Search Results (567)

This study investigates the interplay between infill structure and surface texture in Fused Deposition Modeling (FDM)-printed polymer specimens and their combined influence on tribological and mechanical performance. Unlike previous works that focus on single-variable analysis, this work offers a comparative evaluation of Shore D hardness and coefficient of friction (COF) for PLA and Iglidur materials, incorporating diverse infill patterns. The results reveal that specific combinations (e.g., grid infill with 90% density) optimize hardness and minimize friction, offering practical insights for design optimization in functional parts. Our aim is to provide design insights for enhanced wear resistance and hardness through tailored structural configurations. Carbon Fiber-reinforced PLA (PLA CF), aramid fiber-reinforced Acrylonitrile Styrene Acrylate (Kevlar), and Iglidur I180-BL tribofilament. Disc specimens were fabricated with gyroid infill densities ranging from 10% to 100%. Experimental methodologies included Ball-on-Disc tests conducted under dry sliding conditions (5 N normal load, 150 mm/s sliding speed) to assess friction and wear characteristics. These tribological evaluations were complemented by profilometric and microscopic analyses and Shore D hardness testing. The results show that Iglidur I180-BL achieved the lowest friction coefficients (0.141–0.190) and negligible wear, while PLA specimens with 90% infill demonstrated a polishing-type wear with minimal material loss and a friction coefficient (COF) of ~0.108. In contrast, PLA CF and Kevlar exhibited higher wear depths (up to 154 µm for Kevlar) and abrasive mechanisms due to fiber detachment. Shore hardness values increased with infill density, with PLA reaching a maximum of 82.7 Shore D. These findings highlight the critical interplay between infill architecture and surface patterning and offer actionable guidelines for the functional design of durable FDM components in load-bearing or sliding applications. Full article

This study focuses on producing and processing highly aligned tapes from recycled carbon fibers (rCFs). The rCFs are processed with a modified carding machine, oriented through a specialized subsequent process and consolidated into a semi-finished product. These rCF-tapes are placed onto a two-dimensional tool using an adapted automated fiber placement (AFP) technology to demonstrate a novel approach of producing composites from highly oriented recycled materials. The semi-finished stacks are consolidated in a heating press and test coupons are tested according to corresponding standards. The rCF-tapes are evaluated using methods such as tensile and flexural testing and determination of fiber volume content. Mechanical values are assessed by processing various generations of rCF-tapes and comparing them to each other and to virgin fiber tapes (vCF-tapes) made of the same type of carbon fiber and matrix. Microscopic imaging is also performed to analyze the quality of the resulting composites. In this study, a tensile strength of up to 1100 MPa in the fiber direction and stiffness of up to 80 GPa at a fiber volume content (FVC) of approximately 40% were achieved. The results highlight the strong potential and benefits of using highly oriented rCF-tapes and demonstrate the suitability of fiber placement technologies for those recycled materials. Full article

Material Extrusion (MEX) process is increasingly used to fabricate components for structural applications, driven by the availability of advanced materials and greater industrial adoption. In these contexts, understanding the mechanical performance of printed parts is crucial. However, conventional methods for assessing anisotropic elastic behavior often rely on expensive equipment and time-consuming procedures. The aim of this study is to evaluate the applicability of the impulse excitation of vibration (IEV) in characterizing the dynamic mechanical properties of a 3D-printed composite material. Tensile tests were also performed to compare quasi-static properties with the dynamic ones obtained through IEV. The tested material, Nylon 12CF, contains 35% short carbon fibers by weight and is commercially available from Stratasys. It is used in the fused deposition modeling (FDM) process, a Material Extrusion technology, and exhibits anisotropic mechanical properties. This is further reinforced by the filament deposition process, which affects the mechanical response of printed parts. Young’s modulus obtained in the direction perpendicular to the deposition plane (E₃₃), obtained via IEV, was 14.77% higher than the value in the technical datasheet. Comparing methods, the Young’s modulus obtained in the deposition plane, in an inclined direction of 45 degrees in relation to the deposition direction (E₄₅), showed a 22.95% difference between IEV and tensile tests, while Poisson’s ratio in the deposition plane (v₁₂) differed by 6.78%. This data is critical for designing parts subject to demanding service conditions, and the results obtained (orthotropic elastic properties) can be used in finite element simulation software. Ultimately, this work reinforces the potential of the IEV method as an accessible and consistent alternative for characterizing the anisotropic properties of components produced through additive manufacturing (AM). Full article

Carbon fiber (CF) and carbon fiber-reinforced polymers (CFRPs) are widely used in the aerospace, automotive, and energy sectors due to their high strength, stiffness, and low density. However, significant waste is generated during manufacturing and after the use of CFRPs. Traditional disposal methods like landfilling and incineration are unsustainable. CFRP machining processes, such as drilling and milling, produce fine chips and dust that are difficult to recycle due to their heterogeneity and contamination. This study investigates the oxidation behavior of CFRP drilling waste from two types of materials (tube and plate) under oxidative (non-inert) conditions. Thermogravimetric analysis (TGA) was performed from 200 °C to 800 °C to assess weight loss related to polymer degradation and carbon fiber integrity. Scanning electron microscopy (SEM) was used to analyze morphological changes and fiber damage. The optimal range for removing the polymer matrix without significant fiber degradation has been identified as 500–600 °C. At temperatures above 700 °C, notable surface and internal fiber damage occurred, along with nanostructure formation, which may pose health and environmental risks. The results show that partial fiber recovery is possible under ambient conditions, and this must be considered regarding the harmful risks to the human body if submicron particles are inhaled. This research supports sustainable CFRP recycling and fire hazard mitigation. Full article

Rammed earth (RE), a traditional material aligned with circular economy (CE) principles, has been gaining renewed interest in contemporary construction due to its low environmental impact and compatibility with sustainable building strategies. Though not a modern invention, it is being reintroduced in response to the increasingly strict European Union (EU) regulations on carbon footprint, life cycle performance, and thermal efficiency. RE walls offer multiple benefits, including humidity regulation, thermal mass, plasticity, and structural strength. This study also draws attention to their often-overlooked ability to mitigate indoor overheating. To preserve these advantages while enhancing thermal performance, this study explores insulation strategies that maintain the vapor-permeable nature of RE walls. A parametric analysis using Delphin 6.1 software was conducted to simulate heat and moisture transfer in two main configurations: (a) a ventilated system insulated with mineral wool (MW), wood wool (WW), hemp shives (HS), and cellulose fiber (CF), protected by a jute mat wind barrier and finished with wooden cladding; (b) a closed system using MW and WW panels finished with lime plaster. In both cases, clay plaster was applied on the interior side. The results reveal distinct hygrothermal behavior among the insulation types and confirm the potential of natural, low-processed materials to support thermal comfort, moisture buffering, and the alignment with CE objectives in energy-efficient construction. Full article

In this study, alkali-activated coal gangue-slag material (AACGS) was prepared using coal gangue and slag as precursors, and its feasibility as conductive mortar substrate material was preliminarily investigated. Firstly, this study employed Response Surface Methodology (RSM) to develop statistical models correlating the alkali equivalent, water-to-binder ratio, and slag content with the compressive strength, flexural strength, and resistivity of AACGS, aiming to identify the optimal mix proportions. Secondly, based on the optimal ratio identified above and using carbon fibers (CF) as the conductive phase, an alkali-activated conductive mortar (CF-AACGS) was prepared, and its compressive strength, flexural strength, and resistivity were tested. Lastly, XRD and SEM-EDS were conducted to characterize the mineral composition and microstructure of CF-AACGS. The results indicate that when the alkali equivalent, water-to-binder ratio, and slag content are 13.34%, 0.54, and 57.52%, respectively, the AACGS achieves compressive strength, flexural strength, and resistivity of 72.5 MPa, 7.0 MPa, and 62.41 Ω·m at 28 days. Under the action of the alkali activator, coal gangue and slag undergo hydration reactions, forming a denser N, C-(A)-S-H gel. This effectively improves the interface transition zone between the CF and AACGS, endowing the CF-AACGS with superior mechanical properties. Furthermore, the AACGS matrix enhances the conductive contact point density by optimizing CF dispersion, which significantly reduces the resistivity of the CF-AACGS. Full article

Carbon layer-coated μm-sized carbon fiber has the potential to be developed as an electrode, as it can be directly used as an electrode without any preparation process in the absence of an insulating binder. In our work, a carbon layer-coated carbon fiber (C@CF) coaxial structure is constructed by in situ conversion of the epoxy resin around the carbon fiber into a carbon layer, in which a sandwich scaffold of cover/CFRP/screen is designed and adopted. The activated SC@CF, i.e., A-SC@CF, can be directly served as the electrode, and has excellent supercapacitor performance: a high specific capacity of 227.1 F g⁻¹ at 0.5 A g⁻¹, with a capacitance retention of 98.9% after 20,000 cycles for the electrode, and an energy density of 16.68 Wh kg⁻¹ at the power density of 1400 W kg⁻¹ for its symmetrical supercapacitor (SSC). Full article

This study explores the mechanical behavior of polymer and composite specimens fabricated using fused deposition modeling (FDM), focusing on three material configurations: acrylonitrile butadiene styrene (ABS), carbon fiber-reinforced polyphthalamide (PPA/Cf), and a sandwich-structured composite. A systematic experimental plan was developed using the Box–Behnken design (BBD) to investigate the effects of material type (MT), infill pattern (IP), and printing direction (PD) on tensile and flexural strength. Experimental results showed that the PPA/Cf material with a “Cross” IP printed “Flat” yielded the highest mechanical performance, achieving a tensile strength of 75.8 MPa and a flexural strength of 102.3 MPa. In contrast, the lowest values were observed in ABS parts with a “Grid” pattern and “Upright” orientation, recording 37.8 MPa tensile and 49.5 MPa flexural strength. Analysis of variance (ANOVA) results confirmed that all three factors significantly influenced both outputs (p < 0.001), with MT being the most dominant factor. Machine learning (ML) algorithms, Bayesian linear regression (BLR), and Gaussian process regression (GPR) were employed to predict mechanical performance. GPR achieved the best overall accuracy with R² = 0.9935 and MAPE = 11.14% for tensile strength and R² = 0.9925 and MAPE = 12.96% for flexural strength. Comparatively, the traditional BBD yielded slightly lower performance with MAPE = 13.02% and R² = 0.9895 for tensile strength. Validation tests conducted on three unseen configurations clearly demonstrated the generalization capability of the models. Based on actual vs. predicted values, the GPR yielded the lowest average prediction errors, with MAPE values of 0.54% for tensile and 0.45% for flexural strength. In comparison, BLR achieved 0.79% and 0.60%, while BBD showed significantly higher errors at 1.76% and 1.32%, respectively. Full article

Fused Filament Fabrication (FFF) enables the manufacturing of complex polymer components. However, surface finish and dimensional accuracy remain key limitations for their integration into functional assemblies. This study explores the potential of conventional turning as a post-processing strategy to improve the geometric and surface quality of PLA reinforced with carbon fiber (CF) parts produced by FFF. Machinability was evaluated through the analysis of cutting forces, thermal behavior, energy consumption, and surface integrity under varying cutting speeds, feed rates, and specimen slenderness. The results indicate that feed is the most influential parameter across all performance metrics, with lower values leading to improved dimensional accuracy and surface finish, achieving the most significant reductions of 63% in surface roughness (Sa) and 62% in cylindricity deviation. Nevertheless, the surface roughness is higher than that of metals, and deviations in geometry along the length of the specimen have been observed. A critical shear stress of 0.237 MPa has been identified as the limit for interlayer failure, defining the boundary conditions for viable cutting operation. The incorporation of CNC turning as a post-processing step reduced the total fabrication time by approximately 83% compared with high-resolution FFF, while maintaining dimensional accuracy and enhancing surface quality. These findings support the use of machining operations as a viable and efficient post-processing method for improving the functionality of polymer-based components produced by additive manufacturing. Full article

To address the mechanical deficiencies of traditional pervious concrete and promote its practical implementation, this study developed a high-performance pervious concrete model using conventional materials and methods, achieving a permeability coefficient of 4.5 mm/s with compressive and flexural strengths exceeding 45 MPa and 5 MPa, respectively. Central composite design (CCD) response surface methodology was employed to investigate the individual and synergistic effects of the water–cement ratio (W/C), nano-silica (NS), and carbon fibers (CF) on permeability, compressive strength, and flexural strength. Statistical models demonstrating prediction errors within 7% of experimental values were established, supplemented by a microstructural analysis of the concrete specimens. The results demonstrated that (1) the W/C ratio significantly influences overall performance; (2) NS enhances mechanical strength while reducing permeability, though excessive NS content induces weak interfacial zones that compromise strength; (3) CFs exhibit negligible impact on compressive strength but substantially improve flexural performance; and (4) significant synergistic interactions are present across W/C ratio, NS, and CFs concerning flexural strength parameters, while no significant interaction was observed for compressive strength. Full article

To address the challenges of concrete construction in polar regions, this study investigates the feasibility of fabricating cement-based materials under severely low temperatures using electric-induced heating curing methods. Cement mortars incorporating fly ash (FA-CM), ground granulated blast furnace slag (GGBS-CM), and metakaolin (MK-CM) were cured at environmental temperatures of −20 °C, −40 °C, and −60 °C. The optimal carbon fiber (CF) contents were determined using the initial electric resistivity to ensure a consistent electric-induced heating curing process. The thermal profiles during curing were monitored, and mechanical strength development was systematically evaluated. Hydration characteristics were elucidated through thermogravimetric analysis (TG), X-ray diffraction (XRD), and Fourier-transform infrared spectroscopy (FTIR) to identify phase compositions and reaction products. Results demonstrate that electric-induced heating effectively mitigates the adverse effect caused by the ultra-low temperature constraints, with distinct differences in the strength performance and hydration kinetics among supplementary cementitious materials. MK-CM exhibited superior early strength development with strength increasing rates above 10% compared to the Ref. specimen, which was attributed to the accelerated pozzolanic reactions. Microstructural analyses further verified the macroscopic strength test results that showed that electric-induced heating curing can effectively promote the performance development even under severely cold environments with a higher hydration degree and refined micro-pore structure. This work proposes a viable strategy for polar construction applications. Full article

To solve the problems of carbon fiber (CF) electrodes, including poor frequency response and large potential drift, CFs were subjected to a roughening pretreatment process combining thermal oxidation and electrochemical anodic oxidation and then modified with Ag nanoparticles (AgNPs) using electroplating to prepare a CF electric field sensor. The surface morphology of the as-prepared AgNP-CF electric field sensor was characterized via optical microscopy, scanning electron microscopy, XPS, and energy-dispersive spectroscopy, and its impedance, polarization drift, self-noise, and temperature drift values were determined. Results show that the surface modification of the AgNP-CF electric field sensor is uniform, and its specific surface area is considerably increased. The electrode potential drift, characteristic impedance, self-noise, and temperature drift are 52.1 µV/24 h, 3.6 Ω, 2.993 nV/√Hz@1 Hz, and less than 70 µV/°C, respectively. Additionally, the AgNP-CF electric field sensor demonstrates low polarization and high stability. In field and simulated ocean tests, the AgNP-CF electrode exhibits excellent performance in the field and underwater environments, which renders it promising for the measurement of the ocean and geoelectric fields owing to its advantages, such as low noise and high stability. Full article

Thermoplastic polyurethane (TPU) combines elastomeric and thermoplastic properties but suffers from insufficient rigidity and strength for structural applications. Herein, we developed novel carbon fiber-reinforced TPU (CF/TPU) composites filaments and utilize melt extrusion for 3D printing to maintain elasticity, while achieving enhanced stiffness and strength through multi scale-the control of fiber content and optimization of printing parameters, reaching a rigid–elastic balance. A systematic evaluation of CF content (0–25%) and printing parameters revealed optimal performance to be at 220–230 °C and 40 mm/s for ensuring proper flow to wet fibers without polymer degradation. Compared with TPU, 20% CF/TPU exhibited 63.65%, 105.51%, and 93.69% improvements in tensile, compressive, and impact strength, respectively, alongside 70.88% and 72.92% enhancements in compression and impact energy absorption. This work establishes a fundamental framework for developing rigid–elastic hybrid materials with tailored energy absorption capabilities through rational material design and optimized additive manufacturing processes. Full article

Hybrid fiber-reinforced polymer-laminated composites are often used under icy conditions (such as for reinforcing parts in aircraft frames and bridge beams), where there is an urgent demand for deicing. In this paper, besides the different mechanical properties of laminates along the longitudinal carbon fiber (CF) and glass fiber (GF) directions, the anisotropic electrothermal behavior of a hybrid glass/carbon fiber-reinforced epoxy (GCF/EP) is also investigated, as well as its deicing performance and self-repairing capability. The surface equilibrium temperature of GCF/EP composites can conveniently be adjusted by tuning the current magnitude and its flow direction. Compared to the longitudinal CF direction of the GCF/EP, where 0.3 A was loaded to achieve a surface equilibrium temperature of 122.8 °C, a much weaker current (0.03 A) was needed to load along the longitudinal GF direction to reach almost the same temperature. However, besides the higher flexural strength and fast temperature response, along the longitudinal CF direction, the GCF/EP exhibited excellent deicing performance, including a shorter time and larger energy efficiency. Furthermore, the self-repairing ability of the GCF/EP and its effect on the deicing performance of the composite were characterized. Studying the Joule heating effect of GCF/EP composite laminates and their corresponding deicing performance lays the foundation for their design and practical application in icy environments. Full article

This study addresses the lack of comprehensive understanding regarding how both structural printing parameters and environmental factors influence the mechanical properties of additively manufactured polymer and composite materials. The main problem stems from insufficient data on the combined effects of infill density, number of perimeters, layer height, and exposure to cooling lubricants on the tensile performance of 3D-printed products, which is crucial for their reliable application in demanding environments. In this research, the influence of four critical parameters—infill density, number of perimeters, layer height, and exposure to cooling lubricants—on the tensile properties of specimens produced by fused filament fabrication (FFF), also known as fused deposition modeling (FDM), from polylactic acid (PLA) and polylactic acid reinforced with carbon fibers (PLA+CF) was investigated. Tensile tests were performed in accordance with ISO 527-2 on specimens printed with honeycomb infill structures under controlled process conditions. The results show that increasing infill density from 40% to 100% led to an approximately 60% increase in tensile strength for both PLA (from 30.75 MPa to 49.11 MPa) and PLA reinforced with carbon fibers (PLA+CF; from 17.75 MPa to 28.72 MPa). Similarly, increasing the number of perimeters from 1 to 3 resulted in a 51% improvement in tensile strength for PLA and 50% for PLA+CF. Reducing layer height from 0.40 mm to 0.20 mm improved tensile strength by 5.4% for PLA and 3.1% for PLA+CF, with more pronounced gains in stiffness observed in the composite material. Exposure to cooling lubricants led to mechanical degradation: after 30 days, PLA exhibited a 15.2% decrease in tensile strength and a 3.4% reduction in Young’s modulus, while PLA+CF showed an 18.6% decrease in strength and a 19.5% drop in modulus. These findings underscore the significant impact of both structural printing parameters and environmental exposure on tailoring the mechanical properties of FFF-printed materials, particularly when comparing unfilled PLA with carbon fiber-reinforced PLA. Full article