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Short Note

4-[(2,4-Dichlorophenyl)carbamoyl]butanoic Acid

1
Department of Chemistry, University of Science and Technology, Bannu 28100, Pakistan
2
Center of Excellence in Science and Applied Technology, Islamabad 45400, Pakistan
3
Research Centre for Crystalline Materials, School of Medical and Life Sciences, Sunway University, No. 5 Jalan Universiti, Bandar Sunway 47500, Selangor Darul Ehsan, Malaysia
*
Authors to whom correspondence should be addressed.
Academic Editor: R. Alan Aitken
Molbank 2021, 2021(2), M1227; https://doi.org/10.3390/M1227
Received: 10 May 2021 / Revised: 31 May 2021 / Accepted: 1 June 2021 / Published: 4 June 2021
(This article belongs to the Section Structure Determination)
The synthesis and spectroscopic characterization of the glutaric acid-amide derivative, 2,4-Cl2C6H3N(H)C(=O)(CH2)3C(=O)OH (1), are described. The X-ray crystal structure determination of (1) shows the backbone of the molecule to be kinked about the methylene-C–N(amide) bond as seen in the C(p)–N–C(m)–C(m) torsion angle of −157.0(2)°; m = methylene and p = phenyl. An additional twist in the molecule is noted between the amide and phenyl groups as reflected in the C(m)–N–C(p)–C(p) torsion angle of 138.2(2)°. The most prominent feature of the molecular packing is the formation of supramolecular tapes assembled through carboxylic acid-O–HO(carbonyl) and amide-N–HO(amide) hydrogen bonding. View Full-Text
Keywords: glutaric acid-amide; amide; carboxylic acid; hydrogen bonding; X-ray crystallography glutaric acid-amide; amide; carboxylic acid; hydrogen bonding; X-ray crystallography
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MDPI and ACS Style

Hanifa, B.; Sirajuddin, M.; Ullah, Z.; Mahboob, S.; Lee, S.M.; Lo, K.M.; Tiekink, E.R.T. 4-[(2,4-Dichlorophenyl)carbamoyl]butanoic Acid. Molbank 2021, 2021, M1227. https://doi.org/10.3390/M1227

AMA Style

Hanifa B, Sirajuddin M, Ullah Z, Mahboob S, Lee SM, Lo KM, Tiekink ERT. 4-[(2,4-Dichlorophenyl)carbamoyl]butanoic Acid. Molbank. 2021; 2021(2):M1227. https://doi.org/10.3390/M1227

Chicago/Turabian Style

Hanifa, Bibi; Sirajuddin, Muhammad; Ullah, Zafran; Mahboob, Sumera; Lee, See M.; Lo, Kong M.; Tiekink, Edward R.T. 2021. "4-[(2,4-Dichlorophenyl)carbamoyl]butanoic Acid" Molbank 2021, no. 2: M1227. https://doi.org/10.3390/M1227

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