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Sci. Pharm.Scientia Pharmaceutica
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  • Scientia Pharmaceutica is published by MDPI from Volume 84 Issue 3 (2016). Previous articles were published by another publisher in Open Access under a CC-BY (or CC-BY-NC-ND) licence, and they are hosted by MDPI on mdpi.com as a courtesy and upon agreement with Austrian Pharmaceutical Society (Österreichische Pharmazeutische Gesellschaft, ÖPhG).
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20 April 2002

10 Pages

Oxidative Cyclisierungsreaktionen von 1-(3-Nitro-3-phenylpropyl)piperidin

and
Institut für Pharmazeutische Chemie der Heinrich-Heine-Universität, Universitätsstr. 1, D-40225 Düsseidorf
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Sci. Pharm.2002, 70(2), 113-122;https://doi.org/10.3797/scipharm.aut-02-13
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Abstract

The title compound 2 - prepared by Komblum reaction - reacted with Hg(II)-edta in a two electron withdrawal to a bicyclic compound 6, which showed in solution an equilibrium of two species probably of diastereomers, which was deduced from NMR-measurements. Additionally, resulting of an threefold dehydrogenation two diastereomeric bicyclic lactams 11A and 11B were isolated.

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