Skip to Content

Metals, Volume 15, Issue 9

2025 September - 132 articles

Cover Story: A fresh review delves into ~370 papers on machine learning and AI for select metal additive manufacturing (AM) processes. The intersection of these topics since 2020 indicates that the research is booming and has not plateaued. Top wins include smarter process tuning, live monitoring, defect spotting, and melt-pool prediction. However, gaps remain, including closed-loop control and lack of generalization across systems. Future research directions are outlined, emphasizing the need for integrated thermo-mechanical models, uncertainty quantification, and adaptive control strategies. This review serves as a resource for researchers aiming to advance intelligent control and predictive modeling in directed energy deposition-based AM. View this paper
  • Issues are regarded as officially published after their release is announced to the table of contents alert mailing list .
  • You may sign up for email alerts to receive table of contents of newly released issues.
  • PDF is the official format for papers published in both, html and pdf forms. To view the papers in pdf format, click on the "PDF Full-text" link, and use the free Adobe Reader to open them.

Articles (132)

  • Article
  • Open Access
797 Views
20 Pages

22 September 2025

The existing continuous caster layout curves cause plastic deformation of slabs during bending and straightening segments, while no effective deformation occurs in the basic arc segment, which tends to induce defects, such as cracks, and compromise s...

  • Article
  • Open Access
3 Citations
1,371 Views
44 Pages

22 September 2025

This paper presents three simple and efficient advanced optimization algorithms, namely the best–worst–random (BWR), best–mean–random (BMR), and best–mean–worst–random (BMWR) algorithms designed to address un...

  • Article
  • Open Access
1,201 Views
17 Pages

Research on Hybrid Blue Diode-Fiber Laser Welding Process of T2 Copper

  • Xiangkuan Wu,
  • Na Qi,
  • Shengxiang Liu,
  • Qiqi Lv,
  • Qian Fu,
  • Yue Kang,
  • Min Jin and
  • Miaosen Yang

22 September 2025

This research proposes a non-penetration lap welding process for joining T2 copper power module terminals in high-frequency and high-power electronic applications, using a hybrid laser system combining a 445 nm blue diode laser and a 1080 nm fiber la...

  • Article
  • Open Access
1 Citations
749 Views
20 Pages

22 September 2025

Magnesium alloys have been recently recognized as promising materials for temporary orthopedic applications, thanks to their biocompatibility, nontoxicity and biodegradability, combined with bone-like mechanical properties; nevertheless, their clinic...

  • Article
  • Open Access
983 Views
23 Pages

The Effect of Electrolytic Temperature on the Purity of Electrolytic Pure Iron

  • Di Zhang,
  • Tengshi Liu,
  • Gangsheng Xie,
  • Bo Wang,
  • Xin Cao,
  • Jiaxin Bai,
  • Mingyue Zhong and
  • Han Dong

21 September 2025

The influence of electrolytic temperature on the purity grade of electrolytic pure iron, variations in elemental content, macroscopic morphology, and microstructural characteristics was studied using electrodeposition experiments alongside glow disch...

  • Article
  • Open Access
677 Views
15 Pages

Evaluation of the Resistance of APS-Developed Woka-Diamalloy Carbide Coatings to High-Temperature Damage

  • Yildiz Yarali Ozbek,
  • Okan Odabas,
  • Yasin Ozgurluk and
  • Abdullah Cahit Karaoglanli

21 September 2025

This study was conducted to evaluate the high-temperature protection performance of new hard coating systems. Woka 7202 (Cr3C2-NiCr) and Diamalloy 2002 (WC-NiCrFeBSiC) powders were coated onto 316L stainless steel substrates using the atmospheric pla...

  • Article
  • Open Access
1,298 Views
23 Pages

Influence of Tramp Elements on Phase Transformations, Microstructure and Hardness of a 0.3 wt.%C Low-Alloyed Steel

  • Marek Gocnik,
  • Lukas Hatzenbichler,
  • Michael Meindlhumer,
  • Phillip Haslberger,
  • Matthew Galler,
  • Andreas Stark,
  • Claes-Olof A. Olsson,
  • Jozef Keckes and
  • Ronald Schnitzer

20 September 2025

Decarbonizing the steel industry relies on a transition from carbon-intensive blast furnace technology to scrap-based secondary steelmaking using electric arc furnaces. This transition introduces tramp elements and leads to their gradual accumulation...

  • Article
  • Open Access
759 Views
18 Pages

20 September 2025

Ensuring the long-term integrity of structural materials in extreme environments is a critical challenge in the design of equipment for nuclear fuel cycle operations. In particular, the durability of materials exposed to high temperatures and chemica...

  • Article
  • Open Access
1,057 Views
13 Pages

High-Purity Tungsten Oxide Production from Low-Grade Scheelite Concentrates at Pilot Plant Scale

  • Javier Nieto,
  • Lourdes Yurramendi,
  • Javier Antoñanzas and
  • Jose Luis Aldana

20 September 2025

Tungsten is a critical raw material with increasingly important industrial applications. It is primarily found in minerals such as scheelite and wolframite (0.5% W), which are extracted and processed at the mine site to produce a high-grade scheelite...

  • Article
  • Open Access
539 Views
19 Pages

Insights into Optimizing Heat Treatment for Hot Isostatic Pressing of Ti-48Al-3Nb-1.5Ta Alloy Powder

  • Zhenbo Zuo,
  • Rui Hu,
  • Shaoqiang Li,
  • Chengpeng Liu,
  • Qingxiang Wang,
  • Xiangyu Gao,
  • Yunjin Lai,
  • Xian Luo,
  • Cheng Luo and
  • Lu Kang
  • + 1 author

20 September 2025

In this study, various characterization techniques were utilized to investigate the effects of heat treatments on the microstructure and mechanical properties of Ti-48Al-3Nb-1.5Ta (at. %) alloy prepared by the supreme-speed plasma rotating electrode...

  • Article
  • Open Access
706 Views
17 Pages

20 September 2025

The application of lightweight materials in the automotive industry can effectively achieve further weight reduction while maintaining overall structural strength, thereby reducing energy consumption. Currently, friction stir spot welding (FSSW) is t...

  • Article
  • Open Access
3,881 Views
16 Pages

Solid-State Recycling of AA6063 Aluminum Chips via Accumulative Roll Bonding: A Green Pathway to High-Performance Materials

  • Mauro Carta,
  • Noomane Ben Khalifa,
  • Pasquale Buonadonna,
  • Francesco Aymerich and
  • Mohamad El Mehtedi

19 September 2025

Accumulative Roll Bonding (ARB) is a severe plastic deformation process typically used to produce ultra-fine-grained structures. This study investigates the feasibility of using the ARB process to recycle aluminum chips from an Al-Mg-Si alloy (AA6063...

  • Article
  • Open Access
1,031 Views
22 Pages

19 September 2025

The oxygen blast furnace (OBF) is a promising technology for ironmaking, and its burden distribution pattern plays a key role in optimizing performance. This study investigates the impact of the peripheral opening extent (POE), which reflects the cok...

  • Article
  • Open Access
1 Citations
2,880 Views
19 Pages

19 September 2025

The hot stamping process of aluminum alloys involves multiple parameters, including blank holder force, stamping speed, die temperature, and friction coefficient. Traditional methods often fail to capture the nonlinear interactions among these parame...

  • Article
  • Open Access
832 Views
20 Pages

19 September 2025

In this paper, an optimization strategy for the hydroforming process of bellows is proposed, based on finite element analysis, design of experiments, response surface methodology, and genetic algorithms. A numerical model of the bellows hydroforming...

  • Article
  • Open Access
705 Views
12 Pages

19 September 2025

This study comprehensively evaluates the latent heat of hypoeutectic AlSi5Cu alloys with 1, 2, and 4% of Cu by mass, investigating their solidification behavior under controlled cooling conditions. Latent heat, a critical thermophysical property, sig...

  • Article
  • Open Access
643 Views
22 Pages

Towards a Global Constitutive Formulation for Modeling the Hot Working Behavior of Low-Carbon Steels

  • Unai Mayo,
  • Sergio Fernandez-Sanchez,
  • Isabel Gutierrez,
  • Denis Jorge-Badiola and
  • Amaia Iza-Mendia

19 September 2025

The current study explores the applicability of a single constitutive equation, based on the Arrhenius hyperbolic sine model, to a wide range of chemical compositions and test conditions by using a unique approximation. To address this challenge, a m...

  • Article
  • Open Access
1 Citations
682 Views
20 Pages

Internal SEN Design and Its Influence on Fluid Dynamics in Slab Molds: A Combined Numerical and Experimental Analysis

  • Edith Ramos-Cardona,
  • Ismael Calderon-Ramos,
  • Rodolfo Morales Dávila,
  • Rumualdo Servín-Castañeda,
  • Alejandro Pérez-Alvarado,
  • Sixtos A. Arreola-Villa,
  • Alma R. Méndez-Gordillo and
  • Saúl García-Hernández

19 September 2025

The optimization of submerged entry nozzle (SEN) designs plays a pivotal role in achieving stable flow conditions and high-quality steel production during continuous casting. This study presents a comparative analysis of two SEN geometries under iden...

  • Article
  • Open Access
793 Views
16 Pages

Influence of Pre-Corrosion in NaCl Solution on Cavitation Resistance of Steel Samples (42CrMo4)

  • Stanica Nedović,
  • Ana Alil,
  • Sanja Martinović,
  • Stefan Dikić and
  • Tatjana Volkov-Husović

19 September 2025

Marine applications often involve metallic materials, including steel, that must endure harsh conditions such as cavitation erosion (CE). This study investigates the CE behavior of 42CrMo4 steel, both in its original state and after pre-corrosion in...

  • Article
  • Open Access
1,024 Views
17 Pages

19 September 2025

Selecting appropriate materials is crucial for mitigating the severe economic and safety challenges posed by microbiologically induced corrosion (MIC) in marine and industrial settings. This study focuses on the MIC behavior of 316L austenitic stainl...

  • Article
  • Open Access
930 Views
20 Pages

Recovery of Cu and Fe from a Sphalerite Concentrate by the MnO2–KI Leaching Oxidation System

  • Aleksandar Jovanović,
  • Dimitrije Anđić,
  • Mladen Bugarčić,
  • Ivana Jelić,
  • Nela Vujović,
  • Corby Anderson and
  • Miroslav Sokić

19 September 2025

This study examined the leaching behavior of copper and iron from a sphalerite concentrate in sulfuric acid utilizing an ensemble MnO2–KI oxidizing system. The temperature was shown to significantly influence the leaching kinetics, with the eff...

  • Article
  • Open Access
989 Views
12 Pages

ISE of Precious Metals: Au, Ag, Pd, and Pt

  • Lenka Girmanová,
  • Jozef Petrík,
  • Marek Šolc,
  • Peter Blaško,
  • Alena Pribulová and
  • Peter Futáš

19 September 2025

Precious metals play an important role in various fields, from industry to jewelry and finance. In the industrial field, it is often necessary to know their mechanical properties. Micro-hardness measurement is a suitable test. In this type of test, t...

  • Article
  • Open Access
2 Citations
681 Views
17 Pages

Microstructural Evolution and Tensile Deformation Behavior of FeCoNiCrTi0.2 High-Entropy Alloys Regulated by Cold Rolling and Annealing

  • Peng Zhang,
  • Dehao Liu,
  • Linfu Zhang,
  • Kang Liu,
  • Jie Zhang,
  • Yuxiao Si,
  • Gang Chen and
  • Qiang Zhu

19 September 2025

Novel structural materials, high-entropy alloys (HEAs), have attracted considerable interest owing to their tunable microstructural designs and adjustable mechanical properties. In the present work, the microstructural evolution and tensile deformati...

  • Article
  • Open Access
570 Views
20 Pages

19 September 2025

For the flexible multi-point stretch-bending forming process, which involves complex forming procedures, finite element (FE) modeling can significantly reduce trial-and-error costs and provide a convenient means for determining process parameters in...

  • Article
  • Open Access
2 Citations
1,091 Views
25 Pages

19 September 2025

Precipitation hardening is the primary mechanism for strengthening 6xxx series aluminium alloys. The characteristics of the precipitates play a crucial role in determining the mechanical properties. In particular, predicting yield strength (YS) based...

  • Article
  • Open Access
2,197 Views
23 Pages

Kinetics of the Reduction of Iron Ore Pellets with Hydrogen: A Parametric Experimental and Modeling Study

  • Antoine Marsigny,
  • Jean-Baptiste Letz,
  • Olivier Mirgaux and
  • Fabrice Patisson

18 September 2025

The direct reduction of iron ore by hydrogen is a serious candidate for reducing greenhouse gas emissions in the iron and steelmaking industry by replacing traditional blast furnace technology. The reduction kinetics are key to this process. The pres...

  • Article
  • Open Access
560 Views
19 Pages

18 September 2025

In this study, the newly developed Ti35421 (Ti3Al5Mo4Cr2Zr1Fe wt.%) alloy was prepared by laser directed energy deposition (L-DED) because it contains several major elements that can refine grains, which is expected to enable the transformation from...

  • Article
  • Open Access
1 Citations
1,786 Views
16 Pages

18 September 2025

Traditional natural gas transportation pipeline steels, such as API 5L X42 grade and the higher grades, are currently receiving a lot of attention in terms of their potential implementation in hydrogen transmission infrastructure. However, the micros...

  • Article
  • Open Access
1 Citations
922 Views
13 Pages

Controlled Formation of Nanoislands During Microwave Annealing of Au Thin Films

  • Ali Ghanim Gatea Al-Rubaye,
  • Alaa Alasadi,
  • Khalid Rmaydh Muhammed and
  • Catalin-Daniel Constantinescu

18 September 2025

We present a systematic study on the fabrication of gold nanoislands by microwave-assisted annealing, a rapid and energy-efficient alternative to conventional thermal treatments. Gold thin films with nominal thicknesses of 4, 5, 6, 8, and 10 nm are d...

  • Article
  • Open Access
643 Views
21 Pages

17 September 2025

The keyhole defect located at the termination of the friction stir welding (FSW) seam of 6082 aluminum alloys was repaired utilizing the refilling friction stir spot technique. This study examined the impact of the plunge depths on the microstructure...

  • Article
  • Open Access
894 Views
15 Pages

Austenite Grain Growth Behavior and Dynamic Model of ADB790E Hydropower Steel

  • Yuxuan Liu,
  • Hongmei Zhang,
  • Zhongxiang Yu and
  • Zhengyi Jiang

17 September 2025

The growth behavior of austenite grains in ADB790E hydropower steel under the synergistic effects of heating temperature and holding time was studied using in situ quenching and an in situ high-temperature confocal laser scanning microscope (HT-CLSM)...

  • Article
  • Open Access
1 Citations
714 Views
21 Pages

17 September 2025

A new approach to the multi-criteria optimization of L-PBF process parameters in the face of high variability is proposed, based on the application of the reward function (RF), which is essentially the inverse of the Taguchi quality loss function (QL...

  • Review
  • Open Access
1,166 Views
38 Pages

Nanoparticle Architecture Governing Antibacterial and Osteoinductive Responses in Bone-Integrating Implants

  • Juliana Gaviria,
  • Veronica Gaviria,
  • Kamilla V. R. A. Silva,
  • Ana Alcudia,
  • Eduardo Padrón-Hernández and
  • Yadir Torres

16 September 2025

Metallic nanoparticles (MNPs) have emerged as leading candidates in biomedical applications owing to their unique physicochemical properties and dual functionality, combining potent bactericidal and osteoinductive effects. These bioactivities are int...

  • Article
  • Open Access
715 Views
19 Pages

16 September 2025

The aim of this study is to investigate the influence of Mo on the microstructure and mechanical properties of railway frog steel. To address the challenges of a coarse microstructure and alloy element segregation caused by the current casting method...

  • Article
  • Open Access
969 Views
19 Pages

15 September 2025

To optimize the quality of picosecond laser drilling in stainless steel, this study systematically investigates the key influencing factors and optimization strategies of the laser-drilling process through experimental methods. In the experimental se...

  • Article
  • Open Access
1,062 Views
16 Pages

15 September 2025

In this study, the properties of Cu(Co) alloy films were investigated to assess their utility as an alternative material for interconnections in hybrid bonding applications. Thin films of Cu(Co) were deposited using electrochemical deposition in a st...

  • Article
  • Open Access
2 Citations
1,316 Views
22 Pages

Anodizing 3D-Printed AlSi10Mg Alloy and Its Fatigue Properties

  • Hirotaka Kurita,
  • Shinya Tako,
  • Chika Tanaka,
  • Kenji Hara,
  • Kazunori Matsushima,
  • Koji Satsukawa,
  • Keita Watanabe and
  • Hideki Kyogoku

15 September 2025

Two ways of anodizing 3D-printed AlSi10Mg alloy were characterized, and then their fatigue properties were evaluated. Test specimens were fabricated via a laser-powder bed fusion (L-PBF) process followed by machining. Normal and hard anodizing were b...

  • Article
  • Open Access
1 Citations
1,048 Views
18 Pages

Mechanochemical Activation as a Key Step for Enhanced Ammonia Leaching of Spent LiCoO2 Cathodes

  • Lyazzat Mussapyrova,
  • Bagdatgul Milikhat,
  • Matej Baláž,
  • Aisulu Batkal,
  • Kaster Kamunur and
  • Rashid Nadirov

15 September 2025

The growing demand for lithium-ion batteries (LIBs) has led to an urgent need for sustainable recycling strategies for spent cathode materials. In this study, a mechanochemical approach was developed for the recovery of lithium and cobalt from end-of...

  • Article
  • Open Access
1,223 Views
17 Pages

The Effect of Chromium Contents on the Corrosion Performance of Fe-22Mn-0.6C TWIP Steels in Sulfate-Containing Environments

  • Carolina Garín,
  • Fabiola Pineda,
  • Mamie Sancy,
  • Matias Garrido,
  • Juan Lloncón,
  • José Antonio da Cunha Ponciano Gomes and
  • Flavio De Barbieri

14 September 2025

This study evaluates the corrosion behavior of Fe-22Mn-0.6C TWIP steels containing 0%, 5%, and 10% chromium after 28 days of exposure to a neutral sulfate solution. By combining electrochemical testing with a surface and spectroscopic analysis, we ex...

  • Article
  • Open Access
819 Views
16 Pages

Finite Element Analysis for Restraint Intensity and Welding Residual Stress of the Lehigh Specimen Made of Ti80 Alloy

  • Liang Zhang,
  • Gang Song,
  • Qi Wang,
  • Dongjie Chen,
  • Xiaolei Guo,
  • Chang Dai and
  • Weixin Bu

13 September 2025

Ti80 alloy is one of the most commonly used marine titanium alloys but faces cold cracking risks in thick plate welding. Understanding the relationship between restraint intensity and welding residual stress is critical for industrial applications. T...

  • Article
  • Open Access
846 Views
12 Pages

Effects of Deoxidation Processes on Inclusions in Environmentally Friendly Free-Cutting Steel

  • Dong Wang,
  • Binzhou Li,
  • Luoyi Huang,
  • Dongping Zhan and
  • Hang Gao

13 September 2025

Deoxidation of liquid steel is a key link that affects the quality of environmentally friendly free-cutting steel. The selection and addition sequence of deoxidizer affects the composition, size, distribution, and morphology of non-metallic inclusion...

  • Article
  • Open Access
525 Views
16 Pages

12 September 2025

Ultrasonic-assisted friction stir lap welding (FSLW) was employed to join dissimilar aluminum alloys, namely Al-7075 and Al-5052. The effect of ultrasonic power on the weld performance was systematically investigated. Increasing the ultrasonic power...

  • Article
  • Open Access
2 Citations
1,359 Views
21 Pages

Ultrasonic Enhancement of Tin Dissolution in NaOH/H2O2 System: Electrochemical and Passivation Modulation

  • Dongbin Wang,
  • Mingge Fu,
  • Tian Wang,
  • Wenlong Miao,
  • Liuxin Xiang,
  • Thiquynhxuan Le and
  • Libo Zhang

12 September 2025

In the alkaline process for sodium stannate preparation, the oxidative dissolution of tin in the NaOH-H2O2 system originates from a spontaneous electrochemical reaction. This study elucidates the mechanism of ultrasound-enhanced tin dissolution in Na...

  • Article
  • Open Access
1,086 Views
29 Pages

Constitutive Modeling of Creep–Fatigue Interaction in 1Cr-1Mo-0.25V Steel for Hold-Time Testing

  • Federico Bucciarelli,
  • Alessandro Guazzini,
  • Tommaso Grossi,
  • Giuseppe Macoretta and
  • Bernardo Disma Monelli

12 September 2025

In the field of energy production, creep–fatigue interaction is a typical failure mode that might compromise the structural integrity of both rotating equipment and pressure vessels. Common design practices approach the problem in a conservativ...

  • Article
  • Open Access
658 Views
19 Pages

12 September 2025

The hot deformation discipline of typical 45CrNi steel under a strain rate ranging from 0.01 s−1 to 1 s−1 and deformation temperature between 850 °C and 1200 °C was investigated through isothermal hot compression tests. The activa...

  • Article
  • Open Access
1 Citations
859 Views
13 Pages

11 September 2025

The types of carbides and their effects on the fatigue failure mechanism in carburized CSS-42L steel were systematically studied in the present investigation. The results indicate that the main carbides in carburized CSS-42L steel are Cr-rich M23C6 c...

  • Review
  • Open Access
3 Citations
4,471 Views
29 Pages

11 September 2025

High-entropy alloys have demonstrated significant application potential in many industrial fields due to their outstanding comprehensive properties. However, the complex multi-component compositions pose challenges for traditional design approaches....

  • Article
  • Open Access
1 Citations
881 Views
31 Pages

Optimization of Cold Gas Dynamic Spray Coatings Using Agglomerated Al–Zn–TiO2 Powders on Steel

  • Bauyrzhan Rakhadilov,
  • Kaiyrzhan Berikkhan,
  • Zarina Satbayeva,
  • Ainur Zhassulan,
  • Aibek Shynarbek and
  • Kuanysh Ormanbekov

11 September 2025

Cold gas dynamic spraying (CGDS) enables the production of protective coatings without melting or oxidation. In this study, Al–Zn–TiO2 composite powders were prepared by wet agglomeration with binders and by dry mechanical mixing, and dep...

  • Article
  • Open Access
2 Citations
946 Views
14 Pages

Influence of Adjusted Melt Pool Geometries on Residual Stress in 316L LPBF Processes

  • Fabian Eichler,
  • Nicolae Balc,
  • Sebastian Bremen and
  • Julius Sauren

11 September 2025

Residual stress remains a significant challenge in the widespread adoption of the Laser Powder Bed Fusion (LPBF) process, due to its detrimental impact on dimensional accuracy and post-processing requirements and hinders further processing with metho...

of 3

Get Alerted

Add your email address to receive forthcoming issues of this journal.

XFacebookLinkedIn
Metals - ISSN 2075-4701