • Rajmund Michalski

Perchlorate ion (ClO4) is known as a potent endocrine disruptor and exposure to this compound can result in serious health issues. It has been found in drinking water, swimming pools, and surface water in many countries, however, its occurrence in t...

  • Article
  • Open Access
2 Citations
3,245 Views
13 Pages

The movement of the gas–liquid interface caused by the movement of the bubble position will have an impact on the starting conditions for particle migration. This article quantifies the influence of moving bubbles on the starting conditions of partic...

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Separations - ISSN 2297-8739