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Separations, Volume 9, Issue 3

2022 March - 28 articles

Cover Story: Anthracyclines are a group of pharmaceutical compounds used to treat cancer, and, as with all pharmaceuticals, they are excreted after consumption by patients. These chemicals can be found in wastewater at very low concentration levels, and for this reason, the development of sensitive analytical methodologies capable of determining such highly polar compounds at trace levels is of prime importance. Fabric phase sorptive extraction is a green analytical process that, combined with fluorescence detection, allows the determination of these analytes in less than one hour. In addition, the combination of sample preparation, separation, and detection shows a very low matrix effect and achieves a low limit of detections. View this paper
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Articles (28)

  • Article
  • Open Access
7 Citations
4,318 Views
15 Pages

The wastewater reuse is an important measure to face water shortage, thus improving the resilience of agricultural production chains. However, treated wastewater can contain residual organic micropollutants residues that may result in crop contaminat...

  • Article
  • Open Access
19 Citations
5,866 Views
9 Pages

Many gluten-free products are deficient in amino acids, especially in essential amino acids (EAA). Therefore, the incorporation of additives rich in free amino acids (FAA) into gluten-free products can be a promising strategy to alleviate certain sym...

  • Communication
  • Open Access
7 Citations
4,004 Views
9 Pages

Cuticular waxes can be used in high-value applications, including cosmetics, foods and nutraceuticals, among the others. The extraction process determines their quality and purity that are of particular interest when biocompatibility, biodegradabilit...

  • Article
  • Open Access
23 Citations
5,132 Views
21 Pages

Rice crops are especially vulnerable to arsenic exposure compared to other cereal crops because flooding growing conditions facilitates its uptake. Besides, there are still many unknown questions about arsenic’s mode of action in rice. Here, we apply...

  • Article
  • Open Access
5 Citations
3,115 Views
10 Pages

Pesticides are chemicals used in agriculture to prevent insects, fungi, weeds, and other pests, from damaging crops. In addition, some types of pesticides are used after harvest as sprout suppressant agents help keeping the quality parameters of crop...

  • Article
  • Open Access
11 Citations
3,439 Views
16 Pages

Morus spp. leaves (MSLs) show various beneficial effects in the treatment of metabolic-related diseases, which have created a growing interest in MSL development as dietary supplements and functional foods. The illustration of chemical compositions a...

  • Article
  • Open Access
13 Citations
5,370 Views
12 Pages

One of the plants used in Indonesian traditional medicine, namely, Patiwala (Lantana camara), is traditionally used to treat some diseases, including itching, wounds, ulcers, swelling, eczema, tetanus, malaria, tumors, rheumatism, and headaches. This...

  • Feature Paper
  • Article
  • Open Access
7 Citations
4,370 Views
18 Pages

Study on the Desliming Performance of a Novel Hydrocyclone Sand Washer

  • Xinghua Yang,
  • Guanghui Yang,
  • Peikun Liu,
  • Xiaoyu Li,
  • Lanyue Jiang and
  • Jiashun Zhang

A novel hydrocyclone sand washer featured by connecting a cylindrical hydrocyclone and a conical-cylindric hydrocyclone in series was developed to improve the poor grading performance in current machine-made sand processing technology. The former hyd...

  • Review
  • Open Access
12 Citations
7,120 Views
23 Pages

The Bright and Dark Sides of Reactive Oxygen Species Generated by Copper–Peptide Complexes

  • Urszula K. Komarnicka,
  • Monika K. Lesiów,
  • Maciej Witwicki and
  • Alina Bieńko

Copper ions bind to biomolecules (e.g., peptides and proteins) playing an essential role in many biological and physiological pathways in the human body. The resulting complexes may contribute to the initiation of neurodegenerative diseases, cancer,...

  • Article
  • Open Access
4 Citations
3,839 Views
18 Pages

The Crosslinker Matters: Vinylimidazole-Based Anion Exchange Polymer for Dispersive Solid-Phase Extraction of Phenolic Acids

  • Matthias Harder,
  • Rania Bakry,
  • Felix Lackner,
  • Paul Mayer,
  • Christoph Kappacher,
  • Christoph Grießer,
  • Sandro Neuner,
  • Christian W. Huck,
  • Günther K. Bonn and
  • Matthias Rainer

Crosslinkers are indispensable constituents for the preparation of SPE materials with ethylene glycol dimethacrylate (EGDMA) and divinylbenzene (DVB) among the most prominent representatives. A crosslinker that has not yet been used for the preparati...

  • Article
  • Open Access
12 Citations
4,662 Views
15 Pages

This study investigated the influence of four different methods of cooking (charcoal grilling, electric barbecue grilling, superheated-steam roasting and infrared grilling) on the volatile profile of lamb meat patties. The study included the patties...

  • Feature Paper
  • Article
  • Open Access
11 Citations
4,888 Views
15 Pages

Alternaria toxins (ATs) are frequently found contaminants in foodstuffs (e.g., alternariol), often reaching high concentrations (e.g., tenuazonic acid). They can spoil a wide variety of food categories (e.g., cereals, vegetables, seeds and drinks) an...

  • Article
  • Open Access
4 Citations
3,446 Views
15 Pages

Fabric Phase Sorptive Extraction for the Determination of Anthracyclines in Sewage

  • Sergio Santana-Viera,
  • Alejandro Canino-Byreing,
  • María Esther Torres-Padrón,
  • Zoraida Sosa-Ferrera,
  • José Juan Santana-Rodríguez,
  • Abuzar Kabir and
  • Kenneth G. Furton

Anthracyclines are a group of antineoplastic compounds used to treat acute leukemia and other cancers, and they are excreted after consumption by patients. These chemicals are often found in sewage at very low concentration levels. For this reason, t...

  • Article
  • Open Access
5 Citations
4,466 Views
24 Pages

Application of Untargeted Metabolomics to Determine Volatile Compounds from the Spanish Plant Arctostaphylos uva-ursi Used as Tea

  • Magdalena Wrona,
  • Davinson Pezo,
  • Maria Anna Rovito,
  • Paula Vera,
  • Cristina Nerín and
  • Esther Asensio

One-hundred and seven different volatile compounds were identified in the samples of Arctostaphylos uva-ursi collected from nine locations in Spain. This plant is commonly brewed and used as tea. Volatile compounds profile was detected using solid-ph...

  • Article
  • Open Access
30 Citations
7,101 Views
27 Pages

Chestnut (Castanea sativa Mill.), a valuable fruit crop, is cultivated in small areas in Romania, mostly in the west, where the moderate continental climate has a slight Mediterranean influence. This work aims to investigate the bioactive characteris...

  • Article
  • Open Access
12 Citations
4,763 Views
15 Pages

Fractionation of Metal(loid)s in Three European Mine Wastes by Sequential Extraction

  • Chiamaka Belsonia Opara,
  • Sabine Kutschke and
  • Katrin Pollmann

Mine waste can constitute an environmental hazard, especially when poorly managed. Environmental assessment is essential for estimating potential threats and optimizing mine waste management. This study evaluated the potential environmental risk of s...

  • Article
  • Open Access
22 Citations
14,979 Views
15 Pages

In an effort to combat the risks associated with traditional tobacco products, tobacco product innovation has been redirected towards reducing the consumer’s potential exposure to harmful or potentially harmful constituents (HPHCs). Among these...

  • Article
  • Open Access
7 Citations
3,471 Views
12 Pages

n-Octyltrichlorosilane Modified SAPO-34/PDMS Mixed Matrix Membranes for Propane/Nitrogen Mixture Separation

  • Weibin Cai,
  • Jiangyu Xie,
  • Jingyu Luo,
  • Xiaohan Chen,
  • Mingqian Wang,
  • Yujun Wang and
  • Jiding Li

In this study, zeolite molecular sieve SAPO-34/polydimethylsiloxane (PDMS) mixed matrix membranes (MMMs) were prepared to recover propane. n-Octyltrichlorosilane (OTCS) was introduced to improve compatibility between SAPO-34 and PDMS, and enhance the...

  • Article
  • Open Access
7 Citations
3,684 Views
15 Pages

Wastewater reuse is essential for sustainable water management. However, it requires tertiary treatment within the plant to ensure suitable water quality. This project aims to investigate the comparative performance of conventional tertiary treatment...

  • Article
  • Open Access
7 Citations
3,729 Views
17 Pages

The development of advanced feed spacers under different working conditions can enhance the performance of the reverse osmosis (RO) desalination process. The 3D-printed experimental results on triply periodic minimal surfaces (TPMS)-based spacers in...

  • Article
  • Open Access
7 Citations
4,336 Views
16 Pages

A simple and green ultra-high-performance micellar liquid chromatography (MLC) method was developed here, comparing Tween 20 and Tween 40 for the first time as the only mobile phase modifiers with a C18 column. Its application to the separation of ni...

  • Article
  • Open Access
2 Citations
2,838 Views
15 Pages

The production of bioethanol fuels using extractive fermentation increases the efficiency of the bioconversion reaction by reducing the toxic product inhibition. The choice of appropriate solvents to remove the bioethanol product without inhibiting t...

  • Article
  • Open Access
8 Citations
3,955 Views
17 Pages

Research and Application of In Situ Sample-Processing Methods for Rapid Simultaneous Detection of Pyrethroid Pesticides in Vegetables

  • Bo Mei,
  • Weiyi Zhang,
  • Meilian Chen,
  • Xia Wang,
  • Min Wang,
  • Yinqing Ma,
  • Chunyan Zhu,
  • Bo Deng,
  • Hongkang Wang and
  • Dongsheng Feng
  • + 4 authors

A novel rapid and cost-effective pre-processing method for the simultaneous determination of pyrethroid pesticides in vegetables has been developed and validated. The process of pesticide extraction was carried out by the QuEChERS (quick, easy, cheap...

  • Article
  • Open Access
4,679 Views
12 Pages

Identification of Soluble Degradation Products in Lithium–Sulfur and Lithium-Metal Sulfide Batteries

  • Fabian Horsthemke,
  • Christoph Peschel,
  • Kristina Kösters,
  • Sascha Nowak,
  • Kentaro Kuratani,
  • Tomonari Takeuchi,
  • Hitoshi Mikuriya,
  • Florian Schmidt,
  • Hikari Sakaebe and
  • Simon Wiemers-Meyer
  • + 4 authors

Most commercially available lithium ion battery systems and some of their possible successors, such as lithium (metal)-sulfur batteries, rely on liquid organic electrolytes. Since the electrolyte is in contact with both the negative and the positive...

  • Article
  • Open Access
14 Citations
5,314 Views
12 Pages

Monitoring of Aflatoxin M1 in Various Origins Greek Milk Samples Using Liquid Chromatography Tandem Mass Spectrometry

  • Anthi Panara,
  • Maria Katsa,
  • Marios Kostakis,
  • Erasmia Bizani and
  • Nikolaos S. Thomaidis

Aflatoxin M1(AFM1), a major metabolite of Aflatoxin B1(AFB1), has been identified as a potential contaminant in dairy products. Because of its possible carcinogenicity, the legislation limits as set by Commission Regulation (EC) No. 1881/2006 are ver...

  • Review
  • Open Access
55 Citations
12,521 Views
15 Pages

Separation and Recycling Potential of Rare Earth Elements from Energy Systems: Feed and Economic Viability Review

  • Ajay B. Patil,
  • Viktoria Paetzel,
  • Rudolf P. W. J. Struis and
  • Christian Ludwig

This review explores the potential of separating and recycling rare earth elements (REEs) from different energy conversion systems, such as wind turbines, electric vehicles batteries, or lighting devices. The REEs include 17 elements (with global pro...

  • Article
  • Open Access
4 Citations
4,771 Views
10 Pages

A new open-chain ether-linked polymer has been prepared via nucleophilic aromatic substitution reaction on a C-F bond of 1,4-dibromo-2,5-difluorobenzene by using 2,2-bis(4-hydroxyphenyl) hexafluoropropane (bisphenol AF or BAF). The new polymer (PE-AF...

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Separations - ISSN 2297-8739