Effects of Sintering Temperature Variation on Synthesis of Glass-Ceramic Phosphor Using Rice Husk Ash as Silica Source
Abstract
:1. Introduction
2. Materials and Methods
2.1. Preparation and Synthesis of Silica (SiO2) from Rice Husk
2.2. Synthesis of Zinc-Boro-Silicate (ZBS) Glass-Ceramic
2.3. Characterization of Physical Properties
2.4. Characterization of Structural and Luminescence Properties
3. Results and Discussion
3.1. Chemical and Structural Characterization of Rice Husk Ash (RHA)
3.2. Characterization of the ZnO-B2O3-SiO2 (ZBS) Glass
3.3. Physical Characterization of the ZnO-B2O3-SiO2 (ZBS) Glass-Ceramics
3.4. Structural Characterization of the ZnO-B2O3-SiO2 (ZBS) Glass-Ceramics
3.5. Optical Characterization of the ZnO-B2O3-SiO2 (ZBS) Glass-Ceramics
4. Conclusions
Author Contributions
Funding
Acknowledgments
Conflicts of Interest
References
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Sample(s) | Sintering Temperature (°C) | Holding Time (Hours) |
---|---|---|
A1 | 600 | 2 |
A2 | 600 | 4 |
A3 | 600 | 10 |
B1 | 700 | 2 |
B2 | 700 | 4 |
B3 | 700 | 10 |
C1 | 800 | 2 |
C2 | 800 | 4 |
C3 | 800 | 10 |
D1 | 900 | 2 |
D2 | 900 | 4 |
D3 | 900 | 10 |
Raw Materials | Constituents Oxides (wt%) | |||||
---|---|---|---|---|---|---|
SiO2 | K2O | CaO | Al2O3 | Others | LOI | |
RHA | 95.6 ± 0.1 | 1.4 ± 0.1 | 0.95 ± 0.1 | 0.71 ± 0.1 | 0.64 ± 0.1 | 0.7 ± 0.1 |
Sample (s) | A | B | C | D |
---|---|---|---|---|
true density (g·cm−3) | 4.515 | 4.520 | 4.664 | 4.716 |
bulk density (g·cm−3) | 3.119 | 3.440 | 3.559 | 3.674 |
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Abdul Wahab, R.A.; Mohd Zaid, M.H.; Aziz, S.H.A.; Amin Matori, K.; Fen, Y.W.; Yaakob, Y. Effects of Sintering Temperature Variation on Synthesis of Glass-Ceramic Phosphor Using Rice Husk Ash as Silica Source. Materials 2020, 13, 5413. https://doi.org/10.3390/ma13235413
Abdul Wahab RA, Mohd Zaid MH, Aziz SHA, Amin Matori K, Fen YW, Yaakob Y. Effects of Sintering Temperature Variation on Synthesis of Glass-Ceramic Phosphor Using Rice Husk Ash as Silica Source. Materials. 2020; 13(23):5413. https://doi.org/10.3390/ma13235413
Chicago/Turabian StyleAbdul Wahab, Rabiatul Adawiyah, Mohd Hafiz Mohd Zaid, Sidek Hj. Ab Aziz, Khamirul Amin Matori, Yap Wing Fen, and Yazid Yaakob. 2020. "Effects of Sintering Temperature Variation on Synthesis of Glass-Ceramic Phosphor Using Rice Husk Ash as Silica Source" Materials 13, no. 23: 5413. https://doi.org/10.3390/ma13235413