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Article

Synthesis and X-Ray Structure of [N,N-Bis(3,5-dimethylpyrazol-1-ylmethyl)-1-hydroxy-2-aminoethane](3,5-dimethylpyrazole) copper(II) dinitrate

by
Mohamed El Kodadi
1,
Fouad Malek
1,
Rachid Touzani
1,
Abdelkrim Ramdani
1,*,
Sghir El Kadiri
2 and
Driss Eddike
3
1
Laboratory of Physical Organic Chemistry, Department of Chemistry, Faculty of Sciences, University Mohammed The First, BP 524, 60 000 Oujda, Morocco
2
Laboratory of Chemistry of the Environment and Materials, Department of Chemistry, Faculty of Sciences, University Mohammed The First, BP 524, 60 000 Oujda, Morocco
3
Laboratory of Inorganic Solid Chemistry, Department of Chemistry, Faculty of Sciences, University Mohammed The First, BP 524, 60 000 Oujda, Morocco
*
Author to whom correspondence should be addressed.
Molecules 2003, 8(11), 780-787; https://doi.org/10.3390/81100780
Published: 15 November 2003
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Abstract

The tridentate ligand N,N-Bis(3,5-dimethylpyrazol-1-ylmethyl)-1-hydroxy-2-aminoethane (L) has been prepared in one step by condensation of two equivalents of 1-hydroxymethyl-3,5-dimethylpyrazole with one equivalent of 2-aminoethanol. This reaction is carried out under microwave irradiation (60 W) in the absence of solvent for 20 min [1]. Using this ligand L a new Cu(II) dinitrate complex has been prepared. The singlecrystal X-ray structure of the title compound, [N,N-bis(3,5-dimethylpyrazol-1-ylmethyl)-1-hydroxy-2-aminoethane] (3,5-dimethylpyrazole)copper(II) dinitrate, revels that the copper (II) ion is coordinated to two pyrazole nitrogens, one tertiary amine nitrogen of the ligand L and 3,5-dimethylpyrazole, and in the apical position by an alcohol O atom.
Keywords: Structure; copper complex; tripod; pyrazole; tridentate ligand Structure; copper complex; tripod; pyrazole; tridentate ligand

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MDPI and ACS Style

El Kodadi, M.; Malek, F.; Touzani, R.; Ramdani, A.; El Kadiri, S.; Eddike, D. Synthesis and X-Ray Structure of [N,N-Bis(3,5-dimethylpyrazol-1-ylmethyl)-1-hydroxy-2-aminoethane](3,5-dimethylpyrazole) copper(II) dinitrate. Molecules 2003, 8, 780-787. https://doi.org/10.3390/81100780

AMA Style

El Kodadi M, Malek F, Touzani R, Ramdani A, El Kadiri S, Eddike D. Synthesis and X-Ray Structure of [N,N-Bis(3,5-dimethylpyrazol-1-ylmethyl)-1-hydroxy-2-aminoethane](3,5-dimethylpyrazole) copper(II) dinitrate. Molecules. 2003; 8(11):780-787. https://doi.org/10.3390/81100780

Chicago/Turabian Style

El Kodadi, Mohamed, Fouad Malek, Rachid Touzani, Abdelkrim Ramdani, Sghir El Kadiri, and Driss Eddike. 2003. "Synthesis and X-Ray Structure of [N,N-Bis(3,5-dimethylpyrazol-1-ylmethyl)-1-hydroxy-2-aminoethane](3,5-dimethylpyrazole) copper(II) dinitrate" Molecules 8, no. 11: 780-787. https://doi.org/10.3390/81100780

APA Style

El Kodadi, M., Malek, F., Touzani, R., Ramdani, A., El Kadiri, S., & Eddike, D. (2003). Synthesis and X-Ray Structure of [N,N-Bis(3,5-dimethylpyrazol-1-ylmethyl)-1-hydroxy-2-aminoethane](3,5-dimethylpyrazole) copper(II) dinitrate. Molecules, 8(11), 780-787. https://doi.org/10.3390/81100780

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