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Int. J. Mol. Sci. 2014, 15(2), 1842-1851;

Structural and Optical Properties of Nanoscale Galinobisuitite Thin Films

Department of Zoology, Science College, King Saud University, P.O. Box 2455, Riyadh 11451, Saudi Arabia
Electron Microscope and Thin Films Department, National Research Center (NRC), El-Behooth Street, Dokki, Cairo 12622, Egypt
Laboratory of Surface Chemistry and Catalysis, Physical Chemistry Department, National Research Center, Dokki, Cairo 12622, Egypt
Author to whom correspondence should be addressed.
Received: 26 October 2013 / Revised: 9 January 2014 / Accepted: 13 January 2014 / Published: 27 January 2014
(This article belongs to the Section Materials Science)
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Galinobisuitite thin films of (Bi2S3)(PbS) were prepared using the chemical bath deposition technique (CBD). Thin films were prepared by a modified chemical deposition process by allowing the triethanolamine (TEA) complex of Bi3+ and Pb2+ to react with S2− ions, which are released slowly by the dissociation of the thiourea (TU) solution. The films are polycrystalline and the average crystallite size is 35 nm. The composition of the films was measured using the atomic absorption spectroscopy (AAS) technique. The films are very adherent to the substrates. The crystal structure of Galinobisuitite thin films was calculated by using the X-ray diffraction (XRD) technique. The surface morphology and roughness of the films were studied using scanning electron microscopes (SEM), transmission electron microscopes (TEM) and stylus profilers respectively. The optical band gaps of the films were estimated from optical measurements. View Full-Text
Keywords: Galinobisuitite (Bi2S3)(PbS) thin film; CBD; nanoscale structural; XRD; AAS; optical band gap Galinobisuitite (Bi2S3)(PbS) thin film; CBD; nanoscale structural; XRD; AAS; optical band gap
This is an open access article distributed under the Creative Commons Attribution License (CC BY 3.0).

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Abd-Elkader, O.H.; Deraz, N.M. Structural and Optical Properties of Nanoscale Galinobisuitite Thin Films. Int. J. Mol. Sci. 2014, 15, 1842-1851.

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