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19 pages, 997 KiB  
Review
A Review of Bio-Inspired Actuators and Their Potential for Adaptive Vehicle Control
by Vikram Mittal, Michael Lotwin and Rajesh Shah
Actuators 2025, 14(7), 303; https://doi.org/10.3390/act14070303 - 20 Jun 2025
Viewed by 2059
Abstract
Adaptive vehicle control systems are crucial for enhancing safety, performance, and efficiency in modern transportation, particularly as vehicles become increasingly automated and responsive to dynamic environments. This review explores the advancements in bio-inspired actuators and their potential applications in adaptive vehicle control systems. [...] Read more.
Adaptive vehicle control systems are crucial for enhancing safety, performance, and efficiency in modern transportation, particularly as vehicles become increasingly automated and responsive to dynamic environments. This review explores the advancements in bio-inspired actuators and their potential applications in adaptive vehicle control systems. Bio-inspired actuators, which mimic natural mechanisms such as muscle movement and plant tropism, offer unique advantages, including flexibility, adaptability, and energy efficiency. This paper categorizes these actuators based on their mechanisms, focusing on shape memory alloys, dielectric elastomers, ionic polymer–metal composites, polyvinylidene fluoride-based electrostrictive actuators, and soft pneumatic actuators. The review highlights the properties, operating principles, and potential applications for each mechanism in automotive systems. Additionally, it investigates the current uses of these actuators in adaptive suspension, active steering, braking systems, and human–machine interfaces for autonomous vehicles. The review further outlines the advantages of bio-inspired actuators, including their energy efficiency and adaptability to road conditions, while addressing key challenges like material limitations, response times, and integration with existing automotive control systems. Finally, this paper discusses future directions, including the integration of bio-inspired actuators with machine learning and advancements in material science, to enable more efficient and responsive adaptive vehicle control systems. Full article
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22 pages, 6159 KiB  
Article
A Machine Vision System for Gear Defect Detection
by Pevril Demir Arı, Fatih Akkoyun and Ali Ercetin
Processes 2025, 13(6), 1727; https://doi.org/10.3390/pr13061727 - 31 May 2025
Viewed by 962
Abstract
This study introduces a machine vision system (MVS) developed for the inspection and removal of defective gears to enhance the efficiency of mass production processes. The system employs a rotary table that transports gears through the inspection stage at a controlled speed. Various [...] Read more.
This study introduces a machine vision system (MVS) developed for the inspection and removal of defective gears to enhance the efficiency of mass production processes. The system employs a rotary table that transports gears through the inspection stage at a controlled speed. Various defects, including missing teeth, surface irregularities, and dimensional deviations, are reliably identified through this method. Faulty gears are automatically separated from the production line using a pneumatic actuator. Experimental evaluations confirm the system’s high accuracy and consistency, with a defect detection standard deviation of less than 1%. This level of deviation corresponds to a defect detection accuracy exceeding 98%, with both precision and recall consistently surpassing 96%. By reducing manual intervention and accelerating quality control procedures, the proposed system contributes to improved production efficiency and product quality, offering a practical and effective solution for manufacturing environments. Full article
(This article belongs to the Section AI-Enabled Process Engineering)
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11 pages, 3315 KiB  
Article
Using Frozen Beads from a Mixture of Mesitylene and Meta-Xylene with Rupert’s Drop Properties in Cryogenic Neutron Moderators
by Maksim V. Bulavin and Ivan L. Litvak
J. Nucl. Eng. 2025, 6(2), 9; https://doi.org/10.3390/jne6020009 - 3 Apr 2025
Viewed by 485
Abstract
An experimental study was conducted on the feasibility of using frozen beads with the properties of Rupert’s drops—solid frozen beads with enhanced strength made from a mixture of aromatic hydrocarbons—in cryogenic neutron moderators utilizing bead technology. It is demonstrated that the use of [...] Read more.
An experimental study was conducted on the feasibility of using frozen beads with the properties of Rupert’s drops—solid frozen beads with enhanced strength made from a mixture of aromatic hydrocarbons—in cryogenic neutron moderators utilizing bead technology. It is demonstrated that the use of a new modification of the dosing device with a high discharge rate (approximately 6 units/s) significantly improves process efficiency. With standard pneumatic transport parameters maintained, it was possible to load solid frozen beads made from a mixture of mesitylene and meta-xylene into the cryogenic moderator chamber. The loading speed increased five-fold, while the beads remained intact during pneumatic transport. Full article
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20 pages, 5718 KiB  
Article
Design and Optimization of Divider Head Geometry in Air-Assisted Metering Devices for Enhanced Seed Distribution Accuracy
by Alfarog H. Albasheer, Qingxi Liao, Lei Wang, Elebaid Jabir Ibrahim, Wenli Xiao and Xiaoran Li
Agronomy 2025, 15(4), 769; https://doi.org/10.3390/agronomy15040769 - 21 Mar 2025
Cited by 1 | Viewed by 577
Abstract
Achieving precise seed distribution is essential for optimizing crop yields and agricultural productivity. This study examines the impact of divider head geometry on seed distribution accuracy in pneumatic air seeder systems using rapeseed, wheat, and rice. Three custom-designed divider heads—funnel distributor (A1), closed-funnel [...] Read more.
Achieving precise seed distribution is essential for optimizing crop yields and agricultural productivity. This study examines the impact of divider head geometry on seed distribution accuracy in pneumatic air seeder systems using rapeseed, wheat, and rice. Three custom-designed divider heads—funnel distributor (A1), closed-funnel distributor (A2), and cone-shaped distributor (A3)—were developed for an eight-furrow opener seeding system, each featuring eight outlets per opener. Bench tests at air pressures of 3, 3.5, 4, 4.5, 5, and 5.5 kPa and speeds of 4 and 5 km/h revealed significant variations in seed distribution accuracy among the designs. The A2 distributor demonstrated the lowest coefficient of variation (CV) across all seed types: 4.3%, 2.6%, and 6.95% for A1, A2, and A3 in wheat, respectively; 4.5%, 3.4%, and 6.2% in rice, respectively; and 0.3%, 0.1%, and 1.0% in rapeseed, respectively. Seed types also significantly influenced feed rate uniformity, with average CVs of 2.91% for rapeseed, 3.85% for rice, and 4.90% for wheat. CFD-DEM simulations validated the superior performance of the A2 distributor by analyzing flow fields and velocity distributions, showing reductions in CVs by 19.09–54.55% compared to A1 and A3. Thus, the A2 distributor was identified as the optimal design, significantly improving seeding uniformity across all seed types. In conclusion, this study provides critical insights for redesigning seed drill distribution heads to minimize turbulence in the seed–air mixture transport, enhancing seeding uniformity and increasing crop yields and agricultural productivity. Full article
(This article belongs to the Section Precision and Digital Agriculture)
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20 pages, 7166 KiB  
Article
Drag Force and Heat Transfer Characteristics of Ellipsoidal Particles near the Wall
by Yongkang Yang, Xinyu Dong and Ting Xiong
Water 2025, 17(5), 736; https://doi.org/10.3390/w17050736 - 3 Mar 2025
Cited by 1 | Viewed by 926
Abstract
This study investigates the force and heat transfer characteristics of oblate spheroidal particles in gas–solid two-phase flows near walls, addressing the influence of particle orientation, shape, Reynolds number, and particle–wall distance. These factors are critical in industrial processes such as pneumatic transport and [...] Read more.
This study investigates the force and heat transfer characteristics of oblate spheroidal particles in gas–solid two-phase flows near walls, addressing the influence of particle orientation, shape, Reynolds number, and particle–wall distance. These factors are critical in industrial processes such as pneumatic transport and crop drying, as well as in natural phenomena. Utilizing the Euler–Lagrangian model and large eddy simulation (LES), we simulated flow fields and heat transfer under various conditions. The results indicate that at Re = 500, turbulence mitigates wall interference, leading to a 14.4% increase in the Nusselt number (Nu). Particle orientation plays a crucial role in heat transfer, with Nu decreasing by 20% at = 90° due to restricted interstitial flow. A higher aspect ratio (Ar = 0.8) enhances heat transfer by 25% compared to a lower aspect ratio (Ar = 0.1). Additionally, increasing the particle–wall distance from H = 0.25dv to H = 0.5dv reduces wall-induced drag by 30%. The findings enhance the understanding of particle–fluid interactions near walls, providing a foundation for optimizing computational fluid dynamics models and improving industrial applications. Future work should consider additional variables such as particle roughness to further refine predictive capabilities. This study contributes to advancing theoretical and practical insights into non-spherical particle behaviors in complex flow environments. Full article
(This article belongs to the Section Hydraulics and Hydrodynamics)
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17 pages, 5084 KiB  
Article
Optimization Study of Pneumatic–Electric Combined Braking Strategy for 30,000-ton Heavy-Haul Trains
by Mingtao Zhang, Congjin Shi, Kun Wang, Pengfei Liu, Guoyun Liu, Zhiwei Wang and Weihua Zhang
Actuators 2025, 14(1), 40; https://doi.org/10.3390/act14010040 - 20 Jan 2025
Cited by 2 | Viewed by 1036
Abstract
The normalized operation of 30,000-ton heavy-haul trains is of significant importance for enhancing the transportation capacity of heavy-haul railways. However, with the increase in train formation size, traditional braking strategies result in excessive longitudinal impulse when combined pneumatic and electric braking is applied [...] Read more.
The normalized operation of 30,000-ton heavy-haul trains is of significant importance for enhancing the transportation capacity of heavy-haul railways. However, with the increase in train formation size, traditional braking strategies result in excessive longitudinal impulse when combined pneumatic and electric braking is applied on long, steep gradients. This presents a serious challenge to the braking safety of the train. To this end, this paper establishes a longitudinal dynamic model of a 30,000-ton heavy-haul train based on vehicle system dynamics theory, and validates the model’s effectiveness through line test data. On this basis, the influence of two braking parameters, namely, the distribution of the magnitude of the electric braking force and the matching time of pneumatic braking and electric braking, on the longitudinal dynamic behavior of heavy-haul trains is studied. Thereby, an optimized combined pneumatic and electric braking strategy is formulated to reduce the longitudinal impulse of the trains. The results show that setting reasonable braking parameters can effectively reduce the longitudinal impulse, with the braking matching time having a significant impact on the longitudinal impulse. Specifically, when using a strategy where the electric braking forces of three locomotives are set to 90 kN, 300 kN, and 300 kN, with a 30 s delay in applying the electric braking force, a better optimization effect is achieved. The two proposed braking strategies reduce the maximum longitudinal forces by 20.27% and 47.83%, respectively, compared to conventional approaches. The research results provide effective methods and theoretical guidance for optimizing the braking strategy and ensuring the operational safety of 30,000-ton heavy-haul trains. Full article
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17 pages, 2700 KiB  
Article
Estimating Total Methane Emissions from the Denver-Julesburg Basin Using Bottom-Up Approaches
by Stuart N. Riddick, Mercy Mbua, Abhinav Anand, Elijah Kiplimo, Arthur Santos, Aashish Upreti and Daniel J. Zimmerle
Gases 2024, 4(3), 236-252; https://doi.org/10.3390/gases4030014 - 5 Aug 2024
Cited by 1 | Viewed by 2422
Abstract
Methane is a powerful greenhouse gas with a 25 times higher 100-year warming potential than carbon dioxide and is a target for mitigation to achieve climate goals. To control and curb methane emissions, estimates are required from the sources and sectors which are [...] Read more.
Methane is a powerful greenhouse gas with a 25 times higher 100-year warming potential than carbon dioxide and is a target for mitigation to achieve climate goals. To control and curb methane emissions, estimates are required from the sources and sectors which are typically generated using bottom-up methods. However, recent studies have shown that national and international bottom-up approaches can significantly underestimate emissions. In this study, we present three bottom-up approaches used to estimate methane emissions from all emission sectors in the Denver-Julesburg basin, CO, USA. Our data show emissions generated from all three methods are lower than historic measurements. A Tier 1/2 approach using IPCC emission factors estimated 2022 methane emissions of 358 Gg (0.8% of produced methane lost by the energy sector), while a Tier 3 EPA-based approach estimated emissions of 269 Gg (0.2%). Using emission factors informed by contemporary and region-specific measurement studies, emissions of 212 Gg (0.2%) were calculated. The largest difference in emissions estimates were a result of using the Mechanistic Air Emissions Simulator (MAES) for the production and transport of oil and gas in the DJ basin. The MAES accounts for changes to regulatory practice in the DJ basin, which include comprehensive requirements for compressors, pneumatics, equipment leaks, and fugitive emissions, which were implemented to reduce emissions starting in 2014. The measurement revealed that normalized gas loss is predicted to have been reduced by a factor of 20 when compared to 10-year-old normalization loss measurements and a factor of 10 less than a nearby oil and production area (Delaware basin, TX); however, we suggest that more measurements should be made to ensure that the long-tail emission distribution has been captured by the modeling. This study suggests that regulations implemented by the Colorado Department of Public Health and Environment could have reduced emissions by a factor of 20, but contemporary regional measurements should be made to ensure these bottom-up calculations are realistic. Full article
(This article belongs to the Section Gas Emissions)
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17 pages, 3288 KiB  
Article
Simulation and Experimental Verification of Pipeline Particle Deposition Based on Ellipsoidal Assumption
by Chenchen Niu, Zhen Zhou, Jia Qi and Xu Yang
Processes 2024, 12(8), 1610; https://doi.org/10.3390/pr12081610 - 31 Jul 2024
Viewed by 1293
Abstract
The problem of particle clogging in a conveying pipeline in thin-phase pneumatic transportation is essentially the effect of the particle-deposition mechanism in gas–solid two-phase flow. This paper presents a particle-deposition model of gas–solid two-phase flow based on the ellipsoid hypothesis, and a fast-calculation [...] Read more.
The problem of particle clogging in a conveying pipeline in thin-phase pneumatic transportation is essentially the effect of the particle-deposition mechanism in gas–solid two-phase flow. This paper presents a particle-deposition model of gas–solid two-phase flow based on the ellipsoid hypothesis, and a fast-calculation method of material particle-deposition efficiency in industry based on the tabular-assigned drag-correction coefficient of the particle ellipsoid-shape parameter Ar and incoming flow angle ϕ. A simulation comparison of spherical particles under the same pneumatic transport conditions and experimental verification based on the self-built particle deposition system are given. The validity of the model and the accuracy of the algorithm are verified. This provides a feasible simulation and experimental scheme for the research of pneumatic-conveying technology in the industrial field. Full article
(This article belongs to the Special Issue Flow, Heat and Mass Transfer in Energy Utilization)
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18 pages, 9671 KiB  
Article
Development of a Tool to Manipulate Flexible Pieces in the Industry: Hardware and Software
by Francisco José Martínez-Peral, Jorge Borrell Méndez, José Vicente Segura Heras and Carlos Perez-Vidal
Actuators 2024, 13(4), 149; https://doi.org/10.3390/act13040149 - 16 Apr 2024
Viewed by 2095
Abstract
Currently, the textile industry is a poorly automated sector, due in part to problems in the handling of deformable leather and textile parts during production operations. In this work, several problems in the handling process of leather and textile parts are addressed, introducing [...] Read more.
Currently, the textile industry is a poorly automated sector, due in part to problems in the handling of deformable leather and textile parts during production operations. In this work, several problems in the handling process of leather and textile parts are addressed, introducing methods to increase the automation of the process. A pneumatic actuator designed to pick up textile or leather parts avoiding their deformation during transport has been developed. This actuator maximizes the number of gripping points to improve handling, making it more stable and efficient. Additionally, a vision system has been implemented in the part-picking task which, in conjunction with the CAD information of the part, sends the modified gripping position of the part to the robot. This allows customized handling of each textile or leather part. Finally, validation tests have been carried out on this development, both in simulations and in laboratory conditions, demonstrating its viability and direct applicability in the production line. Full article
(This article belongs to the Section Actuators for Robotics)
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17 pages, 7460 KiB  
Article
Generation and Characteristics of Construction Noise in Rail Transit Engineering Enclosure Structures
by Huanyu Wu, Wei Zhang, Zongbin Liu, Xuhui Bai, Junwei Huang, Jun Huang and Zezhou Wu
Buildings 2024, 14(4), 970; https://doi.org/10.3390/buildings14040970 - 1 Apr 2024
Cited by 3 | Viewed by 1740
Abstract
Rail transit is an important part of the urban transportation system, while the noise generated during construction seriously affects the engineering personnel and surrounding residents. To investigate the noise emissions and characteristics during the construction of the enclosure structures in the rail transit [...] Read more.
Rail transit is an important part of the urban transportation system, while the noise generated during construction seriously affects the engineering personnel and surrounding residents. To investigate the noise emissions and characteristics during the construction of the enclosure structures in the rail transit engineering project, an empirical study is conducted through on-site surveys, semi-structured interviews, and experimental monitoring. The results indicate that during enclosure structure construction, there are nine key noise-emitting machines and four key noise-generating construction processes. Among them, the equivalent average sound levels of six machines, including pneumatic hammers, pneumatic drills, concrete pump trucks, construction drills, rotary drilling rigs, and grooving machines, exceed 80 dB(A). The energy contribution rate curves of machine spectra peak at 63 Hz, 500 Hz, 1000 Hz, and 4000 Hz, which have certain effects on construction personnel and nearby residents. Meanwhile, guide wall construction, groove construction, reinforcement cage fabrication and hoisting, and concrete pouring are identified as key noise-generating construction processes. This empirical investigation helps to establish a theoretical basis for noise control during the construction of enclosure structures in urban rail transit engineering projects, and the results provide valuable references for the formulation of auxiliary noise reduction measures. Full article
(This article belongs to the Section Building Energy, Physics, Environment, and Systems)
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24 pages, 11426 KiB  
Review
Metachronal Motion of Biological and Artificial Cilia
by Zhiwei Cui, Ye Wang and Jaap M. J. den Toonder
Biomimetics 2024, 9(4), 198; https://doi.org/10.3390/biomimetics9040198 - 27 Mar 2024
Cited by 5 | Viewed by 5010
Abstract
Cilia are slender, hair-like cell protrusions that are present ubiquitously in the natural world. They perform essential functions, such as generating fluid flow, propulsion, and feeding, in organisms ranging from protozoa to the human body. The coordinated beating of cilia, which results in [...] Read more.
Cilia are slender, hair-like cell protrusions that are present ubiquitously in the natural world. They perform essential functions, such as generating fluid flow, propulsion, and feeding, in organisms ranging from protozoa to the human body. The coordinated beating of cilia, which results in wavelike motions known as metachrony, has fascinated researchers for decades for its role in functions such as flow generation and mucus transport. Inspired by nature, researchers have explored diverse materials for the fabrication of artificial cilia and developed several methods to mimic the metachronal motion observed in their biological counterparts. In this review, we will introduce the different types of metachronal motion generated by both biological and artificial cilia, the latter including pneumatically, photonically, electrically, and magnetically driven artificial cilia. Furthermore, we review the possible applications of metachronal motion by artificial cilia, focusing on flow generation, transport of mucus, particles, and droplets, and microrobotic locomotion. The overall aim of this review is to offer a comprehensive overview of the metachronal motions exhibited by diverse artificial cilia and the corresponding practical implementations. Additionally, we identify the potential future directions within this field. These insights present an exciting opportunity for further advancements in this domain. Full article
(This article belongs to the Special Issue Advances in Biomimetics: The Power of Diversity)
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16 pages, 3898 KiB  
Article
2-DOF Woven Tube Plane Surface Soft Actuator Using Extensional Pneumatic Artificial Muscle
by Moe Kuriyama and Toshio Takayama
Hardware 2024, 2(1), 50-65; https://doi.org/10.3390/hardware2010003 - 4 Mar 2024
Cited by 1 | Viewed by 2536
Abstract
Soft actuators, designed for fragile item conveyance and navigation in complex environments, have garnered recent attention. This study proposes a cost-effective soft actuator, created by weaving tubes into twill patterns, capable of transportation and movement. The actuator achieves this by inducing traveling waves [...] Read more.
Soft actuators, designed for fragile item conveyance and navigation in complex environments, have garnered recent attention. This study proposes a cost-effective soft actuator, created by weaving tubes into twill patterns, capable of transportation and movement. The actuator achieves this by inducing traveling waves on its upper and lower surfaces through sequential pressurization of tubes. Notably, its fabrication does not require specialized molds, contributing to cost efficiency. The single actuator generates traveling waves with two degrees of freedom. Conventional silicone tube-based actuators demonstrate slow transport speeds (3.5 mm/s). To address this, this study replaced silicone tubes with pneumatic artificial muscles, enhancing overall body deformation and actuator speed. Experiments involving both extensional and contractional artificial muscles demonstrated that soft actuators with extensional artificial muscles significantly improved transportation and movement speed to 8.0 mm/s. Full article
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28 pages, 20130 KiB  
Article
Study on Aerodynamic Drag Reduction by Plasma Jets for 600 km/h Vacuum Tube Train Sets
by Ang Li, Hongjiang Cui, Ying Guan, Jichen Deng, Ying Zhang and Wu Deng
Machines 2023, 11(12), 1078; https://doi.org/10.3390/machines11121078 - 8 Dec 2023
Cited by 3 | Viewed by 2184
Abstract
In order to break through the speed bottleneck, researchers envision using tubes to cover high-speed maglev trains and extract some of the air inside the tubes, creating a low-density environment on the ground, greatly reducing the aerodynamic drag of the trains, and in [...] Read more.
In order to break through the speed bottleneck, researchers envision using tubes to cover high-speed maglev trains and extract some of the air inside the tubes, creating a low-density environment on the ground, greatly reducing the aerodynamic drag of the trains, and in a relatively economical and feasible way, making high subsonic (600 km/h and above) and even supersonic ground transportation possible. The faster the running speed of high-speed trains, the greater the impact of aerodynamic drag on their energy consumption. Studying the aerodynamic characteristics of trains with a speed of 600 km/h can help optimize the aerodynamic shape of the train, reduce aerodynamic drag, and reduce energy consumption. This has positive implications for improving train energy efficiency, reducing energy consumption, and environmental impact. This paper adopts the numerical simulation method to study the drag reduction effect of the plasma arrangement and different excitation speeds on the train set in four positions when the incoming wind speed is 600 km/h, to analyze the mechanism of drag reduction, and then to analyze the combination of working conditions in order to investigate the drag reduction effect of plasma on the vacuum tube train set with an ambient pressure of 10,000 Pa. The findings demonstrate that the plasma induces the directional flow of the gas close to the wall to move the flow separation point backward and delay the separation of the flow, thereby reducing the front and rear differential pressure drag of the train set and lowering the aerodynamic drag coefficient of the entire train. The plasma arrangement is located at the rear of the flow separation point and in close proximity to the flow separation point. The pneumatic drag reduction effect peaks when the excitation speed reaches 0.2 times the train speed and the pneumatic drag reduction ratio is around 0.88%; the pneumatic drag reduction ratio of the rear car peaks when the excitation speed reaches 0.25 times the train speed and the pneumatic drag reduction ratio is 1.62%. The SDBD (Surface Dielectric Barrier Discharge) device is installed at the flow separation point around the nose tip of the rear car. Full article
(This article belongs to the Section Machines Testing and Maintenance)
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21 pages, 25617 KiB  
Article
The Effect of a Three-Blade Tube on the Pneumatic Transport of Pebble Particles
by Yating Hao, Hongyu Chen and Yun Ji
Energies 2023, 16(23), 7884; https://doi.org/10.3390/en16237884 - 2 Dec 2023
Cited by 1 | Viewed by 1355
Abstract
In this paper, the Computational Fluid Dynamics–Discrete Element Method (CFD-DEM) coupling method was used to simulate the pneumatic transport of pebble particles in a three-blade spiral tube. The results showed that the flow field distribution rotated along the circumference after loading. The maximum [...] Read more.
In this paper, the Computational Fluid Dynamics–Discrete Element Method (CFD-DEM) coupling method was used to simulate the pneumatic transport of pebble particles in a three-blade spiral tube. The results showed that the flow field distribution rotated along the circumference after loading. The maximum velocity of the flow field after loading was manifested as rotation along the circumference. In addition, the swirl intensity decreased exponentially with the increase in conveying distance, and the maximum swirl intensity had a saturation value. After reaching the saturation value, it is not evident that increasing the initial air velocity significantly affected swirl variation. The smaller the pitch, the greater the initial swirl intensity. The swirling flow was conducive to the fluidization of particles, but it would bring a significant energy loss. Increasing the swirl can increase the degree of particle dispersion. There is an optimal tangential airflow velocity, which allows the particles to fully spin and stay in the suspension zone without being thrown onto the pipe wall by excessive centrifugal force. At this time, the energy efficiency reaches the highest level. A 5.87 m/s velocity was deemed the optimal tangential airflow velocity for conveying 3 mm particles. Full article
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16 pages, 5509 KiB  
Article
Design, Optimization, and Application of a 3D-Printed Polymer Sample Introduction System for the ICP-MS Analysis of Nanoparticles and Cells
by Gyula Kajner, Ádám Bélteki, Martin Cseh, Zsolt Geretovszky, Tibor Ajtai, Lilla Barna, Mária A. Deli, Bernadett Pap, Gergely Maróti and Gábor Galbács
Nanomaterials 2023, 13(23), 3018; https://doi.org/10.3390/nano13233018 - 25 Nov 2023
Cited by 4 | Viewed by 2867
Abstract
Commonly used sample introduction systems for inductively coupled plasma mass spectrometry (ICP-MS) are generally not well-suited for single particle ICP-MS (spICP-MS) applications due to their high sample requirements and low efficiency. In this study, the first completely 3D-printed, polymer SIS was developed to [...] Read more.
Commonly used sample introduction systems for inductively coupled plasma mass spectrometry (ICP-MS) are generally not well-suited for single particle ICP-MS (spICP-MS) applications due to their high sample requirements and low efficiency. In this study, the first completely 3D-printed, polymer SIS was developed to facilitate spICP-MS analysis. The system is based on a microconcentric pneumatic nebulizer and a single-pass spray chamber with an additional sheath gas flow to further facilitate the transport of larger droplets or particles. The geometry of the system was optimized using numerical simulations. Its aerosol characteristics and operational conditions were studied via optical particle counting and a course of spICP-MS measurements, involving nanodispersions and cell suspensions. In a comparison of the performance of the new and the standard (quartz microconcentric nebulizer plus a double-pass spray chamber) systems, it was found that the new sample introduction system has four times higher particle detection efficiency, significantly better signal-to-noise ratio, provides ca. 20% lower size detection limit, and allows an extension of the upper limit of transportable particle diameters to about 25 µm. Full article
(This article belongs to the Section Synthesis, Interfaces and Nanostructures)
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