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Keywords = abrasive particle

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20 pages, 8312 KiB  
Article
Experimental Investigation of Magnetic Abrasive Finishing for Post-Processing Additive Manufactured Inconel 939 Parts
by Michał Marczak, Dorota A. Moszczyńska and Aleksander P. Wawrzyszcz
Appl. Sci. 2025, 15(15), 8233; https://doi.org/10.3390/app15158233 - 24 Jul 2025
Viewed by 191
Abstract
This study explores the efficacy of magnetic abrasive finishing (MAF) with planetary kinematics for post-processing Inconel 939 components fabricated by laser powder bed fusion (LPBF). Given the critical limitations in surface quality of LPBF-produced parts—especially in hard-to-machine superalloys like Inconel 939—there is a [...] Read more.
This study explores the efficacy of magnetic abrasive finishing (MAF) with planetary kinematics for post-processing Inconel 939 components fabricated by laser powder bed fusion (LPBF). Given the critical limitations in surface quality of LPBF-produced parts—especially in hard-to-machine superalloys like Inconel 939—there is a pressing need for advanced, adaptable finishing techniques that can operate effectively on complex geometries. This research focuses on optimizing the process parameters—eccentricity, rotational speed, and machining time—to enhance surface integrity following preliminary vibratory machining. Custom-designed samples underwent sequential machining, including heat treatment and 4 h vibratory machining, before MAF was applied under controlled conditions using ferromagnetic Fe-Si abrasives. Surface roughness measurements demonstrated a significant reduction, achieving Ra values from 1.21 µm to below 0.8 µm in optimal conditions, representing more than a fivefold improvement compared to the as-printed state (5.6 µm). Scanning Electron Microscopy (SEM) revealed progressive surface refinement, with MAF effectively removing adhered particles left by prior processing. Statistical analysis confirmed the dominant influence of eccentricity on the surface profile parameters, particularly Rz. The findings validate the viability of MAF as a precise, controllable, and complementary finishing method for LPBF-manufactured Inconel 939 components, especially for geometrically complex or hard-to-reach surfaces. Full article
(This article belongs to the Special Issue The Applications of Laser-Based Manufacturing for Material Science)
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14 pages, 5155 KiB  
Article
Erosion of AISI 4340 and AISI 8620 Steels with High Ductility Caused by SiC Particles
by Juan R. Laguna-Camacho, Ezequiel A. Gallardo-Hernández, Manuel Vite-Torres, Celia M. Calderón-Ramón, Víctor Velázquez-Martínez, Silvia M. Sánchez-Yáñez and Karla I. Zermeño-De Lojo
Metals 2025, 15(7), 800; https://doi.org/10.3390/met15070800 - 16 Jul 2025
Viewed by 210
Abstract
In this study, solid particle erosion tests were conducted to evaluate the resistance of AISI 4340 (EN24) and 8620 alloy steels against silicon carbide (SiC). These steels were selected due to their high hardness, yield strength (σy), ultimate tensile strength (σ [...] Read more.
In this study, solid particle erosion tests were conducted to evaluate the resistance of AISI 4340 (EN24) and 8620 alloy steels against silicon carbide (SiC). These steels were selected due to their high hardness, yield strength (σy), ultimate tensile strength (σuts) and elongation (%), which are significant parameters, influencing wear resistance. An erosion rig based on the ASTM G76-95 standard was used to perform the testing. Tests were carried out using different impact angles, 30°, 45°, 60° and 90°, with a particle velocity of 24 ± 2 m/s. The abrasive flow rate was 0.7 ± 0.5 g/min and the temperature was between 35 °C and 40 °C. Characterization techniques such as SEM were employed to identify the chemical composition of AISI 4340 and AISI 8620 steels and optical microscopy to determine the morphology of SiC abrasive particles. In addition, the SiC particle size was between 350 and 450 µm; it was determined by the particle size distribution technique. SEM micrographs were obtained to classify the wear mechanisms, characterized by micro-cutting, micro-ploughing, grooves, pitting actions and embedded particles on the surface at 30° and 90°. The results showed that AISI 8620 steel exhibited higher erosion resistance than AISI 4340 steel. Finally, AFM was used to evaluate the roughness variations before and after erosion tests, specifically in the central zone of the wear scars at 30° and 90° for both materials. Full article
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24 pages, 5956 KiB  
Article
Effects of Different Surface Treatments and Accelerated Aging on Dental Zirconia—An In Vitro Study
by Mihaela Pantea, Lucian Toma Ciocan, Vlad Gabriel Vasilescu, Georgeta Voicu, Adrian-Ionut Nicoară, Florin Miculescu, Robert Ciocoiu, Ana Maria Cristina Țâncu, Elena Georgiana Banu and Marina Imre
J. Funct. Biomater. 2025, 16(7), 263; https://doi.org/10.3390/jfb16070263 - 16 Jul 2025
Viewed by 501
Abstract
This in vitro study aimed to compare the effects of various surface treatments and hydrothermal aging on the phase composition, microstructure, and compressive strength of dental zirconia (ZrO2). Forty-eight zirconia cubes (8 × 8 × 8 mm) were fabricated using CAD/CAM [...] Read more.
This in vitro study aimed to compare the effects of various surface treatments and hydrothermal aging on the phase composition, microstructure, and compressive strength of dental zirconia (ZrO2). Forty-eight zirconia cubes (8 × 8 × 8 mm) were fabricated using CAD/CAM from two materials: infrastructure zirconia (Group S1) and super-translucent multilayered monolithic zirconia (Group S2). Four samples of each material were analyzed in their pre-sintered state (S1-0, S2-0). The remaining specimens were sintered and assigned to sub-groups based on surface treatment: untreated, sandblasted with 30 µm or 50 µm Al2O3, polished, or polished and glazed. Characterization was performed using EDX, SEM, XRD with Rietveld refinement, Raman spectroscopy, and compressive testing before and after accelerated hydrothermal aging, according to EN ISO 13356:2015. EDX revealed a higher yttria content in monolithic zirconia (10.57 wt%) than in infrastructure zirconia (6.51 wt%). SEM images showed minimal changes in polished samples but clear surface damage after sandblasting, which was more pronounced with larger abrasive particles. XRD and Raman confirmed that sandblasting promoted the tetragonal (t-ZrO2) to monoclinic (m-ZrO2) phase transformation (t→m), amplified further by hydrothermal aging. The polished groups showed greater phase stability post-aging. Compressive strength decreased in all treated and aged samples, with monolithic zirconia being more affected. Polished samples displayed the best surface quality and structural resilience across both materials. These findings underline the impact of clinical surface treatments on zirconia’s long-term mechanical and structural behavior. Full article
(This article belongs to the Special Issue New Trends in Biomaterials and Implants for Dentistry (2nd Edition))
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25 pages, 1049 KiB  
Review
The Occurrence and Removal of Microplastics from Stormwater Using Green Infrastructure
by Anna Kwarciak-Kozłowska and Magdalena Madeła
Water 2025, 17(14), 2089; https://doi.org/10.3390/w17142089 - 13 Jul 2025
Viewed by 619
Abstract
Microplastics (MPs) are becoming an increasingly common pollutant in the aquatic environment, including stormwater. This is a serious problem, as stormwater is becoming an essential transport route for MPs from urban areas to surface waters. Rainwater flowing from roofs, roads, and other impermeable [...] Read more.
Microplastics (MPs) are becoming an increasingly common pollutant in the aquatic environment, including stormwater. This is a serious problem, as stormwater is becoming an essential transport route for MPs from urban areas to surface waters. Rainwater flowing from roofs, roads, and other impermeable surfaces contains a variety of plastic particles originating from tire abrasion or waste disposal. This article presents an overview of current research on the occurrence of MPs in stormwater. The potential of selected green infrastructure solutions—particularly bioretention systems, constructed wetlands, and permeable pavements—for their reduction is assessed. Individual solutions present how the change in filter material, selection of vegetation, or the method of conducting the process (e.g., direction of stormwater flow in constructed wetlands) affects their effectiveness. The potential of green infrastructure is also compared with the traditional gray solution of sewage management in cities. This article emphasizes the importance of integrating such solutions in spatial planning as an effective tool to combat climate change and limit the spread of microplastics in the environment. Full article
(This article belongs to the Special Issue Novel Methods in Wastewater and Stormwater Treatment)
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12 pages, 2590 KiB  
Article
Summer Cafe: In Vitro Case Study of Biological Repellents Against the Large Pine Weevil
by Ilze Matisone, Kristaps Ozoliņš, Roberts Matisons, Mārtiņš Spāde, Uldis Grīnfelds and Rinalds Trukšs
Forests 2025, 16(7), 1139; https://doi.org/10.3390/f16071139 - 10 Jul 2025
Viewed by 193
Abstract
Growing environmental concerns have led to the search for alternative biological repellents against the large pine weevil Hylobius abietis L., Europe’s most important coniferous forest regeneration pest. A laboratory study was carried out to assess the effectiveness (damage intensity) of six combinations of [...] Read more.
Growing environmental concerns have led to the search for alternative biological repellents against the large pine weevil Hylobius abietis L., Europe’s most important coniferous forest regeneration pest. A laboratory study was carried out to assess the effectiveness (damage intensity) of six combinations of a novel biological repellent, consisting of plant-based oils, beeswax, calcium carbonate, vanillin, pine bark extractives, terpentine, abrasive particles, solvent, and a viscosity agent, in comparison with commercially available repellent Norfort LDW 115. The application complexity of the repellents, their persistence on seedlings, and the extent of H. abietis damage were evaluated. The five alternative repellents had higher protection compared to the control repellent, highlighting the potential for new alternative repellents. The base (without additives) repellent provided the highest protection, indicating a redundancy of admixtures. A mixed cumulative link model, employed to estimate differences between the repellents, estimated 85% undamaged and none significantly damaged saplings in the case of the base repellent. However, the consistency and hence persistence of certain repellents on plantlets would benefit from improvements; further field studies are needed to upscale the test of the stability and efficiency of high levels in real environments under different H. abietis population pressures. Full article
(This article belongs to the Section Forest Health)
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12 pages, 24352 KiB  
Article
Improving the Wear Properties of Ni Matrix Composites Containing High-Speed Steel Particles
by Marek Konieczny
Metals 2025, 15(7), 772; https://doi.org/10.3390/met15070772 - 8 Jul 2025
Viewed by 221
Abstract
Nickel matrix composites reinforced with T15 high-speed steel (HSS) were prepared using powder metallurgy techniques. A systematic investigation was conducted into the effect of CeO2, MoS2, and graphite additives on the tribological properties of the composites. The results show [...] Read more.
Nickel matrix composites reinforced with T15 high-speed steel (HSS) were prepared using powder metallurgy techniques. A systematic investigation was conducted into the effect of CeO2, MoS2, and graphite additives on the tribological properties of the composites. The results show that when T15 HSS particles are added, nickel grains do not grow as much as they do in pure sintered nickel. It was also observed that the T15 HSS particles were diffusion-bonded to the nickel matrix after sintering. The highest relative density after sintering is obtained for composites containing graphite, but the maximum hardness of 243 HV can be achieved for composites containing 2% of CeO2, which is about 16% higher than that of the Ni-T15 HSS composite. The wear rate of Ni-T15 HSS composites reduces from 3.4782 × 10−7 cm3/N∙m to 2.0222 × 10−7 cm3/N∙m as the content of CeO2 rises from 0 wt.% to 2 wt.%. The wear mechanisms of composites with MoS2 or graphite are abrasive wear and adhesive wear. The introduction of CeO2 enhances the hardness of the investigated composites to the highest degree, leading to a change in the wear mechanism of the composites to slight abrasive wear. The addition of CeO2 can effectively optimize the tribological properties of Ni-T15 HSS composites. Full article
(This article belongs to the Section Metal Matrix Composites)
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15 pages, 10114 KiB  
Article
Effect of Grain Size and Incidence Angle on Erosive Wear of Polyurea Coating
by Justyna Sokolska and Piotr Sokolski
Appl. Sci. 2025, 15(13), 7568; https://doi.org/10.3390/app15137568 - 5 Jul 2025
Viewed by 434
Abstract
This study investigated the erosive wear of a polyurea coating with a hardness of 95 ShA and a thickness of 3 mm applied to a 3 mm thick plate made of S235 steel. The process of erosive wear was carried out using a [...] Read more.
This study investigated the erosive wear of a polyurea coating with a hardness of 95 ShA and a thickness of 3 mm applied to a 3 mm thick plate made of S235 steel. The process of erosive wear was carried out using a stream of compressed air containing abrasive grains of aluminum oxide (Al2O3). The erosive wear was studied using different incidence angles (45°, 60° and 90°) and erosive grain sizes. Thus, the effects of the incidence angle and erosive grain size on the erosive wear of the polyurea coating were analyzed. Erosive wear was determined as linear wear: the depth of the wear trace was measured using an optical profilometer. This study showed a non-linear correlation between erosive wear, incidence angle and erosive particle size. In addition, a qualitative study of the surface of the coating after a wear test was carried out using a scanning electron microscope, which made it possible to describe the mechanisms of erosive wear of the polyurea coating. Full article
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35 pages, 1062 KiB  
Review
Micro- and Nanoplastics in the Environment: Current State of Research, Sources of Origin, Health Risks, and Regulations—A Comprehensive Review
by Anna Kochanek, Katarzyna Grąz, Halina Potok, Anna Gronba-Chyła, Justyna Kwaśny, Iwona Wiewiórska, Józef Ciuła, Emilia Basta and Jacek Łapiński
Toxics 2025, 13(7), 564; https://doi.org/10.3390/toxics13070564 - 2 Jul 2025
Viewed by 1698
Abstract
Small-particle-produced goods, such as those used in industry, medicine, cosmetics, paints, abrasives, and plastic pellets or powders, are the main sources of microplastics. It is also possible to mention tire recycling granules here. Larger components break down in the environment to generate secondary [...] Read more.
Small-particle-produced goods, such as those used in industry, medicine, cosmetics, paints, abrasives, and plastic pellets or powders, are the main sources of microplastics. It is also possible to mention tire recycling granules here. Larger components break down in the environment to generate secondary microplastics. Microplastics, or particles smaller than 5 mm, and nanoplastics, or particles smaller than 1 μm, are the products of degradation and, in particular, disintegration processes that occur in nature as a result of several physical, chemical, and biological variables. Polypropylene, polyethylene, polyvinyl chloride (PVC), polystyrene, polyurethane, and polyethylene terephthalate (PET) are among the chemicals included in this contamination in decreasing order of quantity. Micro- and nanoplastics have been detected in the air, water, and soil, confirming their ubiquitous presence in natural environments. Their widespread distribution poses significant threats to human health, including oxidative stress, inflammation, cellular damage, and potential carcinogenic effects. The aim of this article is to review the current literature on the occurrence of micro- and nanoplastics in various environmental compartments and to analyze the associated health consequences. The article also discusses existing legal regulations and highlights the urgent need for intensified research into the toxicological mechanisms of microplastics and the development of more effective strategies for their mitigation. Full article
(This article belongs to the Section Emerging Contaminants)
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19 pages, 7042 KiB  
Article
Durability of Recycled Concrete Aggregate as a Pavement Base Material Including Drainage: A Laboratory and Simulation Study
by Syed Ashik Ali, Paul Cancino Arevalo, Musharraf Zaman, Royce W. Floyd, Zahid Hossain and Javier Rojas-Pochyla
Sustainability 2025, 17(13), 6050; https://doi.org/10.3390/su17136050 - 2 Jul 2025
Viewed by 309
Abstract
Recycled concrete aggregates (RCAs) have the potential to be used as a sustainable, cost-effective, and environmentally friendly material in pavement base construction. However, there is a lack of information on the durability, strength, and hydraulic properties of RCA. The primary purpose of this [...] Read more.
Recycled concrete aggregates (RCAs) have the potential to be used as a sustainable, cost-effective, and environmentally friendly material in pavement base construction. However, there is a lack of information on the durability, strength, and hydraulic properties of RCA. The primary purpose of this study was to evaluate the properties and performances of commonly available RCAs in Oklahoma as pavement bases through laboratory testing and AASHTOWare Pavement ME simulations. For this purpose, three RCAs (RCA-1, RCA-2, and RCA-3) and a virgin limestone aggregate (VLA-1) were collected from local sources. RCA-1 and RCA-3 were produced in the field by crushing the existing concrete pavement of Interstate 40 and US 69 sections, respectively. RCA-2 was produced by crushing concrete and rubble collected in a local recycling plant. Laboratory testing for this study included particle size distribution, wash loss, optimum moisture content and maximum dry density (OMC-MDD), Los Angeles (LA) abrasion, durability indices (Dc and Df), permeability (k), and resilient modulus (Mr). The properties of aggregates were compared and the service life (performance) of aggregate bases was studied through mechanistic analysis using the AASHTOWare Pavement ME design software (version 2.6, AASHTO, USA). The results indicated that the properties of RCAs can differ greatly based on the origin of the source materials and the methods used in their processing. Recycled aggregates from concrete pavements of interstate and state highways exhibited similar or improved performance as virgin aggregates. RCA produced in a recycling plant was found to show durability and strength issues due to the presence of inferior quality materials and contaminants. Also, the results indicated that the fine aggregate durability test is a useful tool for screening recycled aggregates to ensure quality during production and construction. Bottom-up fatigue cracking was identified as the most affected performance criterion for flexible pavements when using RCA as the base layer. The findings will help increase the use of RCA as pavement base to promote environmental sustainability. Full article
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20 pages, 5119 KiB  
Article
Research on Rotary Magnetorheological Finishing of the Inner Surface of Stainless Steel Slender Tubes
by Zhaoyang Luo, Chunya Wu, Ziyuan Jin, Bing Guo, Shengdong Gao, Kailei Luo, Huiyong Liu and Mingjun Chen
Micromachines 2025, 16(7), 763; https://doi.org/10.3390/mi16070763 - 29 Jun 2025
Viewed by 328
Abstract
316L stainless steel slender tubes with smooth inner surfaces play an important role in fields such as aerospace and medical testing. In order to solve the challenge of difficult machining of their inner surfaces, this paper introduces a novel rotary magnetorheological finishing (RMRF) [...] Read more.
316L stainless steel slender tubes with smooth inner surfaces play an important role in fields such as aerospace and medical testing. In order to solve the challenge of difficult machining of their inner surfaces, this paper introduces a novel rotary magnetorheological finishing (RMRF) method specifically designed for processing the inner surfaces of slender tubes. This method does not require frequent replacement of the polishing medium during the processing, which helps to simplify the processing technology. By combining the rotational motion of a magnetic field with the linear reciprocating movement of the workpiece, uniform material removal on the inner surfaces of 316L stainless steel tubes was achieved. Initially, a finite element model coupling the magnetic and flow fields was developed to investigate the flow behavior of the MPF under a rotating magnetic field, to examine the theoretical feasibility of the proposed polishing principle. Subsequently, experimental validation was performed using a custom-designed polishing apparatus. Through processing experiments, with surface quality designated as the index, the influences of key parameters such as the volume content and sizes of carbonyl iron particles and abrasive particles in the MPF were comprehensively evaluated, and the composition and ratio of the MPF were optimized. Based on the optimized formulation, the optimal processing time was established, reducing the inner surface roughness from an initial Sa of approximately 320 nm to 28 nm, and effectively eliminating the original defects. Full article
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19 pages, 2774 KiB  
Article
Numerical Modeling on the Damage Behavior of Concrete Subjected to Abrasive Waterjet Cutting
by Xueqin Hu, Chao Chen, Gang Wang and Jenisha Singh
Buildings 2025, 15(13), 2279; https://doi.org/10.3390/buildings15132279 - 28 Jun 2025
Viewed by 269
Abstract
Abrasive waterjet technology is a promising sustainable and green technology for cutting underground structures. Abrasive waterjet usage in demolition promotes sustainable and green construction practices by reduction of noise, dust, secondary waste, and disturbances to the surrounding infrastructure. In this study, a numerical [...] Read more.
Abrasive waterjet technology is a promising sustainable and green technology for cutting underground structures. Abrasive waterjet usage in demolition promotes sustainable and green construction practices by reduction of noise, dust, secondary waste, and disturbances to the surrounding infrastructure. In this study, a numerical framework based on a coupled Smoothed Particle Hydrodynamics (SPH)–Finite Element Method (FEM) algorithm incorporating the Riedel–Hiermaier–Thoma (RHT) constitutive model is proposed to investigate the damage mechanism of concrete subjected to abrasive waterjet. Numerical simulation results show a stratified damage observation in the concrete, consisting of a crushing zone (plastic damage), crack formation zone (plastic and brittle damage), and crack propagation zone (brittle damage). Furthermore, concrete undergoes plastic failure when the shear stress on an element exceeds 5 MPa. Brittle failure due to tensile stress occurs only when both the maximum principal stress (σ1) and the minimum principal stress (σ3) are greater than zero at the same time. The damage degree (χ) of the concrete is observed to increase with jet diameter, concentration of abrasive particles, and velocity of jet. A series of orthogonal tests are performed to analyze the influence of velocity of jet, concentration of abrasive particles, and jet diameter on the damage degree and impact depth (h). The parametric numerical studies indicates that jet diameter has the most significant influence on damage degree, followed by abrasive concentration and jet velocity, respectively, whereas the primary determinant of impact depth is the abrasive concentration followed by jet velocity and jet diameter. Based on the parametric analysis, two optimized abrasive waterjet configurations are proposed: one tailored for rock fragmentation in tunnel boring machine (TBM) operations; and another for cutting reinforced concrete piles in shield tunneling applications. These configurations aim to enhance the efficiency and sustainability of excavation and tunneling processes through improved material removal performance and reduced mechanical wear. Full article
(This article belongs to the Section Building Structures)
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18 pages, 4190 KiB  
Article
Intelligent Classification Method for Rail Defects in Magnetic Flux Leakage Testing Based on Feature Selection and Parameter Optimization
by Kailun Ji, Ping Wang and Yinliang Jia
Sensors 2025, 25(13), 3962; https://doi.org/10.3390/s25133962 - 26 Jun 2025
Viewed by 352
Abstract
This study addresses the critical challenge of insufficient classification accuracy for different defect signals in rail magnetic flux leakage (MFL) detection by proposing an enhanced intelligent classification framework based on particle swarm optimized radial basis function neural network (PSO-RBF). Three key innovations drive [...] Read more.
This study addresses the critical challenge of insufficient classification accuracy for different defect signals in rail magnetic flux leakage (MFL) detection by proposing an enhanced intelligent classification framework based on particle swarm optimized radial basis function neural network (PSO-RBF). Three key innovations drive this research: (1) A dynamic PSO algorithm incorporating adaptive learning factors and nonlinear inertia weight for precise RBF parameter optimization; (2) A hierarchical feature processing strategy combining mutual information selection with correlation-based dimensionality reduction; (3) Adaptive model architecture adjustment for small-sample scenarios. Experimental validation shows breakthrough performance: 87.5% accuracy on artificial defects (17.5% absolute improvement over conventional RBF), with macro-F1 = 0.817 and MCC = 0.733. For real-world limited samples (100 sets), adaptive optimization achieved 80% accuracy while boosting minority class (“spalling”) F1-score by 0.25 with 50% false alarm reduction. The optimized PSO-RBF demonstrates superior capability in extracting MFL signal patterns, particularly for discriminating abrasions, spalling, indentations, and shelling defects, setting a new benchmark for industrial rail inspection. Full article
(This article belongs to the Section Fault Diagnosis & Sensors)
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14 pages, 4228 KiB  
Article
A Simple Method to Prepare Superhydrophobic Surfaces Based on Bamboo Cellulose, and an Investigation of Surface Properties
by Yu Wang, Junting Li, JingHai Guo, Tiancheng Yuan and Yanjun Li
Coatings 2025, 15(7), 740; https://doi.org/10.3390/coatings15070740 - 20 Jun 2025
Viewed by 402
Abstract
The present work introduces a sustainable, low-carbon method to fabricate durable, non-toxic superhydrophobic surfaces using bamboo-derived cellulose. Uniform TEMPO-carboxylated cellulose particles (TOC-Ps), approximately 2 μm in diameter, were synthesized through thermal polymerization and spray drying. These particles, featuring a nano-scale convex structure formed [...] Read more.
The present work introduces a sustainable, low-carbon method to fabricate durable, non-toxic superhydrophobic surfaces using bamboo-derived cellulose. Uniform TEMPO-carboxylated cellulose particles (TOC-Ps), approximately 2 μm in diameter, were synthesized through thermal polymerization and spray drying. These particles, featuring a nano-scale convex structure formed by intertwined TOC nanofibers, were applied to substrates and modified with low-surface-energy materials to achieve superhydrophobicity. At an optimal TOC-P mass ratio of 6%, the surface displayed a water contact angle of 156.2° and a sliding angle of 7°. The coating maintained superhydrophobicity after extensive mechanical testing—120 cm of abrasion, 100 bending cycles, and continuous trampling—and exhibited robust chemical stability across harsh conditions, including subjection to high temperatures, UV irradiation, and corrosive solutions (pH 2–12). The hierarchical micro–nano structure was found to enhance both hydrophobicity and durability, offering an environmentally friendly alternative for self-cleaning surfaces, textiles, and building applications. Full article
(This article belongs to the Section Functional Polymer Coatings and Films)
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11 pages, 1353 KiB  
Article
Adhesion of 3D-Printed Versus Milled Resin Posts to Composite Resin Core Build-Up Material: Influence of Surface Treatments
by Khalid K. Alanazi, Ali Robaian Alqahtani, Abdullah Mohammed Alshehri, Abdullah Ali Alqahtani, Abdulellah Almudahi, Omar Abdulaziz Al-Mansour, Nawaf Abdullah Al-Harbi, Sultan Sahman Abdulrahman Alqahtani, Eman Mohamed Raffat Hussein and Tarek Ahmed Soliman
Polymers 2025, 17(12), 1711; https://doi.org/10.3390/polym17121711 - 19 Jun 2025
Viewed by 458
Abstract
Background: There are very few studies in literature concerning the bonding between 3D-printed resin posts and the core build-up material. This study aimed to evaluate and compare the adhesion of 3D-printed and milled resin posts to composite resin core build-up material following different [...] Read more.
Background: There are very few studies in literature concerning the bonding between 3D-printed resin posts and the core build-up material. This study aimed to evaluate and compare the adhesion of 3D-printed and milled resin posts to composite resin core build-up material following different surface treatments. Methods: Three types of resin posts were utilized in this study: ready-made glass-reinforced fiber post (3M ESPE, Germany), milled PEEK POST (Bredent, Germany), and 3D-printed resin post (CROWNTEC, Saremco Dental AG, Switzerland). Each type of post was categorized into three groups based on surface treatments: C: untreated surfaces; SB: Air abrasion with 50 μm aluminum oxide particles was applied to the posts’ surfaces.; HO: the posts’ surfaces were immersed in 30% H2O2 for 5 min. A dual-cured composite resin (Grandio DC; VOCO) was utilized for core build-up in each group to evaluate adhesion through the push-out bond strength test. The modes of failure were analyzed, and the surface morphology of the post was characterized using SEM. Data were analyzed using a two-way analysis of variance (ANOVA) along with Tukey’s test. Results: The two-way ANOVA indicated a significant effect for surface treatment (F = 583.54, p < 001), post type (F = 79.96, p < 0.001), and their interactions (F = 265.74, p < 0.001). Regarding 3D-printed resin post, 30% H2O2 for 5 min recorded the highest statistically significant bond strength value (13.11 ± 1.61) compared to other groups. Regarding the milled PEEK post, the air particle abrasion recorded the highest statistically significant value (23.88 ± 1.66) compared to other groups. Adhesive failure was the predominant failure type, with an occurrence rate of 70.35%. Mixed failure was noted in 24.07% of the cases, with a significant prevalence in the PEEK post within the air particle abrasion group (58.3%). Cohesive failure was noted in 5.54% of cases, with a significant prevalence in the air particle abrasion group, occurring at rates of 16.6% in the resin fiber post group and 33.3% in PEEK posts. Conclusions: Air particle abrasion significantly improved the push-out bond strength of milled PEEK posts, but it did not have a similar effect on the 3D-printed resin posts. The application of 30% H2O2 for 5 min to 3D-printed resin post enhanced the adhesion to core build-up material. The manufacturing method of posts, the surface treatments utilized, and their interactions affect the interfacial bond strength between posts and the composite resin core build-up material. Full article
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15 pages, 4313 KiB  
Article
Fabrication of EP@PDMS@F-SiO2 Superhydrophobic Composite Coating on Titanium Alloy Substrate
by Chaoming Huang, Jinhe Qi, Jie Li, Xinchi Li, Jiawei Chen, Shuo Fu and Yanning Lu
Biomimetics 2025, 10(6), 404; https://doi.org/10.3390/biomimetics10060404 - 16 Jun 2025
Cited by 1 | Viewed by 496
Abstract
In this study, a preparation method of superhydrophobic composite coating based on a titanium alloy (Ti-6Al-4V) substrate is proposed. The micro-scale pit array structure was fabricated via laser etching technology. Utilizing the synergistic effects of epoxy resin (EP), polydimethylsiloxane (PDMS), and fluorinated nanosilica [...] Read more.
In this study, a preparation method of superhydrophobic composite coating based on a titanium alloy (Ti-6Al-4V) substrate is proposed. The micro-scale pit array structure was fabricated via laser etching technology. Utilizing the synergistic effects of epoxy resin (EP), polydimethylsiloxane (PDMS), and fluorinated nanosilica (F-SiO2), we successfully prepared an EP@PDMS@F-SiO2 composite coating. The effects of the contents of EP, PDMS, and F-SiO2 on the surface wettability, mechanical stability, and UV durability were studied by optimizing the coating ratio through orthogonal experiments. The results show that the micro–nano composite structure formed by laser etching can effectively fix the coating particles and provide excellent superhydrophobicity on the surface. The coating retains high hydrophobicity after paper abrasion (1000 cm under a 200 g load), demonstrating the mechanical stability of the armor-like structure, High-content F-SiO2 coatings exhibit greater UV durability. In addition, the coating surface has low droplet adhesion and self-cleaning capabilities for efficient contaminant removal. The research provides theoretical and technical support for the design and engineering application of a non-fluorinated, environmentally friendly superhydrophobic coating. Full article
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