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Keywords = non-oriented silicon steel

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12 pages, 1286 KB  
Article
Influence of Neighboring Orientations on Oriented Stability in Grain-Boundary Regions of Non-Oriented Silicon Steel
by Xi Chen, Guojin Zhang, Fang Zhang and Yuhui Sha
Materials 2026, 19(17), 3733; https://doi.org/10.3390/ma19173733 - 2 Sep 2026
Viewed by 154
Abstract
Orientation rotation in grain-boundary regions plays a critical role in controlling the crystallographic texture of metallic materials. In this study, the ideal λ texture ({001}<uv0>) in non-oriented silicon steel is chosen as the target orientation. The oriented stability in grain-boundary regions during cold [...] Read more.
Orientation rotation in grain-boundary regions plays a critical role in controlling the crystallographic texture of metallic materials. In this study, the ideal λ texture ({001}<uv0>) in non-oriented silicon steel is chosen as the target orientation. The oriented stability in grain-boundary regions during cold rolling is systematically investigated by combining crystal plasticity simulations and quasi in situ electron backscatter diffraction (EBSD) experiments. Oriented stability is defined as the rate of change in the misorientation angle between an arbitrary orientation and the target orientation, thereby quantifying the rotational tendency relative to the target in grain-boundary regions. The results reveal that the oriented stability in grain-boundary regions is highly sensitive to both the initial and neighboring orientations. For initial orientations near the critical boundary separating convergence and divergence zones, the oriented stability is highly susceptible to neighboring orientations, with some neighboring orientations even reversing the rotation direction. In contrast, when the initial orientation is far from this critical boundary, the influence of neighboring orientations becomes weaker. Furthermore, the concept of contributed oriented stability is introduced to statistically evaluate the effect of different neighboring texture components in polycrystals. This work elucidates the underlying mechanism of orientation rotation in grain-boundary regions, and provides a new theoretical framework and a quantitative strategy for optimizing favorable textures. Full article
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21 pages, 4734 KB  
Article
Multiphysics Simulation of Shell Solidification Evolution in CSP Thin Slab Casting of Silicon Steel with Box-Type Electromagnetic Stirring
by Hong Xiao, Jian Liu, Lang Wang, Sheng-Zhao Wang, Yan-Zhong Li and Pu Wang
Materials 2026, 19(12), 2521; https://doi.org/10.3390/ma19122521 - 11 Jun 2026
Viewed by 351
Abstract
In CSP thin slab casting, high casting speeds promote excessive columnar grain growth, leading to low equiaxed grain ratios in non-oriented silicon steel and resulting in wrinkling defects. This study employs a box-type electromagnetic stirrer (B-EMS) to address this issue. A multiphysics model [...] Read more.
In CSP thin slab casting, high casting speeds promote excessive columnar grain growth, leading to low equiaxed grain ratios in non-oriented silicon steel and resulting in wrinkling defects. This study employs a box-type electromagnetic stirrer (B-EMS) to address this issue. A multiphysics model was established, in which grain transformation and its associated effects were neglected. The effects of B-EMS on the flow of molten steel, temperature distribution and evolution of solidified shell were analyzed, and industrial trials were conducted to verify the influence of B-EMS on grains. Results show that B-EMS generates asymmetric magnetic fields and electromagnetic forces, driving width-directional flow that enhances scouring of the solidification front. Compared with the experiment and simulation, the error in the magnetic field excited by B-EMS is within 5%. Under 800 A current, narrow-face center shell thickness increased from 22.88 mm (no stirring) to 23.62 mm (starting side) and 23.21 mm (pushing side). The central mushy zone area and liquid fraction decreased significantly, indicating accelerated solidification and more uniform shell growth. Industrial trials confirmed that the equiaxed grain ratio increased to approximately 30%, with significantly improved internal strand quality. This study demonstrates B-EMS’s metallurgical effects in regulating solidification structure, optimizing shell morphology, and improving continuous casting slab quality. The numerical simulation can be correlated with the industrial production process to better guide manufacturing practices. Full article
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23 pages, 9347 KB  
Article
Factorial Optimization of Secondary Annealing Parameters for Enhanced Magnetic Performance in M4 Grain-Oriented Electrical Steel Toroidal Cores
by Alma Lilia Moreno-Ríos, Luis Adrián Zúñiga-Avilés, José Martín Herrera-Ramírez and Caleb Carreño-Gallardo
Materials 2026, 19(11), 2203; https://doi.org/10.3390/ma19112203 - 23 May 2026
Viewed by 2145
Abstract
Grain-oriented (GO) silicon steel cores in low-voltage current transformers suffer magnetic degradation from residual stress and increased dislocation density during slitting and winding. This study addresses the gap in systematic optimization of secondary annealing on assembled toroidal cores using a 32 full-factorial [...] Read more.
Grain-oriented (GO) silicon steel cores in low-voltage current transformers suffer magnetic degradation from residual stress and increased dislocation density during slitting and winding. This study addresses the gap in systematic optimization of secondary annealing on assembled toroidal cores using a 32 full-factorial design varying temperature (650, 850, 1050 °C) and holding time (60, 90, 120 min) on M4 grade cores. Results showed temperature is the dominant factor, while holding time exhibits a synergistic non-linear effect. The optimal condition (850 °C, 90 min) reduced specific losses from 0.85 W/kg to 0.43 W/kg (49% reduction). Mechanistic analysis confirmed this improvement is driven by complete primary recrystallization (equiaxed grains ~50–60 µm), dislocation annihilation (~10 HV hardness reduction), and reinforcement of the Goss texture ({110} <001>). SEM, EDS, and ICP-OES demonstrated that the Carlite coating remained dimensionally (1.67–1.83 µm) and chemically stable, with beneficial decarburization. Temperatures above 850 °C caused magnetic deterioration due to excessive grain growth. These results provide a validated, industrial framework for recovering magnetic efficiency in wound toroidal cores without compromising coating integrity. Full article
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13 pages, 4560 KB  
Article
Effect of Sn on Normalized Texture and Precipitates in Non-Oriented Silicon Steel for New Energy Vehicles
by Yu Zhang, Baozhi Liu, Zhongwang Wu, Huimin Zhang, Xiaolong Zhao, Yanjun Di, Jun Li, Yongquan Han and Huiping Ren
Crystals 2026, 16(5), 347; https://doi.org/10.3390/cryst16050347 - 19 May 2026
Viewed by 638
Abstract
In the manufacturing process of high-grade non-oriented electrical steel, cast billets are subjected to hot rolling and normalizing treatments. These processes are implemented to optimize the microstructure and texture of steel sheets during production, mitigate corrugated defects, and enhance the magnetic properties of [...] Read more.
In the manufacturing process of high-grade non-oriented electrical steel, cast billets are subjected to hot rolling and normalizing treatments. These processes are implemented to optimize the microstructure and texture of steel sheets during production, mitigate corrugated defects, and enhance the magnetic properties of the final finished sheets. In this study, two types of high-strength non-oriented silicon steel test specimens were prepared via the incorporation of the trace alloying element Sn, namely one without Sn addition and the other with 0.045 wt% Sn. The test specimens were first hot-rolled to a thickness of 2.0 mm, followed by normalization treatment in the laboratory to simulate the continuous normalizing process employed by a domestic steel mill. The effects of Sn on the normalized microstructure, texture, and precipitates of non-oriented silicon steel tailored for new energy vehicles were investigated. The findings reveal that the alloying element Sn can increase the thickness of the recrystallized layer on the surface of hot-rolled sheets and refine the grain size of non-oriented silicon steel. After continuous normalizing treatment, a comparison between the two test specimens shows that as the normalizing temperature rises, the reduction in average grain size of the 0.045 wt% Sn specimen relative to the Sn-free specimen increases from 1.4% to 15.96%. Additionally, the incorporation of Sn reduces the fraction of the {111} texture component (detrimental to magnetic properties) while increasing the fraction of the {100} texture component (beneficial to magnetic properties) in the non-oriented silicon steel. Precipitates exhibited significant coarsening and a reduction in number with increasing temperature, while the addition of Sn exerted a certain inhibitory effect on precipitate growth. Furthermore, the 0.045 wt% Sn-containing test specimen achieved an optimal balance between magnetic and mechanical properties when subjected to normalization at 980 °C and annealing at 920 °C. Under these processing conditions, the magnetic induction B50 reached 1.733 T, the iron loss P1.5/50 was 2.01 W/kg, the yield strength was 410 MPa, and the tensile strength was 529 MPa. Full article
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14 pages, 5532 KB  
Article
Performance Analysis and Temperature-Corrected Core Loss Modeling of Soft Magnetic Materials for Hybrid Stepper Motors in Cryogenic Environments
by Xiong-Jie Hu, Ye Rong, Qing-Yi Kong, Qian Zhang, Guang-Long Wang and Bo Jiang
Processes 2026, 14(10), 1597; https://doi.org/10.3390/pr14101597 - 14 May 2026
Viewed by 436
Abstract
Hybrid stepper (HB) motors are widely used in precision actuation systems such as cryogenic refrigerator robotic arms. Under cryogenic working conditions, the core loss characteristics of magnetic materials change significantly, while conventional core loss models calibrated at room temperature can hardly provide reliable [...] Read more.
Hybrid stepper (HB) motors are widely used in precision actuation systems such as cryogenic refrigerator robotic arms. Under cryogenic working conditions, the core loss characteristics of magnetic materials change significantly, while conventional core loss models calibrated at room temperature can hardly provide reliable prediction accuracy. In this work, the electromagnetic properties of 35SW1900 non-oriented silicon steel were measured from 25 °C − 100 °C using a BROCKHAUS Epstein frame system. Variations in permeability, core loss and coercivity with magnetic flux density, temperature and frequency were obtained. An improved core loss model was developed by introducing a flux-dependent exponent and dual temperature correction coefficients for hysteresis and eddy current losses. Experiments place the prediction error of the proposed model within 4% under cryogenic conditions. Compared with the classical Bertotti model, the proposed model effectively reduces high-frequency deviation caused by the temperature-dependent material properties and skin effect. The core loss of silicon steel increases by 15–30% at −100 °C compared with room temperature, which is mainly attributed to the decrease in resistivity and the strengthening of domain wall pinning. This paper provides an accurate loss prediction method and design references for HB motors applied in ultralow temperature working conditions. Full article
(This article belongs to the Section Manufacturing Processes and Systems)
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20 pages, 3142 KB  
Article
The Influence of Non-Oriented Silicon Steel Core Material on Motor Performance
by Guanglin Li, Jing Zhao, Xiaoqing Guan, Zhizhou Chen and Bin Wang
Machines 2026, 14(5), 538; https://doi.org/10.3390/machines14050538 - 11 May 2026
Viewed by 444
Abstract
Interior permanent magnet synchronous motors (IPMSMs) offer performance advantages such as saliency effect, high mechanical strength, and a wide speed regulation range. The magnetic and mechanical properties of the core material significantly influence IPMSM performance. By investigating the effects of different core materials [...] Read more.
Interior permanent magnet synchronous motors (IPMSMs) offer performance advantages such as saliency effect, high mechanical strength, and a wide speed regulation range. The magnetic and mechanical properties of the core material significantly influence IPMSM performance. By investigating the effects of different core materials on IPMSM performance, an optimal material combination can be identified to enhance the overall motor performance. This paper takes a V¯-shaped IPMSM for use as a main drive motor in new energy vehicles as the research object. First, the influence of the iron loss characteristics of non-oriented silicon steel (NOSS) on IPMSM performance is analyzed, and the material selection principles for the stator and rotor cores under this condition are summarized. Subsequently, the influence of the magnetic flux density characteristics of NOSS on IPMSM performance is analyzed, and the corresponding material selection principles for the stator and rotor cores are summarized. Furthermore, ultra-high-yield-strength NOSS is applied as the motor core material to reduce the width of the rotor magnetic flux barrier, and the resulting performance advantages for the IPMSM are analyzed. Finally, prototypes of the IPMSM are manufactured and tested to validate the results of the analysis. Full article
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20 pages, 9840 KB  
Article
Theoretical Study on the Formation Mechanism of Ti(C,N) Inclusions and Titanium Content Control in High-Grade Non-Oriented Silicon Steel
by Jinwen Liu, Chuanmin Li, Fuqiang Zhou, Ben Zhang, Shanguo Du, Haiyan Tang and Jiaquan Zhang
Materials 2026, 19(9), 1684; https://doi.org/10.3390/ma19091684 - 22 Apr 2026
Viewed by 638
Abstract
High-grade non-oriented silicon steel is a critical material for new energy vehicles and energy-efficient appliances due to its superior magnetic properties. However, these properties are significantly degraded by non-metallic inclusions, particularly Ti(C,N). This study employs integrated thermodynamic and kinetic calculations to systematically analyze [...] Read more.
High-grade non-oriented silicon steel is a critical material for new energy vehicles and energy-efficient appliances due to its superior magnetic properties. However, these properties are significantly degraded by non-metallic inclusions, particularly Ti(C,N). This study employs integrated thermodynamic and kinetic calculations to systematically analyze the formation and growth mechanisms of Ti(C,N) inclusions in high-grade non-oriented silicon steel, trace the sources of [Ti], and propose targeted theoretical control strategies. Results indicate that Ti(C,N) inclusions do not precipitate above the liquidus temperature (1779 K). During solidification, microsegregation enriches Ti, C, and N; however, only TiN precipitates in the final stage as its ion product exceeds the solubility limit, whereas TiC remains undersaturated—findings valid within the present composition window and modeling framework. Inclusion size is governed by cooling rate and initial Ti/N content, where higher cooling rates yield finer inclusions and lower Ti/N content suppresses precipitation. Titanium originates from primary sources (raw materials and alloys) and secondary sources (decomposition or reduction of TiO2 in slag/refractories). Therefore, mitigating [Ti] requires strictly limiting primary input and suppressing secondary formation through optimized process control, such as reducing BOF slag carryover, lowering refining temperature, and controlling [Al] content. Full article
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19 pages, 5075 KB  
Article
Influence of Chemical Composition and Electro-Steel Sheets Manufacturing Parameters on the Adhesion of an Electro-Insulating Self-Bonding Varnish Layer
by Vanda Tomková, Miroslav Tomáš, Stanislav Németh, Matúš Horváth, Vladimír Kundracík, Emil Evin, Ján Slota, Anna Guzanová and Iveta Filipovská
Crystals 2026, 16(4), 253; https://doi.org/10.3390/cryst16040253 - 10 Apr 2026
Viewed by 1096
Abstract
One promising innovative joining process for non-oriented electrical sheets is based on an electro-insulating layer combined with a self-bonding varnish. The aim of this study was to investigate the adhesion of the self-bonding varnish as evaluated by a lap-shear test. During the experiments, [...] Read more.
One promising innovative joining process for non-oriented electrical sheets is based on an electro-insulating layer combined with a self-bonding varnish. The aim of this study was to investigate the adhesion of the self-bonding varnish as evaluated by a lap-shear test. During the experiments, non-oriented electrical steels with low to high silicon content were analyzed and tested. The Si content, the bond thickness, and the surface roughness Ra, as well as the selected steel production parameters—such as the radiation tube furnace temperature (RTF), the grain growth temperature (i.e., heating temperature (HF)), the peak metal temperature (PMT), and the annealing atmosphere (dry or humid, controlled by dew point)—were considered as the variables. The results showed that the lap-shear strength was independent of the surface roughness within the investigated range. In contrast, the bond thickness exhibited a weak positive effect on the lap-shear strength, while the Si content showed condition-dependent behavior. The RTF and the HF resulted in a relatively stable mechanical performance, whereas the PMT and the humid annealing atmosphere were identified as critical factors influencing adhesion. Full article
(This article belongs to the Special Issue Microstructure and Properties of Steel Materials)
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10 pages, 3852 KB  
Article
Influence of Silicon Content on Mechanical and Tribological Properties of FeSi Steels
by Marcela Motýľová, Ivan Petrišinec, Róbert Džunda and Jana Andrejovská
Crystals 2025, 15(12), 1005; https://doi.org/10.3390/cryst15121005 - 22 Nov 2025
Cited by 1 | Viewed by 1001
Abstract
Non-oriented (NO) Fe–Si electrical steels are key materials for magnetic cores of electrical machines, requiring a balance between magnetic and mechanical properties. This study systematically examined the effect of silicon content (1.06 wt%, 2.15 wt%, and 3.09 wt%) on the microstructure, mechanical, and [...] Read more.
Non-oriented (NO) Fe–Si electrical steels are key materials for magnetic cores of electrical machines, requiring a balance between magnetic and mechanical properties. This study systematically examined the effect of silicon content (1.06 wt%, 2.15 wt%, and 3.09 wt%) on the microstructure, mechanical, and tribological behavior of three produced NO steel grades. Mechanical properties were assessed using tensile tests, microhardness, and nanoindentation, while tribological performance was evaluated under dry reciprocating sliding (ball-on-flat) against a 100Cr6 steel ball at loads of 5 N, 10 N, and 25 N. Increasing silicon content led to larger grain size, higher hardness (227 HV–361 HV) and strength, but lower ductility. Tribological behavior depended on both composition and load. The most stable friction regime occurred at 10 N. The medium-Si steel (N3, 2.15 wt%) exhibited the best performance with a low coefficient of friction (COF ≈ 0.52–0.55); N5 (3.09 wt%) showed a similar COF, while N1 (1.06 wt%) had a slightly higher value. At 25 N, an inverse relationship between hardness and friction appeared: softer N1 had the lowest COF (≈0.68–0.70), whereas harder N3 and N5 reached ≈ 0.74–0.78. Scanning electron microscopy (SEM) observations revealed abrasive wear for N3/N5 and plastic flow (galling) for N1. Overall, an optimal silicon content provides the best compromise between hardness and tribological stability depending on load conditions. Full article
(This article belongs to the Special Issue Investigation of Microstructural and Properties of Steels and Alloys)
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13 pages, 10565 KB  
Article
Effect of Annealing Temperature on Microstructure, Texture, and Magnetic Properties of Non-Oriented Silicon Steel for Electric Vehicle Traction Motors
by Shaoyang Chu, Li Xiang, Feihu Guo and Shengtao Qiu
Metals 2025, 15(11), 1235; https://doi.org/10.3390/met15111235 - 10 Nov 2025
Cited by 4 | Viewed by 1792
Abstract
Improving the efficiency of electric vehicle traction motors requires non-oriented silicon steels with low core loss and favorable magnetic induction. This study aims to clarify the influence of annealing temperature on the microstructure, texture, and magnetic properties of a 3.2%Si–0.9%Al steel, providing guidance [...] Read more.
Improving the efficiency of electric vehicle traction motors requires non-oriented silicon steels with low core loss and favorable magnetic induction. This study aims to clarify the influence of annealing temperature on the microstructure, texture, and magnetic properties of a 3.2%Si–0.9%Al steel, providing guidance for process optimization. Optical metallography, X-ray diffraction, and electron backscatter diffraction were employed to characterize the evolution. Recrystallization was completed between 620 °C and 720 °C, during which fine recrystallized grains replaced the deformed structure, accompanied by the nucleation of {111}<112> and {114}<481> grains. With further annealing from 850 °C to 1050 °C, grain growth occurred, resulting in an α*-fiber texture dominated by {114}<481>. The fraction of high-angle {114}<481> grains increased, while low-angle {111}<112> grains decreased. This microstructural evolution significantly influenced the magnetic properties of non-oriented electrical steel. The P1.5/50 and P1.0/400 core losses reached minimum values of 2.02 W/kg and 16.48 W/kg at 1010 °C and 930 °C, respectively, while B50 decreased slightly from 1.670 T to 1.652 T. These findings indicate that precise control of the annealing temperature is an effective strategy to tailor microstructure and texture, thereby optimizing the magnetic properties of non-oriented electrical steel. Full article
(This article belongs to the Special Issue Electrical Steels)
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20 pages, 5035 KB  
Article
Effect of Small Deformations on Optimisation of Final Crystallographic Texture and Microstructure in Non-Oriented FeSi Steels
by Ivan Petrišinec, Marcela Motýľová, František Kováč, Ladislav Falat, Viktor Puchý, Mária Podobová and František Kromka
Crystals 2025, 15(10), 839; https://doi.org/10.3390/cryst15100839 - 26 Sep 2025
Viewed by 910
Abstract
Improving the isotropic magnetic properties of FeSi electrical steels has traditionally focused on enhancing their crystallographic texture and microstructural morphology. Strengthening the cube texture within a ferritic matrix of optimal grain size is known to reduce core losses and increase magnetic induction. However, [...] Read more.
Improving the isotropic magnetic properties of FeSi electrical steels has traditionally focused on enhancing their crystallographic texture and microstructural morphology. Strengthening the cube texture within a ferritic matrix of optimal grain size is known to reduce core losses and increase magnetic induction. However, conventional cold rolling followed by annealing remains insufficient to optimise the magnetic performance of thin FeSi strips fully. This study explores an alternative approach based on grain boundary migration driven by temperature gradients combined with deformation gradients, either across the sheet thickness or between neighbouring grains, in thin, weakly deformed non-oriented (NO) electrical steel sheets. The concept relies on deformation-induced grain growth supported by rapid heat transport to promote the preferential formation of coarse grains with favourable orientations. Experimental material consisted of vacuum-degassed FeSi steel with low silicon content. Controlled deformation was introduced by temper rolling at room temperature with 2–40% thickness reductions, followed by rapid recrystallisation annealing at 950 °C. Microstructure, texture, and residual strain distributions were analysed using inverse pole figure (IPF) maps, kernel average misorientation (KAM) maps, and orientation distribution function (ODF) sections derived from electron backscattered diffraction (EBSD) data. This combined thermomechanical treatment produced coarse-grained microstructures with an enhanced cube texture component, reducing coercivity from 162 A/m to 65 A/m. These results demonstrate that temper rolling combined with dynamic annealing can surpass the limitations of conventional processing routes for NO FeSi steels. Full article
(This article belongs to the Special Issue Microstructure and Deformation of Advanced Alloys (2nd Edition))
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16 pages, 4663 KB  
Article
Magnetic Properties and Strengthening Mechanism of Cu-Bearing Non-Oriented Silicon Steel
by Shi Qiu, Yuhao Niu, Kaixuan Shao, Bing Fu, Haijun Wang and Jialong Qiao
Materials 2025, 18(18), 4233; https://doi.org/10.3390/ma18184233 - 9 Sep 2025
Cited by 2 | Viewed by 1255
Abstract
The effects of Cu content on the microstructure, texture, precipitates, and magnetic and mechanical properties of 0.20 mm-thick non-oriented silicon steel (3.0% Si-0.8% Al-0.5% Mn) were systematically investigated using optical microscopy, X-ray diffraction, electron backscatter diffraction, and transmission electron microscopy. The strengthening mechanisms [...] Read more.
The effects of Cu content on the microstructure, texture, precipitates, and magnetic and mechanical properties of 0.20 mm-thick non-oriented silicon steel (3.0% Si-0.8% Al-0.5% Mn) were systematically investigated using optical microscopy, X-ray diffraction, electron backscatter diffraction, and transmission electron microscopy. The strengthening mechanisms of Cu-bearing high-strength non-oriented silicon steel were further elucidated. Increasing Cu content inhibited grain growth and suppressed the development of the α*-fiber texture in annealed sheets, while promoting the formation of γ-fiber texture. As a result, the P1.0/400 and B50 values deteriorated. The P1.0/400 and B50 values of 1.47% Cu non-oriented silicon steel were 13.930 W/kg and 1.614 T, respectively. However, due to the solid solution strengthening effect of 0.5% Cu and partial precipitation strengthening, the Rp0.2 increased by 43 MPa. After aging treatment at 550 °C for 20 min, the P1.0/400 values of the aged sheets slightly increased, while the B50 values remained almost unchanged. In the aged sheets containing 1.0–1.5% Cu, clustered Cu-rich precipitates with average sizes of 2.71 nm and 13.28 nm were observed. The crystal structure of these precipitates transitioned from the metastable B2-Cu to the stable FCC-Cu. These precipitates enhanced the Rp0.2 of the non-oriented electrical steel to 241 MPa and 269 MPa through cutting and bypass mechanisms, respectively. A high-strength non-oriented silicon steel with balanced magnetic and mechanical properties was developed for driving motors of new energy vehicles by utilizing nanoscale Cu-rich precipitates formed through aging treatment. The optimized steel exhibits a yield strength of 708 MPa, a magnetic induction B50 of 1.639 T, and high-frequency iron loss P1.0/400 of 14.77 W/kg. Full article
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23 pages, 10645 KB  
Article
Analysis of Inclusions in the Entire Smelting Process of High-Grade Rare Earth Non-Oriented Silicon Steel
by Liqiang Xue, Xiangyu Li, Tao Wang, Qi Zhao, Haozheng Wang, Jia Wang, Wanming Lin, Xiaofeng Niu, Wangzhong Mu and Chao Chen
Crystals 2025, 15(9), 779; https://doi.org/10.3390/cryst15090779 - 30 Aug 2025
Cited by 4 | Viewed by 1727
Abstract
Rare earth can modify inclusions in non-oriented silicon steel which is harmful to magnetic properties. This study focused on the 3.1% Si non-oriented silicon steel under industrial production conditions. Samples were taken during the stages before and after addition of rare earth ferrosilicon [...] Read more.
Rare earth can modify inclusions in non-oriented silicon steel which is harmful to magnetic properties. This study focused on the 3.1% Si non-oriented silicon steel under industrial production conditions. Samples were taken during the stages before and after addition of rare earth ferrosilicon alloy in Ruhrstahl-Heraeus (RH) unit, different pouring time in tundish, and continuous casting slab. This study systematically examined the morphology, composition, and size distribution of inclusions throughout the smelting process of non-oriented silicon steel by scanning electron microscopy with energy-dispersive spectroscopy (SEM/EDS), and thermodynamic analysis at liquid steel temperature and thermodynamic analysis of equilibrium solidification. The research results demonstrated that the rare earth treatment ultimately modifies the original Al2O3 inclusions in the non-oriented silicon steel into REAlO3 and RE2O2S inclusions, while also aggregating AlN inclusions to form composite inclusions. After rare earth modification, the average size of the inclusions decreases. In the RH treatment process, the inclusions before the addition of rare earth ferrosilicon alloy are mainly AlN and Al2O3. After the addition of rare earth ferrosilicon alloy, the inclusions are mainly RES and REAlO3. In the tundish and continuous casting, the rare earth content decreased, and the rare earth inclusions transform into RE2O2S and REAlO3. For the size of inclusions, after adding rare earth ferrosilicon alloy, the average size of inclusions rapidly decreased from 16.15 μm to 2.65 μm and reach its minimum size 2.16 μm at the end of RH treatment. When the molten steel entered the tundish, the average size of inclusions increased slightly and gradually decreased with the progress of pouring. The average size of inclusions in the slab is 5.79 μm. Phase stability diagram calculation indicates the most stable rare earth inclusion is Ce2O2S in molten steel. Thermodynamic calculations indicated that Al2O3, Ce2O2S, Ce2S3, AlN, and MnS precipitate sequentially during the equilibrium solidification process of molten steel. Full article
(This article belongs to the Special Issue Crystallization of High Performance Metallic Materials (2nd Edition))
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13 pages, 3688 KB  
Article
Influence Mechanisms of Trace Rare-Earth Ce on Texture Development of Non-Oriented Silicon Steel
by Feihu Guo, Yuhao Niu, Bing Fu, Jialong Qiao and Shengtao Qiu
Materials 2025, 18(15), 3493; https://doi.org/10.3390/ma18153493 - 25 Jul 2025
Cited by 4 | Viewed by 1131
Abstract
The effects of trace Ce on the microstructure and texture of non-oriented silicon steel during recrystallization and grain growth were examined using X-ray diffraction and electron backscatter diffraction. Additionally, this study focused on investigating the mechanisms by which trace Ce influences the evolution [...] Read more.
The effects of trace Ce on the microstructure and texture of non-oriented silicon steel during recrystallization and grain growth were examined using X-ray diffraction and electron backscatter diffraction. Additionally, this study focused on investigating the mechanisms by which trace Ce influences the evolution of the {114} <481> and γ-fiber textures. During the recrystallization process, as the recrystallization fraction of annealed sheets increased, the intensity of α-fiber texture decreased, while the intensities of α*-fiber and γ-fiber textures increased. The {111} <112> grains preferentially nucleated in the deformed γ-grains and their grain-boundary regions and tended to form a colony structure with a large amount of nucleation. In addition, the {100} <012> and {114} <481> grains mainly nucleated near the deformed α-grains, which were evenly distributed but found in relatively small quantities. The hindering effect of trace Ce on dislocation motion in cold-rolled sheets results in a 2–7% lower recrystallization ratio for the annealed sheets, compared to conventional annealed sheets. Trace Ce suppresses the nucleation and growth of γ-grains while creating opportunities for α*-grain nucleation. During grain growth, trace Ce reduces γ-grain-boundary migration rate in annealed sheets, providing growth space for {114} <418> grains. Consequently, the content of the corresponding {114} <481> texture increased by 6.4%, while the γ-fiber texture content decreased by 3.6%. Full article
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15 pages, 2917 KB  
Article
The Dual Influence of Silicon Content and Mechanical Stress on Magnetic Barkhausen Noise in Non-Oriented Electrical Steel
by Aroba Saleem, Mehdi Mehdi, P. Ross Underhill, Youliang He and Thomas W. Krause
Metals 2025, 15(6), 600; https://doi.org/10.3390/met15060600 - 27 May 2025
Cited by 2 | Viewed by 2004
Abstract
Magnetic Barkhausen noise (MBN) analysis is a non-destructive evaluation technique that offers significant advantages in assessing the magnetic properties of electrical steels. It is particularly useful for quality control in electrical steel production and for evaluating magnetic quality during core manufacturing and assembly. [...] Read more.
Magnetic Barkhausen noise (MBN) analysis is a non-destructive evaluation technique that offers significant advantages in assessing the magnetic properties of electrical steels. It is particularly useful for quality control in electrical steel production and for evaluating magnetic quality during core manufacturing and assembly. Despite its potential, MBN has not been widely used in electrical steel characterization. One obstacle is that the effects of silicon content in the electrical steel and the residual stress generated during its processing on MBN have not been thoroughly understood, limiting the practical application of the MBN technique in the electrical steel and electric motor industries. To address this knowledge gap, this paper investigates the MBN responses from four non-oriented electrical steel (NOES) sheets with varying silicon contents (0.88, 1.8, 2.8, and 3.2 wt%) but similar other elements. The measurements were performed both with and without applied tensile stress. It is observed that increasing the Si content increases the pinning density, which, together with the microstructure and texture, largely impacts the MBN response. In addition, the MBN energy increases with the applied stress, which can be attributed to the increase in the number of 180° domain walls (DWs) in the direction of stress. The rate of this MBN increase, however, differs among steels with different silicon concentrations. This difference is due to the combined effect of the DWs and pinning density. When the DW spacing becomes less than the jump distance between the pinning sites, no further increase in the MBN energy is observed with additional stress. The reported results provide a basis for the interpretation of MBN signals for varying wt% Si in NOES when residual stresses are present. Full article
(This article belongs to the Special Issue Recent Advances in High-Performance Steel)
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