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Crystals 2017, 7(10), 290;

Synthesis and X-ray Crystal Structure of N’-Cyano-N,N’-dimethyl-4-nitrobenzohydrazide

Helmholtz-Zentrum Dresden-Rossendorf, Institut für Radiopharmazeutische Krebsforschung, Bautzner Landstraße 400, D-01328 Dresden, Germany
Anorganische Festkörperchemie, Institut für Chemie, Universität Rostock, Albert-Einstein-Straße 3a, D-18059 Rostock, Germany
Author to whom correspondence should be addressed.
Academic Editor: Shujun Zhang
Received: 29 August 2017 / Revised: 18 September 2017 / Accepted: 19 September 2017 / Published: 26 September 2017
(This article belongs to the Section Crystal Engineering)
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Using a two-step procedure, N’-cyano-N,N’-dimethyl-4-nitrobenzohydrazide was synthesized. The structure was established using single crystal X-ray diffraction. It crystalized in the orthorhombic space group P212121 where a = 8.1974(6), b = 10.6696(7), and c = 12.9766(8) Å. The first reported crystal structure of an acyclic cyanohydrazide is discussed with a focus on the geometry of the hydrazide moiety, but intermolecular contacts in the crystal are also considered. View Full-Text
Keywords: N,N’-diacylhydrazines; cyanamides; X-ray structure; resonance electron transfer; enzyme inhibition; bioconjugation N,N’-diacylhydrazines; cyanamides; X-ray structure; resonance electron transfer; enzyme inhibition; bioconjugation

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Löser, R.; Pitzschler, R.; Köckerling, M. Synthesis and X-ray Crystal Structure of N’-Cyano-N,N’-dimethyl-4-nitrobenzohydrazide. Crystals 2017, 7, 290.

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