Skip Content
You are currently on the new version of our website. Access the old version .

Separations, Volume 11, Issue 8

2024 August - 33 articles

Cover Story: Methods for obtaining high-purity perrhenic acid (metallic impurities < 100 ppm) with a concentration > 200 g/dm³ from secondary raw materials were compared. The following three methods were analyzed: electrodialysis, solvent extraction (RenMet project), and ion exchange (Łukasiewicz-IMN). Key comparative indicators included process efficiency, selectivity, product purity, raw material and reagent consumption, necessary equipment, profitability, and ecological aspects like waste management. The analysis identified the ion-exchange method as the most economically and ecologically advantageous, emphasizing product purity, process simplicity, and the use of readily available waste materials and renewable ion-exchange resin, supporting a sustainable circular economy. View this paper
  • Issues are regarded as officially published after their release is announced to the table of contents alert mailing list .
  • You may sign up for email alerts to receive table of contents of newly released issues.
  • PDF is the official format for papers published in both, html and pdf forms. To view the papers in pdf format, click on the "PDF Full-text" link, and use the free Adobe Reader to open them.

Articles (33)

  • Article
  • Open Access
1 Citations
1,335 Views
10 Pages

Analysis of Marker Compounds in Lindera erythrocarpa from Diverse Geographical Regions of Korea

  • Neil Patrick Uy,
  • Jung-Hee Kim,
  • Doo-Young Kim,
  • Jajung Ku and
  • Sanghyun Lee

Lindera erythrocarpa M., a medicinal plant commonly found in China, Japan, and Korea, is well known for its antioxidant, anti-inflammatory, and potential anti-cancer effects. However, data on the quantification of different marker compounds found in...

  • Article
  • Open Access
3 Citations
3,505 Views
16 Pages

Spilanthol is a major N-alkylamide constituent of Acmella oleracea (L.) R.K. Jansen with diverse pharmacological properties. We recently showed the applicability of NADES (natural deep eutectic solvents) for the green extraction of spilanthol. Howeve...

  • Technical Note
  • Open Access
1 Citations
4,248 Views
9 Pages

Lignin is part of the lignocellulosic biomass found in hardwoods, softwoods, and herbaceous plants. It is isolated by fractionation and pulping processes, where it is considered a waste product and is mainly burned to generate electricity and heat. H...

  • Article
  • Open Access
6 Citations
3,047 Views
17 Pages

An Extraction Process Based on the Collaborative Extraction of Coptis chinensis Franch. Phytoconstituents Using a Deep Eutectic Solvent and an Organic Solvent

  • Cheng Liu,
  • Fangyuan Gong,
  • Zhengwei Xiong,
  • Cun Wang,
  • Xinhe Ran,
  • Jiahua Ran,
  • Runzi Li,
  • Yangjin Ou,
  • Qingqing Xia and
  • Jin Guo
  • + 1 author

A low-cost method for the simultaneous extraction of alkaloids and water-insoluble flavonoids and esters from Coptis chinensis Franch. (Abbrev. C. chinensis) was explored to provide a reference for the production of green plant-based preparations and...

  • Article
  • Open Access
2 Citations
1,926 Views
19 Pages

Development of an Enantioselective Method by Liquid Chromatography to Monitor 3,4-Methylenedioxypyrovalerone in Culture Media from Ecotoxicity Assays

  • Ariana Pérez-Pereira,
  • Virgínia M. F. Gonçalves,
  • Ana R. L. Ribeiro,
  • Carla Fernandes,
  • João S. Carrola,
  • Cláudia Ribeiro and
  • Maria E. Tiritan

3,4-Methylenedioxypyrovalerone (MDPV) is an emerging, chiral, new psychoactive substance belonging to the synthetic cathinones group that has been frequently detected in wastewater effluents and aquatic environments. However, the knowledge of its ena...

  • Article
  • Open Access
1 Citations
2,128 Views
14 Pages

Development and Characterization of SBA-15 Imprinted Polymers for Spiramycin Analysis

  • Lorena González-Gómez,
  • Sonia Morante-Zarcero,
  • Damián Pérez-Quintanilla,
  • Gema Paniagua González,
  • Rosa M. Garcinuño,
  • Pilar Fernández Hernando and
  • Isabel Sierra

This work focuses on the development of a hybrid material based on SBA-15 silica with a molecularly imprinted polymer (MIP), using spiramycin (SPI) as a template, for use as sorbent in solid-phase extraction (SPE). Characterization techniques such as...

  • Article
  • Open Access
3 Citations
2,086 Views
14 Pages

Development of a Voltammetric Methodology Based on a Methacrylic Molecularly Imprinted Polymer-Modified Carbon-Paste Electrode for the Determination of Aflatoxin B1

  • Fabiola Hernández-García,
  • Jesús Antonio Cruz-Navarro,
  • Jesús García-Serrano,
  • Miriam Franco-Guzmán,
  • Gabriela Islas and
  • Giaan A. Alvarez-Romero

Aflatoxin B1 (AFB1) is one of the most dangerous mycotoxins found in food, necessitating the development of precise and reliable methodologies for its detection. In this study, a novel electrochemical sensor based on a molecularly imprinted polymer (...

  • Review
  • Open Access
37 Citations
27,705 Views
29 Pages

Recent Developments of Pineapple Leaf Fiber (PALF) Utilization in the Polymer Composites—A Review

  • Murugan Sethupathi,
  • Mandla Vincent Khumalo,
  • Sifiso John Skosana and
  • Sudhakar Muniyasamy

Plant fibers’ wide availability and accessibility are the main causes of the growing interest in sustainable technologies. The two primary factors to consider while concentrating on composite materials are their low weight and highly specific f...

  • Article
  • Open Access
2,133 Views
18 Pages

Alzheimer’s disease (AD) is a progressive neurodegenerative condition characterized by memory and cognitive decline in older individuals. Beta-amyloid (Aβ), a significant component of senile plaques, is recognized as a primary contributor...

  • Article
  • Open Access
2,343 Views
14 Pages

An LC–Orbitrap–HRMS method was developed and validated for the simultaneous determination of four tetracyclines—oxytetracycline (OTC), tetracycline (TC), doxycycline (DC), and chlortetracycline (CTC)—in milk. This method invol...

  • Article
  • Open Access
14 Citations
5,686 Views
16 Pages

Polyphenols Extraction from Different Grape Pomaces Using Natural Deep Eutectic Solvents

  • Alessandro Frontini,
  • Andrea Luvisi,
  • Carmine Negro,
  • Massimiliano Apollonio,
  • Rita Accogli,
  • Mariarosaria De Pascali and
  • Luigi De Bellis

Exploiting by-products from the oenological industry to extract antioxidant chemicals is a shared goal that combines the need to reduce the wine sector’s environmental impact with the need to improve the availability of these biomolecules, acco...

  • Article
  • Open Access
2,591 Views
14 Pages

A Validated Method for the Simultaneous Determination of Oxytocin and Cortisol in Human Saliva

  • Elisa Polledri,
  • Rosa Mercadante,
  • Laura Campo and
  • Silvia Fustinoni

Oxytocin and cortisol (OXY and CORT) are hormones related to stress, cognitive, and social behaviors. Their detection is relevant to epidemiological studies aimed at investigating the effects of stressor factors on human life. The aim of this study w...

  • Article
  • Open Access
2 Citations
4,168 Views
13 Pages

Determination of Gb3 and Lyso-Gb3 in Fabry Disease-Affected Patients by LC-MRM/MS

  • Gennaro Battaglia,
  • Gabriella Pinto,
  • Carolina Fontanarosa,
  • Michele Spinelli,
  • Anna Illiano,
  • Stefania Serpico,
  • Lorenzo Chiariotti,
  • Roberta Risoluti,
  • Stefano Materazzi and
  • Angela Amoresano

Limited or absent activity of the enzyme α-galactosidase A (α-Gal A), due to mutation in the related gene on the X chromosome, leads to the development of a rare hereditary and genetic disease known as Fabry disease (FD). This pathology i...

  • Article
  • Open Access
4 Citations
2,334 Views
20 Pages

Ciguatoxins (CTXs) are neurotoxic marine biotoxins capable of contaminating marine organisms. Approximately 30 CTX analogues have been described; however, only a few have been documented in ciguatera poisoning (CP) outbreaks. Detecting CTXs from comp...

  • Article
  • Open Access
3 Citations
3,104 Views
34 Pages

Characterisation of the Volatile Compounds and Key Odourants in Japanese Mandarins by Gas Chromatography–Mass Spectrometry and Gas Chromatography–Olfactometry

  • Lingyi Li,
  • Rui Min Vivian Goh,
  • Yunle Huang,
  • Kim-Huey Ee,
  • Aileen Pua,
  • Daphne Tan,
  • Shanbo Zhang,
  • Lionel Jublot,
  • Shao Quan Liu and
  • Bin Yu

Japanese mandarins are becoming increasingly popular due to their pleasant aroma. The volatiles in four varieties of Japanese mandarins (Iyokan, Ponkan, Shiranui, and Unshiu mikan) were extracted by headspace solid-phase microextraction (HS-SPME) and...

  • Article
  • Open Access
4 Citations
1,945 Views
15 Pages

Achillea cucullata is a perennial herbaceous plant that has a long history of medical use in many cultures. The present research focuses on the biological activity and therapeutic potential of A. cucullata, namely its antibacterial and anticancer pro...

  • Article
  • Open Access
2 Citations
1,925 Views
12 Pages

The presence of biogenic amines (BAs) in seafood can pose a health risk to consumers, as they have been linked to adverse reactions such as histamine poisoning. Although the only biogenic amine for which maximum limits have been set is histamine, it...

  • Article
  • Open Access
4 Citations
2,042 Views
16 Pages

Ultrasonic flotation is widely used as an efficient mineral separation method. Its efficiency is related to the adhesion behavior between fine particles and flotation bubbles, which can be influenced by the bubbles’ movement behavior. This pape...

  • Review
  • Open Access
12 Citations
10,844 Views
17 Pages

Advances in Therapeutic Peptides Separation and Purification

  • Othman Al Musaimi and
  • Da’san M. M. Jaradat

Peptides are gaining prominence in various fields, including the pharmaceutical industry. To meet regulatory requirements, they must achieve a certain purity threshold to ensure safe administration. Numerous purification technologies have been employ...

  • Review
  • Open Access
12 Citations
2,851 Views
16 Pages

Adsorption of Cobalt onto Zeolitic and Carbonaceous Materials: A Review

  • Eduardo Díez,
  • Rubén Miranda,
  • Juan Manuel López,
  • Arturo Jiménez,
  • Naby Conte and
  • Araceli Rodríguez

At present, cobalt belongs to what are called critical raw materials due to its scarcity and its economic importance. Cobalt is a crucial element in the development of new technologies and applications for decarbonization, with around 40% of cobalt c...

  • Article
  • Open Access
3,150 Views
14 Pages

Determination of Volatilome Profile in Carbonated Beverages Using n-Hexane as an Extractant by GC-MS

  • Li Mu,
  • Xianglong Meng,
  • Huihong Luo,
  • Qianqian Liu,
  • Li Zhang,
  • Xin Li,
  • Ying Xu and
  • Gang Li

A liquid–liquid extraction pretreatment method using n-hexane as the extractant was developed for the analysis of volatile aroma substances in three flavors (six cola samples, six lemon samples, and six orange samples) of carbonated beverages b...

  • Article
  • Open Access
1 Citations
1,784 Views
17 Pages

An Empirical Study on the Upcycling of Glass Bottles into Hydrocyclone Separators

  • Thomas Senfter,
  • Thomas Neuner,
  • Christian Bachmann,
  • Manuel Berger,
  • Christian Mayerl,
  • Tobias Kofler,
  • Michael Kraxner and
  • Martin Pillei

Cyclones are pivotal in mechanical process engineering and crucial in the complex field of separation technology. Their robustness and compact spatial requirements render them universally applicable and versatile across various industrial domains. De...

  • Article
  • Open Access
2 Citations
3,952 Views
16 Pages

LC-MS/MS-QTOF Identification of Phenolic Compounds of Sideritis Species Cultivated in Greece

  • Eleftheria H. Kaparakou,
  • Charalabos D. Kanakis,
  • Maroula G. Kokotou,
  • Georgios Papadopoulos and
  • Petros A. Tarantilis

Phenolic compounds are plant secondary metabolites, one of the most common and widespread groups of substances in plants, as well as a major group of phytochemicals present in medicinal and aromatic plants. The phytochemical composition of the hydroa...

  • Article
  • Open Access
4 Citations
8,357 Views
12 Pages

Technology for Aiding the Cyanide Leaching of Gold Ores

  • Jiahong Han,
  • Shujuan Dai,
  • Jiushuai Deng,
  • Shandong Que and
  • Yugao Zhou

Cyanide leaching technology was studied for low-grade oxidized gold ores in Guangxi Province. The gold grade of the raw ores was 1.32 g/t. The gold leaching rate was 90.91% under the optimal conditions for the following conventional leaching process:...

  • Article
  • Open Access
2 Citations
2,809 Views
16 Pages

Lumen pressure is of crucial importance to achieve simultaneous nitrification and denitrification (SND) in the membrane aerated biofilm reactor (MABR); so, in this study, a laboratory-scale MABR was operated under different lumen pressures (7 kPa, 10...

  • Article
  • Open Access
7 Citations
4,659 Views
15 Pages

Characterization of Alginates of Sargassum from the Archipelago of Guadeloupe

  • Naika Marcin,
  • Valendy Thesnor,
  • Valentin Duvauchelle,
  • Alejandro Ponce-Mora,
  • Lucia Gimeno-Mallench,
  • Stacy Narayanin-Richenapin,
  • Laura Brelle,
  • Eloy Bejarano,
  • Christelle Yacou and
  • Gerardo Cebrian-Torrejon
  • + 4 authors

Sargassum is a genus of brown algae that causes a major impact to marine ecosystems. Although accumulation of this invasive seaweed is considered an environmental problem, Sargassum can also be resource of valuable molecules such as alginates. Algina...

  • Article
  • Open Access
1 Citations
2,186 Views
17 Pages

A Comparison of Production Methods of High-Purity Perrhenic Acid from Secondary Resources

  • Dorota Kopyto,
  • Mateusz Ciszewski,
  • Szymon Orda,
  • Katarzyna Leszczyńska-Sejda,
  • Joanna Malarz,
  • Patrycja Kowalik,
  • Karolina Pianowska,
  • Karolina Goc,
  • Grzegorz Benke and
  • Piotr Dydo
  • + 2 authors

Methods for obtaining high-purity perrhenic acid (with metallic impurities content below 100 ppm) of a high concentration > 200 g/dm3 and entirely from secondary raw materials were compared. Comparative analyses of three methods were performed: el...

  • Article
  • Open Access
1 Citations
1,626 Views
9 Pages

Production of Perrhenic Acid by Solvent Extraction

  • Karolina Pianowska,
  • Grzegorz Benke,
  • Karolina Goc,
  • Joanna Malarz,
  • Patrycja Kowalik,
  • Katarzyna Leszczyńska-Sejda and
  • Dorota Kopyto

The aim of this work was to develop an effective method for obtaining perrhenic acid from available ammonia waste solutions using the solvent extraction method. An ammonia waste solution was used as the test material, with Re and NH4+ concentrations...

  • Article
  • Open Access
1 Citations
1,764 Views
10 Pages

Development of a Two-Dimensional Liquid Chromatography Online Deproteinization Method for Determining Paclitaxel-Related Substances in a Paclitaxel Injection (Albumin-Bound)

  • Jing Yao,
  • Xuejia Zhao,
  • Yifei Jiang,
  • Limin Zuo,
  • Xiaodan Qiu,
  • Xiaofang Lian,
  • Huiyi Liu,
  • Qingying Jia,
  • Huimin Sun and
  • Guangzhi Shan

To determine the paclitaxel-related substances in a paclitaxel injection (albumin-bound), it is necessary to remove human blood albumin from the sample via solid-phase extraction and subsequently perform high-performance liquid chromatography analysi...

  • Article
  • Open Access
2 Citations
2,290 Views
16 Pages

In this study, three geometries were analyzed for sand and microplastic separation to confirm the applicability of cyclones. This research aimed to apply plastic-based samples such as Styrofoam, PET, PP, and PU to an analytical model, characterized b...

  • Article
  • Open Access
2 Citations
2,148 Views
13 Pages

Efficient Photocatalytic Degradation of Triclosan and Methylene Blue by Synthesized Ag-Loaded ZnO under UV Light

  • Myriam Chems,
  • Lázaro Adrián González-Fernández,
  • Manuel Sanchez Polo,
  • Abdellah Anouar and
  • Ventura Castillo Ramos

Industrial discharge of hazardous organic and synthetic chemicals, such as antibacterials and dyes, poses severe risks to human health and the environment. This study was conducted to address the urgent need for efficient and stable zinc-oxide-based...

  • Article
  • Open Access
1,648 Views
13 Pages

Five Significant Phenols from Phyllostachys glauca McClure Leaves Extracted Using Ultrasound-Assisted Deep Eutectic Solvent Extraction

  • Jianqiang Hei,
  • Jianjun Wang,
  • Jin Wang,
  • Daoqi Zhang,
  • Wenting Song,
  • Hang Xun,
  • Xuefeng Guo and
  • Xi Yao

Phyllostachys glauca McClure leaves (PML), as economical natural product material, contain abundant phenols, particularly flavonoids, with significant biological activities that contribute to their widespread applications in food, pharmaceutical, and...

Get Alerted

Add your email address to receive forthcoming issues of this journal.

XFacebookLinkedIn
Separations - ISSN 2297-8739