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(E)-1-(3,4-Dimethoxyphenyl)-2-methyl-3-phenylprop-2-en-1-one: A P-Type Acid-Stable Photochromic α-Methylchalcone
Short Note

4-[(2,4-Dichlorophenyl)carbamoyl]butanoic Acid

Department of Chemistry, University of Science and Technology, Bannu 28100, Pakistan
Center of Excellence in Science and Applied Technology, Islamabad 45400, Pakistan
Research Centre for Crystalline Materials, School of Medical and Life Sciences, Sunway University, No. 5 Jalan Universiti, Bandar Sunway 47500, Selangor Darul Ehsan, Malaysia
Authors to whom correspondence should be addressed.
Academic Editor: R. Alan Aitken
Molbank 2021, 2021(2), M1227;
Received: 10 May 2021 / Revised: 31 May 2021 / Accepted: 1 June 2021 / Published: 4 June 2021
(This article belongs to the Section Structure Determination)
The synthesis and spectroscopic characterization of the glutaric acid-amide derivative, 2,4-Cl2C6H3N(H)C(=O)(CH2)3C(=O)OH (1), are described. The X-ray crystal structure determination of (1) shows the backbone of the molecule to be kinked about the methylene-C–N(amide) bond as seen in the C(p)–N–C(m)–C(m) torsion angle of −157.0(2)°; m = methylene and p = phenyl. An additional twist in the molecule is noted between the amide and phenyl groups as reflected in the C(m)–N–C(p)–C(p) torsion angle of 138.2(2)°. The most prominent feature of the molecular packing is the formation of supramolecular tapes assembled through carboxylic acid-O–HO(carbonyl) and amide-N–HO(amide) hydrogen bonding. View Full-Text
Keywords: glutaric acid-amide; amide; carboxylic acid; hydrogen bonding; X-ray crystallography glutaric acid-amide; amide; carboxylic acid; hydrogen bonding; X-ray crystallography
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MDPI and ACS Style

Hanifa, B.; Sirajuddin, M.; Ullah, Z.; Mahboob, S.; Lee, S.M.; Lo, K.M.; Tiekink, E.R.T. 4-[(2,4-Dichlorophenyl)carbamoyl]butanoic Acid. Molbank 2021, 2021, M1227.

AMA Style

Hanifa B, Sirajuddin M, Ullah Z, Mahboob S, Lee SM, Lo KM, Tiekink ERT. 4-[(2,4-Dichlorophenyl)carbamoyl]butanoic Acid. Molbank. 2021; 2021(2):M1227.

Chicago/Turabian Style

Hanifa, Bibi; Sirajuddin, Muhammad; Ullah, Zafran; Mahboob, Sumera; Lee, See M.; Lo, Kong M.; Tiekink, Edward R.T. 2021. "4-[(2,4-Dichlorophenyl)carbamoyl]butanoic Acid" Molbank 2021, no. 2: M1227.

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