Electron Beam Treatment Technology in Metals

In this study, we present the results of Young’s modulus and coefficient of friction (COF) of Ti–Ta surface alloys formed by electron-beam surface alloying by a scanning electron beam. Ta films were deposited on the top of Ti substrates, and the specimens were then electron-beam surface alloyed, where the beam power was varied from 750 to 1750 W. The structure of the samples was characterized by scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDX), and X-ray diffraction (XRD). Young’s modulus was studied by a nanoindentation test. The coefficient of friction was studied by a micromechanical wear experiment. It was found that at 750 W, the Ta film remained undissolved on the top of the Ti, and no alloyed zone was observed. By an increase in the beam power to 1250 and 1750 W, a distinguished alloyed zone is formed, where it is much thicker in the case of 1750 W. The structure of the obtained surface alloys is in the form of double-phase α’and β. In both surface alloys formed by a beam power of 1250 and 1750 W, respectively, Young’s modulus decreases about two times due to different reasons: in the case of alloying by 1250 W, the observed drop is attributed to the larger amount of the β phase, while at 1750 W is it due to the weaker binding forces between the atoms. The results obtained for the COF show that the formation of the Ti–Ta surface alloy on the top of Ti substrate leads to a decrease in the coefficient of friction, where the effect is more pronounced in the case of the formation of Ti–Ta surface alloys by a beam power of 1250 W. Full article

Increasing the service life of die casting dies is an important goal of the foundry industry. Approaches are either material- or process-related. Despite new material concepts, hot work steels such as H11 are still predominantly used in the uncoated condition for die casting dies. In order to withstand the stresses that occur, this steel is used exclusively in the quenched and tempered condition. Required properties such as high high-temperature strength and high hardness combined with high toughness are, in principle, contradictory and can only be adjusted consistently over the entire die by furnace-based heat treatment. However, the results of various investigations have shown that improvements in the thermal shock resistance and wear resistance of hot work tool steels can be achieved by thermally influencing the microstructure near the surface. Based on these studies and related findings, an approach to surface heat treatment using the electron beam was developed. Due to the particle character of the radiation and the associated possibility of high-frequency beam deflection, the electron beam offers significantly greater flexibility in energy input into the workpiece surface compared with lasers or induction. The overall technological concept envisages replacing furnace-based heat treatment in the production of casting dies by localized and demand-oriented boundary layer heat treatment with the electron beam. The experiments include, on the one hand, the experimental determination of a suitable temperature–time interval with a focus on short-term austenitization. On the other hand, a simulation-based approach of boundary layer heat treatment with validation of a suitable heat source is investigated. Regarding short-term austenitization, the corresponding temperature and time range could be narrowed down more precisely. Some of these parameter combinations seem to be very suitable for practical use. The test specimens show a hard surface layer with a depth of at least up to 6 mm and a very tough buffer layer. Numerical simulation is used to estimate the resulting metallurgical microstructure and the achievable hardness as a function of the temperature–time interval. In addition, the results provided show the possibility of determining and optimizing the material properties by means of a simulation-based approach within the framework of a purely digital process planning and subsequently transferring them into a process planning. In the technical implementation, a temperature control was first established by means of a two-color pyrometer. In the further course of research, the pyrometer will be supplemented by an internally installed infrared camera, which will allow the reproducible setting of specified temperature profiles even for complex, large-area contours in the future. Full article

The reported study discusses the formation of micro- and nanocrystalline surface layers in alloys on the example of Ti-Y and Al-Si-Y systems irradiated by electron beams. The study has established a crystallization mechanism of molten layers in the micro-and nanodimensional range, which involves a variety of hydrodynamic instabilities developing on the plasma–melt interface. As suggested, micro- and nanostructures form due to the combination of thermocapillary, concentration and capillary, evaporation and capillary and thermoelectric instabilities. This mechanism has provided the foundation for a mathematical model to describe the development of structures in focus in the electron beam irradiation. The study has pointed out that thermoelectric field strength E ≥ 10⁶ V/m is attributed to the occurring combination of instabilities in micro- and nanodimensional ranges. A full dispersion equation of perturbations on the melt surface was analyzed. Full article

The machining of the electron beam melting (EBM) produced parts is a challenging task because, upon machining, different part orientations (EBM layers’ orientations) produce different surface quality even when the same machining parameters are employed. In this paper, the EBM fabricated parts are machined in three possible orientations with regard to the tool feed direction, where the three orientations are “tool movement in a layer plane” (TILP), “tool movement perpendicular to layer planes” (TLP), and “tool movement parallel to layers planes” (TPLP). The influence of the feed rate, radial depth of cut, and cutting speed is studied on surface roughness, cutting force, micro-hardness, microstructure, chip morphology, and surface morphology of Ti6Al4V, while considering the EBM part orientations. It was found that different orientations have different effects on the machined surface during milling. The results show that the EBM parts can achieve good surface quality and surface integrity when milled along the TLP orientation. For instance, surface roughness (Sa) can be improved up to 29% when the milling tool is fed along the TLP orientation compared to the other orientations (TILP and TPLP). Furthermore, surface morphology significantly improves with lower micro-pits, redeposited chips, and feed marks in case of the TLP orientation. Full article

During the last decades, electron-beam treatment technologies (EBTT) have been widely used for surface modification of metals and alloys. The EBT methods are known as accurate and efficient. They have many advantages in comparison with the conventional techniques, such as very short technological process time, uniform distribution of the energy of the electron beam, which allows a precise control of the beam parameters and formed structure and properties of the materials, etc. Moreover, electron-beam treatment technologies are a part of the additive techniques, which are known as modern methods for manufacturing of new materials with unique functional properties. Currently, modern trends in the surface treatment of metals and alloys are based on the combination of electron-beam technologies with other methods, such as thin film deposition, plasma nitriding, etc. This approach results in a significant improvement in the surface properties of the materials which opens new potential applications and can involve them into new industrial fields. This paper aims to summarize the topics related to the manufacturing and surface treatment of metals and alloys by means of electron-beam technologies. Based on a literature review, the development and growth of EBT are considered in details. The benefits of these technologies—as well as their combination with other methods—are extensively discussed. Full article