2020 June - 17 articles
Vitamin D and its analogues are fat-soluble vitamins that carry out important functions in human and animal organisms. Many studies have pointed out the relationship between the deficiency of these substances and the development of both skeletal- and...
Clove (Syzygium aromaticum) is a spice widely used for its medical properties, though the species lacks scientific evidence regarding its toxicity and biologic effects. The aim of this study was the chemical identification by GC-MS analysis and evalu...
Analysis imposes substantial challenges, especially when dealing with analytes present at trace levels in complex matrices [...]
Algae are a complex, polyphyletic group of organisms, affordable and naturally rich in nutrients, but also valuable sources of structurally diverse bioactive substances such as natural pigments. The aim of this work was to evaluate the polar and non-...
In this work, non-targeted ultra-high performance liquid chromatography-high-resolution mass spectrometry (UHPLC-HRMS) fingerprints obtained by C18 reversed-phase chromatography were proposed as sample chemical descriptors for the characterization an...
Although chemistry disciplines are often regarded by the public as polluting sciences, in the last three decades, the concept of “Green Chemistry” has fueled the development of more sustainable and environmentally friendly chemical proces...
In reversed-phase liquid chromatography (RPLC), positively charged basic compounds yield broad and asymmetric peaks, as a result of ionic interactions with free silanols that remain on conventional silica-based columns. Diverse solutions have been pr...
Recently, high demand of high-throughput analyses with high sensitivity and selectivity to molecules and drugs in different classes with different physical-chemical properties—and a reduction in analysis time—is a principal milestone for...
The frenetic lifestyle in the developed countries has driven us to be deficient in some nutrients, which may be overcome by supplements. Microalgae, like spirulina (Arthrospira platensis) and chlorella (Chlorella ssp.) are widely used as supplements...
Molecular spectroscopic detection techniques, such as Fourier transform infrared spectroscopy (FTIR), provides additional specificity for isomers where often mass spectrometry (MS) fails, due to similar fragmentation patterns. A hyphenated system of...
Coal tar is a complex mixture of organic compounds obtained from the thermal treatment of coal; it contains several different chemical classes of compounds, such as polycyclic aromatic hydrocarbons, phenols and different heterocyclic compounds includ...
In this work, two online comprehensive two-dimensional liquid chromatography platforms, namely Hydrophilic interaction liquid chromatography × Reversed phase (HILIC × RP) and Reversed phase × Reversed Phase (RP × RP) coupled t...
This study examines the effect of bentonite and zeolite concentration (0.25–5 g/L) on the membrane fouling of a fully automated, pilot-scale membrane bioreactor (MBR) treating high-strength synthetic municipal wastewater. Reversible fouling was...
This paper deals with the characterization of turmeric and related products using the compositional fingerprints of curcuminoids (e.g., curcumin, demethoxycurcumin and bisdemethoxycurcumin) and other phenolic compounds (e.g., hydroxybenzoic and hydro...
Over three billion cups of coffee are consumed daily, making waste coffee grounds readily available throughout the world. Containing approximately 10–15 wt% of oil, they have great potential for biodiesel production. The goal of this work was t...
In this work, Chromabond® HLB was evaluated as an extraction sorbent of a group of seven phthalic acid esters (PAEs; i.e., dipropyl phthalate, DPP, dibutyl phthalate, DBP, diisopentyl phthalate, DIPP, di-n-pentyl phthalate, DNPP, butylbenzyl phth...
In the present work, the kinetics of the extraction process from female inflorescences of Canapa sativa subsp. sativa var. sativa were studied, on the basis of determination of the content of cannabinoids: cannabidiolic acid (CBDA), Δ9-tetrahyd...
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