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Keywords = fiber properties

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18 pages, 5831 KiB  
Article
Cure Kinetics-Driven Compression Molding of CFRP for Fast and Low-Cost Manufacturing
by Xintong Wu, Ming Zhang, Zhongling Liu, Xin Fu, Haonan Liu, Yuchen Zhang and Xiaobo Yang
Polymers 2025, 17(15), 2154; https://doi.org/10.3390/polym17152154 (registering DOI) - 6 Aug 2025
Abstract
Carbon fiber-reinforced polymer (CFRP) composites are widely used in aerospace due to their excellent strength-to-weight ratio and tailorable properties. However, these properties critically depend on the CFRP curing cycle. The commonly adopted manufacturer-recommended curing cycle (MRCC), designed to accommodate the most conservative conditions, [...] Read more.
Carbon fiber-reinforced polymer (CFRP) composites are widely used in aerospace due to their excellent strength-to-weight ratio and tailorable properties. However, these properties critically depend on the CFRP curing cycle. The commonly adopted manufacturer-recommended curing cycle (MRCC), designed to accommodate the most conservative conditions, involves prolonged curing times and high energy consumption. To overcome these limitations, this study proposes an efficient and adaptable method to determine the optimal curing cycle. The effects of varying heating rates on resin dynamic and isothermal–exothermic behavior were characterized via reaction kinetics analysis using differential scanning calorimetry (DSC) and rheological measurements. The activation energy of the reaction system was substituted into the modified Sun–Gang model, and the parameters were estimated using a particle swarm optimization algorithm. Based on the curing kinetic behavior of the resin, CFRP compression molding process orthogonal experiments were conducted. A weighted scoring system incorporating strength, energy consumption, and cycle time enabled multidimensional evaluation of optimized solutions. Applying this curing cycle optimization method to a commercial epoxy resin increased efficiency by 247.22% and reduced energy consumption by 35.7% while meeting general product performance requirements. These results confirm the method’s reliability and its significance for improving production efficiency. Full article
(This article belongs to the Special Issue Advances in High-Performance Polymer Materials, 2nd Edition)
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22 pages, 775 KiB  
Review
Bioactive Compounds, Technological Advances, and Sustainable Applications of Avocado (Persea americana Mill.): A Critical Review
by Amanda Priscila Silva Nascimento, Maria Elita Martins Duarte, Ana Paula Trindade Rocha and Ana Novo Barros
Foods 2025, 14(15), 2746; https://doi.org/10.3390/foods14152746 (registering DOI) - 6 Aug 2025
Abstract
Avocado (Persea americana), originally from Mesoamerica, has emerged as a focus of intense scientific and industrial interest due to its unique combination of nutritional richness, bioactive potential, and technological versatility. Its pulp, widely consumed across the globe, is notably abundant in [...] Read more.
Avocado (Persea americana), originally from Mesoamerica, has emerged as a focus of intense scientific and industrial interest due to its unique combination of nutritional richness, bioactive potential, and technological versatility. Its pulp, widely consumed across the globe, is notably abundant in monounsaturated fatty acids, especially oleic acid, which can comprise over two-thirds of its lipid content. In addition, it provides significant levels of dietary fiber, fat-soluble vitamins such as A, D, E and K, carotenoids, tocopherols, and phytosterols like β-sitosterol. These constituents are consistently associated with antioxidant, anti-inflammatory, glycemic regulatory, and cardioprotective effects, supported by a growing body of experimental and clinical evidence. This review offers a comprehensive and critical synthesis of the chemical composition and functional properties of avocado, with particular emphasis on its lipid profile, phenolic compounds, and phytosterols. It also explores recent advances in environmentally sustainable extraction techniques, including ultrasound-assisted and microwave-assisted processes, as well as the application of natural deep eutectic solvents. These technologies have demonstrated improved efficiency in recovering bioactives while aligning with the principles of green chemistry. The use of avocado-derived ingredients in nanostructured delivery systems and their incorporation into functional foods, cosmetics, and health-promoting formulations is discussed in detail. Additionally, the potential of native cultivars and the application of precision nutrition strategies are identified as promising avenues for future innovation. Taken together, the findings underscore the avocado’s relevance as a high-value matrix for sustainable development. Future research should focus on optimizing extraction protocols, clarifying pharmacokinetic behavior, and ensuring long-term safety in diverse applications. Full article
(This article belongs to the Special Issue Feature Review on Nutraceuticals, Functional Foods, and Novel Foods)
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29 pages, 15691 KiB  
Article
Mechanical Behavior and Response Mechanism of Short Fiber-Reinforced Polymer Structures Under Low-Speed Impact
by Xinke Xiao, Penglei Wang, Anxiao Guo, Linzhuang Han, Yunhao Yang, Yalin He and Xuanming Cai
Materials 2025, 18(15), 3686; https://doi.org/10.3390/ma18153686 (registering DOI) - 6 Aug 2025
Abstract
Short fiber-reinforced polymer (SFRP) has been extensively applied in structural engineering due to its exceptional specific strength and superior mechanical properties. Its mechanical behavior under medium strain rate conditions has become a key focus of ongoing research. A comprehensive understanding of the response [...] Read more.
Short fiber-reinforced polymer (SFRP) has been extensively applied in structural engineering due to its exceptional specific strength and superior mechanical properties. Its mechanical behavior under medium strain rate conditions has become a key focus of ongoing research. A comprehensive understanding of the response characteristics and underlying mechanisms under such conditions is of critical importance for both theoretical development and practical engineering applications. This study proposes an innovative three-dimensional (3D) multiscale constitutive model that comprehensively integrates mesoscopic fiber–matrix interface effects and pore characteristics. To systematically investigate the dynamic response and damage evolution of SFRP under medium strain rate conditions, 3D-printed SFRP porous structures with volume fractions of 25%, 35%, and 45% are designed and subjected to drop hammer impact experiments combined with multiscale numerical simulations. The experimental and simulation results demonstrate that, for specimens with a 25% volume fraction, the strain rate strengthening effect is the primary contributor to the increase in peak stress. In contrast, for specimens with a 45% volume fraction, the interaction between damage evolution and strain rate strengthening leads to a more complex stress–strain response. The specific energy absorption (SEA) of 25% volume fraction specimens increases markedly with increasing strain rate. However, for specimens with 35% and 45% volume fractions, the competition between these two mechanisms results in non-monotonic variations in energy absorption efficiency (EAE). The dominant failure mode under impact loading is shear-dominated compression, with damage evolution becoming increasingly complex as the fiber volume fraction increases. Furthermore, the damage characteristics transition from fiber pullout and matrix folding at lower volume fractions to the coexistence of brittle and ductile behaviors at higher volume fractions. The numerical simulations exhibit strong agreement with the experimental data. Multi-directional cross-sectional analysis further indicates that the initiation and propagation of shear bands are the principal drivers of structural instability. This study offers a robust theoretical foundation for the impact-resistant design and dynamic performance optimization of 3D-printed short fiber-reinforced polymer (SFRP) porous structures. Full article
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16 pages, 931 KiB  
Article
Evaluation of the Effects of Drying Techniques on the Physical and Nutritional Characteristics of Cricket (Gryllus bimaculatus) Powder for Use as Animal Feedstuff
by Warin Puangsap, Padsakorn Pootthachaya, Mutyarsih Oryza, Anusorn Cherdthong, Vibuntita Chankitisakul, Bundit Tengjaroensakul, Pheeraphong Phaengphairee and Sawitree Wongtangtintharn
Insects 2025, 16(8), 814; https://doi.org/10.3390/insects16080814 (registering DOI) - 6 Aug 2025
Abstract
This study aimed to evaluate the effects of three drying methods, namely sun drying, microwave–vacuum drying, and hot-air-oven drying, on the physical and nutritional properties of cricket powder for use in poultry feed. The results showed that the drying method significantly affected color [...] Read more.
This study aimed to evaluate the effects of three drying methods, namely sun drying, microwave–vacuum drying, and hot-air-oven drying, on the physical and nutritional properties of cricket powder for use in poultry feed. The results showed that the drying method significantly affected color parameters (L*, a*, and b*; p < 0.05), and particle size distribution at 850 µm and 250 µm (p = 0.04 and p = 0.02, respectively). Microwave–vacuum drying produced the lightest powder with a higher proportion of coarse particles, while sun drying resulted in a darker color and greater particle retention at 850 µm. Hot-air-oven drying yielded the lowest moisture content (1.99%) and the highest gross energy (6126.43 kcal/kg), with no significant differences observed in crude protein (p = 0.61), ether extract (p = 0.08), crude fiber (p = 0.14), ash (p = 0.22), or amino acid profiles (p > 0.05). These findings indicate that all drying methods preserved the nutritional value of cricket powder, and based on the overall results, hot-air-oven drying is the most suitable method for producing high-quality cricket meal with optimal physical properties and feed value, while also providing a practical balance between drying efficiency and cost. Full article
(This article belongs to the Section Role of Insects in Human Society)
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16 pages, 912 KiB  
Review
Connecting the Dots: Beetroot and Asthma
by Madiha Ajaz, Indu Singh, Lada Vugic, Rati Jani, Shashya Diyapaththugama and Natalie Shilton
J. Respir. 2025, 5(3), 12; https://doi.org/10.3390/jor5030012 - 5 Aug 2025
Abstract
Asthma is a persistent ailment that impacts the respiratory system and stands as a formidable public health challenge globally. Inhaled corticosteroids and bronchodilators, while effective in asthma management, are accompanied by side effects and high costs. Recently, nutraceuticals have gained significant attention as [...] Read more.
Asthma is a persistent ailment that impacts the respiratory system and stands as a formidable public health challenge globally. Inhaled corticosteroids and bronchodilators, while effective in asthma management, are accompanied by side effects and high costs. Recently, nutraceuticals have gained significant attention as adjuvant therapy due to their promising outcomes. Given the antioxidant properties, nutrient richness, and an array of health benefits, beetroot and its bioactive compounds have been tested as an adjuvant therapy for asthma management. Although its main bioactive compound, betalains (betanin), has demonstrated promising results in mouse studies, beetroot juice has been found to worsen asthma. This review investigated the full spectrum of active compounds associated with beetroots to understand the underlying factors contributing to the conflicting findings. The finding suggests that individual bioactive compounds, such as phenolic compounds, flavonoids, nitrates, betalains, saponins, vitamins, fiber, and carotenoids, possess asthma-managing properties. However, the consumption of juice may exacerbate the condition. This discrepancy may be attributed to the presence of sugars and oxalates in the juice, which could counteract the beneficial effects of the bioactive compounds. Full article
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33 pages, 4132 KiB  
Review
Mechanical Properties of Biodegradable Fibers and Fibrous Mats: A Comprehensive Review
by Ehsan Niknejad, Reza Jafari and Naser Valipour Motlagh
Molecules 2025, 30(15), 3276; https://doi.org/10.3390/molecules30153276 - 5 Aug 2025
Abstract
The growing demand for sustainable materials has led to increased interest in biodegradable polymer fibers and nonwoven mats due to their eco-friendly characteristics and potential to reduce plastic pollution. This review highlights how mechanical properties influence the performance and suitability of biodegradable polymer [...] Read more.
The growing demand for sustainable materials has led to increased interest in biodegradable polymer fibers and nonwoven mats due to their eco-friendly characteristics and potential to reduce plastic pollution. This review highlights how mechanical properties influence the performance and suitability of biodegradable polymer fibers across diverse applications. This covers synthetic polymers such as polylactic acid (PLA), polyhydroxyalkanoates (PHAs), polycaprolactone (PCL), polyglycolic acid (PGA), and polyvinyl alcohol (PVA), as well as natural polymers including chitosan, collagen, cellulose, alginate, silk fibroin, and starch-based polymers. A range of fiber production methods is discussed, including electrospinning, centrifugal spinning, spunbonding, melt blowing, melt spinning, and wet spinning, with attention to how each technique influences tensile strength, elongation, and modulus. The review also addresses advances in composite fibers, nanoparticle incorporation, crosslinking methods, and post-processing strategies that improve mechanical behavior. In addition, mechanical testing techniques such as tensile test machine, atomic force microscopy, and dynamic mechanical analysis are examined to show how fabrication parameters influence fiber performance. This review examines the mechanical performance of biodegradable polymer fibers and fibrous mats, emphasizing their potential as sustainable alternatives to conventional materials in applications such as tissue engineering, drug delivery, medical implants, wound dressings, packaging, and filtration. Full article
(This article belongs to the Section Materials Chemistry)
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13 pages, 1436 KiB  
Article
Basalt Fiber Mechanical Properties After Low-Temperature Treatment
by Sergey I. Gutnikov, Evgeniya S. Zhukovskaya, Sergey S. Popov and Bogdan I. Lazoryak
Textiles 2025, 5(3), 32; https://doi.org/10.3390/textiles5030032 - 5 Aug 2025
Abstract
This study investigates the production and characterization of basalt continuous fibers (BCFs) with varying oxide contents (including Na2O, SiO2, CaO, TiO2, and Al2O3), derived from modified basalt bulk glasses. The fibers were created [...] Read more.
This study investigates the production and characterization of basalt continuous fibers (BCFs) with varying oxide contents (including Na2O, SiO2, CaO, TiO2, and Al2O3), derived from modified basalt bulk glasses. The fibers were created through a two-stage process that included the preparation of basalt glasses followed by fiber drawing. A key focus of the research was on evaluating the mechanical properties of BCF after low-temperature treatments. Tensile testing revealed that the maximum tensile strength of the fibers was 1915 MPa at room temperature, which decreased to 1714 MPa at −196 °C, representing a shift of −10.5%. The addition of sodium oxide not only broadened the fiber-forming temperature range but also increased the strength to 2351 MPa. However, significant reductions in strength were observed at cryogenic temperatures, particularly for the Na-rich sample, which experienced a decrease of 32.8%. These findings highlight the importance of optimizing oxide content and minimizing hydroxyl (OH) groups to enhance the performance of basalt fibers in low-temperature applications, positioning them as viable materials for use in extreme environments. Full article
(This article belongs to the Special Issue Advances in Technical Textiles)
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12 pages, 240 KiB  
Communication
Enzymes (α-Amylase, Xylanase, and Cellulase) in Steamed Buckwheat Buns: The Effects on Quality and Predicted Glycemic Response
by Wenjun Liu, Jian Ming, Margaret Brennan and Charles Brennan
Foods 2025, 14(15), 2735; https://doi.org/10.3390/foods14152735 - 5 Aug 2025
Abstract
This study investigated the individual and combined effects of α-amylase (6 and 10 ppm), xylanase (70 and 120 ppm), and cellulase (35 and 60 ppm) on the physicochemical and nutritional properties of Chinese steamed buns (CSBs) supplemented with 15% buckwheat flour. The addition [...] Read more.
This study investigated the individual and combined effects of α-amylase (6 and 10 ppm), xylanase (70 and 120 ppm), and cellulase (35 and 60 ppm) on the physicochemical and nutritional properties of Chinese steamed buns (CSBs) supplemented with 15% buckwheat flour. The addition of individual enzymes did not significantly affect the volume or texture of the buckwheat-enriched CSBs, although it increased the crumb moisture content and porosity. In contrast, enzyme combinations can improve specific volume and reduce hardness. The enzyme combination (α-amylase 6 ppm, xylanase 70 ppm, and cellulase 60 ppm) yielded the highest specific volume (2.50 mL/g) and the lowest hardness (271.46 g). Regarding chemical properties, individual enzymes had minimal impact, while the combined treatment (6, 70, 60 ppm) decreased starch and dietary fiber content. For nutritional properties, the glycemic response of the CSBs varied depending on the concentration of the enzyme combination used. Full article
17 pages, 2855 KiB  
Article
Ballistic Performance of Lightweight Armor Aramid Fabric with Different Bounding Technologies
by István Péter Kondor, János Líska and Zsolt Ferenc Kovács
Fibers 2025, 13(8), 106; https://doi.org/10.3390/fib13080106 - 5 Aug 2025
Abstract
The aim of this research was to develop a lightweight armor that could be used in bulletproof vests or vehicle protection, offering an alternative to the disadvantageous properties of high-strength steel plates. Specifically, the study focused on investigating the properties of different binders [...] Read more.
The aim of this research was to develop a lightweight armor that could be used in bulletproof vests or vehicle protection, offering an alternative to the disadvantageous properties of high-strength steel plates. Specifically, the study focused on investigating the properties of different binders to identify the most suitable one for further development. The bulletproof characteristics of Kevlar (aramid) fiber fabric (200 g/m2, plain weave, CT709) were examined using both the Ansys simulation environment and ballistic laboratory testing. In the experiments, three different layer configurations were tested on 300 × 300 mm specimens, each consisting of 20 layers of Kevlar. The layers were arranged as follows: dry lamination for the first specimen, epoxy binder for the second, and polyurethane binder for the third. Laboratory tests were conducted using 9 mm Parabellum bullets, in accordance with the parameters defined in the MSZ K 1114-1:1999 standard. Both the ballistic and simulation tests indicated that the Kevlar laminated with polyurethane resin demonstrated the most promising performance and is suitable for further development. Full article
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16 pages, 10388 KiB  
Article
Highly-Oriented Polylactic Acid Fiber Reinforced Polycaprolactone Composite Produced by Infused Fiber Mat Process for 3D Printed Tissue Engineering Technology
by Zhipeng Deng, Chen Rao, Simin Han, Qungui Wei, Yichen Liang, Jialong Liu and Dazhi Jiang
Polymers 2025, 17(15), 2138; https://doi.org/10.3390/polym17152138 - 5 Aug 2025
Abstract
Three-dimensional printed polycaprolactone (PCL) tissue engineering scaffolds have drawn increasing interest from the medical industry due to their excellent biocompatibility and biodegradability, yet PCL’s poor mechanical performance has limited their applications. This study introduces a biocompatible and biodegradable polylactic acid (PLA) fiber reinforced [...] Read more.
Three-dimensional printed polycaprolactone (PCL) tissue engineering scaffolds have drawn increasing interest from the medical industry due to their excellent biocompatibility and biodegradability, yet PCL’s poor mechanical performance has limited their applications. This study introduces a biocompatible and biodegradable polylactic acid (PLA) fiber reinforced PCL (PLA/PCL) composite as the filament for 3D printed scaffolds to significantly enhance their mechanical performance: Special-made PLA short fiber mat was infused with PCL matrix and rolled into PLA/PCL filaments through a “Vacuum Assisted Resin Infusion” (VARI) process. The investigation revealed that the PLA fibers are highly oriented along the printing direction when using this filament for 3D printing due to the unique microstructure formed during the VARI process. At the same PLA fiber content, the percentage increase in Young’s modulus of the 3D printed strands using the filaments produced by the VARI process is 127.6% higher than the 3D printed strands using the filaments produced by the conventional melt blending process. The 3D printed tissue engineering scaffolds using the PLA/PCL composite filament with 11 wt% PLA fiber content also achieved an exceptional 84.2% and 143.3% increase in peak load and stiffness compared to the neat PCL counterpart. Full article
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17 pages, 4552 KiB  
Article
Trans-Scale Progressive Failure Analysis Methodology for Composite Materials Incorporating Interfacial Phase Effect
by Zhijie Li, Fei Peng, Jian Zhao, Sujuan Guo, Lefei Hu and Yu Gong
Materials 2025, 18(15), 3667; https://doi.org/10.3390/ma18153667 - 4 Aug 2025
Abstract
Fiber-reinforced resin matrix composites are generally composed of fibers and matrix with significantly different properties, which are non-uniform and anisotropic in nature. Macro-failure criteria generally view composite plies as a uniform whole and do not accurately reflect fiber- and matrix-scale failures. In this [...] Read more.
Fiber-reinforced resin matrix composites are generally composed of fibers and matrix with significantly different properties, which are non-uniform and anisotropic in nature. Macro-failure criteria generally view composite plies as a uniform whole and do not accurately reflect fiber- and matrix-scale failures. In this study, the interface phase effect between fiber and matrix has been introduced into the frame of trans-scale analysis to better model the failure process, and the equivalent mechanical property characterization model of the interface phase has also been established. Combined with the macro–micro-strain transfer method, the trans-scale correlation of the mechanical response of the composite laminates between the macro scale and the fiber, matrix and interface micro scale has been achieved. Based on the micro-scale failure criterion and the stiffness reduction strategy, the trans-scale failure analysis method of composite materials incorporating the interface phase effect has been developed, which can simultaneously predict the failure modes of the matrix, fiber and interface phase. A numerical implementation of the developed trans-scale failure analysis method considering interface phase was carried out using the Python and Abaqus 2020 joint simulation technique. Case studies were carried out for three material systems, and the prediction data of the developed trans-scale failure analysis methodology incorporating interface phase effects for composite materials, the prediction data of the Linde failure criterion and the experimental data were compared. The comparison with experimental data confirms that this method has good prediction accuracy, and compared with the Linde and Hashin failure methods, only it can predict the failure mode of the fiber–matrix interface. The case analysis shows that its prediction accuracy has been improved by about 2–3%. Full article
(This article belongs to the Special Issue Fatigue Damage, Fracture Mechanics of Structures and Materials)
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38 pages, 15791 KiB  
Article
Experimental and Statistical Evaluations of Recycled Waste Materials and Polyester Fibers in Enhancing Asphalt Concrete Performance
by Sara Laib, Zahreddine Nafa, Abdelghani Merdas, Yazid Chetbani, Bassam A. Tayeh and Yunchao Tang
Buildings 2025, 15(15), 2747; https://doi.org/10.3390/buildings15152747 - 4 Aug 2025
Abstract
This research aimed to evaluate the impact of using brick waste powder (BWP) and varying lengths of polyester fibers (PFs) on the performance properties of asphalt concrete (AC) mixtures. BWP was utilized as a replacement for traditional limestone powder (LS) filler, while PFs [...] Read more.
This research aimed to evaluate the impact of using brick waste powder (BWP) and varying lengths of polyester fibers (PFs) on the performance properties of asphalt concrete (AC) mixtures. BWP was utilized as a replacement for traditional limestone powder (LS) filler, while PFs of three lengths (3 mm, 8 mm, and 15 mm) were introduced. The study employed the response surface methodology (RSM) for experimental design and analysis of variance (ANOVA) to identify the influence of BWP and PF on the selected performance indicators. These indicators included bulk density, air voids, voids in the mineral aggregate, voids filled with asphalt, Marshall stability, Marshall flow, Marshall quotient, indirect tensile strength, wet tensile strength, and the tensile strength ratio. The findings demonstrated that BWP improved moisture resistance and the mechanical performance of AC mixes. Moreover, incorporating PF alongside BWP further enhanced these properties, resulting in superior overall performance. Using multi-objective optimization through RSM-based empirical models, the study identified the optimal PF length of 5 mm in combination with BWP for achieving the best AC properties. Validation experiments confirmed the accuracy of the predicted results, with an error margin of less than 8%. The study emphasizes the intriguing prospect of BWP and PF as sustainable alternatives for improving the durability, mechanical characteristics, and cost-efficiency of asphalt pavements. Full article
(This article belongs to the Special Issue Advanced Studies in Asphalt Mixtures)
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20 pages, 1743 KiB  
Article
Encapsulation of Lactobacillus reuteri in Chia–Alginate Hydrogels for Whey-Based Functional Powders
by Alma Yadira Cid-Córdoba, Georgina Calderón-Domínguez, María de Jesús Perea-Flores, Alberto Peña-Barrientos, Fátima Sarahi Serrano-Villa, Rigoberto Barrios-Francisco, Marcela González-Vázquez and Rentería-Ortega Minerva
Gels 2025, 11(8), 613; https://doi.org/10.3390/gels11080613 - 4 Aug 2025
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Abstract
This study aimed to develop a functional powder using whey and milk matrices, leveraging the protective capacity of chia–alginate hydrogels and the advantages of electrohydrodynamic spraying (EHDA), a non-thermal technique suitable for encapsulating probiotic cells under stress conditions commonly encountered in food processing. [...] Read more.
This study aimed to develop a functional powder using whey and milk matrices, leveraging the protective capacity of chia–alginate hydrogels and the advantages of electrohydrodynamic spraying (EHDA), a non-thermal technique suitable for encapsulating probiotic cells under stress conditions commonly encountered in food processing. A hydrogel matrix composed of chia seed mucilage and sodium alginate was used to form a biopolymeric network that protected probiotic cells during processing. The encapsulation efficiency reached 99.0 ± 0.01%, and bacterial viability remained above 9.9 log10 CFU/mL after lyophilization, demonstrating the excellent protective capacity of the hydrogel matrix. Microstructural analysis using confocal laser scanning microscopy (CLSM) revealed well-retained cell morphology and homogeneous distribution within the hydrogel matrix while, in contrast, scanning electron microscopy (SEM) showed spherical, porous microcapsules with distinct surface characteristics influenced by the encapsulation method. Encapsulates were incorporated into beverages flavored with red fruits and pear and subsequently freeze-dried. The resulting powders were analyzed for moisture, protein, lipids, carbohydrates, fiber, and color determinations. The results were statistically analyzed using ANOVA and response surface methodology, highlighting the impact of ingredient ratios on nutritional composition. Raman spectroscopy identified molecular features associated with casein, lactose, pectins, anthocyanins, and other functional compounds, confirming the contribution of both matrix and encapsulants maintaining the structural characteristics of the product. The presence of antioxidant bands supported the functional potential of the powder formulations. Chia–alginate hydrogels effectively encapsulated L. reuteri, maintaining cell viability and enabling their incorporation into freeze-dried beverage powders. This approach offers a promising strategy for the development of next-generation functional food gels with enhanced probiotic stability, nutritional properties, and potential application in health-promoting dairy systems. Full article
(This article belongs to the Special Issue Food Gels: Fabrication, Characterization, and Application)
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20 pages, 3145 KiB  
Article
Determination of Dynamic Elastic Properties of 3D-Printed Nylon 12CF Using Impulse Excitation of Vibration
by Pedro F. Garcia, Armando Ramalho, Joel C. Vasco, Rui B. Ruben and Carlos Capela
Polymers 2025, 17(15), 2135; https://doi.org/10.3390/polym17152135 - 4 Aug 2025
Viewed by 31
Abstract
Material Extrusion (MEX) process is increasingly used to fabricate components for structural applications, driven by the availability of advanced materials and greater industrial adoption. In these contexts, understanding the mechanical performance of printed parts is crucial. However, conventional methods for assessing anisotropic elastic [...] Read more.
Material Extrusion (MEX) process is increasingly used to fabricate components for structural applications, driven by the availability of advanced materials and greater industrial adoption. In these contexts, understanding the mechanical performance of printed parts is crucial. However, conventional methods for assessing anisotropic elastic behavior often rely on expensive equipment and time-consuming procedures. The aim of this study is to evaluate the applicability of the impulse excitation of vibration (IEV) in characterizing the dynamic mechanical properties of a 3D-printed composite material. Tensile tests were also performed to compare quasi-static properties with the dynamic ones obtained through IEV. The tested material, Nylon 12CF, contains 35% short carbon fibers by weight and is commercially available from Stratasys. It is used in the fused deposition modeling (FDM) process, a Material Extrusion technology, and exhibits anisotropic mechanical properties. This is further reinforced by the filament deposition process, which affects the mechanical response of printed parts. Young’s modulus obtained in the direction perpendicular to the deposition plane (E33), obtained via IEV, was 14.77% higher than the value in the technical datasheet. Comparing methods, the Young’s modulus obtained in the deposition plane, in an inclined direction of 45 degrees in relation to the deposition direction (E45), showed a 22.95% difference between IEV and tensile tests, while Poisson’s ratio in the deposition plane (v12) differed by 6.78%. This data is critical for designing parts subject to demanding service conditions, and the results obtained (orthotropic elastic properties) can be used in finite element simulation software. Ultimately, this work reinforces the potential of the IEV method as an accessible and consistent alternative for characterizing the anisotropic properties of components produced through additive manufacturing (AM). Full article
(This article belongs to the Special Issue Mechanical Characterization of Polymer Composites)
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21 pages, 1870 KiB  
Article
Characterization of Bimi® Broccoli as a Convenience Food: Nutritional Composition and Quality Traits Following Industrial Sous-Vide Processing
by Elisa Canazza, Christine Mayr Marangon, Dasha Mihaylova, Valerio Giaccone and Anna Lante
Molecules 2025, 30(15), 3255; https://doi.org/10.3390/molecules30153255 - 3 Aug 2025
Viewed by 233
Abstract
This study investigates Bimi® (Brassica oleracea Italica × Alboglabra), a hybrid between kailan and conventional broccoli, to evaluate its compositional, functional, and sensory properties in relation to industrial sous-vide processing and refrigerated storage. Proximate composition, amino acid and fatty acid profiles, [...] Read more.
This study investigates Bimi® (Brassica oleracea Italica × Alboglabra), a hybrid between kailan and conventional broccoli, to evaluate its compositional, functional, and sensory properties in relation to industrial sous-vide processing and refrigerated storage. Proximate composition, amino acid and fatty acid profiles, and mineral content were determined in raw samples. Color, chlorophyll content, total polyphenols, and antioxidant capacity (FRAP, ABTS, DPPH) were analyzed before and after sous-vide treatment and following 60 days of storage. Microbiological and physicochemical stability was monitored over 90 days under standard (4 °C) and mildly abusive (6–10 °C) storage conditions. Sensory profiling of Bimi® and conventional broccoli was performed on sous-vide samples. The results showed an increase in total polyphenols and antioxidant activity after processing, while chlorophylls decreased. Microbiological safety was maintained under all conditions, with stable water activity and only moderate acidification. Bimi® provided a valuable source of protein (4.32 g/100 g FW, 8.63% RDA), appreciable amounts of dietary fiber (2.96 g/100 g FW, 11.85% RDA), and essential minerals such as potassium (15.59% RDA), phosphorus (14.05% RDA), and calcium (8.09% RDA). Sensory evaluation revealed a milder flavor profile than that of conventional broccoli, accompanied by an asparagus-like aroma. These findings support the suitability of Bimi® for industrial sous-vide processing and its potential as a nutritious convenience food. Full article
(This article belongs to the Special Issue Bioactive Compounds in Food and Their Applications)
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