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22 pages, 14111 KB  
Article
Study on the Dewatering Mechanism of Fine Phosphate Tailings Slurrys Based on the Particle-Agent Interaction and Sedimentation Property
by Fang Li, Yuping Fan, Yuanpeng Fu, Xiaomin Ma, Xianshu Dong, Yangge Zhu, Wei Xiao and Wenjie Fang
Separations 2026, 13(4), 118; https://doi.org/10.3390/separations13040118 - 15 Apr 2026
Viewed by 294
Abstract
Fluorapatite is a typical phosphate rock resource. Fluorapatite tends to generate fine mud agglomeration, which induces dehydration challenges owing to its inherently fine particle size and negative surface charge. In this paper, phosphate tailings slurries from a phosphate mine in Hubei Province, China, [...] Read more.
Fluorapatite is a typical phosphate rock resource. Fluorapatite tends to generate fine mud agglomeration, which induces dehydration challenges owing to its inherently fine particle size and negative surface charge. In this paper, phosphate tailings slurries from a phosphate mine in Hubei Province, China, were selected as the research object, and flocculation–dehydration experiments were conducted using anionic, cationic, and nonionic polyacrylamide (PAM) flocculants. The results show that the maximum settling velocity is 51 mm/s and the moisture content of filter cake is 41.54%, which were obtained when the unit consumption of cationic flocculant with molecular weight 12 million was 1000 g/t. The mechanism of sedimentation and dehydration was studied by infrared spectroscopy and a particle size analyzer. The results showed that polyacrylamide was effectively adsorbed on the mineral surface, and the size of flocs increased significantly. Finally, the mechanism of sedimentation and dehydration was proposed. It has important guiding significance for the efficient solid–liquid separation and water circulation of fluorapatite mineral processing wastewater. Full article
(This article belongs to the Special Issue Separation Technology in Mineral Processing)
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22 pages, 3350 KB  
Article
Toward Mechanism-Driven Control: A Soft-Sensor for Zeta Potential and Settling-Decisive Parameters in Coal Slime Water Treatment
by Jing Chang, Bianbian Guo, Guoyu Bai, Xinyuan Zhang, Hang Zhang, Wei Zhao and Zhen Li
Separations 2026, 13(4), 115; https://doi.org/10.3390/separations13040115 - 13 Apr 2026
Viewed by 291
Abstract
Intelligent dosing in coal slime water treatment remains a challenge due to the lack of real-time and solid hardware-based measurement of key microscopic parameters governing the settling process, particularly zeta potential. This study proposes a soft-sensor method using Sparrow Search Algorithm-optimized Extreme Learning [...] Read more.
Intelligent dosing in coal slime water treatment remains a challenge due to the lack of real-time and solid hardware-based measurement of key microscopic parameters governing the settling process, particularly zeta potential. This study proposes a soft-sensor method using Sparrow Search Algorithm-optimized Extreme Learning Machine (SSA-ELM) to simultaneously predict four critical settling process parameters: settling velocity, supernatant turbidity, sediment layer height, and zeta potential. Key variables influencing the coal slime water settling process, including coal slime water concentration, fines content, water hardness, pH, and chemical dosage, were investigated, and the experimental data were used as inputs for the development of the prediction model. The prediction performance of the proposed SSA-ELM model was evaluated against standard ELM and SSA-optimized Back Propagation (BP) models. The results demonstrate that the SSA-ELM model achieved superior prediction accuracy for all parameters, with R2 values ranging from 0.95 to 0.98, while maintaining favorable computational efficiency. This study establishes a method for virtual measurement of zeta potential, providing a crucial data foundation for developing mechanism-driven, intelligent dosing systems aimed at precise intelligent control and reduced chemical consumption for coal preparation plants. Full article
(This article belongs to the Special Issue Separation Techniques for Wastewater Treatment)
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16 pages, 1007 KB  
Article
Formation of a High-Density Algal-Bacterial Flocculent Biomass in a Pilot-Scale Raceway Pond Treating Municipal Wastewater
by Styliani E. Biliani, Dimitrios Kakavas and Ioannis D. Manariotis
Appl. Sci. 2026, 16(8), 3761; https://doi.org/10.3390/app16083761 - 12 Apr 2026
Viewed by 346
Abstract
This study provides novel insights into the gradual development of an algal-bacterial self-flocculent biomass in a 400 L pilot-scale raceway pond for wastewater treatment to enhance sustainability and minimize environmental footprint. The synergetic interaction of algal-bacteria consortia improves nutrient removal while enabling biomass [...] Read more.
This study provides novel insights into the gradual development of an algal-bacterial self-flocculent biomass in a 400 L pilot-scale raceway pond for wastewater treatment to enhance sustainability and minimize environmental footprint. The synergetic interaction of algal-bacteria consortia improves nutrient removal while enabling biomass concentration increase. Initially, the microalgae-bacteria biomass was gradually developed by increasing the operating volume from 60 to 400 L. After 80 days, the biomass reached a plateau at a concentration of about 4 g L−1, and exhibited excellent settling characteristics. The initial settling velocity was 14.8 cm min−1 and a settling time of 3 min was required to achieve efficient separation. The reactor achieved high treatment efficiency of about 95% for all nutrients (organic matter, nitrogen and phosphorous) after the 80th day. The kinetic analysis showed that nutrient removal followed first-order kinetics, with soluble chemical oxygen demand and ammonia removal reaching 0.017 and 0.020 h−1, respectively. The results demonstrate high pollutant removal efficiencies and design guidelines for the use of increased concentrations of microalgae–bacteria consortia in urban wastewater treatment practice, an alternative green way for solving present-day wastewater treatment problems. Full article
(This article belongs to the Section Environmental Sciences)
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25 pages, 2080 KB  
Article
Design and Simulation Analysis of Attitude Control Algorithms for OPS-SAT-1
by Juan Carlos Crespo, María Royo, Álvaro Bello, Karl Olfe, Victoria Lapuerta and José Miguel Ezquerro
Aerospace 2026, 13(4), 320; https://doi.org/10.3390/aerospace13040320 - 29 Mar 2026
Viewed by 424
Abstract
This work presents the design of an attitude control experiment for onboard OPS-SAT-1 satellite execution, conceived with inherent extensibility to future mission architectures. OPS-SATs are ESA nanosatellite mission series designed as an in-orbit testbed for validating novel software and control techniques under real [...] Read more.
This work presents the design of an attitude control experiment for onboard OPS-SAT-1 satellite execution, conceived with inherent extensibility to future mission architectures. OPS-SATs are ESA nanosatellite mission series designed as an in-orbit testbed for validating novel software and control techniques under real space conditions, OPS-SAT-1 being the first mission. Equipped with an advanced payload computer, OPS-SAT-1 enabled experimentation with innovative mission operations, including real-time attitude control strategies. Two attitude control algorithms, a modified Proportional–Integral–Derivative (mPID) and a fuzzy logic controller, were designed and implemented for the OPS-SAT-1. The design methodology applied to these controllers consisted of (i) modelling the space environment and satellite characteristics, (ii) assessing actuator feasibility, (iii) determining the operational ranges for attitude error and angular velocity, (iv) parametrizing controllers within these ranges, (v) fine-tuning controllers using multi-objective genetic optimization, and (vi) robustness analysis using the Monte Carlo method. Despite the technical issues related to communication with the OPS-SAT-1 hardware, which prevented the execution of the experiment in orbit, this work presents the simulation results that were obtained. These results indicate that fuzzy logic controllers may outperform PID controllers in terms of the accumulated error, settling time and steady-state error, whereas power efficiency appears to be less robust than in the PID. This suggest that a large uncertainty in the model could lead the PID to become more efficient. Near the nominal scenario, the fuzzy controller achieves superior error–cost trade-offs, enabling precise attitude stabilization with lower energy consumption. These findings suggest the potential advantages of modern control approaches compared to classical methods, which will be further assessed through future in-orbit experiments. Full article
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27 pages, 14936 KB  
Article
Experimentally Validated Discrete Phase Model for PM2.5 and PM10 with Numerical Transport Mapping
by Ren Paulo Estaquio, Ma Kevina Canlas, Neil Astrologo, Job Immanuel Encarnacion, Joshua Agar, Ken Bryan Fernandez, Julius Rhoan Lustro and Joseph Gerard Reyes
Fluids 2026, 11(4), 90; https://doi.org/10.3390/fluids11040090 - 29 Mar 2026
Viewed by 592
Abstract
Indoor exposure to particulate matter (PM) depends on ventilation-driven transport, yet sensor placement in real rooms is often based on limited point data. This study develops and experimentally validates a transient CFD framework, using RANS airflow coupled with Lagrangian discrete phase tracking, to [...] Read more.
Indoor exposure to particulate matter (PM) depends on ventilation-driven transport, yet sensor placement in real rooms is often based on limited point data. This study develops and experimentally validates a transient CFD framework, using RANS airflow coupled with Lagrangian discrete phase tracking, to map PM2.5 and PM10 in a full-scale 2.0 × 3.0 × 2.5 m bedroom with a fixed, non-oscillating pedestal fan and an open window. Airflow was verified by grid independence and validated against 10-point velocity measurements (RMSE = 0.108 m·s−1). Incense experiments (≈31 min burn) provided PM time series over the first 60 min at 16 locations on two heights; emission rate, burning time, and air-change rate (1.96–5.39 ACH) were calibrated so that accepted models achieved aggregate R2 > 0.90. Spatial mapping on a 0.5 m grid shows that PM behavior is governed primarily by airflow-defined accumulation pockets rather than by source proximity alone. A near-source region consistently captured strong early-time peaks, whereas remote low-exchange pockets remained elevated during the decay phase. For PM2.5, the most persistent hotspot is a ceiling-adjacent recirculation pocket, while for PM10, gravitational settling shifted the dominant hotspots toward floor-layer, low-velocity regions. An exposure score combining normalized peak and time-averaged concentrations, interpreted together with particle-track persistence metrics, distinguished transiently traversed regions from true retention pockets. The results show that sensor placement should follow the monitoring objective: near-source regions are more responsive to peak events, ceiling pockets are more suitable for persistent PM2.5 monitoring, and floor hotspots are more critical for PM10. No single fixed sensor location adequately represents both particle sizes in the present bedroom and ventilation configuration. Full article
(This article belongs to the Special Issue CFD Applications in Environmental Engineering)
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33 pages, 5971 KB  
Article
Energy-Efficient and Reliable Hydrodynamic Separation of Spent Drilling Fluids: Experiments, Modeling, and Process Stability
by Bakytzhan Kaliyev, Beibit Myrzakhmetov, Bulbul Mauletbekova, Bibinur Akhymbayeva, Gulzada Mashatayeva, Yerik Merkibayev, Vladimir I. Golik and Boris V. Malozyomov
Energies 2026, 19(7), 1659; https://doi.org/10.3390/en19071659 - 27 Mar 2026
Viewed by 453
Abstract
The treatment of spent drilling fluids generated during the drilling of technological wells for uranium production represents an important engineering and environmental challenge associated with high energy consumption, significant waste generation, and the need for rational water use under arid regional conditions. Conventional [...] Read more.
The treatment of spent drilling fluids generated during the drilling of technological wells for uranium production represents an important engineering and environmental challenge associated with high energy consumption, significant waste generation, and the need for rational water use under arid regional conditions. Conventional phase separation methods based on gravitational settling and chemical–mechanical treatment are characterized by limited process controllability, long processing times, and increased consumption of reagents and energy. This study proposes an energy-efficient and reliable hydrodynamic technology for the treatment of spent drilling fluids based on the formation of controlled turbulent structures without the use of mechanical drives. The research object comprised spent drilling fluids (SDFs) generated during the drilling of technological wells for uranium production in the southern regions of the Republic of Kazakhstan and the Kyzylorda region. Experimental investigations were carried out using a laboratory–pilot hydrodynamic disperser with variations in velocity gradient, treatment time, flocculant dosage, and suspension flow rate. A mathematical model linking hydrodynamic process parameters with phase separation kinetics and energy characteristics was developed. Model calibration by weighted nonlinear least squares yielded a stable parameter set with 95% confidence intervals, and model validation demonstrated good agreement between calculated and experimental data (MAPE 8.4%; maximum relative error 11.8%). It was established that the use of a hydrodynamic disperser provides separation efficiency of up to 90–95% under optimal operating conditions while reducing specific energy consumption and maintaining stable repeated-cycle performance within the investigated operating window. Experimental results confirm that implementation of the hydrodynamic technology enables a reduction in sludge volume by 40–60%, recovery of up to 60–80% of process water, and a significant decrease in waste requiring transportation and disposal. The obtained results demonstrate the high environmental and resource-saving efficiency of the proposed technology and its suitability for scaling and industrial implementation at facilities drilling technological wells for uranium production. The developed hydrodynamic approach can be considered an effective engineering platform for creating energy-efficient and sustainable systems for drilling fluid treatment in regions with limited water resources and remote industrial infrastructure. Full article
(This article belongs to the Section B: Energy and Environment)
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19 pages, 3132 KB  
Article
Inorganic–Organic Hybrid Polymer for Fine-Rich Coal Slime Water Treatment: Performance and Interfacial Adsorption Mechanism on Kaolinite Aluminol Surface
by Jing Chang, Hang Zhao, Shizhen Liang, Xihao Feng, Jia Xue and Wei Zhao
Separations 2026, 13(3), 99; https://doi.org/10.3390/separations13030099 - 19 Mar 2026
Viewed by 358
Abstract
High-ash coal slime water, characterized by its stable colloidal suspension of fine kaolinite particles, poses a significant challenge in the coal preparation industry because it is hard to achieve efficient solid–liquid separation. While traditional coagulants and flocculants often suffer from limited bridging capabilities [...] Read more.
High-ash coal slime water, characterized by its stable colloidal suspension of fine kaolinite particles, poses a significant challenge in the coal preparation industry because it is hard to achieve efficient solid–liquid separation. While traditional coagulants and flocculants often suffer from limited bridging capabilities and distinct pH sensitivity, novel molecular architectures offer potential solutions. In this study, a star-shaped inorganic–organic hybrid flocculant (Al-PAM) was synthesized via in situ polymerization. Its flocculation performance and interfacial adsorption mechanism on the specifically targeted aluminol basal plane of kaolinite were systematically investigated and compared with Polyaluminum Chloride (PAC), Non-ionic Polyacrylamide (NPAM), and their combination (PAC + NPAM). Settling tests revealed that Al-PAM exhibited superior performance at a significantly lower dosage (10 mg∙L−1) compared to the PAC + NPAM binary reagent system. It achieved a rapid initial settling velocity and reduced the supernatant turbidity to 48.45 NTU, while maintaining a near-neutral pH favorable for water recycling. Furthermore, Quartz Crystal Microbalance with Dissipation (QCM-D) monitoring confirmed that Al-PAM forms a thick, viscoelastic, and irreversible adsorption layer on the Al2O3 substrate. The dissipation shifts (ΔD) revealed that the star-shaped architecture promotes distinct bridging and electrostatic adsorption, overcoming the limitation of linear polymers. This work elucidates the specific contribution of the alumina-surface interaction with flocculants and proposes an efficient strategy for treating refractory coal slime water. Full article
(This article belongs to the Special Issue Separation Technology in Mineral Processing)
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27 pages, 8914 KB  
Article
Spatial and Vertical Distribution of Suspended Sediment Concentration in Haizhou Bay Based on Remote Sensing: Implications for Sustainable Coastal Management
by Wenjin Zhu, Chunyan Mo, Xiaotian Dong and Weicheng Lv
Sustainability 2026, 18(6), 2965; https://doi.org/10.3390/su18062965 - 17 Mar 2026
Viewed by 311
Abstract
Suspended sediment concentration (SSC) strongly influences estuarine erosion–deposition processes, navigation safety, and coastal engineering stability. However, conventional remote sensing techniques are limited to surface SSC and cannot characterize vertical sediment structures. In this study, Landsat 8 OLI imagery was combined with in situ [...] Read more.
Suspended sediment concentration (SSC) strongly influences estuarine erosion–deposition processes, navigation safety, and coastal engineering stability. However, conventional remote sensing techniques are limited to surface SSC and cannot characterize vertical sediment structures. In this study, Landsat 8 OLI imagery was combined with in situ SSC profiles from six stations in the Guan River Estuary–Haizhou Bay system to retrieve full-depth sediment distributions. A band-combination inversion model using (B3 + B2)/B1 achieved the highest accuracy (R2 = 0.679), and an improved vertical distribution model was developed by incorporating turbulent shear (G) into the Rouse framework. Results indicate that surface SSC ranged from 0.15 to 0.86 kg/m3, while middle- and bottom-layer SSC reached up to 1.20 kg/m3 and 1.77 kg/m3, respectively, exhibiting a consistent east–high and west–low spatial pattern. Settling velocity (SSV) varied from 3 × 10−6 to 1.49 × 10−2 m/s and showed a positive correlation with SSC at low concentrations and a negative correlation at high concentrations due to flocculation effects. This integrated framework provides a rapid, low-cost method for full-water-column sediment assessment in estuaries and coastal zones, supporting engineering design, navigation maintenance, and sediment management. A better understanding of sediment transport processes in Haizhou Bay is important for maintaining shoreline stability and ecological balance in this semi-enclosed coastal system. The findings of this study provide a scientific basis for sediment management and environmental regulation, which can contribute to the long-term sustainable development of coastal environments in the Yellow Sea region. Full article
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19 pages, 20315 KB  
Article
Experimental Quantization of Droplet Spatial Distribution in Icing Wind Tunnel with HACPI
by Letian Zhang, Boyi Wang, Yingchun Wu, Si Li, Zhiqiang Zhang, Xiangdong Guo, Xuecheng Wu, Quanzhong Xia and Zhen Liu
Aerospace 2026, 13(3), 274; https://doi.org/10.3390/aerospace13030274 - 15 Mar 2026
Viewed by 428
Abstract
The cloud spatial uniformity in the test section is crucial for icing wind tunnels in aircraft icing research and airworthiness certification. To achieve uniform supercooled large droplet (SLD) icing conditions, both the spatial variation in droplet size distribution and the concentration should be [...] Read more.
The cloud spatial uniformity in the test section is crucial for icing wind tunnels in aircraft icing research and airworthiness certification. To achieve uniform supercooled large droplet (SLD) icing conditions, both the spatial variation in droplet size distribution and the concentration should be considered. In this study, the spatial distribution of droplets under three SLD conditions is explored in the Aviation Industry Corporation of China Aerodynamics Research Institute (AVICARI)’s FL-61 icing wind tunnel. Measurements are conducted at 12 test points in vertical and horizontal directions using the holographic airborne cloud particle imager (HACPI) in conjunction with a two-axis traversing system. The droplet images obtained at specific test points below the test section centerline show deformation phenomena for droplets larger than 400 μm. Additionally, the aspect ratio of deformed droplets increases with droplet size. The spatial evolution of the median volume diameter (MVD) and liquid water content (LWC) is examined. For two spray arrangements where the activated nozzles are positioned close, the test point where the LWC peak in the vertical direction occurs is higher than that of the MVD peak. Further analysis focuses on the size distribution of droplets in the vertical direction. The results show that the settling effect of the droplets larger than 50 μm is evident under a flow velocity of 78 m/s. Meanwhile, the position where large droplets tend to appear lowers as the droplet size increases. Finally, the spatial uniformity of droplet size distributions at the same radial distance is discussed. Full article
(This article belongs to the Special Issue Deicing and Anti-Icing of Aircraft (Volume IV))
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17 pages, 18685 KB  
Article
Fabrication and Drag Reduction Performance of Bionic Surfaces Featuring Staggered Shield Scale Structures
by Xin Gu, Pan Cao, Xiuqin Bai and Yifeng Fu
Biomimetics 2026, 11(3), 209; https://doi.org/10.3390/biomimetics11030209 - 14 Mar 2026
Viewed by 603
Abstract
To investigate the drag reduction mechanism of shark skin placoid scales and develop high-efficiency drag-reducing surfaces, this study designed and fabricated a biomimetic shark skin surface featuring staggered microscale groove structures. The fabrication process involved laser etching on silicon wafers to create a [...] Read more.
To investigate the drag reduction mechanism of shark skin placoid scales and develop high-efficiency drag-reducing surfaces, this study designed and fabricated a biomimetic shark skin surface featuring staggered microscale groove structures. The fabrication process involved laser etching on silicon wafers to create a placoid microstructure template, followed by polydimethylsiloxane (PDMS) replication to obtain biomimetic shark skin samples. Sedimentation experiments demonstrated that the biomimetic surface significantly reduced settling time compared to a smooth surface, achieving a drag reduction rate of 5.65%. Further computational fluid dynamics (CFD) simulations were conducted to analyze the near-wall flow characteristics around the biomimetic surface. The results revealed that the drag reduction mechanism primarily stems from the effective regulation of near-wall laminar flow by the micro-groove structures: a low-velocity fluid layer formed within the grooves reduces the near-wall velocity gradient, thereby decreasing frictional drag, while stable recirculation zones develop within the grooves, contributing to momentum redistribution and reduced energy dissipation. Additionally, the staggered arrangement of the grooves promotes a smoother pressure distribution along the flow direction, mitigating pressure drag by reducing the pressure differential between windward and leeward surfaces. The experimental and simulation results showed excellent agreement (simulated drag reduction rate: 5.08%), collectively verifying the feasibility and effectiveness of the proposed biomimetic placoid structure in achieving fluid drag reduction. Full article
(This article belongs to the Section Biomimetic Surfaces and Interfaces)
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19 pages, 3695 KB  
Article
Low Reynolds Number Settling of Bent Rods in Quiescent Fluid
by Amirhossein Hamidi, Daniel Daramsing, Mark D. Gordon and Ronald E. Hanson
Fluids 2026, 11(3), 72; https://doi.org/10.3390/fluids11030072 - 9 Mar 2026
Viewed by 419
Abstract
This study experimentally investigates the settling behavior of bent (V-shaped and curved) and straight rods in a quiescent fluid at low and finite Reynolds numbers (Re<3). The impact of the rod morphology on the terminal settling velocity and drag [...] Read more.
This study experimentally investigates the settling behavior of bent (V-shaped and curved) and straight rods in a quiescent fluid at low and finite Reynolds numbers (Re<3). The impact of the rod morphology on the terminal settling velocity and drag coefficient was examined, with a particular focus on V-shaped rods compared to straight rods of the same dimensions (diameter and length) and curved rods of the same dimensions and projected area. The results show that V-shaped rods consistently settle faster than straight rods, with velocity differences influenced by the bend angle. This velocity difference reaches a maximum of 57% for a V-shaped rod with a diameter of 0.50 mm, an aspect ratio of 90, and a bend angle of 45 degrees. When compared to curved rods, V-shaped rods exhibit slightly higher terminal velocities, with a maximum difference of 4% in this study, attributed to differences in mean inclination angles. Furthermore, the drag coefficient trends reflect the interplay between the settling velocity and projected area changes with the rod geometry. A new semi-empirical model with an RMS error of 7.1% was also developed to predict the drag coefficients and terminal velocities of straight and bent rods within the ranges studied. These findings and the model presented underscore the significance of the fibre shape in accurately predicting settling dynamics, with implications for atmospheric transport modeling and industrial applications involving fibrous particles. Full article
(This article belongs to the Section Flow of Multi-Phase Fluids and Granular Materials)
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19 pages, 5971 KB  
Article
Sedimentary and Hydrodynamic Controls on Shale Oil Sweet Spots: A New Storm Deposition Model for the Gulong Sag, Songliao Basin
by Yinfan Li, Ying Song, Bowen Xiong and Jianhua Zhong
Energies 2026, 19(5), 1142; https://doi.org/10.3390/en19051142 - 25 Feb 2026
Viewed by 381
Abstract
The First Member of the Cretaceous Qingshankou Formation (K2qn1) in the Gulong Sag, Songliao Basin, contains vast shale oil resources conventionally interpreted as deposits of suspension settling in a quiescent, anoxic deep-lacustrine environment. However, this static “deep-lake” model fails [...] Read more.
The First Member of the Cretaceous Qingshankou Formation (K2qn1) in the Gulong Sag, Songliao Basin, contains vast shale oil resources conventionally interpreted as deposits of suspension settling in a quiescent, anoxic deep-lacustrine environment. However, this static “deep-lake” model fails to account for the strong lithofacies heterogeneity and high-energy sedimentary records observed in recently acquired core data. This study reconstructs the sedimentary dynamics of the K2qn1 shale through high-resolution core description, thin-section petrography, and flow-loop hydrodynamic simulations. We identify abundant sedimentary structures diagnostic of high-energy combined flows, including Hummocky Cross-Stratification (HCS), Swaley Cross-Stratification (SCS), erosional scour surfaces, and large-scale tabular intraclasts (up to 40 mm). Hydrodynamic simulations, utilizing an “equivalent substitution” method, demonstrate that the Minimum Vertical Suspension Velocity (Vmf) required to transport these large intraclasts exceeds 1.0 m/s. This threshold is 1 to 5 orders of magnitude higher than theoretical values derived from classical settling equations, confirming that the paleolake bottom was frequently perturbed by high-velocity storm-driven currents. Consequently, we propose an “Intermittent High-Energy Deposition Model,” wherein background suspension settling was punctuated by episodic storm events. We argue that these high-energy events facilitated organic matter enrichment through a “Transport-Burial Pump” mechanism, which operated in concert with the chemical stratification associated with the Oceanic Anoxic Event 2 (OAE2) to enable rapid physical burial and sealing of organic matter. These findings challenge the traditional fine-grained sedimentological paradigm and suggest that storm-reworked intervals—characterized by enhanced brittleness and hydrodynamic winnowing—constitute the primary “sweet spots” for lacustrine shale oil exploration. Full article
(This article belongs to the Section H: Geo-Energy)
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21 pages, 5543 KB  
Article
Design and Research of Soil Disinfection Pesticide Application Control System Based on PSO-PID Algorithm
by Mengdi Xu, Zhichong Wang, Xiangjie Niu, Zhen Wang, Wei Zou, Changyuan Zhai and Si Li
Agriculture 2026, 16(4), 481; https://doi.org/10.3390/agriculture16040481 - 21 Feb 2026
Cited by 1 | Viewed by 363
Abstract
Soil-borne diseases and continuous cropping obstacles have become critical factors constraining sustainable agricultural development. Traditional pesticide application methods commonly suffer from uneven dosage distribution, significant chemical waste, and environmental pollution. To enhance the precision and system stability of soil disinfection, this paper designs [...] Read more.
Soil-borne diseases and continuous cropping obstacles have become critical factors constraining sustainable agricultural development. Traditional pesticide application methods commonly suffer from uneven dosage distribution, significant chemical waste, and environmental pollution. To enhance the precision and system stability of soil disinfection, this paper designs a precision pesticide application system for soil disinfection based on the Particle Swarm Optimization Proportional-Integral-Derivative algorithm (PSO-PID). Centered on a C37 controller, the system integrates the application pipeline, pumps, electric ball valves, multiple sensors, and a control terminal. The PSO-PID algorithm was deployed on the Codesys V2.3 platform, achieving precise flow control by adjusting electric ball valve openings in conjunction with velocity feedback. Simulink simulations showed that the PSO-PID algorithm outperforms conventional PID control in terms of settling time, overshoot, and steady-state error. Bench tests further validated the effectiveness of the proposed algorithm. Compared to conventional PID, the PSO-PID algorithm demonstrates superior control accuracy, faster response time, and enhanced application stability, with relative errors of 2.33%, 1.25%, and 1.20% respectively, while those of the conventional PID algorithm reach 3.67%, 3.35% and 4.88% respectively, representing a reduction of approximately 50% compared with the conventional PID algorithm. The results of the system application uniformity test indicated that the PSO-PID algorithm reduces relative error by approximately 40% compared to conventional PID, with the coefficients of variation being 2.02%, 1.73% and 1.81% respectively, which represented a significant improvement over those of the conventional PID algorithm (3.36%, 3.13% and 3.81%). Both application uniformity and stability outperform conventional PID algorithms, effectively minimizing application deviation. It outperforms conventional PID in both application uniformity and stability, effectively minimizing application deviation. The findings demonstrate that the proposed PSO-PID application control method achieves high control accuracy and application stability, providing reliable technical support for precision soil disinfection application. Full article
(This article belongs to the Special Issue Integrated Management of Soil-Borne Diseases—Second Edition)
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23 pages, 2936 KB  
Article
Performance of a High-Molecular-Weight AM/AA Copolymer in a CO2–Water Polymer Hybrid Fracturing Fluid Under High-Temperature and High-Pressure Conditions
by Tengfei Chen, Shutao Zhou, Tingwei Yao, Meilong Fu, Zhigang Wen and Quanhuai Shen
Polymers 2026, 18(3), 418; https://doi.org/10.3390/polym18030418 - 5 Feb 2026
Viewed by 547
Abstract
To reduce water consumption and potential formation damage associated with conventional water-based fracturing fluids while improving the proppant-carrying and flow adaptability of CO2-based systems without relying on specialized CO2 thickeners, a CO2–water polymer hybrid fracturing fluid was developed [...] Read more.
To reduce water consumption and potential formation damage associated with conventional water-based fracturing fluids while improving the proppant-carrying and flow adaptability of CO2-based systems without relying on specialized CO2 thickeners, a CO2–water polymer hybrid fracturing fluid was developed using an AM/AA copolymer (poly(acrylamide-co-acrylic acid), P(AM-co-AA)) as the thickening agent for the aqueous phase. Systematic experimental investigations were conducted under high-temperature and high-pressure conditions. Fluid-loss tests at different CO2 volume fractions show that the CO2–water polymer hybrid fracturing fluid system achieves a favorable balance between low fluid loss and structural continuity within the range of 30–50% CO2, with the most stable fluid-loss behavior observed at 40% CO2. Based on this ratio window, static proppant-carrying experiments indicate controllable settling behavior over a temperature range of 20–80 °C, leading to the selection of 60% polymer-based aqueous phase + 40% CO2 as the optimal mixing ratio. Rheological results demonstrate pronounced shear-thinning behavior across a wide thermo-pressure range, with viscosity decreasing systematically with increasing shear rate and temperature while maintaining continuous and reproducible flow responses. Pipe-flow tests further reveal that flow resistance decreases monotonically with increasing flow velocity and temperature, indicating stable transport characteristics. Phase visualization observations show that the CO2–water polymer hybrid fracturing fluid system exhibits a uniform milky dispersed appearance under moderate temperature or elevated pressure, whereas bubble-dominated structures and spatial phase separation gradually emerge under high-temperature and relatively low-pressure static conditions, highlighting the sensitivity of phase stability to thermo-pressure conditions. True triaxial hydraulic fracturing experiments confirm that the CO2–water polymer hybrid fracturing fluid enables stable fracture initiation and sustained propagation under complex stress conditions. Overall, the results demonstrate that the AM/AA copolymer-based aqueous phase can provide effective viscosity support, proppant-carrying capacity, and flow adaptability for CO2–water polymer hybrid fracturing fluid over a wide thermo-pressure range, confirming the feasibility of this approach without the use of specialized CO2 thickeners. Full article
(This article belongs to the Section Polymer Analysis and Characterization)
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15 pages, 1681 KB  
Article
EPS from Activated Sludge: Prospection of Bioflocculation and Catalytic Properties
by Sara Jaramillo Arvilla, Grazieli Pereira da Silva, Ismael Hernandes Pereira, Sofia Kremer de Souza, Carolina Gommersbach, Guilherme Urbano, Rodrigo de Almeida Mohedano, Paulo Belli Filho, Rejane Helena Ribeiro da Costa and Nelson Libardi
Processes 2026, 14(3), 547; https://doi.org/10.3390/pr14030547 - 4 Feb 2026
Viewed by 613
Abstract
The recovery of extracellular polymeric substances (EPS) from activated sludge (AS) represents a promising strategy to transform wastewater treatment plants (WWTPs) into resource recovery facilities within a circular economy framework. In this study, EPS was extracted from an AS process in a full-scale [...] Read more.
The recovery of extracellular polymeric substances (EPS) from activated sludge (AS) represents a promising strategy to transform wastewater treatment plants (WWTPs) into resource recovery facilities within a circular economy framework. In this study, EPS was extracted from an AS process in a full-scale WWTP, highlighting its catalytic and bioflocculant properties, which represent an innovation in the valorization of this biopolymer. The EPS was subsequently characterized in terms of polysaccharides, proteins, and enzymatic activities (amylase and lipase). The bioflocculation performance of the EPS was evaluated using activated sludge mixed liquor. Results showed that EPS recovery yields using 50 °C and 80 °C were 196.3 ± 38.2 mg EPS/g sludge and 283.5 ± 85.4 mg EPS/g sludge, respectively. Enzymatic assays confirmed amylase activity ranging from 100 to 350 U/g sludge according to the extraction temperature. Lipolytic activity (20 U/g sludge) was comparable to values reported in the literature for EPS from biological sludge. The addition of EPS significantly improved the sludge settling velocity (from 0.86 to 4.48 m/h) and the sludge volume index (from 118.6 to 35.5). However, EPS application also increased the resistance to filtration by 50% and reduced cellular respiration by approximately 40%. Overall, the findings demonstrate that EPS from activated sludge acts as an effective bioflocculant with relevant catalytic properties, highlighting its potential as a high-value biotechnological product while also pointing to operational challenges that require further optimization. Full article
(This article belongs to the Special Issue Enzyme Production Using Industrial and Agricultural By-Products)
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