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Keywords = agricultural use potential of sewage sludge

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22 pages, 2743 KiB  
Article
Effects of the Application of Different Types of Vermicompost Produced from Wine Industry Waste on the Vegetative and Productive Development of Grapevine in Two Irrigation Conditions
by Fernando Sánchez-Suárez, María del Valle Palenzuela, Cristina Campos-Vazquez, Inés M. Santos-Dueñas, Víctor Manuel Ramos-Muñoz, Antonio Rosal and Rafael Andrés Peinado
Agriculture 2025, 15(15), 1604; https://doi.org/10.3390/agriculture15151604 - 25 Jul 2025
Viewed by 324
Abstract
This study evaluates the agronomic potential of two types of vermicompost—one produced solely from wine industry residues (WIR) and one incorporating sewage sludge (WIR + SS)—under rainfed and deficit irrigation conditions in Mediterranean vineyards. The vermicompost was obtained through a two-phase process involving [...] Read more.
This study evaluates the agronomic potential of two types of vermicompost—one produced solely from wine industry residues (WIR) and one incorporating sewage sludge (WIR + SS)—under rainfed and deficit irrigation conditions in Mediterranean vineyards. The vermicompost was obtained through a two-phase process involving initial thermophilic pre-composting, followed by vermicomposting using Eisenia fetida for 90 days. The conditions were optimized to ensure aerobic decomposition and maintain proper moisture levels (70–85%) and temperature control. This resulted in end products that met the legal standards required for agricultural use. However, population dynamics revealed significantly higher worm reproduction and biomass in the WIR treatment, suggesting superior substrate quality. When applied to grapevines, WIR vermicompost increased soil organic matter, nitrogen availability, and overall fertility. Under rainfed conditions, it improved vegetative growth, yield, and must quality, with increases in yeast assimilable nitrogen (YAN), sugar content, and amino acid levels comparable to those achieved using chemical fertilizers, as opposed to the no-fertilizer trial. Foliar analyses at veraison revealed stronger nutrient uptake, particularly of nitrogen and potassium, which was correlated with improved oenological parameters compared to the no-fertilizer trial. In contrast, WIR + SS compost was less favorable due to lower worm activity and elevated trace elements, despite remaining within legal limits. These results support the use of vermicompost derived solely from wine residues as a sustainable alternative to chemical fertilizers, in line with the goals of the circular economy in viticulture. Full article
(This article belongs to the Special Issue Vermicompost in Sustainable Crop Production—2nd Edition)
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24 pages, 2708 KiB  
Article
Sewage Sludge Biochar Improves Water Use Efficiency and Bean Yield in a Small-Scale Field Experiment with Different Doses on Sandy Soil Under Semiarid Conditions
by Raví Emanoel de Melo, Vanilson Pedro da Silva, Diogo Paes da Costa, Maria Fernanda de A. Tenório Alves, Márcio Henrique Leal Lopes, Eline Dias Barbosa, José Henrique de Souza Júnior, Argemiro Pereira Martins Filho, Gustavo Pereira Duda, Antonio Celso Dantas Antonino, Maria Camila de Barros Silva, Claude Hammecker, José Romualdo de Sousa Lima and Érika Valente de Medeiros
AgriEngineering 2025, 7(7), 227; https://doi.org/10.3390/agriengineering7070227 - 9 Jul 2025
Viewed by 463
Abstract
Soil degradation and water scarcity pose major challenges to sustainable agriculture in semiarid regions, requiring innovative strategies to enhance water use efficiency (WUE) and soil fertility. This study assessed the effects of sewage sludge biochar (SSB) on soil properties, WUE, and common bean [...] Read more.
Soil degradation and water scarcity pose major challenges to sustainable agriculture in semiarid regions, requiring innovative strategies to enhance water use efficiency (WUE) and soil fertility. This study assessed the effects of sewage sludge biochar (SSB) on soil properties, WUE, and common bean yield through a small-scale controlled field experiment under rainfed conditions in Northeast Brazil. Four SSB application rates (5, 10, 20, and 40 t ha−1) were compared with conventional NPK fertilization, treated sewage sludge (SS), and chicken manure (CM). The application of 20 t ha−1 (B20) significantly improved soil organic carbon, nitrogen content, water retention, and microbial biomass. B20 also increased WUE by 148% and grain yield by 146% relative to NPK, while maintaining safe levels of potentially toxic elements (PTE) in bean grains. Although 40 t ha−1 (B40) enhanced soil fertility further, it posed a risk of PTE accumulation, reinforcing the advantage of B20 as an optimal and safe dose. These results highlight the potential of SSB to replace or complement conventional fertilizers, especially in sandy soils with limited water retention. The study supports SSB application as a sustainable soil management practice that aligns with circular economy principles, offering a viable solution for improving productivity and environmental resilience in semiarid agriculture. Full article
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22 pages, 2944 KiB  
Article
From Wastewater to Soil Amendment: A Case Study on Sewage Sludge Composting and the Agricultural Application of the Compost
by Csilla Almási, Zoltán Veres, Ibolya Demeter, Viktória Orosz, Tímea Tóth, Mostafa M. Mansour, István Henzsel, Zsolt Bogdányi, Tamás András Szegi and Marianna Makádi
Water 2025, 17(13), 2026; https://doi.org/10.3390/w17132026 - 5 Jul 2025
Viewed by 583
Abstract
The treatment of wastewater and the utilization of the by-products of these processes are an important part of the circular economy. The sewage sludge, a result of wastewater treatment, could be used as a material for plant nutrient supply and/or soil-improving products. The [...] Read more.
The treatment of wastewater and the utilization of the by-products of these processes are an important part of the circular economy. The sewage sludge, a result of wastewater treatment, could be used as a material for plant nutrient supply and/or soil-improving products. The city of Nyíregyháza, Hungary, with 120,000 citizens, has a well-planned water treatment plant operated by Nyírségvíz Ltd., which, in cooperation with the Research Institute of Nyíregyháza, developed a municipal sewage sludge compost (SSC). The closed loop of sewage water treatment and the agricultural utilization of its by-product has been developed and managed. The compost product called Nyírkomposzt was planned for acidic sandy soils. Beyond the agronomic benefits, the sustainable and environmentally sound utilization of SSC reduces sewage sludge disposal. This active involvement of a water utility company demonstrates the potential of cross-sectoral cooperation in solving environmental problems. The quality of the compost fits the Hungarian legislation. To study the effects of 0, 9, 18, and 27 t ha−1 doses of compost on acidic sandy soil, a long-term small plot experiment was started in 2003. The cumulative effects of the regular (every third year, last treatment before sampling in 2021) application of the SSC showed positive changes in basic soil properties, depending on the doses used. Increasing values were found in the case of pH from 4.5 to 6, plant available P2O5 from 240 to 690 ppm, and plant available K2O from 180 to 200 ppm. The plant-available zinc and copper content also increased. Soil organic matter and total N content stabilized at around 0.9% and 0.08%, respectively. The grain yields of winter rye also increased in both investigated years. The yields of 18 t ha−1 treatment were about two times higher compared to the control, but only in 2022 was the difference significant. Our findings underscore the potential of well-planned SSC applications to improve the fertility of ploughed, acidic sandy soil, taking into account the theory of the circular economy by utilizing wastes and decreasing landfilling. Full article
(This article belongs to the Special Issue Treatment and Resource Utilization of Urban Sewage Sludge)
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15 pages, 3453 KiB  
Article
Feasibility of Struvite Crystals Obtained from Swine Wastewater and Urban Sewage Sludge Liquid Fraction as Fertilising Product
by Rubén Rodríguez-Alegre, Sergi Durán-Videra, Manuel Cepero-Sánchez, Laura Pérez Megías, Carlos Andecochea Saiz and Xialei You
Sustainability 2025, 17(13), 6080; https://doi.org/10.3390/su17136080 - 2 Jul 2025
Viewed by 411
Abstract
Increasing global food demand has led to an intensive use of synthetic fertilisers. In this regard, the use of non-conventional streams such as swine wastewater (SW) and urban sewage sludge liquid fraction (USS) for the production of bio-based fertilisers can increase the sustainability [...] Read more.
Increasing global food demand has led to an intensive use of synthetic fertilisers. In this regard, the use of non-conventional streams such as swine wastewater (SW) and urban sewage sludge liquid fraction (USS) for the production of bio-based fertilisers can increase the sustainability of both the fertiliser industry and agriculture while reducing the reliance on imported nutrients. In this work, USS and SW were assessed for the production of struvite at different PO43−:Mg2+ ratios. Significant differences were found in terms of struvite crystals’ shape and size among both feedstocks due to the different saturation indexes, and it was concluded that PO43−:Mg2+ ratios of 1:2 for SW and 1:1 for USS were the most suitable for obtaining big crystals suitable to be used for direct fertilisation. In addition, it was observed that the crystallisation process is highly dependent on the presence of interfering ions (mainly Ca) that can result in the formation of hydroxyapatite instead of struvite. Finally, recovering struvite from SW and USS could potentially reduce the European import of P by up to 6.5%. Full article
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13 pages, 1191 KiB  
Article
Stabilized Sewage Sludge as Fertilizer: Risks Related to the Presence of Microplastics
by Jagoda Worek, Kamil Kawoń, Joanna Chwiej and Katarzyna Styszko
Appl. Sci. 2025, 15(13), 7420; https://doi.org/10.3390/app15137420 - 2 Jul 2025
Viewed by 268
Abstract
Microplastics are an increasingly concerning environmental pollutant. Their presence in agricultural settings is particularly troubling due to their persistence and potential to infiltrate soil, groundwater, and the food chain. This study focused on analyzing fertilizer derived from stabilized sewage sludge collected in June [...] Read more.
Microplastics are an increasingly concerning environmental pollutant. Their presence in agricultural settings is particularly troubling due to their persistence and potential to infiltrate soil, groundwater, and the food chain. This study focused on analyzing fertilizer derived from stabilized sewage sludge collected in June and July. The average mass of microplastics isolated per 100 g of fertilizer was 461.28 mg in June and 458.92 mg in July. The analysis revealed a substantial quantity of microplastics, with fragments and fibers being the predominant forms. In the June samples, an average of 860 microplastic particles was detected, compared to 734 in July (507 fragments and 227 fibers). The most common particle sizes in June ranged from 1500 to 2000 µm and 2000 to 2500 µm, with a significant proportion also exceeding 4000 µm. In July, particles larger than 4000 µm were the most prevalent. Qualitative analysis using Raman microscopy identified polyethylene—a widely used, inexpensive, and chemically stable polymer—as one of the main types of plastic present. Full article
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24 pages, 1360 KiB  
Review
Biomass Ash: A Review of Chemical Compositions and Management Trends
by Izabella Maj, Kamil Niesporek, Piotr Płaza, Jörg Maier and Paweł Łój
Sustainability 2025, 17(11), 4925; https://doi.org/10.3390/su17114925 - 27 May 2025
Cited by 1 | Viewed by 1285
Abstract
With the increasing global emphasis on renewable energy, the generation of biomass fly ash is anticipated to rise substantially in the coming years. This trend highlights the urgent need for effective strategies to manage and utilize this byproduct sustainably. This study reviews and [...] Read more.
With the increasing global emphasis on renewable energy, the generation of biomass fly ash is anticipated to rise substantially in the coming years. This trend highlights the urgent need for effective strategies to manage and utilize this byproduct sustainably. This study reviews and classifies selected types of biomass ashes, treating them as representative examples that illustrate the wide variability in chemical compositions and physical properties across different biomass sources. These include ashes derived from woody biomass, agricultural residues, animal-origin biomass, and sewage sludge. Biomass ashes exhibit significant heterogeneity compared to coal ashes, which makes understanding their chemical composition—particularly the major components such as calcium (Ca), silicon (Si), and phosphorus (P)—critical for identifying suitable industrial applications. Special categories of ashes with elevated heavy metals and chlorine (Cl) levels are also identified and discussed. This approach enables the identification of sustainable utilization pathways, ranging from traditional uses, such as agricultural fertilizers and construction materials, to emerging applications in advanced engineering materials. Additionally, this paper addresses the assessment and mitigation of potential risks related to hazardous metals in biomass ashes. Full article
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23 pages, 2691 KiB  
Article
Production and Quality Assessment of Fertilizer Pellets from Compost with Sewage Sludge Ash (SSA) Addition
by Paweł Cwalina, Sławomir Obidziński, Aneta Sienkiewicz, Małgorzata Kowczyk-Sadowy, Jolanta Piekut, Ewelina Bagińska and Jacek Mazur
Materials 2025, 18(5), 1145; https://doi.org/10.3390/ma18051145 - 4 Mar 2025
Cited by 2 | Viewed by 1261
Abstract
This article examines the process of pressure agglomeration of garden waste compost mixed with sewage sludge ash (SSA) to produce granulated fertilizer material, using a flat die rotating compaction roller system. The study evaluated the effects of adding SSA at mass fractions of [...] Read more.
This article examines the process of pressure agglomeration of garden waste compost mixed with sewage sludge ash (SSA) to produce granulated fertilizer material, using a flat die rotating compaction roller system. The study evaluated the effects of adding SSA at mass fractions of 0%, 10%, 20%, 30%, 40%, and 50% on the process of pelleting and the quality of pellets. Increasing the SSA content from 0% to 50% reduced the power demand of the pellet mill by 13.5% (from 4.92 kW to 4.25 kW), decreased the kinetic strength of the pellets by 0.7% (from 98.21% to 97.56%), and slightly increased the pellet density, by 2.6% (from 1641.17 kg·m−3 to 1684.09 kg·m−3). The high density of the pellets, i.e., over 1600 kg·m−3, indicates that they are of market quality. A chemical analysis revealed that SSA addition positively influenced fertilizer properties. A higher SSA content (up to 50%) decreased the nitrogen content (1.4% to 0.73%) but significantly increased the phosphorus content (0.32% to 2.67%). The potassium content remained stable, at approximately 1.3%. The process of co-pelleting also diluted the heavy metals present in SSA, reducing the final product’s lead and cadmium levels to meet the standards set for fertilizers. Although the SSA contained high levels of heavy metals (lead: 93.89 mg·kgd.m.−1, cadmium: 11.28 mg·kgd.m.−1), these elements were not detected in the compost. Co-pelleting of compost and SSA produces high-density, high-quality fertilizer pellets with favorable nutrient profiles and heavy metal contents, complying with regulatory standards. Moreover, by converting garden waste and SSA into valuable agricultural products, the process supports sustainable waste management. This study evaluated the impact of SSA additives on the composition and water absorption of the granulate, providing insights into its suitability as an eco-friendly fertilizer alternative and its potential implications for sustainable agricultural practices. Full article
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20 pages, 2678 KiB  
Article
Low-Temperature Slow Pyrolysis: Exploring Biomass-Specific Biochar Characteristics and Potential for Soil Applications
by Matheus Antonio da Silva, Adibe Luiz Abdalla Filho, Ruan Carnier, Juliana de Oliveira Santos Marcatto, Marcelo Saldanha, Aline Renee Coscione, Thaís Alves de Carvalho, Gabriel Rodrigo Merlotto and Cristiano Alberto de Andrade
Technologies 2025, 13(3), 100; https://doi.org/10.3390/technologies13030100 - 3 Mar 2025
Cited by 1 | Viewed by 1939
Abstract
The pyrolysis process of residues has emerged as a sustainable method for managing organic waste, producing biochars that offer significant benefits for agriculture and the environment. These benefits depend on the properties of the raw biomass and the pyrolysis conditions, such as washing [...] Read more.
The pyrolysis process of residues has emerged as a sustainable method for managing organic waste, producing biochars that offer significant benefits for agriculture and the environment. These benefits depend on the properties of the raw biomass and the pyrolysis conditions, such as washing and drying. This study investigated biochar production through slow pyrolysis at 300 °C, using eight biomass types, four being plant residues (PBR)—sugarcane bagasse, filter cake, sawdust, and stranded algae—and four non-plant-based residues (NPBR)—poultry litter, sheep manure, layer chicken manure, and sewage sludge. The physicochemical properties assessed included yield, carbon (C) and nitrogen (N) content, electrical conductivity, pH, macro- and micronutrients, and potentially toxic metals. Pyrolysis generally increased pH and concentrated C, N, phosphorus (P), and other nutrients while reducing electrical conductivity, C/N ratio, potassium (K), and sulfur (S) contents. The increases in the pH of the biochars in relation to the respective biomasses were between 0.3 and 1.9, with the greatest differences observed for the NPBR biochars. Biochars from sugarcane bagasse and sawdust exhibited high C content (74.57–77.67%), highlighting their potential use for C sequestration. Filter cake biochar excelled in P (14.28 g kg⁻1) and micronutrients, while algae biochar showed elevated N, calcium (Ca), and boron (B) levels. NPBR biochars were rich in N (2.28–3.67%) and P (20.7–43.4 g kg⁻1), making them ideal fertilizers. Although sewage sludge biochar contained higher levels of potentially toxic metals, these remained within regulatory limits. This research highlights variations in the composition of biochars depending on the characteristics of the original biomass and the pyrolysis process, to contribute to the production of customized biochars for the purposes of their application in the soil. Biochars derived from exclusively plant biomasses showed important aspects related to the recovery of carbon from biomass and can be preferred as biochar used to sequester carbon in the soil. On the other hand, biochars obtained from residues with some animal contributions are more enriched in nutrients and should be directed to the management of soil fertility. Full article
(This article belongs to the Special Issue Recent Advances in Applied Activated Carbon Research)
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14 pages, 1600 KiB  
Article
From House to Farm: Life Cycle Assessment of Sewage Sludge as a Circular Fertiliser at Regional European Level
by Jessica Pérez-García, Pedro Villanueva-Rey, Leticia Rodríguez-Hernández, Teresa Alvarino and Lucía González-Monjardin
Sustainability 2025, 17(4), 1698; https://doi.org/10.3390/su17041698 - 18 Feb 2025
Viewed by 992
Abstract
This study evaluates the environmental performance of stabilised sewage sludge used as a circular fertiliser across three European regions: Central, Mediterranean, and Northern Europe, comparing its performance against non-renewable fertilisers. The research applies a life cycle assessment approach, considering a mix of the [...] Read more.
This study evaluates the environmental performance of stabilised sewage sludge used as a circular fertiliser across three European regions: Central, Mediterranean, and Northern Europe, comparing its performance against non-renewable fertilisers. The research applies a life cycle assessment approach, considering a mix of the most used stabilisation technologies in each region, such as anaerobic digestion, chemical treatment, thermal drying, composting, and aerobic digestion. Environmental impacts were assessed based on key categories, including climate change, acidification, eutrophication, and resource use. The environmental performance of circular fertiliser production outperformed non-renewable fertilisers in all assessed categories, showcasing its potential as a sustainable alternative. Findings reveal that the choice of stabilisation process is key to the overall environmental performance of the region. High energy-driven technologies such as thermal drying present the bigger impacts. Regional disparities highlight the need for context-specific technology selection to optimise environmental outcomes. The study underscores the importance of integrating energy recovery and nutrient recycling in sludge management practices. These findings advocate for the promotion of circular fertilisers within a sustainable agricultural framework, emphasising technology adaptation based on local conditions to enhance ecological and economic benefits. Full article
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25 pages, 2051 KiB  
Review
Biochar in the Bioremediation of Metal-Contaminated Soils
by Małgorzata Majewska and Agnieszka Hanaka
Agronomy 2025, 15(2), 273; https://doi.org/10.3390/agronomy15020273 - 22 Jan 2025
Cited by 3 | Viewed by 2817
Abstract
Biochar is produced from a wide variety of feedstocks (algal biomass, forest, agricultural and food residues, organic fraction of municipal waste, sewage sludge, manure) by thermochemical conversion. In general, it is a dark, porous material with a large surface area, low density, high [...] Read more.
Biochar is produced from a wide variety of feedstocks (algal biomass, forest, agricultural and food residues, organic fraction of municipal waste, sewage sludge, manure) by thermochemical conversion. In general, it is a dark, porous material with a large surface area, low density, high cation exchange capacity, and alkaline pH. By reducing the content of harmful substances in the soil, the application of biochar increases the activity, number, and diversity of microorganisms and improves plant growth in contaminated areas. The aim of the review was to explore the advantages and drawbacks of biochar use in soil bioremediation. General issues such as methods of biochar production, its physical and chemical properties, and various applications are presented. As biochar is an efficient adsorbent of heavy metals, the review focused on its benefits in (I) soil bioremediation, (II) improvement of soil parameters, (III) reduction of metal toxicity and bioaccumulation, (IV) positive interaction with soil microorganisms and soil enzymatic activity, and (V) promotion of plant growth. On the other hand, the potential risks of biochar formulation and utilization were also discussed, mainly related to the presence of heavy metals in biochar, dust hazard, and greenhouse gases emission. Full article
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13 pages, 2062 KiB  
Article
Evaluating Urban Sewage Sludge Distribution on Agricultural Land Using Interpolation and Machine Learning Techniques
by Andrea Lazzari, Simone Giovinazzo, Giovanni Cabassi, Massimo Brambilla, Carlo Bisaglia and Elio Romano
Agriculture 2025, 15(2), 202; https://doi.org/10.3390/agriculture15020202 - 17 Jan 2025
Cited by 1 | Viewed by 1128
Abstract
The European Union promotes the development of a sustainable approach to solid waste management and disposal. Sewage sludge (SWS) is a good example of this economic model because it has fertilizing and soil-conditioning characteristics. This study employed a conventional manure spreader to evaluate [...] Read more.
The European Union promotes the development of a sustainable approach to solid waste management and disposal. Sewage sludge (SWS) is a good example of this economic model because it has fertilizing and soil-conditioning characteristics. This study employed a conventional manure spreader to evaluate the distribution of SWS on agricultural land. Various interpolation methods and machine learning models were employed to analyze the spatial distribution patterns of the sludge. Data were collected from 15 sampling trays across a controlled field during three separate trials. Statistical analysis using ANOVA highlighted significant variations in sludge quantities along the longitudinal axis but not along the latitudinal one. Interpolation methods, such as spline, cubic spline, and inverse distance weighting (IDW) were used to model the distribution, while machine learning models (k-nearest neighbors, random forest, neural networks) classified spatial patterns. Different performance metrics were calculated for each model. Among the interpolation methods, the IDW model combined with neural networks achieved the highest accuracy, with an MCC of 0.9820. The results highlight the potential for integrating advanced techniques into precision agriculture, improving application efficiency and reducing environmental impact. This approach provides a solid basis for optimizing the operation of agricultural machinery and supporting sustainable waste management practices. Full article
(This article belongs to the Section Agricultural Technology)
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25 pages, 6068 KiB  
Article
Optimization of Compost and Peat Mixture Ratios for Production of Pepper Seedlings
by Anita Zapałowska, Wacław Jarecki, Andrzej Skwiercz and Tadeusz Malewski
Int. J. Mol. Sci. 2025, 26(2), 442; https://doi.org/10.3390/ijms26020442 - 7 Jan 2025
Cited by 1 | Viewed by 1259
Abstract
Substituting peat moss with compost derived from organic waste in plant nurseries presents a promising solution for reducing environmental impact, improving waste management, and enhancing soil health while promoting sustainable agricultural practices. However, selecting the appropriate proportions of both materials is crucial for [...] Read more.
Substituting peat moss with compost derived from organic waste in plant nurseries presents a promising solution for reducing environmental impact, improving waste management, and enhancing soil health while promoting sustainable agricultural practices. However, selecting the appropriate proportions of both materials is crucial for each plant species. This study investigates the effects of different ratios of compost and peat mixtures on the growth and development of pepper seedlings. The compost mixtures used in the study included the following combinations: sewage sludge with sawdust (A), sewage sludge with sawdust and biodegradable garden/park waste (B), and biodegradable garden/park waste with sawdust (C). The final substrates used for seedling production were composed of composts (A, B, C) and peat (O) as a structural additive, mixed in different proportions by mass: I-O 25%, II-O 50%, and III-O 75%. Seedlings grown in these substrates were assessed using biometric and physiological measurements. Nematode species present in substrates were identified by metabarcoding analysis. The results revealed that substrate productivity depended not only on nutrient content but also on structural properties, which were significantly influenced by the peat proportion. Among the tested compost mixtures, variant A I emerged as the most effective substrate, promoting optimal seedling growth. Molecular nematode analysis revealed significant nematode contamination in substrates with higher peat proportions (C II and C III), including Meloidogyne sp. Lichtenburg (26%), Meloidogyne hispanica (5%), Meloidogyne sp. Mi_c1 (3%), Meloidogyne ethiopica (2%), and Meloidogyne thailandica (1%). The findings underscore the critical importance of achieving an optimal balance between nutrient content and structural properties in substrates to support the healthy growth and development of pepper seedlings. To further enhance crop performance and reduce the risk of pest-related damage, it is essential to prioritize the improvement of substrate selection strategies. Monitoring for nematode contamination is crucial to prevent potential compromises in seedling quality and overall productivity. Full article
(This article belongs to the Section Bioactives and Nutraceuticals)
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14 pages, 3113 KiB  
Article
Assessment of the Presence of Microplastics in Stabilized Sewage Sludge: Analysis Methods and Environmental Impact
by Jagoda Worek, Kamil Kawoń, Joanna Chwiej, Katarzyna Berent, Rosa Rego and Katarzyna Styszko
Appl. Sci. 2025, 15(1), 1; https://doi.org/10.3390/app15010001 - 24 Dec 2024
Cited by 4 | Viewed by 1172
Abstract
Wastewater treatment processes can fragment microplastics (MPs), which may subsequently enter fertilizers applied in agricultural settings. This study aimed to quantify the occurrence of MPs in stabilized sewage sludge intended for fertilizer production. Matrix elimination was performed using an oxidative method to isolate [...] Read more.
Wastewater treatment processes can fragment microplastics (MPs), which may subsequently enter fertilizers applied in agricultural settings. This study aimed to quantify the occurrence of MPs in stabilized sewage sludge intended for fertilizer production. Matrix elimination was performed using an oxidative method to isolate MPs, followed by MPs separation with a saturated salt solution of appropriate density to enhance the accuracy of identification. The resulting samples were analyzed using spectroscopic and microscopic techniques to provide the detailed characterization of MPs content. The highest concentrations of MPs were recorded during the months of June, July, and May, with average values of 2942, 2341, and 1746 fragments per 100 g of dry weight, respectively. The analysis revealed that fragments were the dominant morphological form, and low-density polyethylene was the most common polymer type detected. These findings underscore a significant risk of MPs re-emission into the environment through the agricultural application of fertilizers derived from sewage sludge. Such practices may lead to the introduction of between 6110 and 13,889 MPs per square meter of soil, depending on the application rates, thereby posing potential risks to soil health and the broader ecosystem. This study highlights the importance of monitoring MPs content in fertilizers derived from wastewater treatment by-products. Full article
(This article belongs to the Section Environmental Sciences)
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23 pages, 865 KiB  
Article
Microbiological Characterization and Pathogen Control in Drying Bed-Processed Sewage Sludge
by Laid Bouchaala, Nedjoud Grara, Nabil Charchar, Heidar Nourine, Kamal Dahdah, Youssouf Driouche, Abdeltif Amrane, Huda Alsaeedi, David Cornu, Mikhael Bechelany and Ahmed Barhoum
Water 2024, 16(22), 3276; https://doi.org/10.3390/w16223276 - 14 Nov 2024
Cited by 3 | Viewed by 1414
Abstract
This study investigated the microbiological and parasitic quality of sewage sludge treated in drying beds in Algeria, aiming to contribute to a better understanding of the factors influencing sludge safety for potential agricultural applications in the Algerian context. The research focused on various [...] Read more.
This study investigated the microbiological and parasitic quality of sewage sludge treated in drying beds in Algeria, aiming to contribute to a better understanding of the factors influencing sludge safety for potential agricultural applications in the Algerian context. The research focused on various sludge types (liquid, semi-solid, and solid) and their behavior across different seasons. Standard microbiological methods were employed to quantify total coliforms, fecal streptococci, E. coli, and Clostridium. Controls were implemented to ensure accuracy, with positive controls validating detection methods using known quantities of microorganisms and parasites, while negative controls confirmed the absence of contamination in the testing environment. Parasitic contamination was assessed through microscopic examination for protozoa and helminths. Results revealed substantial variation in microbial concentrations across sludge types and seasons. Liquid sludge, particularly during summer, exhibited the highest levels of total coliforms (up to 7.021 log10) and E. coli (up to 6.049 log10), while solid sludge showed lower counts. Seasonal trends indicated increased microbial levels during warmer months. Parasitic contamination was prevalent in 81% of samples, with protozoan cysts (e.g., Giardia intestinalis and Endolimax nanus) and helminth eggs detected. Despite reducing microbial loads, drying processes alone were insufficient, leaving significant contamination. Enhanced protocols are needed, such as longer drying periods, chemical disinfectants, or advanced technologies like anaerobic digestion or composting. This highlights the need for locally adapted treatment strategies. Furthermore, this research provides specific recommendations for improving sewage sludge management practices in Algeria, taking into account the unique environmental and agricultural context of the country. Full article
(This article belongs to the Special Issue Resource Use of Sewage Sludge for Soil Application)
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14 pages, 3849 KiB  
Article
Ultrasound-Assisted Community Bureau of Reference (BCR) Procedure for Heavy Metal Removal in Sewage Sludge
by Nicoleta Mirela Marin, Toma Galaon and Luoana Florentina Pascu
Materials 2024, 17(22), 5452; https://doi.org/10.3390/ma17225452 - 8 Nov 2024
Cited by 3 | Viewed by 1172
Abstract
Sewage sludge (SS) resulting from wastewater treatment plants (WWTP) is commonly applied worldwide as a fertilizer in agriculture. This can be done following a rigorous analysis of the sewage sludge composition. Due to its toxic potential, heavy metal ion content is one of [...] Read more.
Sewage sludge (SS) resulting from wastewater treatment plants (WWTP) is commonly applied worldwide as a fertilizer in agriculture. This can be done following a rigorous analysis of the sewage sludge composition. Due to its toxic potential, heavy metal ion content is one of the key parameters to test when evaluating SS sample usage as fertilizer. The distribution of metals present in SS samples produced by five municipal WWTPs in Romania was studied. To obtain information regarding metal distribution in SS, a modified ultrasound-assisted extraction procedure of the Community Bureau of Reference (BCR) was employed for As, Cd, Cr, Cu, Mo, Ni, Pb, Zn, and Co quantitation. Concentrations of these metals were measured using ICP-EOS spectrometry. Method extraction accuracy was verified using CRM-483 certified reference material. Results show that extraction efficiency was lowest for the exchangeable fraction for all studied metals. The detected ion metals were found distributed in fractions (F) 2, 3 and 4, which are unavailable for plants and groundwater under natural environmental conditions. One noteworthy finding was that using ultrapure water for the leachate test resulted in low metal solubility, indicating slight metal desorption in real environmental samples. Furthermore, maize stalk bio-adsorbent was used to minimize metal ion content in WWTP leachate samples produced by the storage of SS in terms of metal ion adsorption. Full article
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