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Keywords = high-temperature bending test

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21 pages, 1228 KB  
Article
Characteristics of the Rheology and Microscopic Mechanism of Asphalt Damage Under the Influence of Multicomponent Couplings
by Wei Wang, Ping Zheng, Zebin Nan, Jiusheng Cao, Chao Pu and Peng Yin
Coatings 2026, 16(7), 782; https://doi.org/10.3390/coatings16070782 - 30 Jun 2026
Viewed by 147
Abstract
As the core binder material of asphalt pavement, the rheological properties of asphalt directly determine the service performance and service life of the pavement. Under actual service conditions, asphalt is constantly exposed to a multi-coupling environment involving temperature variation, vehicle load, and ultraviolet [...] Read more.
As the core binder material of asphalt pavement, the rheological properties of asphalt directly determine the service performance and service life of the pavement. Under actual service conditions, asphalt is constantly exposed to a multi-coupling environment involving temperature variation, vehicle load, and ultraviolet aging, which easily leads to irreversible rheological deterioration and induces diseases such as rutting and cracking. Aiming at the insufficient research on the rheological evolution law and microscopic damage mechanism under the coupling of the above three factors, this study took 70# base asphalt as the research object and adopted a combination of macro-performance testing and microstructure characterization. The high- and low-temperature rheological properties, permanent deformation resistance, and fatigue resistance of asphalt under multi-coupling effects were systematically evaluated through three conventional index tests: dynamic shear rheology (DSR), multiple stress creep recovery (MSCR), linear amplitude sweep (LAS) and bending beam rheology (BBR). Combined with gel permeation chromatography (GPC) and thin-layer chromatography with flame ionization detection (TLC–FID), the evolution laws of molecular distribution and chemical components were revealed, and the deterioration mechanism of multi-coupling effects was clarified. The results show that compared with the control group, after 72 h of coupling treatment, the penetration decreases by 32.6%, the softening point increases by 18.3%, and the ductility decreases by 45.8%. The high-temperature complex modulus decreases by 51.2%, the low-temperature creep stiffness increases by 76.4%, and the fatigue life decreases by 58.6% on average. At the microscopic level, obvious molecular polymerization and component weight gain occur in asphalt: the content of macromolecular components rises from 18.7% to 32.1%, asphaltene content increases from 12.3% to 25.8%, and aromatic content decreases from 42.6% to 28.3%. Temperature variation, load, and ultraviolet aging present significant deterioration effects, rather than a simple superposition of single factors. Prolonged aging and increased load aggravate the hardening of asphalt, while extreme temperature variation further weakens the rheological properties through microscopic damage. This study clarifies the internal relationship between the microscopic structure and macroscopic properties of asphalt under multi-coupling effects, improves the theory of anti-coupling damage to asphalt, and provides an important theoretical basis and experimental support for damage-resistant design, material selection, and service life prediction of asphalt pavement. Full article
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16 pages, 2968 KB  
Article
Balanced Mix Design and Performance Analysis of High-Modulus Asphalt Mixtures
by Qirong Li, Jiwei Liu, Jilong Yang, Xinquan Xu, Xinhai Liu, Peiwen Hao and Ningbo Li
Materials 2026, 19(13), 2777; https://doi.org/10.3390/ma19132777 - 30 Jun 2026
Viewed by 115
Abstract
The objective of this study was to design mixtures that satisfy multiple performance criteria to build long-life pavement. A balanced mix design was employed to optimize AC-16, BBME-13, and EME-20 mixtures. The initial asphalt contents were determined using 4% air voids for the [...] Read more.
The objective of this study was to design mixtures that satisfy multiple performance criteria to build long-life pavement. A balanced mix design was employed to optimize AC-16, BBME-13, and EME-20 mixtures. The initial asphalt contents were determined using 4% air voids for the AC-16 mixture and the abundance coefficient K for BBME-13 and EME-20. Mixtures with two additional asphalt contents were also tested. A uniaxial penetration test, semi-circle bending test (to measure the flexibility index), and semi-circle bending test (to measure fracture energy) were used as performance tests. Then, a performance space diagram was created for a balanced analysis of the mixtures’ high-, intermediate-, and low-temperature performance. Finally, fatigue performance was verified. The results show that BMD could be used to evaluate different asphalt mixtures. The 20# BBME-13 (5.1%, 5.4%, and 5.7%), 50# BBME-13 5.4%, and 20# AC-16 4.7% mixtures had well-balanced performances and are recommended. The BBME-13 and EME-20 mixtures had higher fatigue lives and lower sensitivity to stress than the AC-16 mixture. For the BBME-13 and AC-16 mixtures, reducing the asphalt grade significantly increased fatigue life and decreased the sensitivity to stress. At a low stress ratio, the 20# EME-20 mixture had the best fatigue performance, whereas at a high stress ratio, the 20# BBME-13 mixture had the best fatigue performance. Full article
(This article belongs to the Section Advanced Materials Characterization)
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17 pages, 2863 KB  
Article
Flexible Iontronic Pressure Sensor Based on Ammonium Bicarbonate In-Situ Pore-Forming Porous Ionic Gel
by Zhiling Li, Zhixian Li, Liming Qin, Xiaodong Huang and Pan Pei
Micromachines 2026, 17(7), 787; https://doi.org/10.3390/mi17070787 - 28 Jun 2026
Viewed by 187
Abstract
To address prevalent industrial challenges, including the high cost of fabricating microstructures via photolithography and 3D printing, impurity residues easily generated by conventional physical/chemical pore-forming techniques, and the limited sensitivity of regular capacitive sensors, this paper innovatively proposes an integrated low-temperature in situ [...] Read more.
To address prevalent industrial challenges, including the high cost of fabricating microstructures via photolithography and 3D printing, impurity residues easily generated by conventional physical/chemical pore-forming techniques, and the limited sensitivity of regular capacitive sensors, this paper innovatively proposes an integrated low-temperature in situ gas foaming strategy using ammonium bicarbonate for the fabrication of porous TPU-based ionic gels. Relying on the complete gaseous decomposition property of ammonium bicarbonate upon heating, a three-dimensionally interconnected continuous porous network is spontaneously constructed inside the polymer matrix. Thermoplastic polyurethane (TPU) is selected as the continuous polymer phase, and [EMIM][TFSI] imidazolium ionic liquid is blended as the ion source to synthesize composite ionic gel substrates. A PDMS composite slurry filled with graphene is employed to prepare flexible substrates, followed by low-temperature oxygen plasma surface modification to introduce polar functional groups such as hydroxyl and carboxyl onto electrode surfaces. A standard sandwich-structured ionic pressure sensor with the configuration of “top modified electrode—porous ionic gel dielectric layer—bottom modified electrode” is finally assembled. The porous framework and modified electrodes constitute a dual synergistic enhancement system: the porous structure markedly reduces the equivalent elastic modulus of the gel and improves its compressive deformation capacity; polar-modified electrodes optimize the interfacial compatibility between electrodes and gels, shorten ion migration paths and lower interfacial contact resistance. Systematic calibration of multiple batches of parallel samples reveals that the as-fabricated sensor achieves a high sensitivity of 25.3 kPa−1 across the full measuring range from 0 to 1000 kPa with a linear fitting coefficient R2 = 0.992. The loading response time and unloading recovery time of the device are 60 ms and 80 ms respectively, with a performance degradation of less than 3% after 1000 consecutive loading–unloading cycles, featuring low hysteresis error and excellent signal repeatability. Multi-scenario in vivo wearable tests on human subjects verify that the device can precisely capture subtle fluctuations of radial artery pulse and periodic laryngeal deformation during swallowing, distinguish characteristic waveform patterns of various English words according to differences in vocal cord vibration, and accurately detect bending motions when attached to finger joints. The entire fabrication process adopts common chemical raw materials and standard laboratory equipment without expensive micro-nano processing facilities, featuring convenient raw material procurement and high process fault tolerance, which enables large-area coating-based mass production. This work delivers a novel technical route for the low-cost large-scale production of high-performance ionic flexible sensors and bears significant industrialization reference value for applications in wearable medical monitoring, bionic robotic electronic skin, flexible human–machine interactive touch panels and other related fields. Full article
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22 pages, 1228 KB  
Article
Comparative Analysis of Pavement Performance–Environmental–Cost Nexus for Desulfurized Rubber Powder Composite SBS-Modified Asphalt Mixture
by Mingcheng Jing, Hui Dou, Chunyu Zhang, Liangying Li, Jing Li and Bo Li
Materials 2026, 19(13), 2750; https://doi.org/10.3390/ma19132750 - 27 Jun 2026
Viewed by 186
Abstract
This study aims to systematically evaluate the balancing mechanism between road performance, carbon emissions, and economic cost when selecting asphalt materials for severe cold regions, filling the gap in multi-criteria decision-making for composite chemical modifications. To address alternating temperatures, heavy traffic, and modified [...] Read more.
This study aims to systematically evaluate the balancing mechanism between road performance, carbon emissions, and economic cost when selecting asphalt materials for severe cold regions, filling the gap in multi-criteria decision-making for composite chemical modifications. To address alternating temperatures, heavy traffic, and modified asphalt transport difficulties, this study presents a novel evaluation framework focusing on the performance–environmental–cost nexus of a desulfurized rubber powder composite SBS-modified asphalt mixture, which provides a clear technological breakthrough for high-ratio scrap tire recycling in seasonal frost zones. Two reference mixtures serve as comparisons: a conventional rubber powder composite SBS (styrene–butadiene–styrene triblock)-modified asphalt mixture (CR-SBS) and an SBS-modified asphalt mixture (SBS). A comparative experiment was conducted between the two materials and the SBS-modified asphalt mixture (ACR-SBS) compounded with desulfurized rubber powder. High-temperature stability was tested by the rutting test, low-temperature crack resistance by the beam bending test, and water stability by the immersion Marshall and freeze–thaw splitting tests. Life cycle carbon emissions and economic costs were quantified from raw material acquisition to construction. The results show that desulfurized rubber powder composite with ACR-SBS delivers the most superior overall road performance. However, it also generates the highest life cycle carbon footprint. Its total carbon emission reaches 162,800 kgCO2eq, which is 13.7% (19,600 kgCO2eq) higher than SBS (143,200 kgCO2eq) and 7.7% (11,600 kgCO2eq) higher than CR-SBS (151,200 kgCO2eq). The total cost of ACR-SBS is 391,000 CNY, which is 1.5% (6000 CNY) higher than SBS (385,000 CNY) and 1.3% (5000 CNY) lower than CR-SBS (396,000 CNY). These findings provide a basis for the selection of high-performance, low-carbon, and economical composite-modified asphalt in severe cold regions. Full article
(This article belongs to the Special Issue Development of Sustainable Asphalt Materials)
44 pages, 27226 KB  
Article
From Waste to Performance: Advancing Asphalt Recycling with Waste Oil Rejuvenators
by Bushra S. Mankhi, Saja A. Sead, Noha Shakir Kadhim, Zainab Al-Khafaji, Tameem Mohammed Hashim, Mohammed Salah Nasr and Ali Shubbar
Constr. Mater. 2026, 6(4), 40; https://doi.org/10.3390/constrmater6040040 - 26 Jun 2026
Viewed by 126
Abstract
The growing use of reclaimed asphalt pavement (RAP) in hot mix asphalt (HMA) is an important practice to achieve more sustainable pavements, as it reduces the consumption and environmental impact of virgin materials. However, aging induces binder stiffening that requires effective rejuvenation to [...] Read more.
The growing use of reclaimed asphalt pavement (RAP) in hot mix asphalt (HMA) is an important practice to achieve more sustainable pavements, as it reduces the consumption and environmental impact of virgin materials. However, aging induces binder stiffening that requires effective rejuvenation to restore overall performance. This study provides a comprehensive comparative analysis of ten chemically different waste oils—waste engine oil (WEO), waste cooking oil (WCO), yellow grease (YG), waste hydraulic oil (WHO) waste electric transformer oil (WETO), slop oil (SO), sludge-derived bio-oil (SDBO), tire pyrolysis oil (TPO), plastic pyrolysis oil (PPO), and algal residue oil (ARO)—as recycled HMA mixture rejuvenators, linking oil composition to binder regeneration and mixture performance. Binder properties were determined by rotational viscosity (RV), dynamic shear rheometer (DSR) and bending beam rheometer (BBR), whereas mixture performance was assessed in terms of Superpave mechanical properties, Hamburg wheel-tracking test (HWTT) for rutting resistance and mixture BBR for low-temperature cracking resistance. Performance grade (PG) evaluations showed that WETO and WEO restored the 50% and 75% RAP binders, respectively, to a grade close to PG 64-16 at the lowest dosages. The Superpave volumetric properties of all restored mixtures were similar to those of the control mixture, denoting corrected mixture balance and compaction level. HWTT results indicated that WETO-recycled mixtures revealed the lowest rut depth at 50% RAP, while WEO-recycled mixtures exhibited the lowest rut depth at 75% RAP after 20000 passes. Additional evidence supporting these results can be found in BBR mixture data, which demonstrated that WETO at 50% RAP and WEO/WETO at 75% RAP showed the most reduction in creep stiffness and improvement in creep rate. The correlation, regression, and PI analyses were in good agreement with the experimental results, where WETO and WEO exhibited the best overall performance at 50% and 75% RAP, respectively. In summary, these results indicate that the performance of waste oil rejuvenator in recycled HMA mixtures is highly dependent on RAP content and point to WETO and WEO as feasible, environmentally friendly options for high-RAP recycled HMA. Full article
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19 pages, 28769 KB  
Article
Differences in Microstructure and Properties of 16 mm Thick 6082 Aluminum Alloy Under Different Heat Source Conditions
by Zan Ju, Ruxu Huang, Xiaozhong Xie, Shu Liu, Feiyun Wang and Juan Fu
Coatings 2026, 16(6), 739; https://doi.org/10.3390/coatings16060739 (registering DOI) - 21 Jun 2026
Viewed by 237
Abstract
6082 aluminum alloy is widely applied in marine engineering, rail transportation and other industries owing to its excellent comprehensive performance. Welding heat source characteristics exert a decisive influence on the microstructure and mechanical properties of welded joints and become a major constraint for [...] Read more.
6082 aluminum alloy is widely applied in marine engineering, rail transportation and other industries owing to its excellent comprehensive performance. Welding heat source characteristics exert a decisive influence on the microstructure and mechanical properties of welded joints and become a major constraint for the application of medium-thick aluminum alloy welded structures. In this work, comparative tests of TIG and MIG welding were carried out on 16 mm thick 6082 aluminum alloy plates. Combining thermal simulation, metallographic observation and mechanical property tests, the temperature field distribution, microstructure, microhardness, tensile properties and bending properties of the two kinds of joints were systematically studied. The results show that TIG welding possesses high heat input, forming a broad temperature field with steep thermal gradients. Its weld microstructure is coarse and accompanied by severe coarsening of Mg2Si precipitates, and the joint presents a highly fluctuating M-shaped microhardness distribution. The average tensile strength of TIG welded joints is 194 MPa, and all specimens fracture in the heat-affected zone. By contrast, MIG welding with low heat input produces a uniform temperature field, as well as a fine and homogeneous weld microstructure with dispersed precipitates. Its microhardness distribution is stable, and the average tensile strength reaches 256 MPa, 32% higher than that of TIG joints. Both welding methods deliver favorable bending performance. The difference in heat input and cooling behavior changes the grain evolution and precipitate characteristics and further dominates the final mechanical performance of joints. MIG welding is more suitable for multi-layer, multi-pass welding of 16 mm thick 6082 aluminum alloy. This work clarifies the correlation between heat input, microstructure and mechanical properties, and the optimized process can effectively improve the microstructural uniformity of the weld joint and enhance its mechanical properties. Full article
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24 pages, 4421 KB  
Article
Experimental Characterization and Numerical Assessment of Cu-Al-Be Shape Memory Alloys for U-Shaped Flexural Plates
by Catalina Santibañez, Ramiro Bazáez, Luis Pérez, Yessica L. Avila-Avila and Gabriel Lara-Rodríguez
Materials 2026, 19(12), 2617; https://doi.org/10.3390/ma19122617 - 17 Jun 2026
Viewed by 259
Abstract
This study presents an experimental characterization and numerical assessment of Cu–Al–Be (CAB) shape memory alloys (SMAs) for potential applications in U-shaped flexural plate (UFP) seismic dampers. Six alloy compositions were evaluated through monotonic tensile tests, ASTM F2516 superelastic protocols, and increasing-amplitude cyclic loading [...] Read more.
This study presents an experimental characterization and numerical assessment of Cu–Al–Be (CAB) shape memory alloys (SMAs) for potential applications in U-shaped flexural plate (UFP) seismic dampers. Six alloy compositions were evaluated through monotonic tensile tests, ASTM F2516 superelastic protocols, and increasing-amplitude cyclic loading to identify the material exhibiting stable superelastic behavior at room temperature. Among the tested materials, alloy CAB4.76-A showed the most favorable response, with high transformation stress, stable pseudoelastic behavior, and strain recovery exceeding 95% for strains up to 2.5%. A phenomenological finite element model based on the Auricchio constitutive formulation was calibrated using experimental data within the validated strain range (ε ≤ 0.025), showing good agreement in stiffness and stress prediction. The calibrated model was subsequently applied to simulate the response of a UFP device under orthogonal cyclic loading. The results indicate a strong dependence on loading orientation due to coupled bending–torsion effects, with the 90° direction exhibiting significantly higher strength and energy dissipation capacity. Comparison with analytical formulations originally developed for steel UFPs showed that these expressions provide approximate estimates when applied to SMA-based devices. The results suggest that Cu–Al–Be alloys are a promising alternative for UFP applications, while highlighting the importance of loading orientation and the need for future experimental validation at a device scale. Full article
(This article belongs to the Special Issue Plastic Deformation and Mechanical Properties of Metallic Materials)
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20 pages, 10213 KB  
Article
GA/KH792 Surface Chemical Co-Modification for Enhancing Performance and Interfacial Properties of PET Fiber-Reinforced Asphalt Mastic
by Yingdong Zhao, Jiefen Kang, Yanan Guo, Yongling Ding, Huiling Yu, Qinxi Dong, Huadong Sun, Wenshu Cheng, Shuhua Song, Hong Yin and Kunpeng Zhao
Coatings 2026, 16(6), 703; https://doi.org/10.3390/coatings16060703 - 11 Jun 2026
Viewed by 219
Abstract
Polyester (PET) fibers are widely used to reinforce asphalt materials; however, their smooth and hydrophobic surfaces limit interfacial bonding and restrict their reinforcing efficiency. This study develops an eco-friendly surface modification method based on the chemical modification of gallic acid (GA) and aminosilane [...] Read more.
Polyester (PET) fibers are widely used to reinforce asphalt materials; however, their smooth and hydrophobic surfaces limit interfacial bonding and restrict their reinforcing efficiency. This study develops an eco-friendly surface modification method based on the chemical modification of gallic acid (GA) and aminosilane (KH792) to enhance the compatibility between PET fibers and asphalt. Modified fibers with various molar ratios of GA/KH792 were prepared and incorporated into asphalt mastic. Their performance was evaluated using softening point, cone penetration, dynamic shear rheometer (DSR), multiple stress creep recovery (MSCR), linear amplitude sweep (LAS), and bending beam rheometer (BBR) tests, combined with interfacial interaction analysis and scanning electron microscopy (SEM). The results show that surface modification significantly improves the reinforcing effect of PET fibers. In particular, the co-modified fiber with a GA/KH792 ratio of 1:1 exhibits the best performance, with increases of 27% in softening point and 105% in shear strength, as well as notable improvements in rutting resistance, fatigue performance, and temperature stability. Interfacial indices and SEM observations confirm enhanced adhesion, dispersion, and load transfer capacity. However, the improvement in low-temperature performance is limited. Overall, GA/KH792 chemical modification effectively enhances fiber asphalt interfacial interaction and provides a simple and sustainable approach for developing high-performance asphalt materials. Full article
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29 pages, 1713 KB  
Article
Preparation and Rheological Properties of Waterborne Epoxy Resin Emulsified Asphalt
by Siyu Wu, Huaxin Chen, Suining Zheng, Yonglu Dong and Wenlan Zhang
Materials 2026, 19(12), 2493; https://doi.org/10.3390/ma19122493 - 10 Jun 2026
Viewed by 228
Abstract
To address the lack of systematic quantitative studies on waterborne epoxy resin (WER)-modified emulsified asphalt regarding its rheological optimization and engineering applicability, this study fills the gap by preparing WER-modified emulsified asphalt via a two-step process. New findings reveal that 20% WER content [...] Read more.
To address the lack of systematic quantitative studies on waterborne epoxy resin (WER)-modified emulsified asphalt regarding its rheological optimization and engineering applicability, this study fills the gap by preparing WER-modified emulsified asphalt via a two-step process. New findings reveal that 20% WER content significantly enhances elastic components, creep–recovery, fatigue life, and fracture energy. The main objective is to establish a theoretical basis for high-performance pavement materials. Modified emulsified asphalt specimens with different waterborne epoxy resin contents were prepared using a two-step method of “emulsification followed by compounding”. The stability of the emulsions was quantitatively evaluated by zeta potential, storage stability, particle size distribution, and demulsification time. Their rheological parameters, multi-stress creep–recovery characteristics, fatigue life, and low-temperature crack resistance were systematically tested across the full temperature range using a dynamic shear rheometer and a bending beam rheometer. In addition, the bonding performance, strength development behavior, and water resistance durability were comprehensively assessed through pull-out tests, Marshall stability and splitting strength tests, as well as freeze–thaw cycle tests. These properties were compared with those of unmodified emulsified asphalt (UEA-0) and SBR-modified emulsified asphalt (SBR-EA). With an increase in waterborne epoxy resin content, the elastic component of the modified asphalt improved significantly, and the phase angle continuously decreased. The specimen with 20% waterborne epoxy resin content (WER-EA-20) exhibited the best performance: its phase angle was lower than those of the other groups under high-, medium-, and low-temperature conditions. After seven creep–recovery cycles, its creep–recovery rate remained at 33%, substantially higher than the 8% observed for the unmodified specimen. The fatigue life reached 15,000 cycles under a shear stress of 2.1 MPa. At −10 °C, the fracture strength was 0.92 MPa, and the fracture energy reached 21.4 J. Furthermore, the pull-out strength of WER-EA-20 was 0.86 MPa, with the failure mode identified as asphalt cohesive failure. After 37 days of curing, the Marshall stability reached 22.5 kN, and the splitting strength was 1.36 MPa. After 40 freeze–thaw cycles, the freeze–thaw splitting strength ratio (TSR) of WER-EA-20 remained above 75%, representing an improvement of more than 110% compared to the unmodified UEA-0 (TSR ≈ 35.5%), which highlights the significant enhancement in water resistance imparted by the waterborne epoxy resin. Compared to SBR-EA, WER-EA-20 has a higher softening point, a lower suitable mixing temperature, and better anti-aging properties. Waterborne epoxy resin can effectively improve the viscoelastic properties and overall road performance of emulsified asphalt, and the modification effect increases with increasing dosage. Full article
(This article belongs to the Special Issue Mechanical Dynamics and Rheological Insights in Advanced Materials)
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24 pages, 6670 KB  
Article
Effects of USP Warm-Mix Modifier on Rheological Properties of PG76-22 Asphalt Binder and Performance of Modified Mixture
by Liusheng Hu, Xiyuan Shen, Zheng Wang, Ji Ma and Weiguang Zhang
Materials 2026, 19(12), 2470; https://doi.org/10.3390/ma19122470 - 9 Jun 2026
Viewed by 185
Abstract
The USP modifier is an environmentally friendly warm-mix asphalt additive that can reduce asphalt viscosity and contribute to energy savings and emission mitigation. In this study, the PG76-22 asphalt binder was used as the control material, and a USP-modified PG76-22 asphalt binder was [...] Read more.
The USP modifier is an environmentally friendly warm-mix asphalt additive that can reduce asphalt viscosity and contribute to energy savings and emission mitigation. In this study, the PG76-22 asphalt binder was used as the control material, and a USP-modified PG76-22 asphalt binder was prepared. Microscopic characterization tests, asphalt binder performance tests, and asphalt mixture performance tests were conducted to investigate the effects of the USP modifier on the PG76-22 asphalt binder and its mixtures. The FM observations showed that the USP modifier was relatively uniformly dispersed in the binder without obvious large-scale agglomeration, while the FTIR results showed no new major characteristic absorption peaks after USP modification. These results suggest that no evident chemical reaction was detected under the adopted test conditions. At the binder level, the USP modifier improved the low-temperature ductility of the PG76-22 asphalt binder but reduced its high-temperature deformation resistance, as indicated by a lower rutting factor, increased non-recoverable deformation under high stress, and enhanced stress sensitivity. The LAS results further showed that the fatigue life of the USP-modified asphalt binder was lower than that of the PG76-22 asphalt binder. At the mixture level, USP modification increased the dynamic stability, residual stability, and tensile strength ratio by 6.2%, 5%, and 3%, respectively, and resulted in longer four-point bending fatigue life at the tested strain levels. These results indicate limited improvements in the measured mixture-level performance under the present laboratory conditions. However, the reduced binder-level rutting resistance and LAS fatigue life suggest that USP modification exhibits different effects at the binder and mixture levels, and the mixture-level results should not be directly extrapolated from binder-level rheological performance alone. Full article
(This article belongs to the Special Issue Sustainable Recycling Techniques of Pavement Materials (3rd Edition))
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17 pages, 4160 KB  
Article
High-Concentration Gold Nanoparticle Pastes for Advanced Deposition-Based Sensor Manufacturing
by Aleksandra Motyka, Sławomir Drozdek, Nina Szczotka, Iwona Grądzka-Kurzaj, Krzysztof Kubica, Aneta Wiatrowska and Karol Malecha
Sensors 2026, 26(11), 3507; https://doi.org/10.3390/s26113507 - 2 Jun 2026
Viewed by 563
Abstract
There is a growing demand for extreme miniaturization and enhanced sensitivity in next-generation sensing systems, including wearable devices and bioelectronics. Such advanced platforms require highly conductive, biocompatible, and mechanically robust architectures capable of conforming to dynamic surfaces. Conventional metallic thin-film fabrication techniques have [...] Read more.
There is a growing demand for extreme miniaturization and enhanced sensitivity in next-generation sensing systems, including wearable devices and bioelectronics. Such advanced platforms require highly conductive, biocompatible, and mechanically robust architectures capable of conforming to dynamic surfaces. Conventional metallic thin-film fabrication techniques have reached their fundamental physicochemical limits, often suffering from suboptimal mechanical strength, complex multi-step processing, and high costs. In contrast, additive manufacturing methodologies offer streamlined microfabrication, yet traditional printing methods frequently struggle with low-viscosity constraints, insufficient metal loading, and significant material losses. This paper covers the morphological fidelity, mechanical resilience, and electrical performance of rheologically tailored, high-concentration (above 90%) gold nanoparticle paste deposited via Ultra-Precise Dispensing (UPD) technology. The capability of the UPD system to print complex, high-density fractal geometries with linewidths down to 5 μm is evaluated on both rigid and flexible substrates, glass and polyimide, respectively. The mechanical structural integrity of these conductive traces is characterized under initial 360-degree bending tests. Finally, the electrical stability and thermal response of a printed proof-of-concept temperature sensor are evaluated. The printed fractal microstructures exhibit good resolution and the fabricated sensor demonstrates good stability, displaying a linear thermal response with a temperature coefficient of resistance of 1.98·10−3 °C−1, validating this combined material-deposition approach for microelectronics. Full article
(This article belongs to the Section Industrial Sensors)
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18 pages, 4205 KB  
Article
Performance Evaluation of Warm-Mix Agents on Crumb Rubber-Modified Asphalt
by Bo Huang, Song Xu, Shishui Liulin, Xiangjie Niu, Jihong Zhou and Xiong Xu
Materials 2026, 19(11), 2333; https://doi.org/10.3390/ma19112333 - 1 Jun 2026
Viewed by 265
Abstract
To achieve warm-mix production of crumb rubber-modified asphalt (CRA), an organic warm-mix agent, a surfactant-based warm-mix agent, and a composite warm-mix agent were employed to prepare warm-mix CRA. The effects of warm-mix agents on the physical properties of CRA were evaluated using the [...] Read more.
To achieve warm-mix production of crumb rubber-modified asphalt (CRA), an organic warm-mix agent, a surfactant-based warm-mix agent, and a composite warm-mix agent were employed to prepare warm-mix CRA. The effects of warm-mix agents on the physical properties of CRA were evaluated using the penetration test, softening point test, viscosity test, ductility test, and elastic recovery test. The effects of warm-mix agents on the high- and low-temperature rheological properties were investigated through dynamic shear rheometer (DSR), multiple stress creep recovery (MSCR), and bending beam rheometer (BBR) tests. Moreover, the viscosity–temperature characteristics and the VOC emissions of different warm-mix CRAs were explored. The results show that Sasobit, an organic warm-mix agent, increases the elastic fraction and stiffness of CRA, which enhances its high-temperature resistance to permanent deformation but compromises its low-temperature cracking resistance. UWM, a surfactant-based warm-mix agent, elevates the viscous fraction and flexibility of CRA, which improves its low-temperature cracking resistance but weakens its high-temperature rutting resistance. The composite warm-mix agent, consisting of 2 wt.% Sasobit and 5 wt.% UWM, can balance the stiffness and flexibility of CRA, endowing CRA with satisfactory pavement performance. All three warm-mix agents effectively reduce the viscosity, mixing temperature, and VOC emissions of CRA. The composite warm-mix agent reduces the VOC emissions of CRA by 53.0%, exhibiting the most pronounced reduction. Full article
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19 pages, 2475 KB  
Article
Adhesion Enhancement and Performance Evolution of Waste Plastic Modified Asphalt with Liquid Anti-Stripping Agents
by Jian Zhou, Juntao Wu, Di Yu and Xiaoyong Tan
Coatings 2026, 16(6), 661; https://doi.org/10.3390/coatings16060661 - 1 Jun 2026
Viewed by 295
Abstract
Waste plastics have attracted widespread attention in asphalt modification because of their environmental and economic benefits. However, the incorporation of waste plastics may weaken asphalt–aggregate interfacial adhesion, thereby increasing the risk of moisture damage in asphalt pavements. Although liquid anti-stripping agents have been [...] Read more.
Waste plastics have attracted widespread attention in asphalt modification because of their environmental and economic benefits. However, the incorporation of waste plastics may weaken asphalt–aggregate interfacial adhesion, thereby increasing the risk of moisture damage in asphalt pavements. Although liquid anti-stripping agents have been widely used in conventional asphalt systems, their effectiveness and performance evolution in waste plastic-modified asphalt (WPA) remain insufficiently understood. To address this gap, this study systematically investigated the effects of two liquid anti-stripping agents, AJ-1 and AMR-II, on the adhesion, rheological properties, and aging behavior of WPA. Specifically, asphalt–aggregate adhesion was evaluated using water-boiling and binder bond strength tests, rheological properties were characterized by dynamic shear rheometer and bending beam rheometer tests, and aging behavior was analyzed through rolling thin-film oven test, pressurized aging vessel, and Fourier transform infrared spectroscopy. The results show that waste plastics reduce the adhesion performance at the asphalt-aggregate interface, whereas anti-stripping agents compensate for this loss. Compared with AJ-1, AMR-II showed stronger adhesion enhancement, increasing the asphalt residual coating ratio by approximately 1.5%–3.5% and the pull-off tensile strength by 17.4%–28.1%, while the corresponding improvements for AJ-1 were approximately 1.3%–2.7% and 13.0%–25.0%, respectively. As the dosage of both anti-stripping agents increased, the penetration index decreased, the temperature susceptibility increased, the softening point generally decreased, and the ductility increased markedly. Temperature sweep results show that both AJ-1 and AMR-II reduce the high-temperature performance of WPA. According to the bending beam rheometer results, AMR-II also enhances the low-temperature performance of WPA. Aging test results indicate that both anti-stripping agents increase the aging sensitivity of WPA to some extent, but the adverse effect of AMR-II on aging resistance is smaller than that of AJ-1, and AMR-II better preserves the low-temperature ductility and adhesion performance after aging. Overall, this study provides a binder scale evaluation showing that 0.4% AMR-II may offer a more balanced strategy for improving the adhesion and service performance of WPA. Full article
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19 pages, 3188 KB  
Article
Investigation of Fatigue Failure and Electrical Insulation Properties of Glass Fiber-Reinforced Epoxy Resin (EPGF) Composites Under Different Temperatures
by Bowen Xu, Jinghan Wang, Chenglu Wang and Chen Cao
Energies 2026, 19(11), 2497; https://doi.org/10.3390/en19112497 - 22 May 2026
Viewed by 445
Abstract
This study investigates the influence of temperature on the bending properties, fatigue life, and breakdown voltage of glass fiber/epoxy composites (EPGF). The three-point bending tests were conducted at room temperature (RT) and 60 °C, and the bending fatigue tests were carried out under [...] Read more.
This study investigates the influence of temperature on the bending properties, fatigue life, and breakdown voltage of glass fiber/epoxy composites (EPGF). The three-point bending tests were conducted at room temperature (RT) and 60 °C, and the bending fatigue tests were carried out under three displacement amplitudes (0.80, 0.75, 0.70). At the same time, fatigue life prediction was conducted using the Weibull distribution fitting, microscopic structure analysis by scanning electron microscopy (SEM), and breakdown voltage tests in accordance with the GB/T1408-2006 standard. The results show that at 60 °C, the ultimate bending strength and flexural modulus of EPGF decreased by 52.67% and 65.45%, respectively. At high displacement amplitudes (S = 0.80, 0.75), 60 °C leads to a sharp rise in data dispersion with the coefficient of variation (CV) surging by 1.56 and 2.32 times separately. S and temperature exert a significant synergistic degradation effect on fatigue life, and the two-parameter Weibull distribution (R2 > 0.85) can well characterize the fatigue life of EPGF. In terms of dielectric properties, 60 °C reduces the initial breakdown voltage of EPGF by 4.23% (p < 0.05). Fatigue damage causes a continuous drop in breakdown voltage. At RT with 80% damage, the reduction rate increases from 16.28% to 26.95% as S rises, showing a synergistic characteristic between amplitude and fatigue damage. Moreover, 60 °C only affects the initial breakdown voltage and has no significant effect on the fatigue-induced decrease in breakdown voltage. SEM observations indicate that 60 °C induces matrix cracking, fiber curling and interfacial debonding in EPGF. This study provides key experimental data and theoretical support for the fatigue life prediction and insulation performance evaluation of EPGF under different temperature fatigue conditions. Full article
(This article belongs to the Special Issue Advanced Control and Monitoring of High Voltage Power Systems)
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22 pages, 3251 KB  
Article
A Steel-Reinforced Recycled Thermoplastic Composite for Wind Turbine Towers: Experimental and Full-Scale Validation
by Cihan Ciftci and Hasan Tolga Altikaya
J. Compos. Sci. 2026, 10(5), 275; https://doi.org/10.3390/jcs10050275 - 19 May 2026
Viewed by 542
Abstract
The increasing demand for sustainable and lightweight structural systems has motivated the development of alternative materials for wind turbine tower applications, where conventional steel structures are associated with high material consumption and environmental impact. In this study, a novel steel-reinforced recycled thermoplastic composite [...] Read more.
The increasing demand for sustainable and lightweight structural systems has motivated the development of alternative materials for wind turbine tower applications, where conventional steel structures are associated with high material consumption and environmental impact. In this study, a novel steel-reinforced recycled thermoplastic composite system is proposed as an alternative structural solution. To enable the design and practical application of such composite systems, the mechanical properties of the recycled thermoplastic matrix were experimentally characterized. Compression and tensile tests revealed average yield strengths of approximately 32 MPa in compression and 7.8 MPa in tension. To account for the environmental conditions encountered in field applications, the temperature-dependent mechanical behavior of the material was investigated. Since the critical mechanical response of the thermoplastic matrix in the composite system is governed by compression rather than tension, the study was limited to compression tests under elevated temperatures. The results show that the compressive yield strength decreases to approximately 31 MPa at 55 °C. An analytical model based on the transformed-section approach was also developed to predict the flexural behavior of the composite section and was validated through three-point bending tests, with an analytically predicted yield load of approximately 31.5 kN showing good agreement with experimental results. To assess structural applicability at a larger scale, a full-scale composite wind turbine tower was designed and manufactured, and its dynamic performance was evaluated through field measurements under natural wind loading conditions. The results indicate that the composite tower exhibits comparable dynamic behavior to a conventional steel tower, with a first natural frequency of approximately 3.08 Hz compared to 2.89 Hz for the steel tower, along with enhanced damping characteristics. These findings demonstrate that steel-reinforced recycled thermoplastic composites offer a promising and sustainable alternative for wind turbine tower applications, with potential for broader use in structural systems. Full article
(This article belongs to the Section Composites Applications)
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