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Separations, Volume 9, Issue 6

June 2022 - 22 articles

Cover Story: Nowadays, due to the increasing attention paid to healthy food and alternative diets, the consumption of hemp-flour-based products, hemp seeds and oil is spreading widely. The substantial growth of the hemp market necessitates guidelines for hemp cultivation that guarantee its value, origin and quality. This study determined the specific stable isotope ratio ranges of five bioelements (δ2H, δ13C, δ15N, δ18O and δ34S in Italian industrial hemp intended for food use, setting the groundwork for the first isotopic database for this little-investigated high-value crop. Research findings corroborate the reliability of using light stable isotope ratios to characterize origin and types of fertilization of Cannabis sativa cultures, paving the way for future studies on the authentication and traceability of hemp-derived food products and the verification of their organic labeling. View this paper
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Articles (22)

  • Article
  • Open Access
20 Citations
5,638 Views
12 Pages

For non-bovine milks, information regarding bioactive lipids is fragmented, unreliable or unavailable. The purpose of the current study was to analyse bioactive lipids in the milk of dairy animals using modern analytical methods to achieve the most r...

  • Article
  • Open Access
14 Citations
2,932 Views
21 Pages

Educational and research laboratories often produce relatively small amounts of highly diverse organic wastes. Treating waste can contribute significantly to the cost of running laboratories. This study introduced a simple and economical waste manage...

  • Article
  • Open Access
2 Citations
4,176 Views
10 Pages

Sensitive Ion-Chromatographic Determination of Citric Acid in Urine

  • Michele Petrarulo,
  • Marta Leporati,
  • Federica Pullara,
  • Maura Frattini,
  • Vita Nannavecchia,
  • Martino Marangella and
  • Domenico Cosseddu

Urine citrate analysis is relevant in the screening and monitoring of patients with calcium nephrolithiasis. A sensitive, fast, easy, and low-maintenance ion chromatographic (IC) method with conductivity detection for the analysis of urine citrate is...

  • Article
  • Open Access
7 Citations
3,157 Views
12 Pages

In this experiment, the Box–Behnken design (BBD) of the response surface methodology (RSM) was used to optimize the ultrasound-assisted extraction variables (liquid-to-solid ratio, extraction temperature, and time) to obtain the maximum yield o...

  • Article
  • Open Access
8 Citations
3,507 Views
15 Pages

Measuring Vitamin D3 Metabolic Status, Comparison between Vitamin D Deficient and Sufficient Individuals

  • Laura de los Santos Castillo-Peinado,
  • Mónica Calderón-Santiago,
  • Aura Dulcinea Herrera-Martínez,
  • Soraya León-Idougourram,
  • María Ángeles Gálvez-Moreno,
  • Rafael Luis Sánchez-Cano,
  • Roger Bouillon,
  • Jose Manuel Quesada-Gómez and
  • Feliciano Priego-Capote

The main branch of vitamin D3 metabolism involves several hydroxylation reactions to obtain mono-, di- and trihydroxylated metabolites, including the circulating and active forms—25(OH)D3 and 1,25(OH)2D3, respectively. However, most clinical tr...

  • Article
  • Open Access
8 Citations
3,699 Views
10 Pages

Quantitative Analysis of Anthocyanins in Grapes by UPLC-Q-TOF MS Combined with QAMS

  • Xue Li,
  • Wei Wang,
  • Suling Sun,
  • Junhong Wang,
  • Jiahong Zhu,
  • Feng Liang,
  • Yu Zhang and
  • Guixian Hu

A method for quantifying the anthocyanins in grapes was firstly developed by ultra-high performance liquid chromatography-quadrupole-time of flight mass spectrometry (UPLC-Q-TOFMS) combined with quantitative analysis of multi-components by single mar...

  • Review
  • Open Access
40 Citations
6,939 Views
30 Pages

A Review of the Removal of Dyestuffs from Effluents onto Biochar

  • Prakash Parthasarathy,
  • Samra Sajjad,
  • Junaid Saleem,
  • Mohammad Alherbawi and
  • Gordon Mckay

The study provides a review of various applications of biomass-derived biochars, waste-derived biochars, and modified biochars as adsorbent materials for removing dyestuff from process effluents. Processing significant amounts of dye effluent dischar...

  • Article
  • Open Access
2 Citations
2,748 Views
15 Pages

Phytochemical Characterization and Heavy Metal and Thermal Analyses of Saussurea hypoleuca Root and Evaluation of Its Anthelmintic and Antioxidant Activity In Vitro and In Silico

  • Sameh S. Elhady,
  • Numera Arshad,
  • Saiqa Ishtiaq,
  • Roula Bayram,
  • Adnan Amin,
  • Hanin A. Bogari,
  • Reda F. A. Abdelhameed,
  • Fadia S. Youssef and
  • Mohamed L. Ashour

Phytochemical characterization of the ethyl acetate fraction of Saussurea hypoleuca root extract resulted in the isolation of oleic acid (1) and luteolin (2), which were isolated for the first time from Saussurea hypoleuca root. A heavy metal analysi...

  • Article
  • Open Access
6 Citations
6,311 Views
15 Pages

In this study, the steam distillation process of volatile oil from Angelicaesinensis Radix was optimized according to the concept of quality-by-design. A homemade glass volatile oil extractor was used to achieve better cooling of the volatile oil. Fi...

  • Communication
  • Open Access
12 Citations
4,574 Views
13 Pages

Isotopic Characterization of Italian Industrial Hemp (Cannabis sativa L.) Intended for Food Use: A First Exploratory Study

  • Marco Calvi,
  • Luana Bontempo,
  • Sarah Pizzini,
  • Lorenzo Cucinotta,
  • Federica Camin and
  • Barbara Stenni

In this study, Italian industrial hemp (Cannabis sativa L.) intended for food use was isotopically characterized for the first time. The stable isotope ratios of five bioelements were analyzed in different parts of the plant (i.e., roots, stems, infl...

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Separations - ISSN 2297-8739