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Molbank, Volume 2015, Issue 3 (September 2015) – 3 articles

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Open AccessShort Note
1-(3-Amino-1-phenylpropyl)-3-(2-fluorophenyl)-1,3-dihydro-2H-benzimidazol-2-one
Molbank 2015, 2015(3), M867; https://doi.org/10.3390/M867 - 21 Aug 2015
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Abstract
Starting from 1-(2-fluorophenyl)-1,3-dihydro-2H-benzimidazol-2-one (1) and (1-bromo-3-chloropropyl)benzene (2), the target compound 3, which represents a precursor for future radiolabeling, is prepared in a three-step synthesis. Full article
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3,4-Dihydro-3-(2-hydroxyethyl)-4-(nitromethyl)quinazolin-2(1H)-one
Molbank 2015, 2015(3), M866; https://doi.org/10.3390/M866 - 10 Jul 2015
Cited by 3 | Viewed by 1677
Abstract
A one-pot, direct synthesis of 3,4-dihydro-3-(2-hydroxyethyl)-4-(nitromethyl)quinazolin-2(1H)-one from methyl (2-formylphenyl)carbamate, ethanolamine and nitromethane in AcOH is reported. The reaction proceeds via a cascade three-component aza-Henry reaction under microwave irradiation and the title compound was characterized by 1H NMR, 13C NMR and ESI/MS analysis. Full article
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Hexakis{4-[(4′-hydroxybiphenyl-4-yl)ethynyl]phenyl}benzene
Molbank 2015, 2015(3), M865; https://doi.org/10.3390/M865 - 02 Jul 2015
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Abstract
A novel polyphenolic backbone, hexakis{4-[(4′-hydroxybiphenyl-4-yl)ethynyl]phenyl}benzene, was synthesised using a common synthetic protocol used for the synthesis of similar polyphenolic compounds. Full article
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