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Crystals, Volume 10, Issue 2

February 2020 - 89 articles

Cover Story: An XtalController was used to monitor the crystallization of two enzymes, the CCA-adding enzyme of the psychrophilic bacterium Planococcus halocryophilus, and the hen egg-white lysozyme in the presence of the Tb-Xo4 crystallophore. Using light scattering, the XtalController allowed us to follow the nucleating effect of Tb-Xo4 on lysozyme and produce high-diffraction-quality crystals for structure determination. This novel technology opens a way to the rational production of samples for crystallography, ranging from nanocrystals for electron diffraction to microcrystals for serial or conventional X-ray diffraction and larger crystals for neutron diffraction. View this paper
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Articles (89)

  • Article
  • Open Access
8 Citations
3,361 Views
11 Pages

The Cyclic Oxidation and Hardness Characteristics of Thermally Exposed Titanium Prepared by Inductive Sintering-Assisted Powder Metallurgy

  • Fahamsyah H. Latief,
  • El-Sayed M. Sherif,
  • Agus S. Wismogroho,
  • Wahyu B. Widayatno and
  • Hany S. Abdo

11 February 2020

The oxidation and hardness of thermally exposed titanium (Ti) prepared using inductive sintering-assisted powder metallurgy was evaluated through cyclic tests in air at 700–900 °C for 100 h (5 cycles). In general, the oxidation kinetics of...

  • Article
  • Open Access
7 Citations
4,897 Views
13 Pages

In Situ Neutron Diffraction Study of Phase Transformation of High Mn Steel with Different Carbon Content

  • Youngsu Kim,
  • Wookjin Choi,
  • Hahn Choo,
  • Ke An,
  • Ho-Suk Choi and
  • Soo Yeol Lee

10 February 2020

In situ neutron diffraction was employed to examine the phase transformation behavior of high-Mn steels with different carbon contents (0.1, 0.3, and 0.5 wt.%C). With increasing carbon contents from 0.1 C to 0.5 C, the austenite phase fraction among...

  • Article
  • Open Access
4 Citations
4,160 Views
9 Pages

The Characterization and Application of Two Liquid Crystal Mixtures in the Low THz Region

  • Andong Zheng,
  • Xiujun Chu,
  • Pengjun Wang,
  • Peng Wang,
  • Sheng Gao,
  • Jun Yang,
  • Hongbo Lu,
  • Guangsheng Deng and
  • Zhiping Yin

9 February 2020

In the previous work, two new nematic liquid crystal (NLC) mixtures, E7-2 and S200-2, were produced by adding eight LC monomers to two commercial LCs S200 and E7, respectively. At λ = 589 nm, the birefringence (Δn) characteristics of the...

  • Article
  • Open Access
12 Citations
4,099 Views
12 Pages

Correlation between Crystal Structure and Thermoelectric Properties of Sr1−xTi0.9Nb0.1O3−δ Ceramics

  • J. Prado-Gonjal,
  • C. A. López,
  • R. M. Pinacca,
  • F. Serrano-Sánchez,
  • N. M. Nemes,
  • O. J. Dura,
  • J.L. Martínez,
  • M.T. Fernández-Díaz and
  • J.A. Alonso

9 February 2020

Polycrystalline Sr1−xTi0.9Nb0.1O3−δ (x = 0, 0.1, 0.2) ceramics have been prepared by the solid state method and their structural and thermoelectric properties have been studied by neutron powder diffraction (NPD), thermal, and transport measurements....

  • Article
  • Open Access
9 Citations
3,643 Views
14 Pages

8 February 2020

Two metal complexes of theophylline were synthesized. Namely, 1 with the formula [Cu(theop)2(H2O)3]·2H2O and 2, [Zn(theop)2]∙H2O (where: theop = theophylline ion). Their properties were thoroughly investigated by the elemental analysis (EA), f...

  • Article
  • Open Access
4 Citations
3,023 Views
11 Pages

8 February 2020

A novel cobalt(II) complex, namely [Co(tpa)2(H2O)4]·2H2O (1) (Htpa = 5-(1,2,4-triazol-1-yl)pyridine-3-carboxylic acid) has been solvothermally synthesized and structurally characterized by single-crystal X-ray diffraction. Complex 1 was furthe...

  • Article
  • Open Access
7 Citations
6,463 Views
19 Pages

Tools to Ease the Choice and Design of Protein Crystallisation Experiments

  • Nicholas Rosa,
  • Marko Ristic,
  • Luke Thorburn,
  • Gabriel J. Abrahams,
  • Bevan Marshall,
  • Christopher J. Watkins,
  • Alex Kruger,
  • Alex Khassapov and
  • Janet Newman

7 February 2020

The process of macromolecular crystallisation almost always begins by setting up crystallisation trials using commercial or other premade screens, followed by cycles of optimisation where the crystallisation cocktails are focused towards a particular...

  • Article
  • Open Access
8 Citations
3,854 Views
14 Pages

6 February 2020

In this work, photomechanical molecular crystals of 4-(4-(6-Hydroxyhexyloxy) phenylazo) pyridine (6cazpy) and its zinc(II) organic complex (complex-I) were synthesized and crystallized. DSC and TGA were used to characterize and compare properties of...

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Crystals - ISSN 2073-4352