Topic Editors

Institute of Machine Design, Faculty of Mechanical Engineering, Poznan University of Technology, Piotrowo 3, 60-965 Poznań, Poland
Faculty of Mechanical Engineering, Poznan University of Technology, 60-965 Poznan, Poland
INSA Centre Val de Loire, Université d’Orléans, PRISME EA4229, Bourges, France

Processing, Analysis, Modelling and Mechanics of Materials and Structures

Abstract submission deadline
closed (20 October 2022)
Manuscript submission deadline
closed (20 December 2022)
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Topic Information

Dear Colleagues,

This collection of articles includes original research articles, review articles and short memos covering the topic of the processing, analysis, modelling and mechanics of materials and structures. The main focus of the contributed papers may be either on material machining or forming processes, or on the design of machines that enable such processes. The combined approach, which helps to better understand the nature of the analysed process and its influence on the machine design, is highly desirable, but not required. Additionally, in order to follow modern needs and trends in technological development, research papers related to mechatronics and bioengineering are encouraged. Due to the variety of engineering materials, forming and machining methods and structures of mechanisms and machines used nowadays, this topic covers a wide range of studies. We invite you to publish papers presenting the application of either analytical, numerical or experimental methods to solve scientific and engineering problems. We also encourage research papers describing calculations using the finite element method to simulate the behaviour of the processed materials or to perform the optimization process, to either find effective design of the machine or mechatronic device or to select effective mechanical properties.

Prof. Dr. Krzysztof Talaśka
Prof. Dr. Szymon Wojciechowski
Prof. Dr. Antoine Ferreira
Topic Editors

Keywords

  • material machining
  • forming processes
  • design of machine
  • mechatronics
  • bioengineering
  • biomaterials

Participating Journals

Journal Name Impact Factor CiteScore Launched Year First Decision (median) APC
Materials
materials
3.4 5.2 2008 13.9 Days CHF 2600
Metals
metals
2.9 4.4 2011 15 Days CHF 2600
Processes
processes
3.5 4.7 2013 13.7 Days CHF 2400
Applied Sciences
applsci
2.7 4.5 2011 16.9 Days CHF 2400
Infrastructures
infrastructures
2.6 4.3 2016 16.9 Days CHF 1800

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Published Papers (135 papers)

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15 pages, 9322 KiB  
Article
Acoustic Emission Characterization Analysis of Quasi-Static and Fatigue Compression Properties of Aluminum Foam
by Qiong Song, Jian Shi and Xu Chen
Processes 2023, 11(4), 998; https://doi.org/10.3390/pr11040998 - 24 Mar 2023
Cited by 1 | Viewed by 1180
Abstract
In order to explore the evolution of physical and mechanical properties and acoustic emission (AE) characteristics of aluminum foam under fatigue and quasi-static compression from a microscopic point of view, the AE monitoring technology was used to analyze the deformation, hardening, and energy [...] Read more.
In order to explore the evolution of physical and mechanical properties and acoustic emission (AE) characteristics of aluminum foam under fatigue and quasi-static compression from a microscopic point of view, the AE monitoring technology was used to analyze the deformation, hardening, and energy absorption characteristics of open-cell aluminum foam under quasi-static compression at different rates (2, 10 and 50 mm/min) and fatigue loading tests with different peak stress ratios k (k = maximum stress/yield stress) by means of MTS fatigue testing machine and CCD camera. The results indicated that under different compression rates, the AE ring down count had the same trend as the engineering stress–strain response of the specimens, the AE ring down count rate at the plastic deformation stage showed the same performance as the work hardening rate, and the AE energy absorption efficiency corresponded well to the experimental results. The specimen entered the densification stage with the stability of AE count and the decrease in energy absorption efficiency. During the fatigue tests of different k values, the change trend of strain was consistent with the response of acoustic emission characteristic parameters, and the fatigue compression damage caused by the deformation process of the specimen can be monitored by the change in AE characteristics. The AE characteristics can dynamically monitor the compression process and provide a new research method and idea for the study of mechanical properties of aluminum foam. Full article
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14 pages, 15510 KiB  
Article
Effect of Femtosecond Laser Processing Parameters on the Ablation Microgrooves of RB-SiC Composites
by Feng Yang, Renke Kang, Hongbin Ma, Guangyi Ma, Dongjiang Wu and Zhigang Dong
Materials 2023, 16(6), 2536; https://doi.org/10.3390/ma16062536 - 22 Mar 2023
Cited by 1 | Viewed by 1271
Abstract
Because of the high hardness, brittleness, and anisotropy of reaction-bonded silicon carbide composites (RB-SiC), it is challenging to process high-quality textures on their surfaces. With the advantages of high processing accuracy and low processing damage, femtosecond laser processing is the preferred technology for [...] Read more.
Because of the high hardness, brittleness, and anisotropy of reaction-bonded silicon carbide composites (RB-SiC), it is challenging to process high-quality textures on their surfaces. With the advantages of high processing accuracy and low processing damage, femtosecond laser processing is the preferred technology for the precision processing of difficult-to-process materials. The present work used a femtosecond laser with a linear scanning path and a spot diameter of 18 µm to process microgrooves on RB-SiC. The influence of different processing parameters on the microgroove profile, dimensions, and ablation rate (AR) was investigated. The ablation width Wa and average ablation depth Da of microgrooves were evaluated, and the various patterns of varying processing parameters were obtained. A model for Wa prediction was developed based on the laser fluence within the finite length (FL). As a result, the experimental values were distributed near the prediction curve with a maximum error of 20.4%, showing an upward trend of gradually decreasing increments. For a single pass, the AR value was mainly determined by the laser energy, which could reach the scale of 106 μm3/s when the laser energy was greater than 50 μJ. For multiple passes, the AR value decreased as the number of passes increased and it finally stabilized. The above research will provide theoretical and experimental support for the high-quality and efficient processing of RB-SiC surface textures. Full article
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26 pages, 10114 KiB  
Article
Correlation between Orientation Spread and Ear Forming of As-Annealed AA5151 Aluminum Alloy
by Shih-Chieh Hsiao, Chia-Yu Li, Chih-I Chang, Tien-Yu Tseng, Yeong-Tsuen Pan and Jui-Chao Kuo
Materials 2023, 16(6), 2408; https://doi.org/10.3390/ma16062408 - 17 Mar 2023
Viewed by 928
Abstract
In the present work, we take the influences of activated slip systems and the orientation spread into account to predict the cup height using analytical earing models and compare the predicted results with experimental results. The effect of boundary conditions of the various [...] Read more.
In the present work, we take the influences of activated slip systems and the orientation spread into account to predict the cup height using analytical earing models and compare the predicted results with experimental results. The effect of boundary conditions of the various stress states and the work hardening exponents are compared and discussed for profile of single crystals. A stress ratio of −0.3 and a hardening exponent of 0.3 are selected for the prediction of earing profiles. The combination of activation of the single slip systems and orientation spread provides the best prediction of deep-drawing profiles. With further consideration of the orientation spread, an increase in the total orientation leads to peak-broadening, i.e., broad and smooth ears. Furthermore, the difference of the height between the maximum and minimum value of cup profiles is reduced because of the orientation spread. The profile for C is found with single ear at 45°, while the other components individually reveal double ears at 35° and 50° for S, at 15° and 45° for B, at 0° and 90° for Cube, at 5° and 90° for r-Cube, and at 15° and 90° for G. Herein, simple analytical earing models are proposed to understand the effects of slip systems and the orientation spread. The deep-drawing profiles are predicted with six major texture components. Full article
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17 pages, 3565 KiB  
Article
Development of Combined Methods Using Non-Destructive Test Methods to Determine the In-Place Strength of High-Strength Concretes
by Tuba Demir, Muhammed Ulucan and Kürşat Esat Alyamaç
Processes 2023, 11(3), 673; https://doi.org/10.3390/pr11030673 - 23 Feb 2023
Cited by 6 | Viewed by 1474
Abstract
This study aims to develop combined methods with dual and triple use of different non-destructive test (NDT) methods and to examine the effectiveness of these methods. For this purpose, nine different high-strength concrete series were produced, and destructive and NDT methods were applied [...] Read more.
This study aims to develop combined methods with dual and triple use of different non-destructive test (NDT) methods and to examine the effectiveness of these methods. For this purpose, nine different high-strength concrete series were produced, and destructive and NDT methods were applied to these samples on the 3rd and 90th days. Surface hardness, ultrasonic pulse velocity, and penetration resistance were considered from NDT methods. Analyses were made on the response surface method using the NDT measurements and compressive strength values obtained, and four different mathematical models were developed. Models 1, 2, and 3 were designed with dual use of NDT methods, and model 4 was designed with triple use. The absolute relative deviation values for all the developed models’ early and final-age strengths were below 10%. It is of great importance to determine concrete quality with high accuracy and practicality, especially in places like Elazig, where there are thousands of newly constructed buildings since the Sivrice-Elazig earthquake, and rapid production is required. Therefore, it is thought that determining the strength values with high accuracy using the developed combined methods without damaging the building element will provide benefits in terms of time, labor, and cost. Full article
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14 pages, 2629 KiB  
Article
Three-Parameter P-S-N Curve Fitting Based on Improved Maximum Likelihood Estimation Method
by Xiufeng Tan, Qiang Li, Guanqin Wang and Kai Xie
Processes 2023, 11(2), 634; https://doi.org/10.3390/pr11020634 - 19 Feb 2023
Cited by 1 | Viewed by 1493
Abstract
The P-S-N curve is a vital tool for dealing with fatigue life analysis, and its fitting under the condition of small samples is always concerned. In the view that the three parameters of the P-S-N curve equation can better describe the relationship between [...] Read more.
The P-S-N curve is a vital tool for dealing with fatigue life analysis, and its fitting under the condition of small samples is always concerned. In the view that the three parameters of the P-S-N curve equation can better describe the relationship between stress and fatigue life in the middle- and long-life range, this paper proposes an improved maximum likelihood method (IMLM). The backward statistical inference method (BSIM) recently proposed has been proven to be a good solution to the two-parameter P-S-N curve fitting problem under the condition of small samples. Because of the addition of an unknown parameter, the problem exists in the search for the optimal solution to the three-parameter P-S-N curve fitting. Considering that the maximum likelihood estimation is a commonly used P-S-N curve fitting method, and the rationality of its search for the optimal solution is better than that of BSIM, a new method combining BSIM and the maximum likelihood estimation is proposed. In addition to the BSIM advantage of expanding the sample information, the IMLM also has the advantage of more reasonable optimal solution search criteria, which improves the disadvantage of BSIM in parameter search. Finally, through the simulation tests and the fatigue test, the P-S-N curve fitting was carried out by using the traditional group method (GM), BSIM, and IMLM, respectively. The results show that the IMLM has the highest fitting accuracy. A test arrangement method is proposed accordingly. Full article
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18 pages, 2167 KiB  
Article
Development of a Non-Integral Form of Coordination Number Equation Based on Pair Distribution Function and Gaussian Function
by Chunlong Wang, Xiumin Chen and Dongping Tao
Metals 2023, 13(2), 384; https://doi.org/10.3390/met13020384 - 13 Feb 2023
Cited by 3 | Viewed by 1047
Abstract
The coordination number (CN) is an important structure property of liquid metals. A simple yet extremely precise method for calculating CN is proposed, the classical CN methods are evaluated systematically, and the mathematical forms of the symmetry method are corrected. Using the Gaussian [...] Read more.
The coordination number (CN) is an important structure property of liquid metals. A simple yet extremely precise method for calculating CN is proposed, the classical CN methods are evaluated systematically, and the mathematical forms of the symmetry method are corrected. Using the Gaussian function construct, the first coordination shell of the pair distribution function (PDF), the right-hand side of the first peak of the pair distribution function is extrapolated, and the CN expression is simplified with a Gaussian function to obtain its non-integral form. The first coordination shell is used to explain the Tao coordination number model (Tao CN) and obtain a Modified Tao CN. The Gaussian function is combined with the Tao CN, obtaining the function expression for the peak with peak position. These are important for the structural research of liquid metals. The CN of 27 liquid metals is calculated by these methods. The average relative deviation of the Gaussian function extrapolation method is ±6.46%, of the Modified Tao CN is ± 18.51%; those of the four classical methods range from ±15% to ±42%. The Modified Tao CN and extrapolation methods to calculate CN are more accurate for calculating CN than the classical method; they are more suitable for use in quantitative applications of CN. The equations derived in this work can be applied to the problem of integration of distribution functions to obtain simple mathematical models. Full article
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12 pages, 4847 KiB  
Article
CAE Prediction for Compression Behavior in Multi-Stacked Packages with an EPS-Based Cushioning System: Modeling of Compression and Compressive Creep Behavior
by Jong Min Park, Gun Yeop Lee, Dong Hyun Kim and Hyun Mo Jung
Appl. Sci. 2023, 13(4), 2215; https://doi.org/10.3390/app13042215 - 09 Feb 2023
Viewed by 1035
Abstract
The compression and compressive creep behavior of target shipping containers, which are material properties based on finite element analysis, and the lifetime and load-sharing rate, were analyzed in this study to develop a computer-aided engineering prediction technology for predicting the multi-stage compression behavior [...] Read more.
The compression and compressive creep behavior of target shipping containers, which are material properties based on finite element analysis, and the lifetime and load-sharing rate, were analyzed in this study to develop a computer-aided engineering prediction technology for predicting the multi-stage compression behavior of three target packages with different logistics conditions. In the experiment performed in the study, the relative humidity levels were 50%, 70%, and 90%, with creep measurements performed for 12 h for a combination of three levels of applied load and relative humidity. Using the nonlinear model of the stress–strain and creep behavior of the target shipping container, the lifetime was analyzed by estimating the average creep rate of the target shipping container. The load-sharing rate for each logistics situation of the target packages was also analyzed. The reduction rate of the compression strength of the container with respect to the increase in relative humidity was greater in the ‘horizontal long’ container than in the ‘vertical long’ container. As the applied load increased, the rate of increase in the average creep rate increased, i.e., the higher the applied load, the larger the difference in the average creep rate with respect to the relative humidity. The lifetime estimated from the failure strain and average creep rate of the container gradually decreased as the applied load increased at all relative humidity levels. However, as the applied load increased, the difference with respect to the relative humidity tended to decrease. In the target packages used in this study, the ratio of the load-sharing rate between the shipping container and an expanded polystyrene cushioning material was determined to be 2%:98%, with most of the stacking load applied to the product through the cushioning material. Full article
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16 pages, 4874 KiB  
Article
Analysis and Test of Internal Blowing Anti-Tangle Bag-Breaking Device for Domestic Waste
by Mengyu Guo, Bin Hu and Xin Luo
Processes 2023, 11(2), 511; https://doi.org/10.3390/pr11020511 - 08 Feb 2023
Viewed by 1307
Abstract
The mechanized resource utilization of domestic waste is the development trend in the field of waste treatment. The difficulty of bag breaking and the easy entanglement of domestic waste are the factors restricting the mechanization of waste separation and recycling. In response to [...] Read more.
The mechanized resource utilization of domestic waste is the development trend in the field of waste treatment. The difficulty of bag breaking and the easy entanglement of domestic waste are the factors restricting the mechanization of waste separation and recycling. In response to the above problems, an internal blowing anti-tangle bag-breaking device for domestic waste was developed by combining the arc-type cutter and the internal flow field of the rotary. In addition, the motion trajectory of the cutters and the support rods were theoretically analyzed, as well as the force during the bag-breaking process of domestic waste. A three-factor, five-level orthogonal test was carried out to complete the regression ANOVA, and a relationship model was constructed between the test factors such as the cutting–support speed ratio, the center distance, the inlet flow rate and the response indicators such as the bag film length–perimeter ratio and bag film winding specific gravity. The key parameters and their significant interactions with the bag-breaking efficiency were analyzed to obtain the optimal combination of parameters for the device. Under the same conditions, the errors between the physical test and model predictions for the two response indicators were 5.46% and 7.90%, respectively, indicating that the verification test results were basically consistent with the model prediction results. Full article
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20 pages, 5111 KiB  
Article
Analysis of Cold Composite Sheet Rolling Considering Anisotropic Effect and Position-Dependent Friction Model
by Jiageng Liu, Jiang Wu, Qian Liu, Shuai Ji, Xinlu Zheng, Feng Wang and Jiang Wang
Metals 2023, 13(2), 259; https://doi.org/10.3390/met13020259 - 28 Jan 2023
Cited by 1 | Viewed by 981
Abstract
The large difference in mechanical properties and plastic deformation ability of each layer will have a great impact on the overall performance of a composite sheet prepared by cold-roll bonding. The effect of rolling and material variables on the stress distribution and bonding [...] Read more.
The large difference in mechanical properties and plastic deformation ability of each layer will have a great impact on the overall performance of a composite sheet prepared by cold-roll bonding. The effect of rolling and material variables on the stress distribution and bonding state in the rolling deformation zone should be studied. In this work, an accurate cold-rolling deformation model considering the anisotropic effect and position-dependent friction model is established using the slab method. Effects of different process and material variables are analyzed. Related experiments were performed on Ti-Al clads and calculation results from the deformation model were compared with the experimental results. This model can well predict the Ti/Al thickness ratio after rolling, and the smaller the initial aluminum strength, the more accurate the predicted value; the minimum error is within 1%. The deformation coordination between the titanium and aluminum layers becomes better with the increase in rolling reduction and initial aluminum strength. At 50% reduction, the deformation ratio of titanium and aluminum increases from 93.8% to 98.1%, which is consistent with the trend of the results calculated using this model. Full article
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16 pages, 4567 KiB  
Article
Gripping Prospective of Non-Shear Flows under High-Pressure Torsion
by Yan Beygelzimer, Yuri Estrin, Oleksandr Davydenko and Roman Kulagin
Materials 2023, 16(2), 823; https://doi.org/10.3390/ma16020823 - 14 Jan 2023
Cited by 6 | Viewed by 1115
Abstract
The article presents a theoretical study of the regimes of high-pressure torsion (HPT) for which slippage of the deforming material on the interfaces with anvils is possible. The approach taken is a generalisation of the currently accepted view of the HPT process. It [...] Read more.
The article presents a theoretical study of the regimes of high-pressure torsion (HPT) for which slippage of the deforming material on the interfaces with anvils is possible. The approach taken is a generalisation of the currently accepted view of the HPT process. It enables a rational explanation of its salient features and the effects observed experimentally. These include a lag in the rotation angle of the specimen behind that of the anvils, an outflow of the material from the deformation zone, enhancement in gripping the specimen with anvils with increasing axial pressure, etc. A generalised condition for gripping the specimen with anvils, providing a basis for an analytical investigation of the HPT deformation at a qualitative level, is established. The results of the analytical modelling are supported by finite-element calculations. It is shown that for friction stress below the shear stress of the specimen material (i.e., for the friction factor m < 1), plastic deformation is furnished by non-shear flows, which expands the range of possible process regimes. The potential of these flow modes is impressive, which is reflected in the second meaning of the word “gripping” in the title of the article. Non-shear flows manifest themselves in the spreading of the material over the anvil surfaces whose cessation signifies the end of deformation and the beginning of slippage of the specimen as a whole. The model shows that for m < 1 such a finale is inevitable at any axial pressure. It predicts, however, that the highest achievable strain is increased when the axial pressure is raised in the course of the HPT process. Unlimited deformation of the specimen is only possible for m = 1, when slippage of the deforming material relative to the anvils is suppressed. Full article
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20 pages, 6409 KiB  
Article
Transient Responses of Repeated Transverse Impacts on Beams
by Hui Wang, Shunyuan Mao, Xiaomao Wu and Huiling Zhang
Appl. Sci. 2023, 13(2), 1115; https://doi.org/10.3390/app13021115 - 13 Jan 2023
Viewed by 1096
Abstract
In this paper, the eigenfunction expansion method combined with local contact models are presented to analyze the repeated impact behaviors between the sphere and the beam. The simulations are verified with the experimental results of a simply-supported beam struck 91 times by a [...] Read more.
In this paper, the eigenfunction expansion method combined with local contact models are presented to analyze the repeated impact behaviors between the sphere and the beam. The simulations are verified with the experimental results of a simply-supported beam struck 91 times by a sphere. In order to clarify the validity of the eigenfunction expansion method to solve the repeated transverse impacts on beams, the simulation results of the spring-mass method are also compared with the experiments. It shows that with appropriate contact models, the eigenfunction expansion method can predict agreeable results with the experimental results, especially the impact behaviors (including the accumulated permanent indentation, the coefficient of restitution and the separation velocity of the sphere) representing energy dissipations, due to the consideration of structural vibrations, local impact behaviors, as well as the wave propagations. The comparisons between the eigenfunction expansion method and the spring-mass model show that the wave propagations are important for energy dissipations, which cannot be neglected in flexible structure impacts. The studies are important for the analysis of repeated impact response of beam structures. Full article
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21 pages, 3912 KiB  
Article
A Bi-Modulus Material Model for Bending Test on NHL3.5 Lime Mortar
by Rebecca Grazzini, Giulia Misseri and Luisa Rovero
Materials 2023, 16(2), 486; https://doi.org/10.3390/ma16020486 - 04 Jan 2023
Cited by 4 | Viewed by 1408
Abstract
The research provides an innovative contribution to the interpretation of three-point and four-point bending tests on mortars by employing a bi-modulus material model, which assumes an asymmetric constitutive law, i.e., different elastic moduli in tension and in compression. To this aim, Euler–Bernoulli and [...] Read more.
The research provides an innovative contribution to the interpretation of three-point and four-point bending tests on mortars by employing a bi-modulus material model, which assumes an asymmetric constitutive law, i.e., different elastic moduli in tension and in compression. To this aim, Euler–Bernoulli and Timoshenko bi-modulus beam models are defined, and the related displacement fields are reported for three-point loading, and provided for the first time for the four-point bending layout. A wide experimental campaign, including uni-axial tensile and compressive tests, three-point and four-point bending tests, and on notched specimens three-point tests for mode-I fracture energy, has been carried out on lime mortar specimens exploiting traditional contact (CE-DT) and contactless (DIC) measurement systems. Experimental results provided the values of tensile and compressive mechanical characteristics, which are employed to validate estimations of the analytical model. The tension-to-compression moduli ratio experimentally observed is on average 0.52. Experimental outcomes of the DIC analysis proved the bi-modulus behaviour during the four-point bending tests showing visible shifting of the neutral axis. The bi-modulus analytical model provides closer results to the experimental ones for the slender specimens subjected to four-point bending. Full article
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16 pages, 5339 KiB  
Article
Structural Design and Optimization of Separated Air-Rib Tents Based on Response Surface Methodology
by Ying Liu, Yi Ru, Feng Li, Lei Zheng, Jun Zhang, Xiaoyang Chen and Shengchao Liang
Appl. Sci. 2023, 13(1), 55; https://doi.org/10.3390/app13010055 - 21 Dec 2022
Cited by 2 | Viewed by 1323
Abstract
Air-rib tents are widely used because they are lightweight and site adaptable, but the large deformation of these tents reduces their effective space. It is important to reduce the displacement of the air-rib tent by parameter optimization. The influences of external factors on [...] Read more.
Air-rib tents are widely used because they are lightweight and site adaptable, but the large deformation of these tents reduces their effective space. It is important to reduce the displacement of the air-rib tent by parameter optimization. The influences of external factors on the tent are studied in this paper. Four parameters of the tent’s wind ropes are the angle of the wind ropes, the number of the wind ropes, and the initial prestress of the wind ropes on the side or end faces. The influence of the angle of the wind ropes and the number of the wind ropes on the displacement is larger than the other two parameters. The closer the wind ropes are to the center of the tarpaulin, the greater the displacement of the tent. Based on an analysis using response surface methodology, the optimal parameters are as follows: the angle of the wind ropes is 41°, the number of the wind ropes on the side is two, the initial prestress of the wind ropes on the end face is 800 Pa, and the initial prestress of the wind ropes on the side is 0 Pa. Under these optimal parameters, the maximum displacement decreases by 10.2%, and the maximum stress barely changes. Full article
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14 pages, 5418 KiB  
Article
Creep Simulation and Validation for a Finite Element Analysis of Expanded Polystyrene-Based Cushioning Systems
by Jong Min Park, Gun Yeop Lee, Dong Hyun Kim and Hyun Mo Jung
Appl. Sci. 2022, 12(24), 12663; https://doi.org/10.3390/app122412663 - 10 Dec 2022
Cited by 1 | Viewed by 1598
Abstract
The creep strain resistance of expanded polystyrene (EPS) is important; thus, time-dependent creep properties of EPS have been of significant interest. This study is a part of the computer-aided engineering (CAE) prediction-technology development for the inclination of unitized loads of packaged appliances applied [...] Read more.
The creep strain resistance of expanded polystyrene (EPS) is important; thus, time-dependent creep properties of EPS have been of significant interest. This study is a part of the computer-aided engineering (CAE) prediction-technology development for the inclination of unitized loads of packaged appliances applied to EPS-based cushioning systems. Creep properties are validated to ensure finite element analysis (FEA) reliability regarding the creep behavior of EPS-based cushioning systems. The elastic modulus and Poisson’s ratio (EPS elastic properties) as well as creep properties (plastic properties) were measured. The EPS density range was 16–30 kg/m3, and the temperature range was 0–60 °C. Because the measured mechanical properties were not temperature-dependent, only their density dependence was analyzed. The EPS behavior, measured over 12 h, exhibited a significant creep amount and rate, depending on the applied stress level. FEA was performed on 7-day-long EPS creep, using the measured EPS elastic and plastic properties. The FEA and experimental results were strongly concordant. These EPS creep validation results are expected to improve the reliability of FEA for creep behavior studies of EPS-based cushioning systems. Full article
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11 pages, 4447 KiB  
Article
Microstructure and Magnetic Properties Dependence on the Sputtering Power and Deposition Time of TbDyFe Thin Films Integrated on Single-Crystal Diamond Substrate
by Zhenfei Lv, Xiulin Shen, Jinxuan Guo, Yukun Cao, Chong Lan, Yanghui Ke, Yixian Yang and Junyi Qi
Processes 2022, 10(12), 2626; https://doi.org/10.3390/pr10122626 - 07 Dec 2022
Cited by 2 | Viewed by 1330
Abstract
As giant magnetostrictive material, TbDyFe is regarded as a promising choice for magnetic sensing due to its excellent sensitivity to changes in magnetic fields. To satisfy the requirements of high sensitivity and the stability of magnetic sensors, TbDyFe thin films were successfully deposited [...] Read more.
As giant magnetostrictive material, TbDyFe is regarded as a promising choice for magnetic sensing due to its excellent sensitivity to changes in magnetic fields. To satisfy the requirements of high sensitivity and the stability of magnetic sensors, TbDyFe thin films were successfully deposited on single-crystal diamond (SCD) substrate with a Young’s modulus over 1000 GPa and an ultra-stable performance by radio-frequency magnetron sputtering at room temperature. The sputtering power and deposition time effects of TbDyFe thin films on phase composition, microstructure, and magnetic properties were investigated. Amorphous TbDyFe thin films were achieved under various conditions of sputtering power and deposition time. TbDyFe films appeared as an obvious boundary to SCD substrate as sputtering power exceeded 100 W and deposition time exceeded 2 h, and the thickness of the films was basically linear with the sputtering power and deposition time based on a scanning electron microscope (SEM). The film roughness ranged from 0.15 nm to 0.35 nm, which was measured by an atomic force microscope (AFM). The TbDyFe film prepared under a sputtering power of 100 W and a deposition time of 3 h possessed the coercivity of 48 Oe and a remanence ratio of 0.53, with a giant magnetostriction and Young’s modulus effect, suggesting attractive magnetic sensitivity. The realization of TbDyFe/SCD magnetic material demonstrates a foreseeable potential in the application of high-performance sensors. Full article
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21 pages, 12028 KiB  
Article
Unlocking Novel Ultralow-Frequency Band Gap: Assembled Cellular Metabarrier for Broadband Wave Isolation
by Xiao Liang, Fang Zhang, Jinhui Jiang, Cang He and Hongji Yang
Materials 2022, 15(23), 8326; https://doi.org/10.3390/ma15238326 - 23 Nov 2022
Viewed by 1320
Abstract
Admittedly, the design requirements of compactness, low frequency, and broadband seem to constitute an impossible trinity, hindering the further development of elastic metamaterials (EMMs) in wave shielding engineering. To break through these constraints, we propose theoretical combinations of effective parameters for wave isolation [...] Read more.
Admittedly, the design requirements of compactness, low frequency, and broadband seem to constitute an impossible trinity, hindering the further development of elastic metamaterials (EMMs) in wave shielding engineering. To break through these constraints, we propose theoretical combinations of effective parameters for wave isolation based on the propagation properties of Lamb waves in the EMM layer. Accordingly, we design compact EMMs with a novel ultralow-frequency bandgap, and the role of auxeticity in the dissociation between the dipole mode and the toroidal dipole mode is clearly revealed. Finally, under the guidance of the improved gradient design, we integrate multiple bandgaps to assemble metamaterial barriers (MMBs) for broadband wave isolation. In particular, the original configuration is further optimized and its ultralow-frequency and broadband performance are proven by transmission tests. It is foreseeable that our work will provide a meaningful reference for the application of the new EMMs in disaster prevention and protection engineering. Full article
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20 pages, 13134 KiB  
Article
Study on the Work Hardening and Metamorphic Layer Characteristics of Milling Contour Bevel Gears
by Mingyang Wu, Jianyu Zhang, Chunjie Ma, Yali Zhang, Yaonan Cheng, Shi Wu and Lubin Li
Materials 2022, 15(22), 7975; https://doi.org/10.3390/ma15227975 - 11 Nov 2022
Cited by 1 | Viewed by 924
Abstract
High temperature and strain will occur in the cutting area during dry milling of contour bevel gears, which causes plastic deformation of the workpiece, resulting in changes in the physical properties of the machined surface’s metamorphic layer, reducing the quality of the workpiece’s [...] Read more.
High temperature and strain will occur in the cutting area during dry milling of contour bevel gears, which causes plastic deformation of the workpiece, resulting in changes in the physical properties of the machined surface’s metamorphic layer, reducing the quality of the workpiece’s machined surface. Therefore, it is necessary to investigate the properties of the metamorphic layer and the work hardening behavior of the machined surfaces of contour bevel gears. The paper first establishes a single-tooth finite element simulation model for a contour bevel gear and extracts the temperature field, strain field and strain rate at different depths from the machined surface. Then, based on the simulation results, the experiment of milling contour bevel gears is carried out, the microscopic properties of the machined metamorphic layer are studied using XRD diffractometer and ultra-deep field microscopy, and the work hardening behavior of the machined metamorphic layer under different cutting parameters is studied. Finally, the influence of the cutting parameters on the thickness of the metamorphic layer of the machined surface is investigated by scanning electron microscopy. The research results can not only improve the surface quality and machinability of the workpiece, but are also significant for increasing the fatigue strength of the workpiece. Full article
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13 pages, 5291 KiB  
Article
Influence of Si Content on the Microstructure and Tensile Properties of Weathering Bridge Steel Produced via Thermal Mechanical Control Process
by Zhenye Chen, Genhao Shi, Jianjun Qi, Liyang Zhao, Yanli Liu, Qingfeng Wang and Guodong Wang
Metals 2022, 12(11), 1901; https://doi.org/10.3390/met12111901 - 07 Nov 2022
Viewed by 1211
Abstract
In this study, the effects of Si on the microstructure and tensile properties of weathering bridge steel were elucidated. The thermal mechanical control process (TMCP), containing two stages of controlled rolling and accelerated cooling process, was simulated using a thermo-mechanical simulator for four [...] Read more.
In this study, the effects of Si on the microstructure and tensile properties of weathering bridge steel were elucidated. The thermal mechanical control process (TMCP), containing two stages of controlled rolling and accelerated cooling process, was simulated using a thermo-mechanical simulator for four experimental steels with varying Si contents (0.15–0.77 wt.%). Micro-tensile tests were performed, and the microstructures were observed via optical microscope (OM), scanning electron microscope (SEM), transmission electron microscope (TEM), and electron back-scattered diffraction (EBSD). Furthermore, the tensile properties and microstructures of these steels were analyzed. The results show that a mixed microstructure comprising granular bainitic ferrite (GBF), quasi-polygonal ferrite (QF), and martensite/austenite (M/A) constituent was formed in each sample. With an increase in Si content, the GBF content decreased, QF content increased, mean equivalent diameter (MED) of the QF+GBF matrix increased, and the fraction and average size of the M/A constituent increased. With a rise in Si content from 0.15 to 0.77 wt.%, the contributions of dislocation strengthening, grain boundary strengthening, and precipitation strengthening decreased from 149, 220, and 21 MPa to 126, 179, and 19 MPa, respectively. However, the combined contribution of solution strengthening, lattice strengthening, and M/A strengthening increased from 41 to 175 MPa, which augmented the final yield strength from 431 to 499 MPa. The decreasing yield ratio shows that strain hardening capacity is enhanced due to an increase in the fraction of the M/A constituent as well as in the MED of the QF+GBF matrix. Furthermore, the mechanisms by which Si content controls the microstructure and mechanical properties of weathering bridge steel were also discussed. Full article
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9 pages, 2296 KiB  
Article
Microbiologically Pure Cotton Fabrics Treated with Tetrabutylammonium OXONE as Mild Disinfection Agent
by Bogdan Bujnicki, Przemyslaw Sowinski, Tomasz Makowski, Dorota Krasowska, Patrycja Pokora-Sobczak, Inna Shkyliuk, Józef Drabowicz and Ewa Piorkowska
Materials 2022, 15(21), 7749; https://doi.org/10.3390/ma15217749 - 03 Nov 2022
Viewed by 1174
Abstract
The microbiological purity of textiles plays a pivotal role in the use of textiles, especially in hospitals and other medical facilities. Microbiological purity of cotton fabric was achieved by a new disinfection method using tetrabutyloammonium OXONE (TBA-OXONE) before washing. As a result of [...] Read more.
The microbiological purity of textiles plays a pivotal role in the use of textiles, especially in hospitals and other medical facilities. Microbiological purity of cotton fabric was achieved by a new disinfection method using tetrabutyloammonium OXONE (TBA-OXONE) before washing. As a result of the disinfection, the cotton fabric became microbiologically pure, despite the markedly decreased washing time with respect to the widely used standard procedure. Shortening of the washing time allowed for significant energy savings. In addition, the effect of the number of disinfection and washing cycles on the tensile properties and tearing force of the fabric was examined. After 120 disinfection and washing cycles the mechanical properties of cotton fabric were only slightly worsened. Full article
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13 pages, 4196 KiB  
Article
Advantageous Implications of Reversed Austenite for the Tensile Properties of Super 13Cr Martensitic Stainless Steel
by Peng Wang, Weiwei Zheng, Xinpan Yu and Yanli Wang
Materials 2022, 15(21), 7697; https://doi.org/10.3390/ma15217697 - 01 Nov 2022
Cited by 2 | Viewed by 1318
Abstract
The advantageous implications of the microstructure and volume fraction of reversed austenite for the tensile properties of super 13Cr martensitic stainless steel (13Cr SMSS) in an experiment with quenching and double-step tempering treatment in the temperature range of 550–750 °C were investigated. The [...] Read more.
The advantageous implications of the microstructure and volume fraction of reversed austenite for the tensile properties of super 13Cr martensitic stainless steel (13Cr SMSS) in an experiment with quenching and double-step tempering treatment in the temperature range of 550–750 °C were investigated. The results show that, with increases in one-step tempering temperature, the content of reversed austenite was enhanced considerably from 0.9% to 13.3%. The reversed austenite distributed in the martensitic lath boundary conformed to the (11¯1)γ//(011)α’ and [011]γ//[1¯1¯1]α’ Kurdjumov–Sachs orientation relationship with the matrix. When tempered at 675 °C for 3 h for the first stage and 600 °C for 2 h for the second stage, the maximum volume fraction of reversed austenite was approximately 13.3%, achieving uniform elongation of 10.4% and total elongation of 27.2%. Moreover, the product of strength and elongation (PSE) was 23.5 GPa·% higher than other samples. The outstanding combination of high strength and commendable plasticity was due to the phase transformation of the reversed austenite into secondary martensite during tensile straining. The reversed austenite consumed the plastic energy at the tip of the microcrack and made the crack tip blunt, which hindered the further propagation of the crack, consequently increasing the total elongation and improving toughness. Full article
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12 pages, 2401 KiB  
Article
Liquid-Ammonia-Mediated Dyeing Process of Wool at a Lower Temperature
by Xianqin Shang, Qiang Wang, Zhe Jiang, Haitao Ma and Denglu Zhang
Processes 2022, 10(11), 2172; https://doi.org/10.3390/pr10112172 - 24 Oct 2022
Viewed by 1934
Abstract
Liquid ammonia as a non-aqueous medium has many physical properties close to water, such as small molecular weight and strong permeability. It has been widely used for the ecological processing of cellulosic fibers to improve their luster, softness and dyeing properties. However, there [...] Read more.
Liquid ammonia as a non-aqueous medium has many physical properties close to water, such as small molecular weight and strong permeability. It has been widely used for the ecological processing of cellulosic fibers to improve their luster, softness and dyeing properties. However, there are few reports on the dyeing of wool treated with liquid ammonia, especially at a lower temperature. Herein, a continuous liquid ammonia finishing machine was used to batch process wool followed by dyeing in a commonly-used wool dyeing machine. The results showed that many scale flakes and some cuticle cracking were seen on the fiber surface, and the disulfide bonds of cystine were broken down after liquid ammonia treatment, which promoted the diffusion of dyestuff into the fiber. Moreover, the uptakes and K/S value of wool dyed with Lanaset and Lanasol CE dyes were higher than the untreated wool, and the dyeing temperature could decrease to 85 °C, while the degree of fiber strength reduction merely decreased by 3–5%. Furthermore, for the reactive dyes, the dyeing temperature can reduce to 70 °C with the chemical auxiliaries Miralan LTD, while the degree of strength reduction decrease by 8–10%. Liquid ammonia treatment can be used for dyeing at a lower temperature than boiling temperature (100 °C), reduce energy consumption and reduce the degree of fiber strength reduction of wool. The method shows considerable to great value and is significant in providing a feasible approach for the industrial application of low-temperature dyeing technology. Full article
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16 pages, 561 KiB  
Article
Real-Time Prediction Model of Carbon Content in RH Process
by Jeongheon Heo, Tae-Won Kim, Soon-Jong Jung and Soohee Han
Appl. Sci. 2022, 12(21), 10753; https://doi.org/10.3390/app122110753 - 24 Oct 2022
Viewed by 1208
Abstract
In the Ruhrstahl–Heraeus (RH) vacuum degassing process, we propose a real-time prediction model for the carbon content in molten steel, and show that the decarburization endpoint can be accurately determined using this model. Firstly, we applied a novel off-gas analyzer that can measure [...] Read more.
In the Ruhrstahl–Heraeus (RH) vacuum degassing process, we propose a real-time prediction model for the carbon content in molten steel, and show that the decarburization endpoint can be accurately determined using this model. Firstly, we applied a novel off-gas analyzer that can measure the carbon oxide concentration produced in the decarburization reaction faster and more accurately. Next, we generate decarburization curves using the off-gas components measured by the new analyzer. The decarburization curve describes the carbon content profile well during operation, and shows good agreement with the actual carbon content. In order to predict the carbon content during operation in real time, we create an artificial neural network (ANN) using the decarburization curves and operation data. By comparing the endpoint carbon content measured at the end of the operation with the predicted values, we confirmed the excellent predictive performance of the ANN model. Finally, we show that it is possible to accurately determine the decarburization endpoint using the prediction model. We expect that the proposed real-time prediction model can increase the productivity of the RH process. Full article
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37 pages, 3956 KiB  
Article
Use of Multiscale Data-Driven Surrogate Models for Flowsheet Simulation of an Industrial Zeolite Production Process
by Vasyl Skorych, Moritz Buchholz, Maksym Dosta, Helene Katharina Baust, Marco Gleiß, Johannes Haus, Dominik Weis, Simon Hammerich, Gregor Kiedorf, Norbert Asprion, Hermann Nirschl, Frank Kleine Jäger and Stefan Heinrich
Processes 2022, 10(10), 2140; https://doi.org/10.3390/pr10102140 - 20 Oct 2022
Cited by 4 | Viewed by 1947
Abstract
The production of catalysts such as zeolites is a complex multiscale and multi-step process. Various material properties, such as particle size or moisture content, as well as operating parameters—e.g., temperature or amount and composition of input material flows—significantly affect the outcome of each [...] Read more.
The production of catalysts such as zeolites is a complex multiscale and multi-step process. Various material properties, such as particle size or moisture content, as well as operating parameters—e.g., temperature or amount and composition of input material flows—significantly affect the outcome of each process step, and hence determine the properties of the final product. Therefore, the design and optimization of such processes is a complex task, which can be greatly facilitated with the help of numerical simulations. This contribution presents a modeling framework for the dynamic flowsheet simulation of a zeolite production sequence consisting of four stages: precipitation in a batch reactor; concentration and washing in a block of centrifuges; formation of droplets and drying in a spray dryer; and burning organic residues in a chain of rotary kilns. Various techniques and methods were used to develop the applied models. For the synthesis in the reactor, a multistage strategy was used, comprising discrete element method simulations, data-driven surrogate modeling, and population balance modeling. The concentration and washing stage consisted of several multicompartment decanter centrifuges alternating with water mixers. The drying is described by a co–current spray dryer model developed by applying a two-dimensional population balance approach. For the rotary kilns, a multi-compartment model was used, which describes the gas–solid reaction in the counter–current solids and gas flows. Full article
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29 pages, 11005 KiB  
Article
Numerical Simulation of the Elastic–Ideal Plastic Material Behavior of Short Fiber-Reinforced Composites Including Its Spatial Distribution with an Experimental Validation
by Natalie Rauter
Appl. Sci. 2022, 12(20), 10483; https://doi.org/10.3390/app122010483 - 17 Oct 2022
Cited by 2 | Viewed by 1617
Abstract
For the numerical simulation of components made of short fiber-reinforced composites, the correct prediction of the deformation including the elastic and plastic behavior and its spatial distribution is essential. When using purely deterministic modeling approaches, the information of the probabilistic microstructure is not [...] Read more.
For the numerical simulation of components made of short fiber-reinforced composites, the correct prediction of the deformation including the elastic and plastic behavior and its spatial distribution is essential. When using purely deterministic modeling approaches, the information of the probabilistic microstructure is not included in the simulation process. One possible approach for the integration of stochastic information is the use of random fields. In this study, numerical simulations of tensile test specimens were conducted utilizing a finite deformation elastic–ideal plastic material model. A selection of the material parameters covering the elastic and plastic domain are represented by cross-correlated second-order Gaussian random fields to incorporate the probabilistic nature of the material parameters. To validate the modeling approach, tensile tests until failure were carried out experimentally, which confirmed the assumption of the spatially distributed material behavior in both the elastic and plastic domain. Since the correlation lengths of the random fields cannot be determined by pure analytic treatments, additionally numerical simulations were performed for different values of the correlation length. The numerical simulations endorsed the influence of the correlation length on the overall behavior. For a correlation length of 5 mm, a good conformity with the experimental results was obtained. Therefore, it was concluded that the presented modeling approach was suitable to predict the elastic and plastic deformation of a set of tensile test specimens made of short fiber-reinforced composite sufficiently. Full article
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30 pages, 11616 KiB  
Article
Fatigue Performance Analysis of an Existing Orthotropic Steel Deck (OSD) Bridge
by Mattia Mairone, Rebecca Asso, Davide Masera, Stefano Invernizzi, Francesco Montagnoli and Alberto Carpinteri
Infrastructures 2022, 7(10), 135; https://doi.org/10.3390/infrastructures7100135 - 12 Oct 2022
Cited by 3 | Viewed by 2364
Abstract
Orthotropic steel deck (OSD) bridges are lightweight constructions which are convenient, especially for the achievement of long spans. Conversely, due to the stress concentration in correspondence to the numerous and unavoidable welded construction details, this bridge typology is prone to fatigue cracking under [...] Read more.
Orthotropic steel deck (OSD) bridges are lightweight constructions which are convenient, especially for the achievement of long spans. Conversely, due to the stress concentration in correspondence to the numerous and unavoidable welded construction details, this bridge typology is prone to fatigue cracking under the effect of cyclic loading with high-stress amplitudes. Existing OSD bridges are particularly vulnerable to fatigue damage accumulation because of the dated standards adopted at the time of their design and the fact that heavy lorries have increased in travel frequency and weight. In the present paper, a case study of a northern Italian existing highway viaduct, built in the 1990s, is presented and analyzed. The fatigue damage accumulation was carried out according to the fatigue load models for road bridges reported in Eurocode EN 1991-2 and the assessment criteria indicated in EN 1993-1-9. The stress amplitude, in correspondence to the critical details of the bridge, is assessed by means of detailed finite-element calculations carried out with the software MIDAS GEN®. The amplitude and frequency of the travelling weights are assessed based on real traffic monitoring from the highway. Moreover, an automatic “rain-flow” algorithm is implemented, which is able to detect each nominal stress variation above the fatigue limit. In general, the bridge is not fully compliant with today’s standards when considering the entire duration of the prescribed life of the design. Countermeasures, like lane number reductions and lane reshaping, are critically analyzed since their effectiveness is questionable as far as the reduction in heavy traffic is concerned. Other interventions, like the replacement of the pavement in order to improve the stress redistribution upon the connection details below the wheel footprint, and continuous bridge inspections or monitoring, look more promising. Full article
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13 pages, 2543 KiB  
Article
Study on the Solidification Mechanism of Cr in Ettringite and Friedel’s Salt
by Ke Wang, Dong Xu, Keqing Li and Wen Ni
Metals 2022, 12(10), 1697; https://doi.org/10.3390/met12101697 - 11 Oct 2022
Cited by 2 | Viewed by 1182
Abstract
The solidification of heavy metal Cr has always been a challenge in the treatment of Cr-containing wastes, due to its high mobility in alkaline environments. In addition, the solidification mechanism of Cr has not been fully investigated. In this study, blast furnace slag [...] Read more.
The solidification of heavy metal Cr has always been a challenge in the treatment of Cr-containing wastes, due to its high mobility in alkaline environments. In addition, the solidification mechanism of Cr has not been fully investigated. In this study, blast furnace slag (BFS)-based cementitious materials were used as binders for the immobilization of heavy metal Cr to investigate the solidification mechanism of Cr in different hydration products. From XRD, FTIR, XPS, and XANES analyses, it could be seen that SO42− in ettringite was replaced by Cr in the form of CrO42−, making SO42− re-dissolve in the liquid phase. The SO42− in the solution would compete with CrO42− ions, leading to the direct influence of SO42− content on the solidification efficiency of Cr. In ettringite, Cr mainly existed in the form of Cr6+, accounting for more than 84% however, Cr was solidified in Friedel’s salt under two coexisting valence states (Cr6+ and Cr3+). This resulted not only from the slow excitation rate of the BFS in the cementitious system that did not contain sulfate, but also from the existence of a certain amount of reducing substances in the BFS, such as Fe2+ and S2−, which could reduce some of Cr6+ to Cr3+. In Friedel’s salt, the residual Cr6+ replaced Cl in the form of CrO42−, whereas the Cr3+ replaced Al3+. The binding energies of Cr 2p3/1 and Cr 2p3/2 decreased with the addition of Cr, indicating that the coordination numbers of Cr3+ and Cr6+ increased, and that the binding energies of Cr3+ and Cr6+ decreased after entering the structure of Friedel’s salt. Full article
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16 pages, 6604 KiB  
Article
Hot Deformation Behavior and Microstructure Evolution of a Novel Al-Zn-Mg-Li-Cu Alloy
by Shuaishuai Wu, Baohong Zhu, Wei Jiang, Haochen Qiu and Yang Guo
Materials 2022, 15(19), 6769; https://doi.org/10.3390/ma15196769 - 29 Sep 2022
Cited by 6 | Viewed by 1206
Abstract
Lightweight structural alloys have broad application prospects in aerospace, energy, and transportation fields, and it is crucial to understand the hot deformation behavior of novel alloys for subsequent applications. The deformation behavior and microstructure evolution of a new Al-Zn-Mg-Li-Cu alloy was studied by [...] Read more.
Lightweight structural alloys have broad application prospects in aerospace, energy, and transportation fields, and it is crucial to understand the hot deformation behavior of novel alloys for subsequent applications. The deformation behavior and microstructure evolution of a new Al-Zn-Mg-Li-Cu alloy was studied by hot compression experiments at temperatures ranging from 300 °C to 420 °C and strain rates ranging from 0.01 s−1 to 10 s−1. The as-cast Al-Zn-Mg-Li-Cu alloy is composed of an α-Al phase, an Al2Cu phase, a T phase, an η phase, and an η′ phase. The constitutive relationship between flow stress, temperature, and strain rate, represented by Zener–Hollomon parameters including Arrhenius terms, was established. Microstructure observations show that the grain size and the fraction of DRX increases with increasing deformation temperature. The grain size of DRX decreases with increasing strain rates, while the fraction of DRX first increases and then decreases. A certain amount of medium-angle grain boundaries (MAGBs) was present at both lower and higher deformation temperatures, suggesting the existence of continuous dynamic recrystallization (CDRX). The cumulative misorientation from intragranular to grain boundary proves that the CDRX mechanism of the alloy occurs through progressive subgrain rotation. This paper provides a basis for the deformation process of a new Al-Zn-Mg-Li-Cu alloy. Full article
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11 pages, 2960 KiB  
Article
Effect of Nb Addition on the Phase Stability, Microstructure, and Mechanical Properties of Powder Metallurgy Ti-5Fe-xNb Alloys
by Balakrishnan Manogar, Fei Yang and Leandro Bolzoni
Metals 2022, 12(9), 1528; https://doi.org/10.3390/met12091528 - 15 Sep 2022
Cited by 3 | Viewed by 1796
Abstract
Ti alloys contemplating the simultaneous addition of Fe and Nb are available in the literature as Fe enhances the strength and Nb improves the biological behaviour of Ti. Nevertheless, casting has been the main manufacturing process, the Nb content is normally ≥10 wt.%, [...] Read more.
Ti alloys contemplating the simultaneous addition of Fe and Nb are available in the literature as Fe enhances the strength and Nb improves the biological behaviour of Ti. Nevertheless, casting has been the main manufacturing process, the Nb content is normally ≥10 wt.%, and no tensile properties are available. In this study, Ti-5Fe-xNb alloys (x = 2, 6, and 9 wt.%) were produced via powder metallurgy, which is more energy efficient than casting, with the aim of understanding the relationship between the mechanical behaviour and the microstructural changes brought about by the progressive addition of a greater amount of Nb. This study shows that the increment of the Nb content reduces the densification of the alloys, as the relative density decreases from 98.2% to 95.0%, but remarkably increases the volume fraction of the stabilised β phase (14→36%). Accordingly, the Ti-5Fe-xNb alloys are characterised by Widmanstätten microstructures, which become finer for higher Nb contents, and progressively higher mechanical properties including yield stress (725–949 MPa), ultimate tensile strength (828–995 MPa), and hardness (66.5–67.6 HRA), but lower elongation to fracture (4.0–5.1%). It is found that the ductility is much more influenced by the presence of the residual pores, whereas the strength greatly depends on the microstructural changes brought about by the addition of the alloying elements. Full article
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12 pages, 2922 KiB  
Article
A Study on the Design of Bending Process According to the Shape of Initial Billets for Bi-Metal Elbow
by Seonghun Ha, Daehwan Cho, Joonhong Park and Seongjae Kim
Metals 2022, 12(9), 1474; https://doi.org/10.3390/met12091474 - 04 Sep 2022
Cited by 1 | Viewed by 1551
Abstract
Studies have been steadily conducted on the forming process of the bending pipe that enables the transport of underground resources. Recently, it has been suggested that bent pipes for transport withstand high pressure during the forming process, but it is judged that the [...] Read more.
Studies have been steadily conducted on the forming process of the bending pipe that enables the transport of underground resources. Recently, it has been suggested that bent pipes for transport withstand high pressure during the forming process, but it is judged that the research on methods able to overcome the limitations of non-uniform dimensional distribution due to the difference in the mechanical properties and thickness of the outer and inner pipes is insufficient. This study proposes a new precision forging method called the cut-forged-joint process (CFJP) for the manufacture of bent pipe containing bi-metal. The initial billet and mandrel were designed considering the standard dimensions of bent pipes, and pre-simulation was performed applied to the designed models. The results of dimensional accuracy obtained by forging experiments and the computational forming simulation were compared with each other to verify the reliability. As a final outcome, it was confirmed that it is possible to secure the dimensional accuracy of bi-metal bent pipes by applying the newly proposed CFJP. Full article
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13 pages, 13001 KiB  
Article
Failure Analysis of Drill Pipe during Working Process in a Deep Well: A Case Study
by Luchun Li, Zhanghua Lian and Changhong Zhou
Processes 2022, 10(9), 1765; https://doi.org/10.3390/pr10091765 - 03 Sep 2022
Viewed by 4154
Abstract
The failure of a 101.6 mm drill pipe was studied by combining experimental testing and finite element simulation. The macro analysis, metallographic structure and energy spectrum, chemical composition and a mechanical property test of the failed drill pipe sample were firstly carried out. [...] Read more.
The failure of a 101.6 mm drill pipe was studied by combining experimental testing and finite element simulation. The macro analysis, metallographic structure and energy spectrum, chemical composition and a mechanical property test of the failed drill pipe sample were firstly carried out. Then, a three-dimensional finite element model of drill pipe failure was established based on the experimental results. Finally, the failure mechanism of drill pipe was analyzed and the mitigation measures were put forward. The results showed that solids settling sticking was the direct cause of fracture failure of the drill pipe joint. Due to the violent friction and wear between the drill pipe joint and the settled sand, the large amount of heat generated caused the microstructure of the joint material to undergo phase transformation and the bearing capacity to be reduced. Finally, fracture occurs under tensile and torsional loads. Full article
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21 pages, 10972 KiB  
Article
Thermal Modelling and Experimental Validation in the Perspective of Tool Steel Laser Polishing
by Bastian Meylan, Alexandre Masserey, Eric Boillat, Ivan Calderon and Kilian Wasmer
Appl. Sci. 2022, 12(17), 8409; https://doi.org/10.3390/app12178409 - 23 Aug 2022
Cited by 2 | Viewed by 1331
Abstract
Laser polishing (LP) is a process that allows a significant reduction of the surface roughness of a metal workpiece via re-melting a shallow layer of material. However, the practical use of LP is limited due to the difficulty of satisfying the high surface [...] Read more.
Laser polishing (LP) is a process that allows a significant reduction of the surface roughness of a metal workpiece via re-melting a shallow layer of material. However, the practical use of LP is limited due to the difficulty of satisfying the high surface polishing quality for industries such as jewelry. Hence, this study presents a thermal model based on the Chernoff formula for fixed and moving LP processes. The model was validated via a sensitivity analysis of the coefficient of absorption of the solid and liquid phase and through comparing the results with the corresponding experimental observations of the melt pools produced. In this investigation, a continuous wave, high power diode laser (980 nm wavelength, Ø 0.9 mm spot size with a flat top distribution) was coupled to a fixed focusing head. The material was a hardened tool steel (X38CrMVo5-1 steel-1.2343) with an initial surface state obtained by electrical discharge machining (EDM) of CH30 on the Charmilles scale for EDM, which corresponds to a roughness Ra of 3.15 µm. The results show that the model is able to represent the thermal behavior of the tool steel during LP. The best results are obtained with two constant coefficients, one for the solid based on the measurement at room temperature (as = 35%) and one for the liquid fixed so that the model fits the experiment data (al = 25%). Full article
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18 pages, 6064 KiB  
Article
Surface Morphology Evolution during Chemical Mechanical Polishing Based on Microscale Material Removal Modeling for Monocrystalline Silicon
by Jingjing Xia, Jun Yu, Siwen Lu, Qiushi Huang, Chun Xie and Zhanshan Wang
Materials 2022, 15(16), 5641; https://doi.org/10.3390/ma15165641 - 17 Aug 2022
Cited by 9 | Viewed by 2083
Abstract
Chemical–mechanical polishing (CMP) is widely adopted as a key bridge between fine rotation grinding and ion beam figuring in super-smooth monocrystalline silicon mirror manufacturing. However, controlling mid- to short-spatial-period errors during CMP is a challenge owing to the complex chemical–mechanical material removal process [...] Read more.
Chemical–mechanical polishing (CMP) is widely adopted as a key bridge between fine rotation grinding and ion beam figuring in super-smooth monocrystalline silicon mirror manufacturing. However, controlling mid- to short-spatial-period errors during CMP is a challenge owing to the complex chemical–mechanical material removal process during surface morphology formation. In this study, the nature of chemical and mechanical material removal during CMP is theoretically studied based on a three-system elastic–plastic model and wet chemical etching behavior. The effect of the applied load, material properties, abrasive size distribution, and chemical reaction rate on the polishing surface morphology is evaluated. A microscale material removal model is established to numerically predict the silicon surface morphology and to explain the surface roughness evolution and the source of nanoscale intrinsic polishing scratches. The simulated surface morphology is consistent with the experimental results obtained by using the same polishing parameters tested by employing profilometry and atomic force microscopy. The PSD curve for both simulated surface and experimental results by profilometry and atomic force microscopy follows linear relation with double-logarithmic coordinates. This model can be used to adjust the polishing parameters for surface quality optimization, which facilitates CMP manufacturing. Full article
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16 pages, 3472 KiB  
Article
Rock Brittleness Evaluation Index Based on Ultimate Elastic Strain Energy
by Xiaowu Zhang, Jinhai Xu, Faiz Shaikh, Lei Sun and Yue Cao
Processes 2022, 10(7), 1367; https://doi.org/10.3390/pr10071367 - 13 Jul 2022
Cited by 4 | Viewed by 1674
Abstract
Brittleness is an essential parameter to determine the deformation and failure behavior of rocks, and it is useful to quantify the brittleness of rocks in numerus engineering practices. A novel energy-based brittleness evaluation index is proposed in this study, which redefines the dissipated [...] Read more.
Brittleness is an essential parameter to determine the deformation and failure behavior of rocks, and it is useful to quantify the brittleness of rocks in numerus engineering practices. A novel energy-based brittleness evaluation index is proposed in this study, which redefines the dissipated proportion of ultimate elastic strain energy relative to post-peak failure energy and residual elastic strain energy. A series of conventional triaxial compression (CTC) tests were performed on shale rock to verify the reliability and accuracy of the brittleness index. The results show that the proposed index can precisely reflect the deformation and failure characteristic of rocks under different confining pressures. Based on the testing data from six types of rocks in previous studies, the universality of the novel index was verified. According to comparison with existing brittleness indices, the new brittleness index can more precisely characterize the brittleness of rock. Full article
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14 pages, 5413 KiB  
Article
Structure Characterization and Impact Effect of Al-Cu Graded Materials Prepared by Tape Casting
by Jianian Hu, Ye Tan, Xuemei Li, Youlin Zhu, Guoqiang Luo, Jian Zhang, Ruizhi Zhang, Yi Sun, Qiang Shen and Lianmeng Zhang
Materials 2022, 15(14), 4834; https://doi.org/10.3390/ma15144834 - 11 Jul 2022
Cited by 3 | Viewed by 1473
Abstract
With the need of developing new materials, exploring new phenomenon, and discovering new mechanisms under extreme conditions, the response of materials to high-pressure compression attract more attention. However, the high-pressure state deviating from the Hugoniot line is difficult to realize by conventional experiments. [...] Read more.
With the need of developing new materials, exploring new phenomenon, and discovering new mechanisms under extreme conditions, the response of materials to high-pressure compression attract more attention. However, the high-pressure state deviating from the Hugoniot line is difficult to realize by conventional experiments. Gas gun launching graded materials could reach the state. In our work, the corresponding Al-Cu composites and graded materials are prepared by tape casting and hot-pressing sintering. The microstructure and the acoustic impedance of the corresponding Al-Cu composites are analyzed to explain the impact behavior of Al-Cu graded materials. Computed tomographic testing and three-dimension surface profilometry machine results demonstrated well-graded structure and parallelism of the graded material. Al-Cu GMs with good parallelism are used to impact the Al-LiF target at 2.3 km/s using a two-stage light-gas gun, with an initial shock impact of 20.6 GPa and ramping until 27.2 GPa, deviating from the Hugoniot line. Full article
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34 pages, 13724 KiB  
Article
Influence of Meso-Scale Pore Structure on Mechanical Behavior of Concrete under Uniaxial Compression Based on Parametric Modeling
by Hao Yang, Eryu Zhu and Lei Liu
Materials 2022, 15(13), 4594; https://doi.org/10.3390/ma15134594 - 30 Jun 2022
Viewed by 1517
Abstract
Existing concrete random aggregate modeling methods (CRAMMs) have deficiencies in in the parameterization of the mesoscale pore structure. A novel CRAMM is proposed, whose pore structure is determined by the pore gradation, total porosity, sub-porosity, and pore size of each pore gradation segment. [...] Read more.
Existing concrete random aggregate modeling methods (CRAMMs) have deficiencies in in the parameterization of the mesoscale pore structure. A novel CRAMM is proposed, whose pore structure is determined by the pore gradation, total porosity, sub-porosity, and pore size of each pore gradation segment. To study the influence of pore structure on the mechanical properties of concrete, 25 mesoscopic concrete specimens with the same aggregate structure but different meso-scale pore structures are constructed and subjected to uniaxial compression tests. For the first time, the influence of sub-porosity of each pore gradation segment, average pore radius (APR), pore specific surface area (PSSA), and total porosity on concrete failure process, compressive strength, peak strain, and elastic modulus were quantitatively and qualitatively analyzed. Results indicate that the pore structure makes the germination and propagation of the damage in cement mortar show obvious locality and affects the formation and expansion of macroscopic cracks. However, it does not accelerate the propagation of the damage in cement mortar from the periphery to the center of the specimen, nor does it change the phenomenon that the ITZ is more damaged than other meso-components of concrete before peak stress. Macroscopic cracks occur in the descending section of the stress–strain curve, and the sudden drops in the descending section of the stress–strain curve are often accompanied by the generation and expansion of macroscopic cracks. The quadratic polynomial, exponential, and power functions can well fit the relationship between total porosity and compressive strength and the relationship between PSSA and compressive strength. The linear, exponential, and power functions can well reflect the relationship between total porosity and compressive modulus and the relationship between compressive modulus and PSSA. For concrete specimens with the same total porosity, the elastic modulus and strength show randomness with the increase in the sub-porosity of macropores and are basically not affected by the APR. Based on the grey relational analysis, the effects of pore structure parameters on the elastic modulus and compressive strength are in the same order: total porosity > T [k1,k2] > T [k2,k3] > T [k3,k4] > T [k4,k5] > AVR > PSSA. The order of influence of the pore structure parameters on the peak strain is: T [k2,k3] > T [k1,k2] > T [k3,k4] > T [k4,k5] > APR > PSSA > total porosity. Full article
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19 pages, 12735 KiB  
Article
A Multiphysics Model for Predicting Microstructure Changes and Microhardness of Machined AerMet100 Steel
by Wenqian Zhang, Xupeng Chen, Chongwen Yang, Xuelin Wang, Yansong Zhang, Yongchun Li, Huan Xue and Zhong Zheng
Materials 2022, 15(13), 4395; https://doi.org/10.3390/ma15134395 - 21 Jun 2022
Cited by 2 | Viewed by 1271
Abstract
The machined-surface integrity plays a critical role in corrosion resistance and fatigue properties of ultra-high-strength steels. This work develops a multiphysics model for predicting the microstructure changes and microhardness of machined AerMet100 steel. The variations of stress, strain and temperature of the machined [...] Read more.
The machined-surface integrity plays a critical role in corrosion resistance and fatigue properties of ultra-high-strength steels. This work develops a multiphysics model for predicting the microstructure changes and microhardness of machined AerMet100 steel. The variations of stress, strain and temperature of the machined workpiece are evaluated by constructing a finite-element model of the orthogonal cutting process. Based on the multiphysics fields, the analytical models of phase transformation and dislocation density evolution are built up. The white layer is modeled according to the phase-transformation mechanism and the effects of stress and plastic strain on real phase-transformation temperature are taken into consideration. The microhardness changes are predicted by a model that accounts for both dislocation density and phase-transformation evolution processes. Experimental tests are carried out for model validation. The predicted results of cutting force, white-layer thickness and microhardness are in good agreement with the measured data. Additionally, from the proposed model, the correlation between the machined-surface characteristics and processing parameters is established. Full article
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11 pages, 2902 KiB  
Article
Experimental Study on Activated Diatomite Modified Asphalt Pavement in Deep Loess Area
by Ting Du, Peng Song and Liping Liu
Processes 2022, 10(6), 1227; https://doi.org/10.3390/pr10061227 - 20 Jun 2022
Cited by 4 | Viewed by 1344
Abstract
In order to effectively prevent and control the rutting problem of asphalt pavement in the deep loess area of Eastern Gansu and reduce road diseases, diatomite was added into the asphalt mixture for laboratory tests. Through Marshall test and rutting test, the optimum [...] Read more.
In order to effectively prevent and control the rutting problem of asphalt pavement in the deep loess area of Eastern Gansu and reduce road diseases, diatomite was added into the asphalt mixture for laboratory tests. Through Marshall test and rutting test, the optimum mix proportion of the diatomite asphalt mixture, and the optimal mix amount of the diatomite in this area were determined. The pavement performance of activated diatomite asphalt pavement and SBS asphalt pavement in this area is compared and analyzed through laboratory tests and on-site road paving. The test results show that under the same ambient temperature, the activated diatomite asphalt pavement has the advantages of lower surface temperature, high stability, and low-water permeability coefficient than SBS modified asphalt pavement. In addition, by fitting the fatigue test data of these two asphalt pavements, it is found that the fatigue life of diatomite asphalt mixture is more sensitive to the change in stress level and has better fatigue resistance. Therefore, it is concluded that the use of diatomite modified asphalt pavement in the loess area can improve the temperature stability of the pavement, prolong the service life, and reduce the cost of construction, which can be popularized. Full article
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17 pages, 8448 KiB  
Article
Study on Piezomagnetic Effect of Iron Cobalt Alloy and Force Sensor
by Ruichuan Li, Jilu Liu, Jikang Xu, Xinkai Ding, Yi Cheng and Qi Liu
Processes 2022, 10(6), 1218; https://doi.org/10.3390/pr10061218 - 18 Jun 2022
Viewed by 1625
Abstract
Based on the nonlinear piezomagnetic equation, the piezomagnetic effect of prismatic iron-cobalt alloy is analyzed by using the ANSYS finite element simulation platform. The variation of the dynamic piezomagnetic coefficient of the iron-cobalt alloy under different bias magnetic fields and different stress was [...] Read more.
Based on the nonlinear piezomagnetic equation, the piezomagnetic effect of prismatic iron-cobalt alloy is analyzed by using the ANSYS finite element simulation platform. The variation of the dynamic piezomagnetic coefficient of the iron-cobalt alloy under different bias magnetic fields and different stress was studied through simulation. Referring to the working condition of the tractor force sensor and according to the principle of magnetic circuit superposition, a piezomagnetic force sensor was designed and manufactured using iron-cobalt alloy. According to the electromagnetic theory and piezomagnetic effect, the three-dimensional model and magnetic circuit mathematical model of the sensor are established, and the system simulation model of the piezomagnetic sensor was established based on the MATLAB/Simulink module. The experimental platform of the magnetostrictive force sensor was built to verify the correctness of the simulation model, and the effects of bias magnetic field and force on the output characteristics are studied. The simulation and experimental results show that the maximum piezomagnetic coefficient was 9.2 T/GPA when the bias magnetic field intensity was 14.74 kA/m. The force measuring range of the sensor is 0–120 kN, and the sensor has high sensitivity within 0–80 kN. The sensor has a simple structure, is suitable for the force measurement and control of an electro-hydraulic lifter under heavy load, and can better adapt to the harsh working environment. Full article
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20 pages, 6311 KiB  
Article
Comprehensive Penetration Evaluation Method in Collisions between a Supply Ship and a Semi-Submersible Platform
by Yuan Xiao, Zhi Yao and Xu Zhang
Processes 2022, 10(6), 1212; https://doi.org/10.3390/pr10061212 - 17 Jun 2022
Viewed by 1570
Abstract
Collisions between ships and offshore platforms frequently occur, with severe consequences. Predicting the collision depth under different conditions is very important to evaluate the severity of the consequences. Considering the time-consuming numerical simulation problem and the accuracy problems of existing approximation algorithms, this [...] Read more.
Collisions between ships and offshore platforms frequently occur, with severe consequences. Predicting the collision depth under different conditions is very important to evaluate the severity of the consequences. Considering the time-consuming numerical simulation problem and the accuracy problems of existing approximation algorithms, this paper proposes a comprehensive approach to estimating penetration depths by obtaining two collision coefficients for specific collision structures based on the partial results of numerical simulations and simplified theoretical analysis. In this study, the collision process between a supply ship with a transverse framing stern and an offshore semi-platform was first numerically simulated based on the explicit dynamic method. The changes in ship velocity, impact force, and energy conversion before and after the collision processes were obtained through numerical simulations of the collisions with different speeds and angles. Then, by combining the external dynamics and numerical results, the analytical results of dissipated energy under other collision conditions were obtained using a simulated restitution coefficient. For the following internal dynamics analysis, according to the failure modes of specific structural components in different regions, an appropriate structural energy absorption formula was combined to obtain the relationship between the penetrations and energy absorption in a particular collision area. According to the friction energy ratio derived by the simulation, the penetration depths in the offshore platform were calculated. The results showed that the deviations between the proposed method and direct simulation results were less than 15% in the cases of a medium- to high-energy collision. It can be concluded that the restitution coefficient and friction energy ratio in different collision conditions can be approximately determined for a specific collision system by typical numerical simulations, thus quickly calculating the penetration depths of other conditions. Full article
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14 pages, 2214 KiB  
Article
Variability in the Solid Particle Density and Its Influence on the Corresponding Void Ratio and Dry Density: A Case Study Conducted on the MBT Reject Waste Stream from the MBT Plant in Marišćina, Croatia
by Igor Petrovic, Nikola Kaniski, Nikola Hrncic and Dino Bosilj
Appl. Sci. 2022, 12(12), 6136; https://doi.org/10.3390/app12126136 - 16 Jun 2022
Cited by 4 | Viewed by 1350
Abstract
In this study, a functional relationship between the solid particle density (ρs), void ratio e, and dry density (ρd) of mechanically and biologically treated (MBT) municipal solid waste (MSW) was examined. In total, 60 waste [...] Read more.
In this study, a functional relationship between the solid particle density (ρs), void ratio e, and dry density (ρd) of mechanically and biologically treated (MBT) municipal solid waste (MSW) was examined. In total, 60 waste specimens were tested with an air pycnometer device and corresponding triplets (e, ρd,and ρs) of values were obtained. In addition, a long-term oedometer test with an allowed decomposition process was also conducted. Based on the obtained results, the variability in the solid particle density caused by heterogeneity and decomposition, as well as its influence on the corresponding void ratio and dry density values, were critically evaluated. The obtained results showed that the variability in the solid particle density caused by waste heterogeneity had a significant influence on the initial void ratio value. Furthermore, the obtained results also showed that the change in the solid particle density, caused by the degradation process, had a significant impact on the final void ratio and dry density values. In addition, an empirical relationship, ρd=fe, was proposed. The proposed function allows a landfill operator to establish the corresponding dry density at an arbitrary chosen void ratio, and vice versa, without having the exact knowledge of the corresponding solid particle density value. Full article
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18 pages, 11213 KiB  
Article
Large-Sized GaN Crystal Growth Analysis in an Ammonothermal System Based on a Well-Developed Numerical Model
by Pengfei Han, Bing Gao, Botao Song, Yue Yu, Xia Tang and Botao Liu
Materials 2022, 15(12), 4137; https://doi.org/10.3390/ma15124137 - 10 Jun 2022
Cited by 2 | Viewed by 1331
Abstract
The ammonothermal method is considered the most promising method of fabricating bulk gallium nitride (GaN) crystals. This paper improves the ammonothermal growth model by replacing the heater-long fixed temperature boundary with two resistance heaters and considering the real thermal boundary outside the shell. [...] Read more.
The ammonothermal method is considered the most promising method of fabricating bulk gallium nitride (GaN) crystals. This paper improves the ammonothermal growth model by replacing the heater-long fixed temperature boundary with two resistance heaters and considering the real thermal boundary outside the shell. The relationship between power values and temperatures of dissolution and crystallization is expressed by the backpropagation (BP) neural network, and the optimal power values for specific systems are found using the non-dominated sorting genetic algorithm (NSGAII). Simulation results show that there are several discrepancies between updated and simplified models. It is necessary to build an ammonothermal system model with resistance heaters as a heat source. Then large-sized GaN crystal growth is analyzed based on the well-developed numerical model. According to the simulation results, both the increasing rate and maximum stable values of the metastable GaN concentration gradient are reduced for a larger-sized system, which is caused by the inhomogeneity of heat transfer in the autoclave. Full article
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18 pages, 5728 KiB  
Article
Effect of Batch Dissimilarity on Permeability of Stacked Ceramic Foam Filters and Incompressible Fluid Flow: Experimental and Numerical Investigation
by Shahin Akbarnejad, Anders Tilliander, Dong-Yuan Sheng and Pär Göran Jönsson
Metals 2022, 12(6), 1001; https://doi.org/10.3390/met12061001 - 10 Jun 2022
Cited by 2 | Viewed by 1369
Abstract
Ceramic foam filters (CFFs) are used to remove inclusions and/or solid particles from molten metal. In general, the molten metal poured on the top of a CFF should reach a certain height to form the pressure (metal head) required to prime the filter. [...] Read more.
Ceramic foam filters (CFFs) are used to remove inclusions and/or solid particles from molten metal. In general, the molten metal poured on the top of a CFF should reach a certain height to form the pressure (metal head) required to prime the filter. For estimating the required metal head and obtaining the permeability coefficients of the CFFs, permeability experiments are essential. Recently, electromagnetic priming and filtration of molten aluminum with low and high grades of CFF, i.e., 30, 50 and 80 pore per inch (PPI) CFFs, have been introduced. Since then, there has been interest in exploring the possibility of obtaining further inclusion entrapment and aluminum refinement by using electromagnetic force to prime and filter with stacked CFFs. The successful execution of such trials requires a profound understanding concerning the permeability parameters of the stacked filters. Such data were deemed not to exist prior to this study. As a result, this study presents experimental findings of permeability measurements for stacks of three 30, three 50 and three 80 PPI commercial alumina CFFs from different industrial batches and compares the findings to numerically modelled data as well as previous research works. Both experimental and numerical findings showed a good agreement with previous results. The deviation between the experimentally and numerically obtained data lies in the range of 0.4 to 6.3%. Full article
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23 pages, 4946 KiB  
Article
Frequency Domain Analysis of Fluid–Structure Interaction in Aircraft Hydraulic Pipe with Complex Constraints
by Haihai Gao, Changhong Guo, Lingxiao Quan and Shuai Wang
Processes 2022, 10(6), 1161; https://doi.org/10.3390/pr10061161 - 09 Jun 2022
Cited by 3 | Viewed by 1690
Abstract
This paper focuses on the frequency domain fluid–structure interaction (FSI) vibration characteristics of aircraft hydraulic pipe with complex constraints. The linear partial differential fourteen-equation model is applied to describe the nonlinear FSI dynamics of pipes conveying fluid with high-speed, high-pressure, a wide Reynolds [...] Read more.
This paper focuses on the frequency domain fluid–structure interaction (FSI) vibration characteristics of aircraft hydraulic pipe with complex constraints. The linear partial differential fourteen-equation model is applied to describe the nonlinear FSI dynamics of pipes conveying fluid with high-speed, high-pressure, a wide Reynolds number, and the vibration frequency range. The excitation, complex boundary, and middle constraint models of liquid-filled pipes are analytically established and added into the global model of the pipe system. These resulting models are solved by the improved Laplace transform transfer matrix method (LTTMM) in the frequency domain. Then, the dynamic response characteristics of an aircraft hydraulic pipe containing diverse constraints are investigated numerically and experimentally under four types of working conditions, and the improvement conditions for the numerical instabilities are presented. In general, the present method is highly efficient and convenient for rapid model parameter modifications, in order to be fully applicable to different pipe systems and analysis cases. The results reveal the complex resonant laws regarding aircraft hydraulic pipes with complex constraints in the broad frequency band, which can also provide theoretical reference and technical support for FSI vibration analysis and the control of aircraft hydraulic pipes. Full article
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11 pages, 2663 KiB  
Article
The Seal Performance of Compliant Foil Gas Seal Based on Multi-Scale Analysis
by Xueliang Wang and Meihong Liu
Processes 2022, 10(6), 1123; https://doi.org/10.3390/pr10061123 - 03 Jun 2022
Cited by 1 | Viewed by 1479
Abstract
Compliant foil gas seal is a non-contact and high-efficiency sealing technology. The dynamic performance of compliant foil gas seal with different structure parameters was analyzed in this paper. These parameters include the seal diameter, gas film thickness and the ratio of groove. Compared [...] Read more.
Compliant foil gas seal is a non-contact and high-efficiency sealing technology. The dynamic performance of compliant foil gas seal with different structure parameters was analyzed in this paper. These parameters include the seal diameter, gas film thickness and the ratio of groove. Compared with the rigid film, the advantage of compliant film is analyzed. The stability performance and dynamic performance with the different structures are obtained. The results show that the larger diameter is a disadvantage for the stability performance. However, the increase of seal length can decrease the leakage. Otherwise, the increase of gas thickness improves the dynamic characteristics with the leakage rising and gas force dramatically decreasing. While the groove length ratio is around 0.6, the seal performance and dynamic characteristics are best. The compliant structure benefits the improvement of the sealing performance. Full article
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13 pages, 3270 KiB  
Article
Bifurcation Diagram and Dynamic Response of a Drill String Applied in NGH Drilling
by Baojin Wang, Liuci Wang, Xiaotong Liu and Fushen Ren
Processes 2022, 10(6), 1111; https://doi.org/10.3390/pr10061111 - 02 Jun 2022
Cited by 4 | Viewed by 1334
Abstract
Natural gas hydrate (NGH) is a kind of unique resource among hydrocarbon fuels. It is stable within its sedimentary hosts and will only convert to its constituent gas and water phases relatively quickly if reservoir pressure-temperature conditions are artificially disturbed. The unwanted vibrations [...] Read more.
Natural gas hydrate (NGH) is a kind of unique resource among hydrocarbon fuels. It is stable within its sedimentary hosts and will only convert to its constituent gas and water phases relatively quickly if reservoir pressure-temperature conditions are artificially disturbed. The unwanted vibrations from the drill string with the complex external environment and excitation usually cause instability in the NGH. In this paper, a nonlinear mathematical model is presented taking into account the fluid–solid coupling vibration caused by the drilling fluid inside and outside the drill string, the non-smooth rub-impact between the drill string and borehole wall, and the influence of centralizer setting interval on nonlinear resonant vibration of the drill string. The relationship between the variable parameters of the drill string and the complex dynamics of the drill string is analyzed. Finally, the bifurcation diagram is given. The results show that the system response exhibits complex dynamic behavior due to rub-impact and nonlinear effects. However, there is always a suitable parameter in the bifurcation diagram of each parameter change, so that the amplitude of the system is small and the failure probability of the drill string is reduced. The research results have reference significance for exploring the nonlinear dynamic mechanism of a drill string under complex working conditions and reasonably optimizing drilling parameters. Full article
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25 pages, 12092 KiB  
Article
Experimental and Numerical Analysis of Steel Beams’ Efficiency with Different Shapes of Corrugated Webs under Free Vibrations
by Ahmed Mohamed Sayed, Yassir G. Elaraki and Oussama Elalaoui
Metals 2022, 12(6), 938; https://doi.org/10.3390/met12060938 - 29 May 2022
Cited by 2 | Viewed by 1889
Abstract
The use of corrugated webs in steel beams has become one of the most practical ways to increase the efficiency of beams in resisting loads, natural frequencies, and their resulting displacements. Such a practice has the benefit of achieving the same efficiency as [...] Read more.
The use of corrugated webs in steel beams has become one of the most practical ways to increase the efficiency of beams in resisting loads, natural frequencies, and their resulting displacements. Such a practice has the benefit of achieving the same efficiency as beams with a flat web with a greater thickness. Consequently, the effect of the types of corrugated webs on the flexure mode shapes and natural frequencies in the steel beams has been investigated by analyzing 23 beams with flat and corrugated webs using the finite element (FE) numerical analysis technique. Hence, two flat web steel beams with and without stiffeners were experimentally tested and compared to FE numerical modeling results. Moreover, three types (trapezoidal, rectangular, triangular) of corrugated webs were tested and studied in addition to other parameters such as thickness, width, length, and angle. The investigation results show that FE numerical analysis is very highly accurate in predicting the natural frequencies and flexure mode shape changes of beams with corrugated webs. Accordingly, a saving of at least 33% in thickness could be realized as compared to the flat type. The triangular corrugated web is more efficient in the 1st mode shape, while rectangular is better for the other modes. The effectiveness of the angle for the triangular type in resisting mode shape and frequencies was clearly noticed, and decreases of 0.60 and 0.78, respectively, were recorded. It is also perceived that the effect of thickness and angle is linear for specified cases. Full article
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17 pages, 4920 KiB  
Article
Production of Closed-Cell Foams Out of Aluminum Chip Waste: Mathematical Modeling and Optimization
by Jure Krolo, Branimir Lela, Karla Grgić and Sonja Jozić
Metals 2022, 12(6), 933; https://doi.org/10.3390/met12060933 - 28 May 2022
Cited by 3 | Viewed by 1676
Abstract
The main aim of this research is to mathematically describe the influence of the processing parameters of metal foam production from machining chip waste. Using this method, metal foams were produced without a remelting step, which should be both economically and environmentally effective. [...] Read more.
The main aim of this research is to mathematically describe the influence of the processing parameters of metal foam production from machining chip waste. Using this method, metal foams were produced without a remelting step, which should be both economically and environmentally effective. Firstly, expensive metal powders were replaced with waste in the form of machining chips. Secondly, machining chip waste was recycled without any significant material losses, which usually occurs during conventional recycling (using the melting process). To describe the innovative process and to relate metal foam properties to foaming temperature, the blowing agent weight percentage, and foam density (controlled by foaming height), response surface methodology, and the design of experiments were used. The quality of the produced metal foams was evaluated by determination of density, yield strength, compression strength, plateau stress, energy absorption, pore perimeter, and pore inhomogeneity for specimens obtained following the experimental plan. It was proven that pore inhomogeneity increased in the range from 1.41 to 4.81 mm with a higher temperature and the addition of a foaming agent. However, higher energy absorption and yield strength were obtained with a higher temperature but a lower percentage of TiH2. Despite the production from machining chips, pores were homogenous without significant cracks. These kinds of metal foams are comparable to commercial foams made of metal powders. Full article
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9 pages, 2319 KiB  
Article
The Mechanism of Porcelain Toughened by Activated Kaolinite in a Lower Sintering Temperature
by Shaomin Lin, Yaling Yu, Yue Tan, Huan Yang, Mingfeng Zhong, Chenyang Zhang, Zhijie Zhang and Yunying Wu
Materials 2022, 15(11), 3867; https://doi.org/10.3390/ma15113867 - 28 May 2022
Cited by 1 | Viewed by 1680
Abstract
A high sintering temperature is usually required to acquire excellent performance in the ceramic industry, but it results in high fuel consumption and high pollution. To reduce the sintering temperature and to toughen the porcelain, a self-produced sintering additive of citric acid activated [...] Read more.
A high sintering temperature is usually required to acquire excellent performance in the ceramic industry, but it results in high fuel consumption and high pollution. To reduce the sintering temperature and to toughen the porcelain, a self-produced sintering additive of citric acid activated kaolinite was added to the raw material; X-ray powder diffraction (XRD), transmission electron microscope (TEM), scanning electron microscope (SEM), and thermal gravity analysis and differential scanning calorimetry (TG-DSC) were used to characterize the samples, and the toughening mechanism was discussed. The citric acid activated kaolinite obtained high activity and a large specific surface area. After introducing the activated kaolinite, the bending strength of porcelain at 1270 °C increased from 100.08 MPa to 124.04 Mpa, which was 11.45% higher than that of porcelain without activated kaolinite at 1350 °C. The results of XRD revealed that the content of mullite increased and the quartz decreased at 1270 °C, and the well-distributed needle-like mullite was observed in the images of SEM with the addition of citric acid activated kaolinite. The TG-DSC results indicated adding activated kaolinite to porcelain raw materials reduced the formation of mullite to 994.6 °C. The formation of mullite in a lower temperature served as mullite seeds in a green body during firing, and it enhanced the growth of mullite. These contributed to the appropriate phase composition and the excellent microstructure of porcelain. Thus, the distinguished mechanical performance of porcelain was obtained. Moreover, the sintering additive had no adverse effect on the porcelain body as citric acid-activated kaolinite was one of the main components of the porcelain raw material. Full article
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25 pages, 7675 KiB  
Article
Study on Intrinsic Influence Law of Specimen Size and Loading Speed on Charpy Impact Test
by Wang Jia, Aiguo Pi, Zhang Zhao, Shaohong Wang, Chen Wei, Zhou Jie and Fenglei Huang
Materials 2022, 15(11), 3855; https://doi.org/10.3390/ma15113855 - 28 May 2022
Cited by 4 | Viewed by 2189
Abstract
Charpy impact energy/impact toughness is closely related to external factors such as specimen size. However, when the sample size is small, the linear conversion relationship between the Charpy impact energy of the sub-size and full-size Charpy specimens does not hold; the Charpy impact [...] Read more.
Charpy impact energy/impact toughness is closely related to external factors such as specimen size. However, when the sample size is small, the linear conversion relationship between the Charpy impact energy of the sub-size and full-size Charpy specimens does not hold; the Charpy impact toughness varies with the size of the specimen and other factors. This indicates that studying the internal influence of external factors on impact energy or impact toughness is the key to accurately understanding and evaluating the toughness and brittleness of materials. In this paper, the effects of strain rate on the flow behavior and the effects of stress triaxiality on the fracture behavior of 30CrMnSiNi2A high-strength steel were investigated using quasi-static smooth bar and notched bar uniaxial tensile tests and Split Hopkinson Tensile Bar (SHTP). Based on the flow behavior and strain rate dependences of the yield behavior, a modified JC model was established to describe the flow behavior and strain rate behavior. Charpy impact tests were simulated using the modified JC model and JC failure model with the determined parameters. Reasonable agreements between the simulation and experimental results have been achieved, and the validity of the model was proved. According to the simulation results, the impact energy was divided into crack initiation energy, crack stability propagation energy and crack instability propagation energy. On this basis, the effects of striker velocity and specimen width on the energy and characteristic load of each part were studied. The results show that each part of the impact energy has a negligible dependence on the hammer velocity, but there is a significantly different positive linear relationship with the width of the sample. The energy increment of each part also showed an inverse correlation with the increase in the sample width. The findings reveal that the internal mechanism of Charpy impact toughness decreases with the increase in sample width; to a certain extent, it also reveals the internal reason why the linear transformation relationship of Charpy impact energy between sub-size specimens and standard specimens is not established when the specimens are small. The analytical method and results presented in this paper can provide a reference for the study of the dynamic behavior of high-strength steel, the relationship between material properties and sample size, and the elastic–plastic impact dynamic design. Full article
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18 pages, 8383 KiB  
Article
Numerical Simulation and Experimental Test of the Sliding Core Dynamics of a Pressure Controlled Jet Crushing Tool for Natural Gas Hydrate Exploitation
by Yang Tang, Peng Zhao, Xushen Li, Xiaoyu Fang and Pu Yang
Processes 2022, 10(5), 1033; https://doi.org/10.3390/pr10051033 - 23 May 2022
Cited by 2 | Viewed by 1692
Abstract
A pressure-controlled jet crushing tool (PJCT) for the exploitation of deep-sea natural gas hydrate (NGH) was invented to achieve sediment crushing and cavity creation. The opening and closing of tool is controlled by changing the internal flow rate remotely. It can realize the [...] Read more.
A pressure-controlled jet crushing tool (PJCT) for the exploitation of deep-sea natural gas hydrate (NGH) was invented to achieve sediment crushing and cavity creation. The opening and closing of tool is controlled by changing the internal flow rate remotely. It can realize the controllable continuous switching of the working state between horizontal well drilling and cavity creation. A dynamic simulation model of the sliding core was established based on the innovative design scheme of the PJCT and the motion law of its slide core was analyzed under the influence of spring stiffness, friction coefficient, and flow rate loading scheme. Moreover, an engineering prototype of the PJCT was manufactured so that a sliding core motion experiment of the prototype was carried out. When the drilling fluid flow rate reaches 455 L/min, the PJCT can stably complete the self-locking and unlocking functions. Its sliding core needs more time to stabilize with an increase in spring stiffness. Meanwhile, the PJCT could achieve continuous fast switching between the mechanical drilling state and the jet crushing state within a cycle of continuous flow changes. Finally, the kinematic and dynamic working mechanism of the PJCT is verified by the combination of the numerical simulation and the experimental analysis above. Full article
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10 pages, 4410 KiB  
Article
High Densification of Tungsten via Hot Pressing at 1300 °C in Carbon Presence
by Oleksii Popov and Vladimir Vishnyakov
Materials 2022, 15(10), 3641; https://doi.org/10.3390/ma15103641 - 19 May 2022
Cited by 1 | Viewed by 1394
Abstract
A reactive sintering technique with a small addition of carbon (up to 1.9 wt.%) has been used for tungsten powder consolidation. The process allowed procurement of the nonporous and fully densified material at 1300 °C and 30 MPa in 12 min. The SEM [...] Read more.
A reactive sintering technique with a small addition of carbon (up to 1.9 wt.%) has been used for tungsten powder consolidation. The process allowed procurement of the nonporous and fully densified material at 1300 °C and 30 MPa in 12 min. The SEM and EDX analysis showed that the milling of 5 μm tungsten powder with 0.6, 1.3, and 1.9 wt.% of carbon in a planetary mill led to the formation of the nanostructured mix, which appears to be W-C nanopowder surrounding tungsten grains. X-Ray Diffractometry data indicated tungsten hemicarbide (W2C) nucleation during the hot pressing of the milled powders. The exothermic reaction 2W + C → W2C occurs during the sintering process and promotes charge densification. The Vickers hardness and indentation toughness of W-1.3 wt.%C composition reached 5.7 GPa and 12.6 MPa∙m1/2, respectively. High toughness and high material densification allow proposing the W-WC2 for use as a plasma-facing material in fusion applications. Full article
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13 pages, 3874 KiB  
Article
Effect of Spray Parameters on Electrical Characteristics of Printed Layer by Morphological Study
by Gye Hyeon Kim, Eun Ae Shin, Je Young Jung, Jun Young Lee and Chang Kee Lee
Processes 2022, 10(5), 999; https://doi.org/10.3390/pr10050999 - 18 May 2022
Viewed by 1770
Abstract
Products are manufactured as printed electronics through electro-conductive ink having properties suitable for flexible substrates. As printing process conditions affect the quality of the electronic properties of the final devices, it is essential to understand how the parameters of each process affect print [...] Read more.
Products are manufactured as printed electronics through electro-conductive ink having properties suitable for flexible substrates. As printing process conditions affect the quality of the electronic properties of the final devices, it is essential to understand how the parameters of each process affect print quality. Spray printing, one of several printing processes, suits flexible large-area substrates and continuous processes with a uniform layer for electro-conductive aqueous ink. This study adopted the spray printing process for cellulose nanofiber (CNF)/carbon nanotube (CNT) composite conductive printing. Five spray parameters (nozzle diameter, spray speed, amount of sprayed ink, distance of nozzle to substrate, and nozzle pressure) were chosen to investigate the effects between process parameters and electrical properties relating to the morphology of the printing products. This study observed the controlling morphology through parameter adjustment and confirmed how it affects the final electrical conductivity. It means that the quality of the electronic properties can be modified by adjusting several spray process parameters. Full article
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14 pages, 3928 KiB  
Article
Numerical Modeling and Simulation of Blood Flow in a Rat Kidney: Coupling of the Myogenic Response and the Vascular Structure
by Wei Deng and Ken-ichi Tsubota
Processes 2022, 10(5), 1005; https://doi.org/10.3390/pr10051005 - 18 May 2022
Cited by 1 | Viewed by 1830
Abstract
A numerical simulation was carried out to investigate the blood flow behavior (i.e., flow rate and pressure) and coupling of a renal vascular network and the myogenic response to various conditions. A vascular segment and an entire kidney vascular network were modeled by [...] Read more.
A numerical simulation was carried out to investigate the blood flow behavior (i.e., flow rate and pressure) and coupling of a renal vascular network and the myogenic response to various conditions. A vascular segment and an entire kidney vascular network were modeled by assuming one single vessel as a straight pipe whose diameter was determined by Murray’s law. The myogenic response was tested on individual AA (afferent artery)–GC (glomerular capillaries)–EA (efferent artery) systems, thereby regulating blood flow throughout the vascular network. Blood flow in the vascular structure was calculated by network analysis based on Hagen–Poiseuille’s law to various boundary conditions. Simulation results demonstrated that, in the vascular segment, the inlet pressure Pinlet and the vascular structure act together on the myogenic response of each individual AA–GC–EA subsystem, such that the early-branching subsystems in the vascular network reached the well-regulated state first, with an interval of the inlet as Pinlet = 10.5–21.0 kPa, whereas the one that branched last exhibited a later interval with Pinlet = 13.0–24.0 kPa. In the entire vascular network, in contrast to the Pinlet interval (13.0–20.0 kPa) of the unified well-regulated state for all AA–GC–EA subsystems of the symmetric model, the asymmetric model exhibited the differences among subsystems with Pinlet ranging from 12.0–17.0 to 16.0–20.0 kPa, eventually achieving a well-regulated state of 13.0–18.5 kPa for the entire kidney. Furthermore, when Pinlet continued to rise (e.g., 21.0 kPa) beyond the vasoconstriction range of the myogenic response, high glomerular pressure was also related to vascular structure, where PGC of early-branching subsystems was 9.0 kPa and of late-branching one was 7.5 kPa. These findings demonstrate how the myogenic response regulates renal blood flow in vascular network system that comprises a large number of vessel elements. Full article
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13 pages, 3121 KiB  
Article
Design and Experimental Verification on Performance of a Novel Integrated Electro-Hydraulic Vane Pump
by Weiwei Yang, Yilin Wang, Yaodong Yang and Wenming Zhang
Appl. Sci. 2022, 12(10), 5006; https://doi.org/10.3390/app12105006 - 16 May 2022
Cited by 2 | Viewed by 1603
Abstract
The integrated electric-hydraulic pump has the advantages of no leakage, compact structure, and low noise. Here, we propose a novel integrated electric-hydraulic vane pump (IEHVP) to solve the problem of low reliability of the existing ordinary axially arranged hydraulic oil source in the [...] Read more.
The integrated electric-hydraulic pump has the advantages of no leakage, compact structure, and low noise. Here, we propose a novel integrated electric-hydraulic vane pump (IEHVP) to solve the problem of low reliability of the existing ordinary axially arranged hydraulic oil source in the harsh deep-sea environments. IEVP combines an external-rotor brushless motor and a balanced vane pump. In order to obtain the external characteristic curve of the designed IEHVP, the theoretical analysis of coupling analysis between the operating characteristics of the electric motor and the vane pump is designed. The results reveal that the output flow of the proposed IEHVP increases linearly with the increase of the input voltage and decreases non-linearly as the outlet pressure increase. Finally, the proposed IEHVP is tested. The relationship between the output flow and volumetric efficiency and its outlet pressure and input voltage is obtained. The experimental results verify the characteristics of the proposed IEHVP design. Full article
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11 pages, 2455 KiB  
Article
Nanomechanical Characterization of Bacterial Polyhydroxyalkanoates Using Atomic Force Microscopy
by Simone Bagatella, Riccardo Ciapponi and Stefano Turri
Appl. Sci. 2022, 12(10), 4994; https://doi.org/10.3390/app12104994 - 15 May 2022
Cited by 1 | Viewed by 2025
Abstract
Polyhydroxyalkanoates are a promising class of biopolymers that can allow the production of sustainable plastic materials. The mechanical properties of such materials are very important for possible industrial applications, but the amount of polymer required for common mechanical testing can be orders of [...] Read more.
Polyhydroxyalkanoates are a promising class of biopolymers that can allow the production of sustainable plastic materials. The mechanical properties of such materials are very important for possible industrial applications, but the amount of polymer required for common mechanical testing can be orders of magnitude more than what is possible to achieve with a lab-scale process. Nanoindentation with the Atomic Force Microscope allows an estimation of the Elastic Modulus that can be used as a preliminary measurement on PHA when only a limited amount of material is available. Poly(hydroxybutyrate-co-hydroxyvalerate) copolymers were analyzed, with moduli ranging from 528 ± 62 MPa to 1623 ± 172 MPa, according to both the composition and the crystallization kinetics. Full article
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18 pages, 6618 KiB  
Article
Dry Sliding Wear and Corrosion Performance of Mg-Sn-Ti Alloys Produced by Casting and Extrusion
by Davoud Bovand, Hassan Abdollah-Pour, Omid Mirzaee and Sara Bagherifard
Materials 2022, 15(10), 3533; https://doi.org/10.3390/ma15103533 - 14 May 2022
Cited by 3 | Viewed by 1484
Abstract
The aim of the present study is to investigate the role of Ti on corrosion and the wear properties of Mg-5Sn-xTi (x = 0, 0.15, 0.75, 1.5 wt.%) alloys. The samples were fabricated by conventional casting followed by hot extrusion, and the studies [...] Read more.
The aim of the present study is to investigate the role of Ti on corrosion and the wear properties of Mg-5Sn-xTi (x = 0, 0.15, 0.75, 1.5 wt.%) alloys. The samples were fabricated by conventional casting followed by hot extrusion, and the studies were examined by means of a pin-on-disc tribometer at various loads of 6, 10, and 20 N with constant sliding velocities of 0.04 m/s at ambient temperature. The corrosion performance, using potentiodynamic polarization and electrochemical impedance spectroscopy (EIS), was studied in a basic solution containing 3.5 wt.% NaCl. The observation indicated a drop in the wear rate with an increase in Ti, while the average coefficient of friction was raised in higher Ti contents compared to the base material. The sample with 0.75 wt.% Ti exhibited superior wear properties at 6 and 10 N of normal force, while the sample with 0.15 wt.% Ti presented better wear resistance for 20 N. Electrochemical test observations demonstrated that the Ti deteriorated the corrosion features of the Mg-5Sn alloy, owing to the galvanic effects of Ti. The Mg-5Sn alloy exhibited excellent corrosion behavior (corrosion potential (Ecorr) = −1.45V and current density (Icorr) = 43.92 A/cm2). The results indicated the significant role of Ti content in modulating wear and corrosion resistance of the Mg-5Sn alloy. Full article
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11 pages, 3004 KiB  
Article
Characteristic of Precipitate Evolution during High Temperature Annealing in Grain-Oriented Silicon Steel
by Qian Gao, Jun Li, Xianhui Wang, Jian Gong and Bo Li
Metals 2022, 12(5), 824; https://doi.org/10.3390/met12050824 - 11 May 2022
Cited by 1 | Viewed by 1513
Abstract
Precipitate evolution during high temperature annealing plays an important role in the magnetic property of grain-oriented silicon steel but was rarely studied. Aluminum was one of the important components of precipitates. Grain-oriented silicon steels with three levels of aluminum content were prepared and [...] Read more.
Precipitate evolution during high temperature annealing plays an important role in the magnetic property of grain-oriented silicon steel but was rarely studied. Aluminum was one of the important components of precipitates. Grain-oriented silicon steels with three levels of aluminum content were prepared and the interrupted extraction experiments were carried out. The results showed that during high temperature annealing, the precipitates were polygonal with the main composition of (Al,Si)N. Both the distribution density and volume fraction of precipitates showed first increasing and then decreasing tendencies, while the precipitate size remained approximately constant at first and then increased. Aluminum had a significant effect on the density and volume fraction of precipitates, which resulted in different secondary recrystallization structures. A small amount of aluminum with 0.015 wt.% led to low precipitate density, resulting in a low onset secondary recrystallization temperature as well as a Goss texture with large deviation angles. With the aluminum content of 0.025 wt.%, the secondary recrystallization was developed exactly right in the optimum temperature range, resulting in a perfect magnetic property. When the aluminum content was overcommitted to 0.035 wt.%, Goss grains could not show the preferential growth advantage and the secondary recrystallization structure could not be well developed. Full article
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14 pages, 5901 KiB  
Article
Numerical Simulation Experimental Study of the Deformation and Failure of Granite with Multiaxial Tension
by Lang Zhou, Zhenqian Ma, Hongfei Xie, Wei Yang and Hanghang Zheng
Processes 2022, 10(5), 949; https://doi.org/10.3390/pr10050949 - 10 May 2022
Cited by 2 | Viewed by 1349
Abstract
A numerical simulation method is proposed to study the deformation and failure rule of granite with multi-directional tensile stress, based on the importance of the rock tension. This investigation took into consideration the fact that the current experimental equipment cannot complete multi-directional tension [...] Read more.
A numerical simulation method is proposed to study the deformation and failure rule of granite with multi-directional tensile stress, based on the importance of the rock tension. This investigation took into consideration the fact that the current experimental equipment cannot complete multi-directional tension experiments for rock. The deformation and failure rule of the granite material model with biaxial and triaxial tensile stress are studied using the numerical simulation software CASRock. The results show that in a biaxial tensile stress state, the tensile strength of granite decreases with the increase in the confining pressure, but the influence of the compression confining pressure on the strength reduction is greater than the tensile confining pressure. The number of cracks generated during failure decreases with the increase in the compressive confining pressure, and the inclination angle of the failure surface increases with the increase in the compressive confining pressure. In the three-direction tension stress state, the tensile strength of granite decreases slightly with the increase in the compressive confining pressure. However, when the compressive confining pressure in one direction is close to the uniaxial tensile strength, the tensile strength of granite will decrease quickly, and the failure result is similar to that of the uniaxial tensile failure. Full article
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19 pages, 11908 KiB  
Article
Effect of Grain Size on Mechanical and Creep Rupture Properties of 253 MA Austenitic Stainless Steel
by Mochammad Syaiful Anwar, Robert R. Widjaya, Leonardo Bayu Adi Prasetya, Abdul Aziz Arfi, Efendi Mabruri and Eddy S. Siradj
Metals 2022, 12(5), 820; https://doi.org/10.3390/met12050820 - 10 May 2022
Cited by 4 | Viewed by 2632
Abstract
The effect of grain size on the mechanical properties and creep rupture of 253 microalloyed (MA) austenitic stainless steel (ASS) was investigated. The cold rolling process with a 53% reduction in thickness was applied to the steel followed by annealing at 1100 °C [...] Read more.
The effect of grain size on the mechanical properties and creep rupture of 253 microalloyed (MA) austenitic stainless steel (ASS) was investigated. The cold rolling process with a 53% reduction in thickness was applied to the steel followed by annealing at 1100 °C over 0, 900, 1800, and 3600 s to obtain grain sizes of 32.4, 34.88, 40.35, and 43.77 µm, respectively. Uniaxial tensile and micro-Vickers hardness tests were carried out to study the effect of grain size on mechanical properties at room temperature. The creep rupture test was performed at 700 °C under a load of 150 MPa. The results showed that there was a correlation between grain size, mechanical properties, and creep rupture time. The fine initial grain size showed relatively good mechanical properties with a short creep rupture time, while the coarse initial grain size produced low mechanical properties with a long creep rupture time. The initial grain size of 40.35 µm was the optimum grain size for a high value of creep rupture time due to the low hardness and elongation values at room temperature and low creep ductility value. The intergranular fracture was found on the initial grain size below 40.35 µm, and a mixed mode of intergranular and transgranular fracture was found on the initial grain size above 40.35 µm after the creep rupture test. Full article
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26 pages, 7029 KiB  
Article
Bending Behavior of a Frictional Single-Layered Spiral Strand Subjected to Multi-Axial Loads: Numerical and Experimental Investigation
by Biwen Zhou, Yumei Hu, Xingyuan Zheng and Hao Zhu
Appl. Sci. 2022, 12(9), 4792; https://doi.org/10.3390/app12094792 - 09 May 2022
Cited by 3 | Viewed by 1778
Abstract
Bending deformation gives rise to interwire slippage for spiral strands subjected to multi-axial loads, and further induces wear or fatigue phenomena in practice. The interwire friction would resist bending deformation and lead to uneven tension distribution of individual constituent wires but little research [...] Read more.
Bending deformation gives rise to interwire slippage for spiral strands subjected to multi-axial loads, and further induces wear or fatigue phenomena in practice. The interwire friction would resist bending deformation and lead to uneven tension distribution of individual constituent wires but little research has quantified these effects. To figure out this issue, a beam finite element (FE) is established, into which a penalty stiffness algorithm and a Coulomb friction model are incorporated. A series of free bending simulations are developed for parametric study on deflection near the terminations and tension distribution of individual wire for strands with different levels of length and friction coefficient as well as external loads. Based on the simulation results, it is found that strand length has little influence on bending deformation and tension distribution if the strand length exceeds six times the pitch length. A deflection formula extended from the classical Euler beam model well predicts the sag deflections and the relative error with respect to experimental measurements is less than 10%. Furthermore, additional axial tension induced by the friction is clearly characterized and an approximate expression is proposed to estimate tension distribution for outer layer wires. Its predictions are encouraging for longer strands. Full article
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14 pages, 8670 KiB  
Article
Numerical Investigation on the Flow-Induced Vibration Characteristics of Fire Turbopump with the Turbine-Pump Structure
by Ye Yuan, Rong Jin and Lingdi Tang
Appl. Sci. 2022, 12(9), 4650; https://doi.org/10.3390/app12094650 - 06 May 2022
Cited by 1 | Viewed by 1343
Abstract
The vibration characteristics induced by radial hydraulic force on the fire turbopump have been investigated by numerical simulations in this paper. The numerical model was validated with corresponding experimental measurements. The turbopump has the special structure with two hydraulic machineries of a turbine [...] Read more.
The vibration characteristics induced by radial hydraulic force on the fire turbopump have been investigated by numerical simulations in this paper. The numerical model was validated with corresponding experimental measurements. The turbopump has the special structure with two hydraulic machineries of a turbine and a pump. The hydraulic force characteristics on the separate turbine and the separate pump were first studied. There is one period in the force variation for one cycle of impeller rotation, and pressure fluctuations are observed in 15 times and 30 times the shaft rotating frequency of the turbine. Meanwhile, there are five periods in the force fluctuation in one full working cycle, and obvious fluctuation amplitudes on 5 times, 10 times and 15 times the shaft rotating frequency of the pump are found. Then, the coupled effect of force fluctuations on the turbine and pump was explored. For the turbopump, the periodicity of force fluctuation in the time domain and force characteristics in the frequency domain are dominated by pump structure. The hydraulic force fluctuation on the impeller is enhanced, while that on the housing is damped by counteracting the forces between turbine suction and pump volute. Full article
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14 pages, 5387 KiB  
Article
Study on Influencing Factors of High-Temperature Basic Characteristics of Iron Ore Powder and Optimization of Ore Blending
by Shuangping Yang, Haijin Liu, Haixing Sun, Tiantian Zhang and Shouman Liu
Materials 2022, 15(9), 3329; https://doi.org/10.3390/ma15093329 - 06 May 2022
Cited by 5 | Viewed by 1466
Abstract
In order to explore the reasonable ore blending of low-silicon magnetite in sintering, it I necessary to realize the efficient utilization of low-silicon ore, further reduce cost, and increase yield. In this study, based on the high-temperature basic characteristics of iron ore powder [...] Read more.
In order to explore the reasonable ore blending of low-silicon magnetite in sintering, it I necessary to realize the efficient utilization of low-silicon ore, further reduce cost, and increase yield. In this study, based on the high-temperature basic characteristics of iron ore powder used in the experiment, sinter pot tests were carried out with different low-silicon ore ratios, and the microstructure of the sinter was observed by scanning electron microscopy (SEM) and energy spectrum analysis (EDS) to determine the optimal matching law of low-silicon ore. The result showed that SiO2, Al2O3, and burning loss in iron ore powder composition were positively correlated with its assimilation, whereas MgO and basicity R2 were negatively correlated with the assimilation of iron ore powder. When the ratio of low-silicon ore was not more than 35%, increasing the ratio of hematite improved the liquid production and increased the production of acicular calcium ferrite. Therefore, the optimization of ore blending based on assimilation can improve the quality of sinter and strengthen the sintering process. This study has certain reference significance for the industrial production of low-silica sintering. Full article
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9 pages, 7614 KiB  
Article
Effect of Niobium Content on the Microstructure and Mechanical Properties of Simulated Coarse-Grained Heat-Affected Zone (CGHAZ) of High-Strength Low-Alloy (HSLA) Steels
by Hongwei Yu, Kaiming Wu, Baoqi Dong, Liling Yu, Jingxi Liu, Zicheng Liu, Daheng Xiao, Xing Jing and Hankun Liu
Materials 2022, 15(9), 3318; https://doi.org/10.3390/ma15093318 - 05 May 2022
Cited by 4 | Viewed by 1591
Abstract
The effect of Nb-content and heat input rate on the mechanical properties and microstructure of simulated coarse-grained heat-affected zone (CGHAZ) of high-strength low-alloy steel (HSLA) was investigated. While using a low heat input (20 kJ/cm), the toughness of simulated CGHAZ was improved by [...] Read more.
The effect of Nb-content and heat input rate on the mechanical properties and microstructure of simulated coarse-grained heat-affected zone (CGHAZ) of high-strength low-alloy steel (HSLA) was investigated. While using a low heat input (20 kJ/cm), the toughness of simulated CGHAZ was improved by increasing the Nb-content. The maximum toughness was obtained when the Nb-content was 0.110 wt.% and the heat input was 20 kJ/cm. The samples made at this condition had fine martensite/austenite (M/A-constituent), acicular ferrite and refined austenite grains. As the heat input was increased to 200 kJ/cm, the toughness of simulated CGHAZ was significantly decreased irrespective of the Nb-content because of the formation of coarse austenite grains, low angle grain boundaries, and massive M/A-constituents. Full article
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14 pages, 1458 KiB  
Article
Evaluation of Circumferential Mechanical Properties of Tubular Material by Flaring Test
by Zicheng Zhang, Bin Li, Ken-Ichi Manabe and Hideki Sato
Metals 2022, 12(5), 764; https://doi.org/10.3390/met12050764 - 29 Apr 2022
Cited by 2 | Viewed by 1669
Abstract
The investigation into the circumferential mechanical properties of tubular materials has been receiving increasing attention, since the tube hydroforming process has been used in the tubular materials forming field, because the circumferential mechanical properties have a significant effect on the hydroformability of the [...] Read more.
The investigation into the circumferential mechanical properties of tubular materials has been receiving increasing attention, since the tube hydroforming process has been used in the tubular materials forming field, because the circumferential mechanical properties have a significant effect on the hydroformability of the tubular materials. In the present study, a method for evaluation of the circumferential mechanical properties of the tubular materials with the flaring test was proposed. The expressions for the yield stress, strain hardening coefficient and exponent values of the tube were successfully derived based on the geometrical and mechanical relationships in the tube flaring test. To verify the reliability of this method, the calculated results of the yield stress, strain hardening coefficient and exponent values, obtained from the newly proposed method, were compared to the ones obtained with the conventional tensile tests. It was found that the method proposed in the current study is reliable, with high accuracy. The method is appropriate to evaluate the circumferential mechanical properties of the tubular materials. Full article
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14 pages, 3161 KiB  
Article
Explicit Analysis of Nonuniform Irradiation Swelling Pressure Exerting on Dispersion Fuel Matrix Based on the Equivalent Inclusion Method
by Yingxuan Dong, Junnan Lv, Hong Zuo and Qun Li
Materials 2022, 15(9), 3231; https://doi.org/10.3390/ma15093231 - 29 Apr 2022
Cited by 1 | Viewed by 1244
Abstract
Under irradiation, dispersion nuclear fuel meat consists of a three-phase composite of fuel particles surrounded by an interaction layer dispersed within a metal matrix. Nonuniform swelling pressures are exerted on the matrix, generated by irradiation swelling of the fuel particles. As these are [...] Read more.
Under irradiation, dispersion nuclear fuel meat consists of a three-phase composite of fuel particles surrounded by an interaction layer dispersed within a metal matrix. Nonuniform swelling pressures are exerted on the matrix, generated by irradiation swelling of the fuel particles. As these are considerable, they can cause matrix failure, but they are difficult to calculate. In this paper, taking into account thermal expansion, nonuniform fission pores and the interaction layer, nonuniform irradiation swelling pressure has been formulated, based on the equivalent inclusion method. By means of doubly equivalent transformations, a porous fuel particle, surrounded by an interaction layer, which is under irradiation, can be simplified as a homogeneous particle with the eigenstrain. With the aid of Green’s function, nonuniform irradiation swelling pressure can be numerically analyzed. The simulation results of swelling pressures are in good agreement with numerical calculations. Furthermore, several simplified examples have been given to investigate the factors of influence and the impact mechanisms. Conclusions are drawn that nonuniform irradiation swelling pressure can be analyzed numerically and adopted to explore matrix failure. It is identified that the number and locations of fission pores inside a fuel particle are key factors for nonuniformity of swelling pressures. The volatility of swelling pressures is aggravated by burnup, while the average values of swelling pressures are intensely affected by temperature. This work provides a perspective to investigate the strength and integrity of dispersion fuel meat under high burnup. Full article
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16 pages, 5808 KiB  
Article
Flow Analysis of PM/NOX Aftertreatment System for Emergency Generator
by Giyoung Park, Hyowon Bang and Seangwock Lee
Appl. Sci. 2022, 12(9), 4404; https://doi.org/10.3390/app12094404 - 27 Apr 2022
Cited by 1 | Viewed by 1447
Abstract
Emergency generators normally use diesel engines. The generators need to conduct weekly no-load operation inspections to ensure stable performance in emergency situations. In particular, the generators with large diesel engines mainly use rectangle-type filter substrates. To minimize hazardous emissions generated by generators, optimizing [...] Read more.
Emergency generators normally use diesel engines. The generators need to conduct weekly no-load operation inspections to ensure stable performance in emergency situations. In particular, the generators with large diesel engines mainly use rectangle-type filter substrates. To minimize hazardous emissions generated by generators, optimizing the reduction efficiency through computational fluid dynamics (CFD) analysis of flow characteristics of particulate matter (PM)/NOX reduction system is important. In this study, we analyzed internal flow by CFD, which is difficult to confirm by experimental method. The main factors in our numerical study are the changes of flow uniformity and back pressure. As a result, the flow distribution characteristics according to the cross-sectional shape are similar at high engine loads. Spraying urea in the reverse direction increases static pressure, greatly improving flow uniformity. Raising the selective catalyst reduction (SCR) diffuser angle to 30 degrees improves both back pressure and flow uniformity characteristics, and when the porosity increases, both flow uniformity and back pressure decrease. Full article
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14 pages, 6529 KiB  
Article
Temperature Load Mode of Bridge in Permafrost Region of Qinghai–Tibet Railway
by Bin Yan, Ruiqi Cheng, Haoran Xie and Xiangmin Zhang
Appl. Sci. 2022, 12(9), 4377; https://doi.org/10.3390/app12094377 - 26 Apr 2022
Cited by 2 | Viewed by 1482
Abstract
The Qinghai–Tibet railway is the plateau permafrost railway with the highest altitude and the longest line in the world. The natural conditions along the line are harsh, with many unfavorable factors such as low temperature, strong ultraviolet radiation, and large changes in daily [...] Read more.
The Qinghai–Tibet railway is the plateau permafrost railway with the highest altitude and the longest line in the world. The natural conditions along the line are harsh, with many unfavorable factors such as low temperature, strong ultraviolet radiation, and large changes in daily temperature, resulting in frequent bridge damage. In order to study the bridge temperature field and its effect in the permafrost region of the Qinghai–Tibet railway, a long-term field test was carried out, and a calculation model of sunshine temperature field of concrete two-piece T-beam was established based on the principle of meteorology and heat transfer. On this basis, the beam temperature difference load mode, beam section temperature distribution law, and temperature effect were obtained. As revealed, the daily temperature difference of the Qinghai–Tibet railway bridge is large in winter, which is related to the ground’s effective radiation and surface reflectivity, and the maximum value has exceeded the current codes. The beam section temperature field shows “internal heat and external cold” in the morning and “internal cold and external heat” from noon to evening. Under the action of strong radiation and large temperature difference, bridge displacement occurs frequently, by which it is easy to cause damage to rail fasteners and bridge bearings. Based on the field test and finite element analysis, the bridge temperature difference load mode was proposed, which makes up for the deficiency that the relevant codes do not consider the plateau’s special climatic conditions and can provide a reference for the construction of plateau railways such as the Sichuan–Tibet railway. Full article
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14 pages, 6866 KiB  
Article
Prediction of Hardenability Curves for Non-Boron Steels via a Combined Machine Learning Model
by Xiaoxiao Geng, Shuize Wang, Asad Ullah, Guilin Wu and Hao Wang
Materials 2022, 15(9), 3127; https://doi.org/10.3390/ma15093127 - 26 Apr 2022
Cited by 6 | Viewed by 2420
Abstract
Hardenability is one of the most basic criteria influencing the formulation of the heat treatment process and steel selection. Therefore, it is of great engineering value to calculate the hardenability curves rapidly and accurately without resorting to any laborious and costly experiments. However, [...] Read more.
Hardenability is one of the most basic criteria influencing the formulation of the heat treatment process and steel selection. Therefore, it is of great engineering value to calculate the hardenability curves rapidly and accurately without resorting to any laborious and costly experiments. However, generating a high-precision computational model for steels with different hardenability remains a challenge. In this study, a combined machine learning (CML) model including k-nearest neighbor and random forest is established to predict the hardenability curves of non-boron steels solely on the basis of chemical compositions: (i) random forest is first applied to classify steel into low- and high-hardenability steel; (ii) k-nearest neighbor and random forest models are then developed to predict the hardenability of low- and high-hardenability steel. Model validation is carried out by calculating and comparing the hardenability curves of five steels using different models. The results reveal that the CML model works well for its distinguished prediction performance with precise classification accuracy (100%), high correlation coefficient (≥0.981), and low mean absolute errors (≤3.6 HRC) and root-mean-square errors (≤3.9 HRC); it performs better than JMatPro and empirical formulas including the ideal critical diameter method and modified nonlinear equation. Therefore, this study demonstrates that the CML model combining material informatics and data-driven machine learning can rapidly and efficiently predict the hardenability curves of non-boron steel, with high prediction accuracy and a wide application range. It can guide process design and machine part selection, reducing the cost of trial and error and accelerating the development of new materials. Full article
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13 pages, 4358 KiB  
Article
Polymeric Structure Evolution Behavior Analysis of Aluminosilicate-Based Smelting Slag
by Jihui Liu, Weiguo Kong, Xin Yang, Qi Wang, Zhijun He and Xinmei Hou
Metals 2022, 12(5), 715; https://doi.org/10.3390/met12050715 - 22 Apr 2022
Cited by 1 | Viewed by 1242
Abstract
The physical and chemical properties of the CaO–SiO2–Al2O3–MgO slag system depend on structure evolution caused by the synergistic mechanism among the components at high temperature, especially the structural complexity of the anion group. In this study, Si–O, [...] Read more.
The physical and chemical properties of the CaO–SiO2–Al2O3–MgO slag system depend on structure evolution caused by the synergistic mechanism among the components at high temperature, especially the structural complexity of the anion group. In this study, Si–O, Al–O, and Al–Si–O anion groups were found in the high-temperature slag systems at 1773 K. The [Si2O5]2− (Q3) structural unit of the silicate polymer changed to [Si2O6]4− (Q2), [Si2O7]6− (Q1), and [SiO4]4− (Q0) as the binary basicity (R2) and ω(MgO)/ω(Al2O3) increased, while there was a trend toward a simplified structure. That is, the stability of each structural unit weakened, and the relative content of non-bridging oxygen increased. As a result, the degree of polymerization of slag decreased, and the experimental results of the relative content of non-bridge oxygen can be fitted well with the calculations from the reference documents. At the same time, the number of Si–O–Al structural units gradually decreased. The 27Al-MAS-NMR spectroscopy results showed that the structure of aluminate changed from [AlO4]5− tetrahedral structure to [AlO5]7− pentahedral and [AlO6]9− octahedral structure, and the degree of polymerization of the slag decreased. Comprehensive analysis showed that basicity controlled within 1.2 with the ω(MgO)/ω(Al2O3) ratio; less than 0.55 allows for suitable fluidity and energy-saving ability, which is beneficial for the stable and smooth production of the blast furnace. Full article
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14 pages, 1959 KiB  
Article
Young’s Modulus Calculus Using Split Hopkinson Bar Tests on Long and Thin Material Samples
by Adrian-Nicolae Rotariu, Eugen Trană and Liviu Matache
Materials 2022, 15(9), 3058; https://doi.org/10.3390/ma15093058 - 22 Apr 2022
Cited by 3 | Viewed by 1482
Abstract
Young’s modulus is a key parameter of materials. The method of its calculation in the current paper is concerned with the mismatch of the mechanical impedance at the bar/specimen interface for a compression SHPB (split Hopkinson pressure bar) test. By using long and [...] Read more.
Young’s modulus is a key parameter of materials. The method of its calculation in the current paper is concerned with the mismatch of the mechanical impedance at the bar/specimen interface for a compression SHPB (split Hopkinson pressure bar) test. By using long and thin specimens, the signal recorded in the transmission bar presents itself as a multistep signal. The ratio between the heights of two successive steps represents the experimental data that are considered in the formula of the elastic modulus this article is devoted to. The oscillatory nature of the real signals on the horizontal or quasi-horizontal segments prevents a precise determination of the two successive step heights ratio. A fine tuning of this value is made based on the characteristic time necessary for the signal to rise from one level to the next one. The FEM (Finite Element Method) simulations are also used in calculation of the Poisson coefficient of the tested complex concentrated alloy. Full article
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12 pages, 5463 KiB  
Article
Deep Cryogenic Treatment Characteristics of a Deformation-Processed Cu-Ni-Co-Si Alloy
by Keming Liu, Xiaochun Sheng, Xiaolong Li, Mulin Li, Zhi Shen, Kai Fu, Haitao Zhou and Andrej Atrens
Materials 2022, 15(9), 3051; https://doi.org/10.3390/ma15093051 - 22 Apr 2022
Cited by 2 | Viewed by 1368
Abstract
This paper investigated the influence of deep cryogenic treatments (DCT) on the tensile strength, elongation to fracture and conductivity of a deformation-processed Cu-Ni-Co-Si alloy. The tensile properties were measured using a mechanical testing machine. The conductivity was evaluated using a low-resistance tester. The [...] Read more.
This paper investigated the influence of deep cryogenic treatments (DCT) on the tensile strength, elongation to fracture and conductivity of a deformation-processed Cu-Ni-Co-Si alloy. The tensile properties were measured using a mechanical testing machine. The conductivity was evaluated using a low-resistance tester. The microstructure and precipitated phases were analyzed using scanning electron microscopy (SEM), transmission electron microscopy (TEM), an energy dispersive spectrometer (EDS) and an X-ray diffractometer (XRD). The tensile strength, elongation to fracture and conductivity of the Cu-1.34Ni-1.02Co-0.61Si alloy before and after cold rolling at 47% reduction increased with increasing DCT time and tended to be stable at about 36 h. The microstructure became more uniform after the DCT. The grain size was refined and was smallest after DCT for 48 h. The DCT promoted the precipitation of the solid solution elements Ni, Co and Si from the Cu matrix to form many fine and evenly distributed 20–70 nm spherical second-phase particles in the grains and grain boundaries. Full article
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19 pages, 5652 KiB  
Article
A Multi-Scale Simulation Study of Irradiation Swelling of Silicon Carbide
by Chunyu Yin, Baoqin Fu, Yongjun Jiao, Zhengang Duan, Lei Wu, Yu Zou and Shichao Liu
Materials 2022, 15(9), 3008; https://doi.org/10.3390/ma15093008 - 21 Apr 2022
Viewed by 1653
Abstract
Silicon carbide (SiC) is a promising structural and cladding material for accident tolerant fuel cladding of nuclear reactor due to its excellent properties. However, when exposed to severe environments (e.g., during neutron irradiation), lattice defects are created in amounts significantly greater than normal [...] Read more.
Silicon carbide (SiC) is a promising structural and cladding material for accident tolerant fuel cladding of nuclear reactor due to its excellent properties. However, when exposed to severe environments (e.g., during neutron irradiation), lattice defects are created in amounts significantly greater than normal concentrations. Then, a series of radiation damage behaviors (e.g., radiation swelling) appear. Accurate understanding of radiation damage of nuclear materials is the key to the design of new fuel cladding materials. Multi-scale computational simulations are often required to understand the physical mechanism of radiation damage. In this work, the effect of neutron irradiation on the volume swelling of cubic-SiC film with 0.3 mm was studied by using the combination of molecular dynamics (MD) and rate theory (RT). It was found that for C-vacancy (CV), C-interstitial (CI), Si-vacancy (SiV), Si-interstitial (SiI), and Si-antisite (SiC), the volume of supercell increases linearly with the increase of concentration of these defects, while the volume of supercell decreases linearly with the increase of defect concentration for C-antisite (CSi). Furthermore, according to the neutron spectrum of a certain reactor, one RT model was constructed to simulate the evolution of point defect under neutron irradiation. Then, the relationship between the volume swelling and the dose of neutrons can be obtained through the results of MD and RT. It was found that swelling typically increases logarithmically with radiation dose and saturates at relatively low doses, and that the critical dose for abrupt transition of volume is consistent with the available experimental data, which indicates that the rate theory model can effectively describe the radiation damage evolution process of SiC. This work not only presents a systematic study on the relationship between various point defect and excess volume, but also gives a good example of multi-scale modelling through coupling the results of binary collision, MD and RT methods, etc., regardless of the multi-scale modelling only focus on the evolution of primary point defects. Full article
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19 pages, 5051 KiB  
Article
Dynamic Analysis on the Parametric Resonance of the Tower–Multicable–Beam Coupled System
by Shuanhai He, Kefan Chen, Yifan Song, Binxian Wang, Kang Wang and Wei Hou
Appl. Sci. 2022, 12(9), 4095; https://doi.org/10.3390/app12094095 - 19 Apr 2022
Cited by 3 | Viewed by 1402
Abstract
Considering the effect of the bridge deck’s bending stiffness and the indirect effect of adjacent cables (CEB), this paper aims to propose a refined model to reliably analyze the complex internal resonance mechanism of the tower–multicable–beam coupled system (MCS) under nonlinear geometric conditions. [...] Read more.
Considering the effect of the bridge deck’s bending stiffness and the indirect effect of adjacent cables (CEB), this paper aims to propose a refined model to reliably analyze the complex internal resonance mechanism of the tower–multicable–beam coupled system (MCS) under nonlinear geometric conditions. To accurately analyze the dynamic behavior, the shear difference effect is applied to simulate the continuous rigidity of the single beam. The dynamic equations of the whole resonance system are derived based on the D’Alembert Principle and the Finite Difference Method, the Galerkin Method and verified by the case study. The results of the numerical simulation based on the Fourth Runge–Kutta Method show that the dynamic parameter of each component is closely related to the coupled resonance of the system. The dynamic behavior under two conditions, tower–cable 1:1 resonance (TCR) or cable–beam 1:2 resonance (CBR), is deeply analyzed. Additionally, the excitation effect of the maximum amplitude by two excitation approaches, the initial displacement or initial velocity, both show a linear increase. The mutual transmission process of vibration excitation on the cable through the bridge beam or the tower as the medium is also further discussed. Full article
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20 pages, 4698 KiB  
Article
Flux-Barrier Design and Torque Performance Analysis of Synchronous Reluctance Motor with Low Torque Ripple
by Jing Liang, Yan Dong, Hexu Sun, Rongzhe Liu and Guantong Zhu
Appl. Sci. 2022, 12(8), 3958; https://doi.org/10.3390/app12083958 - 14 Apr 2022
Cited by 9 | Viewed by 2567
Abstract
In this paper, an improved rotor structure with cross-shaped flux-barriers was proposed to improve the torque output capacity and reduce the torque ripple of the synchronous reluctance motor (SynRM). Firstly, an improved rotor structure of synchronous reluctance motor with cross-shaped flux-barriers, which can [...] Read more.
In this paper, an improved rotor structure with cross-shaped flux-barriers was proposed to improve the torque output capacity and reduce the torque ripple of the synchronous reluctance motor (SynRM). Firstly, an improved rotor structure of synchronous reluctance motor with cross-shaped flux-barriers, which can be described by two main parameters, is presented. Second, the improved motor is qualitatively analyzed by using magnetic equivalent circuit (MEC), and then the effects of the main parameters of the improved flux-barriers on the distribution of air-gap flux density, average torque, and torque ripple were analyzed by using the finite element method. Based on the above analysis, the rotor structure parameters of the proposed cross-shaped flux-barriers were obtained, and the performance was compared with that of the initial motor. The results show that the proposed rotor structure with cross-shaped flux-barriers can significantly reduce the torque ripple and increase the average torque. Full article
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12 pages, 5132 KiB  
Article
Tensile Test Coupled with an EBSD Study of a GH4169 Ring Rolled Product
by Hao Wang, Haoyi Niu, Hao Wu, Rengeng Li and Guohua Fan
Materials 2022, 15(8), 2891; https://doi.org/10.3390/ma15082891 - 14 Apr 2022
Cited by 3 | Viewed by 1754
Abstract
An in situ tensile test of the ring-rolled GH4169 alloy is performed to investigate the plastic deformation behavior at the micro level. Slip system activations are identified by slip traces captured by a scanning electron microscope and lattice orientation data acquired by electron [...] Read more.
An in situ tensile test of the ring-rolled GH4169 alloy is performed to investigate the plastic deformation behavior at the micro level. Slip system activations are identified by slip traces captured by a scanning electron microscope and lattice orientation data acquired by electron backscattered diffraction. Our results demonstrated that the fraction of low-angle grain boundaries gradually increased upon tensile deformation, and the misorientation evolution in the grain interior was severely inhomogeneous. The Schmid factors at the grains of interest are calculated for comparison with the actual activated slip systems. Most of the slip system activation coincides with the Schmid law, as opposed to the initiation of other potential slip systems at some grains. Full article
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17 pages, 2806 KiB  
Review
Review on Zigzag Air Classifier
by Alexandra Kaas, Thomas Mütze and Urs A. Peuker
Processes 2022, 10(4), 764; https://doi.org/10.3390/pr10040764 - 13 Apr 2022
Cited by 17 | Viewed by 4175
Abstract
The zigzag (ZZ) classifier is a sorting and classification device with a wide range of applications (e.g. recycling, food industry). Due to the possible variation of geometry and process settings, the apparatus is used for various windows of operation due to the specifications [...] Read more.
The zigzag (ZZ) classifier is a sorting and classification device with a wide range of applications (e.g. recycling, food industry). Due to the possible variation of geometry and process settings, the apparatus is used for various windows of operation due to the specifications of the separation (e.g. cut sizes from 100 µm to several decimetres, compact and fluffy materials as well as foils). Since the ZZ classifier gains more and more interest in recycling applications, it is discussed in this paper, with regards to its design, mode of operation, influencing parameters and the research to date. Research on the ZZ-classifier has been ongoing on for more than 50 years and can be divided into mainly experimental studies and modelling approaches. Full article
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19 pages, 5253 KiB  
Article
On the Effects of Disc Deformation on the Tilting-Induced Vibration of a Spline-Guided Spinning Disc with an Axial-Fixed Boundary
by Jiaqi Xue, Biao Ma, Man Chen, Liang Yu and Liangjie Zheng
Appl. Sci. 2022, 12(7), 3637; https://doi.org/10.3390/app12073637 - 04 Apr 2022
Cited by 1 | Viewed by 1484
Abstract
This paper investigates the effects of disc deformation on the tilting-induced vibration of a splined spinning disc with axial-fixed boundaries.The purpose is to provide an intuitive interpretation of the vibration variance of the wet clutch system with different deformed discs. First, tilting models [...] Read more.
This paper investigates the effects of disc deformation on the tilting-induced vibration of a splined spinning disc with axial-fixed boundaries.The purpose is to provide an intuitive interpretation of the vibration variance of the wet clutch system with different deformed discs. First, tilting models of flat and deformed discs are derived by introducing distinctive shape functions. Additionally, the inner spline interface is chosen as the friction boundary. Then, an impact model between friction pairs and the rigid boundary is established by adopting Hertz’s contact theory. Finally, the dynamic equations are solved via numerical methods, and the responses are analyzed in both time and frequency domains. The deformation can increase the nonlinearity of the dynamic response of the spinning disc. Moreover, the effects of increasing the impulse force and reducing the boundary distance are quite similar; they both increase the motion intensity. Full article
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11 pages, 4690 KiB  
Article
Mechanical Characteristics of the Flebogrif System—The New System of Mechano-Chemical Endovenous Ablation
by Piotr Terlecki, Marek Boryga, Paweł Kołodziej, Krzysztof Gołacki, Zbigniew Stropek, Dariusz Janczak, Maciej Antkiewicz and Tomasz Zubilewicz
Materials 2022, 15(7), 2599; https://doi.org/10.3390/ma15072599 - 01 Apr 2022
Cited by 1 | Viewed by 1794
Abstract
Non-thermal endovenous ablations, due to the lowest probability of complications, are the new method of treating chronic venous insufficiency—one of the most common diseases globally. The Flebogrif system (Balton Sp. z o.o., Warsaw, Poland) is a new mechano-chemical ablation system causing the mechanical [...] Read more.
Non-thermal endovenous ablations, due to the lowest probability of complications, are the new method of treating chronic venous insufficiency—one of the most common diseases globally. The Flebogrif system (Balton Sp. z o.o., Warsaw, Poland) is a new mechano-chemical ablation system causing the mechanical damage of endothelium that allows for better sclerosant penetration into its wall. The purpose of the article is to provide mechanical characteristics in the form of force–displacement dependence for a single cutting element, and a bundle of cutting elements of Flebogrif as a whole for different levels of protrusion of the bundle of cutting elements. A TA.HD plus (Stable Micro Systems, Godalming, UK) analyzer equipped with special handles, was used for characteristics testing. The head movement speed used was 5 mm·s−1. The Flebogrif system was tested for three cutting element protrusion levels: L = Lmax, L = 0.9·Lmax, and L = 0.8·Lmax. Before testing, geometric measurement of the spacing of the cutting elements for three proposed protrusions was performed. It was established that decreasing the working length of the cutting elements will increase their rigidity, and, as a result, increase the force exerted on the internal surface of the vein wall. The obtained characteristics will allow for specifying contact force variability ranges and the corresponding diameter ranges of operated veins. Full article
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1 pages, 170 KiB  
Correction
Correction: Al-Qhtani et al. Half Metallic Ferromagnetism and Transport Properties of Zinc Chalcogenides ZnX2Se4 (X = Ti, V, Cr) for Spintronic Applications. Materials 2022, 15, 55
by Mohsen Al-Qhtani, Ghulam M. Mustafa, Nasheeta Mazhar, Sonia Bouzgarrou, Qasim Mahmood, Abeer Mera, Zaki I. Zaki, Nasser Y. Mostafa, Saad H. Alotaibi and Mohammed A. Amin
Materials 2022, 15(7), 2521; https://doi.org/10.3390/ma15072521 - 30 Mar 2022
Cited by 1 | Viewed by 1019
Abstract
In the original publication [...] Full article
15 pages, 4911 KiB  
Article
Temperature Estimation during Pulsed Laser Sintering of Silver Nanoparticles
by Arif Hussain, Hee-Lak Lee, Yoon-Jae Moon, Heuiseok Kang, Seung-Jae Moon and Jun-Young Hwang
Appl. Sci. 2022, 12(7), 3467; https://doi.org/10.3390/app12073467 - 29 Mar 2022
Cited by 10 | Viewed by 2061
Abstract
During the thermal sintering of metal nanoparticles (NPs) the process temperature plays the most important role in the outcome of the sintering results and the selection of a suitable substrate. Here, temperature calculation during pulsed laser sintering of silver (Ag) nanoparticles (NPs) inkjet-printed [...] Read more.
During the thermal sintering of metal nanoparticles (NPs) the process temperature plays the most important role in the outcome of the sintering results and the selection of a suitable substrate. Here, temperature calculation during pulsed laser sintering of silver (Ag) nanoparticles (NPs) inkjet-printed on glass substrates is presented. During the pulsed laser sintering of Ag NPs, a minimum line resistivity less than twice the bulk silver resistivity was obtained within around 52 s under a laser power of 276 mW. The temperature field during the pulsed laser sintering of Ag NPs was estimated via a three-dimensional numerical model in which a temperature-dependent thermal conductivity of Ag NPs was adopted. An algorithm for treating the thermal conductivity of the heated Ag NPs in a region by a previous laser shot was devised for the improvement of the temperature field estimation. A maximum temperature of approximately 204 °C over the Ag NPs line was obtained with a 276 mW laser power and a scanning speed of 135 μm/s. Full article
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16 pages, 9126 KiB  
Article
Simulation and Optimization of Connection-Strength Performance of Axial Extrusion Joint
by Jianguo Wu, Jingyu Zhai, Yangyang Yan, Hongwei Lin, Siquan Chen and Jianping Luo
Materials 2022, 15(7), 2433; https://doi.org/10.3390/ma15072433 - 25 Mar 2022
Viewed by 1653
Abstract
Axial extrusion-connection technology is one of the important connection technologies for hydraulic piping systems, with high sealing performance and mechanical strength. In this paper, the finite-element-modeling method is used to simulate the experimental process of the connection strength of the axial extrusion joint. [...] Read more.
Axial extrusion-connection technology is one of the important connection technologies for hydraulic piping systems, with high sealing performance and mechanical strength. In this paper, the finite-element-modeling method is used to simulate the experimental process of the connection strength of the axial extrusion joint. The generation mechanism and calculation method of the connection strength are analyzed. To optimize the joint strength, orthogonal testing and grey correlation analysis are used to analyze the influencing factors of joint strength. The key factors affecting joint strength are obtained as the friction coefficient μ1, μ2 between joint components and the groove angle θ1 of the fittings body. The back-propagation (BP) neural-network algorithm is used to establish the connection-strength model of the joint and the genetic algorithm is used to optimize it. The optimal connection strength is 8.237 kN and the optimal combination of influencing factors is 0.2, 0.4 and 76.8°. Compared with the prediction results of the neural-network genetic algorithm, the relative error of the finite-element results is 3.9%, indicating that the method has high accuracy. The results show that the extrusion-based joining process offers significant advantages in the manufacture of high-strength titanium tubular joints. Full article
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16 pages, 1829 KiB  
Review
A Comprehensive Review of Layered Double Hydroxide-Based Carbon Composites as an Environmental Multifunctional Material for Wastewater Treatment
by Yongxiang Huang, Chongmin Liu, Saeed Rad, Huijun He and Litang Qin
Processes 2022, 10(4), 617; https://doi.org/10.3390/pr10040617 - 22 Mar 2022
Cited by 14 | Viewed by 2612
Abstract
As is well known, hydrotalcite-like compounds, such as layered-double-hydroxide (LDH) materials, have shown great potential applications in many fields owing to their unique characteristics, including a higher anion exchange capacity, a structure memory effect, low costs, and remarkable recyclability. While the lower surface [...] Read more.
As is well known, hydrotalcite-like compounds, such as layered-double-hydroxide (LDH) materials, have shown great potential applications in many fields owing to their unique characteristics, including a higher anion exchange capacity, a structure memory effect, low costs, and remarkable recyclability. While the lower surface area and leaching of metal ions from LDH composites reduce the process efficiency of the catalyst, combining LDH materials with other materials can improve the surface properties of the composites and enhance the catalytic performance. Among organic compounds, carbon materials can be used as synergistic materials to overcome the defects of LDHs and provide better performance for environmental functional materials, including adsorption materials, electrode materials, photocatalytic materials, and separation materials. Therefore, this article comprehensively reviews recent works on the preparation and application of layered double-hydroxide-based carbon (LDH–C) composites as synergistic materials in the field of environmental remediation. In addition, their corresponding mechanisms are discussed in depth. Finally, some perspectives are proposed for further research directions on exploring efficient and low-cost clay composite materials. Full article
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23 pages, 5055 KiB  
Article
Theoretical Analysis Method of Variable Thickness GFRP Tray
by Jianjun Li, Zhaolong Du, Shaobo Geng, Wenmei Han, Yuxuan Wu and Hao Feng
Materials 2022, 15(7), 2346; https://doi.org/10.3390/ma15072346 - 22 Mar 2022
Cited by 1 | Viewed by 1332
Abstract
Glass-fiber reinforced polymer (GFRP) bars are increasingly widely used in slope support instead of steel bars or steel pipes. GFRP Bars are generally connected with the slope by combining conical nut and tray, but the tray stress still lacks corresponding theoretical calculation and [...] Read more.
Glass-fiber reinforced polymer (GFRP) bars are increasingly widely used in slope support instead of steel bars or steel pipes. GFRP Bars are generally connected with the slope by combining conical nut and tray, but the tray stress still lacks corresponding theoretical calculation and strength verification methods. Therefore, assuming that the tray is an equal thickness thin plate, the internal force distribution of the tray is calculated using the thin plate bending and cavity expansion theory, and compared with the finite element numerical analysis results of the tray. The calculation and analysis show that the elastic theoretical solution of internal force distribution of equal thickness tray is basically the same as the numerical simulation solution of variable thickness tray. The tray loading and free surface are controlled by hoop tensile and radial compressive stress, respectively. The inner wall of the free surface of the tray is the weakest part of the tray, and the ultimate strength of a GFRP tray is 35.81–53.00% of the standard tensile strength of Φ20 GFRP bars by distortion energy density. This theoretical method can be used for stress analysis of variable thickness trays and has played technical support for promoting the application of GFRP bars in slope support. Full article
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13 pages, 6954 KiB  
Article
A Numerical Analysis of Ductile Deformation during Nanocutting of Silicon Carbide via Molecular Dynamics Simulation
by Bing Liu, Xiaolin Li, Ruijie Kong, Haijie Yang and Lili Jiang
Materials 2022, 15(6), 2325; https://doi.org/10.3390/ma15062325 - 21 Mar 2022
Cited by 4 | Viewed by 2287
Abstract
As a typical third-generation semiconductor material, silicon carbide (SiC) has been increasingly used in recent years. However, the outstanding performance of SiC component can only be obtained when it has a high-quality surface and low-damage subsurface. Due to the hard–brittle property of SiC, [...] Read more.
As a typical third-generation semiconductor material, silicon carbide (SiC) has been increasingly used in recent years. However, the outstanding performance of SiC component can only be obtained when it has a high-quality surface and low-damage subsurface. Due to the hard–brittle property of SiC, it remains a challenge to investigate the ductile machining mechanism, especially at the nano scale. In this study, a three-dimensional molecular dynamics (MD) simulation model of nanometric cutting on monocrystalline 3C-SiC was established based on the ABOP Tersoff potential. Multi-group MD simulations were performed to study the removal mechanism of SiC at the nano scale. The effects of both cutting speed and undeformed cutting thickness on the material removal mechanism were considered. The ductile machining mechanism, cutting force, hydrostatic pressure, and tool wear was analyzed in depth. It was determined that the chip formation was dominated by the extrusion action rather than the shear theory during the nanocutting process. The performance and service life of the diamond tool can be effectively improved by properly increasing the cutting speed and reducing the undeformed cutting thickness. Additionally, the nanometric cutting at a higher cutting speed was able to improve the material removal rate but reduced the quality of machined surface and enlarged the subsurface damage of SiC. It is believed that the results can promote the level of ultraprecision machining technology. Full article
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13 pages, 22906 KiB  
Article
High-Speed Spiral Bevel GEAR Dynamic Rules Considering the Impact of Web Thicknesses and Angles
by Xiangying Hou, Linyue Qiu, Yuzhe Zhang, Zhengminqing Li, Rupeng Zhu and Sung-Ki Lyu
Appl. Sci. 2022, 12(6), 3084; https://doi.org/10.3390/app12063084 - 17 Mar 2022
Cited by 3 | Viewed by 2063
Abstract
Gear transmission system dynamic responses under high-speed and heavy-duty working conditions were obviously affected by support structures, especially in lightweight design. However, web thicknesses and angles were usually ignored in dynamic modeling process. Therefore, a full mesh model with web structure was built [...] Read more.
Gear transmission system dynamic responses under high-speed and heavy-duty working conditions were obviously affected by support structures, especially in lightweight design. However, web thicknesses and angles were usually ignored in dynamic modeling process. Therefore, a full mesh model with web structure was built and its dynamic characteristics were analyzed by a modified vector form intrinsic finite element (VFIFE), which is proposed to solve high-speed dynamic problems with good efficiency. For spiral bevel gear pair dynamic characteristics, the impacts of web thicknesses and angles were simulated and discussed. Simulation results showed that web support angles will affect gear meshing performance and dynamic characteristics more remarkable than web thickness did. In addition, the good performance of the proposed modified VFIFE method was proved, which showed good computing efficiency. Full article
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18 pages, 5821 KiB  
Article
Influence of Materials Parameters of the Coil Sheet on the Formation of Defects during the Manufacture of Deep-Drawn Cups
by Wojciech Baran, Krzysztof Regulski and Andrij Milenin
Processes 2022, 10(3), 578; https://doi.org/10.3390/pr10030578 - 16 Mar 2022
Cited by 1 | Viewed by 2093
Abstract
During the process of deep drawing of cylindrical thin-walled products from aluminum sheets, the occurrence of product defects in the form of breaking the material continuity is observed. This has a very large impact on the efficiency of production lines and the number [...] Read more.
During the process of deep drawing of cylindrical thin-walled products from aluminum sheets, the occurrence of product defects in the form of breaking the material continuity is observed. This has a very large impact on the efficiency of production lines and the number of generated scraps. The number of defects depends on many factors, including the material and the process properties. Because the problem appears after changing one material to another, while the process parameters do not change, it was assumed that the material has the main influence on the number of defects. To reduce the number of defects, a tool is needed to predict threats to the process. Decision tree models were used for this purpose. Using the tree interaction algorithms, the influence of the chemical composition and strength parameters of the 3xxx series aluminum alloy on the number of generated defects was investigated. Increased Silicon (Si) and Iron (Fe) values generated a higher number of defects. Increased yield strength (YS) and decreased elongation (E) also generated a higher number of defects. Based on the results, a defect prediction tool was created, where after entering the parameters of the material, it is possible to predict production hazards. Full article
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10 pages, 4104 KiB  
Article
Optimizing the Electrical and Mechanical Properties of Cu-Cr Alloys by Hf Microalloying
by Yin Yang, Gui Kuang and Rengeng Li
Metals 2022, 12(3), 485; https://doi.org/10.3390/met12030485 - 13 Mar 2022
Cited by 9 | Viewed by 1876
Abstract
Cu-0.4Cr (wt.%) alloys with the microalloying of Hf elements were subjected to a modified rolling–aging process to achieve high strength, high electrical conductivity and high ductility simultaneously. Transmission electron microscopy and X-ray line broadening analysis were conducted to characterize the microstructures of these [...] Read more.
Cu-0.4Cr (wt.%) alloys with the microalloying of Hf elements were subjected to a modified rolling–aging process to achieve high strength, high electrical conductivity and high ductility simultaneously. Transmission electron microscopy and X-ray line broadening analysis were conducted to characterize the microstructures of these alloys. Deformation twins and high-density dislocations were introduced into the copper alloys via the modified rolling–aging process and the microalloying of Hf, improving the mechanical properties of copper alloys. The Cu-Cr-Hf alloy with a reduced Hf content performed well in terms of strength, electrical conductivity and ductility. The microalloying of 0.4 wt.% Hf in the Cu-0.4Cr alloy was sufficient to achieve a good combination of high tensile strength (593 MPa), high uniform elongation (~5%) and high electrical conductivity (80.51% IACS). Full article
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23 pages, 7934 KiB  
Article
Optimization Design and Performance Evaluation of a Hybrid Excitation Claw Pole Machine
by Yu Cao, Shushu Zhu, Junyue Yu and Chuang Liu
Processes 2022, 10(3), 541; https://doi.org/10.3390/pr10030541 - 10 Mar 2022
Cited by 5 | Viewed by 3156
Abstract
Claw pole machines (CPMs) have the advantages of a simple structure and low cost; therefore, they are commonly used in electric vehicles (EV). However, the methods to improve reliability and efficiency should be studied. So, a new type of hybrid excitation claw pole [...] Read more.
Claw pole machines (CPMs) have the advantages of a simple structure and low cost; therefore, they are commonly used in electric vehicles (EV). However, the methods to improve reliability and efficiency should be studied. So, a new type of hybrid excitation claw pole machine (HE-CPM) for EV is proposed. The permanent magnet (PM) is inserted in the rotor, and the field winding is placed on the front and back ending cover. Because the hybrid flux path of the proposed machine is three-dimensional (3D) and 3D finite element analysis (FEA) is time-consuming, a 3D magnet equivalent circuit (MEC) method considering rotor position is proposed and results between 3D MEC and FEA are compared. Particle swarm optimization (PSO) and 3D MEC are combined in the optimization design of HE-CPM. The optimized results prove the effectiveness of the optimization method. Finally, the flux density distribution, electromagnetic characteristics of HE-CPM are evaluated. The thermal analysis and mechanical stress analysis are carried out. The HE-CPM prototype was manufactured. The direct current (DC) bus voltages under different excitation currents and load currents are measured and compared with those of FEA. When the armature current and the excitation current are 7 A and 4 A, respectively, the rated power and rated speed of HE-CPM are 10.28 kW and 3000 rpm, respectively. The maximum efficiency is 89%. FEA results are basically consistent with the experimental results. Accurate results and time savings can be achieved by combining PSO and 3D MEC. Full article
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20 pages, 7452 KiB  
Article
Modeling of Polycrystalline Material Microstructure with 3D Grain Boundary Based on Laguerre–Voronoi Tessellation
by Xingshuai Zheng, Tengfei Sun, Jixing Zhou, Rupeng Zhang and Pingmei Ming
Materials 2022, 15(6), 1996; https://doi.org/10.3390/ma15061996 - 08 Mar 2022
Cited by 14 | Viewed by 3169
Abstract
Voronoi tessellations are shown to be statistically representative of polycrystalline microstructures, which have been widely accepted for the modeling of microstructures of metallurgic and ceramic materials. In this paper, a new implementation of the Voronoi diagram in Laguerre geometry is presented for the [...] Read more.
Voronoi tessellations are shown to be statistically representative of polycrystalline microstructures, which have been widely accepted for the modeling of microstructures of metallurgic and ceramic materials. In this paper, a new implementation of the Voronoi diagram in Laguerre geometry is presented for the generation of numerical models of polycrystalline microstructures, where the size and shape of the grains can be controlled, and the 3D grain boundaries can be modeled with a specified thickness. The distribution of grain sizes in the models is fitted to a lognormal distribution, compared with the normal distribution in the Voronoi tessellation methods. Finally, statistical analyses of grain face and grain size distribution are performed with the models, and the macroscopic elastic properties of polycrystalline ceramic materials are simulated to verify the capability of the presented method. Full article
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10 pages, 2800 KiB  
Article
Annihilation Mechanism of Low-Angle Grain Boundary in Nanocrystalline Metals
by Guofeng Zhou, Qishan Huang, Yingbin Chen, Xiongqing Yu and Haofei Zhou
Metals 2022, 12(3), 451; https://doi.org/10.3390/met12030451 - 05 Mar 2022
Cited by 4 | Viewed by 2213
Abstract
Due to the high density of grain boundaries (GBs), nanocrystalline metals possess superior properties, including enhanced strength, work hardening, and fatigue resistance, in comparison to their conventional counterparts. The expectation of GB migration is critical for grain coarsening and GB annihilation in these [...] Read more.
Due to the high density of grain boundaries (GBs), nanocrystalline metals possess superior properties, including enhanced strength, work hardening, and fatigue resistance, in comparison to their conventional counterparts. The expectation of GB migration is critical for grain coarsening and GB annihilation in these materials, significantly affecting the polycrystalline network and mechanical behavior. Here, we perform molecular dynamics (MD) simulations on gold (Au) nanocrystals containing multiple parallelly arranged GBs, with a focus on the investigation of annihilation mechanisms of low-angle grain boundaries (LAGBs). It is observed that the shear-coupled motion of LAGBs, consisting of dislocations, gives rise to their preliminary migration with the reduced separation distance between GBs. With subsequent GB motion, the LAGBs encountered with neighboring GBs, and can be annihilated by various mechanisms, including dislocations interpenetration, dislocations interaction, or dislocations absorption, depending on the specific configuration of the neighboring GB. These findings enhance our understanding of GB interactions and shed light on the controlled fabrication of high-performance nanocrystalline metals. Full article
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11 pages, 3496 KiB  
Article
Microstructure and Mechanical Properties of Medium-Carbon Si-Rich Steel Processed by Austempering after Intercritical Annealing
by Xin Jia, Yuefeng Wang, Lin Wang, Xiaowen Sun, Ting Zhao and Tiansheng Wang
Metals 2022, 12(3), 441; https://doi.org/10.3390/met12030441 - 03 Mar 2022
Viewed by 1767
Abstract
In the present paper, the medium-C Si-rich steel with a quenched martensite microstructure was heated to intercritical annealing temperatures at 750 °C, 760 °C and 770 °C after warm rolling deformation to obtain ferrite with varying volume fractions. Subsequently, bainite/ferrite multiphase microstructures were [...] Read more.
In the present paper, the medium-C Si-rich steel with a quenched martensite microstructure was heated to intercritical annealing temperatures at 750 °C, 760 °C and 770 °C after warm rolling deformation to obtain ferrite with varying volume fractions. Subsequently, bainite/ferrite multiphase microstructures were attained via austempering near Ms temperature. The microstructures of the test steel after different heat treatments were characterized by scanning electron microscopy, transmission electron microscopy and electron backscatter diffraction, and corresponding tensile and impact properties were tested. The results showed that, with the increase of intercritical annealing temperature, the austenite content increased, which limited the growth of ferrite grains, and the grain size decreased from ~1.6 μm to ~1.4 μm. In addition, the degree of ferrite recrystallization was almost complete. At the same intercritical annealing temperature, compared with austempering above Ms, prior athermal martensite (PAM) was obtained after austempering below Ms, which effectively refined the size of bainite ferrite lath. Moreover, with the increase of intercritical annealing temperature, the bainite content of the test steel increased after austempering, resulting in the increase of yield strength, tensile strength and impact energy. In contrast, while the decrease in ferrite content led to a significant decrease in uniform elongation. At constant intercritical annealing temperature, the tensile strength decreased slightly, and the impact property improved after austempering above Ms. Full article
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19 pages, 10281 KiB  
Article
Microstructural Variation of Clay during Land Subsidence and the Correlation between Macroscopic and Microscopic Parameters
by Shengtong Di, Chao Jia, Pengpeng Ding and Xiao Zhu
Materials 2022, 15(5), 1817; https://doi.org/10.3390/ma15051817 - 28 Feb 2022
Cited by 4 | Viewed by 1499
Abstract
The nonlinear deformation, visco-elasto-plasticity and other macroscopic properties of soil are the concentrated manifestations of its microstructural state. In order to study the microstructural characteristics and variations of the clay under the action of additional stress caused by groundwater exploitation, borehole sampling was [...] Read more.
The nonlinear deformation, visco-elasto-plasticity and other macroscopic properties of soil are the concentrated manifestations of its microstructural state. In order to study the microstructural characteristics and variations of the clay under the action of additional stress caused by groundwater exploitation, borehole sampling was carried out on the clay layers at different depths in a typical land subsidence area. Consolidation tests, freeze-drying, ion sputtering, and scanning electron microscope (SEM) were conducted in order to scan and analyze the microstructure of the test samples at different scales. The Particles and Cracks Analysis System (PCAS) was used to quantify the microscopic parameters, the variations of the microstructural parameters with consolidation loads at different sizes were revealed, and the correlation between the macroscopic and microscopic parameters were discussed. The results show that: (1) the microstructural characteristics of soils with different buried depths have directivity, to a certain extent; (2) as the consolidation load increases, the average unit area and average form factor of the soil microstructure generally decrease, the structural arrangement of the unit gradually tends to be orderly, and the average pore area, apparent void ratio and the number of pores generally show a decreasing trend; (3) under the action of a consolidation load, when the microstructure at a relatively large scale is basically stable, the microstructure at a smaller scale will continue to adjust; (4) the apparent void ratio has a good linear regression relationship with the conventional void ratio, and the apparent void ratio has a good exponential growth relationship with the compressibility. Full article
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9 pages, 1143 KiB  
Article
Surface Characterization and Performance Evaluation of Nitrogen Implanted Coinage Dies
by João Cruz, Victoria Corregidor, Bruno Nunes, Luís Alves, Rogério Colaço and Eduardo Alves
Processes 2022, 10(3), 479; https://doi.org/10.3390/pr10030479 - 27 Feb 2022
Viewed by 1672
Abstract
Very high fluence implantation of 14N+ ions was used to promote the formation of a nitride layer on the surface of steel coinage dies used by the Portuguese Mint. Die steel samples were studied before and after implantation at 90 keV [...] Read more.
Very high fluence implantation of 14N+ ions was used to promote the formation of a nitride layer on the surface of steel coinage dies used by the Portuguese Mint. Die steel samples were studied before and after implantation at 90 keV plus 30 keV for two nominal fluences, 5.0 × 1017 at/cm2 and 1.0 × 1018 at/cm2, and for two implantation temperatures, room and liquid nitrogen temperature. Surface characterization was carried out by ultramicrohardness indentation, Atomic Force Microscopy (AFM), and Rutherford Backscattering Spectrometry (RBS). A significant increase (factor two) in depth reached by the implanted nitrogen was observed for LN2 implantations, which, to our knowledge, was never reported before. Results point out the benefit of nitrogen implantation at room temperature with a nominal fluence of 5.0 × 1017 at/cm2, which raised the hardness of the dies by ∼40% (from 6.2 ± 0.5 to 8.7 ± 0.7 GPa). Nitrogen implanted dies were used to mint circulating two cents euro coins and their performance was assessed, showing that when compared to Vautrol coated dies (standard coating used by the Portuguese Mint), the crack density was lower and similar wear resistance was observed. Full article
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18 pages, 4969 KiB  
Article
Experimental Study on Static and Dynamic Response of Aluminum Honeycomb Sandwich Structures
by Radosław Ciepielewski, Roman Gieleta and Danuta Miedzińska
Materials 2022, 15(5), 1793; https://doi.org/10.3390/ma15051793 - 27 Feb 2022
Cited by 12 | Viewed by 2619
Abstract
Honeycomb aluminum structures are used in energy-absorbing constructions in military, automotive, aerospace and space industries. Especially, the protection against explosives in military vehicles is very important. The paper deals with the study of selected aluminum honeycomb sandwich materials subjected to static and dynamic [...] Read more.
Honeycomb aluminum structures are used in energy-absorbing constructions in military, automotive, aerospace and space industries. Especially, the protection against explosives in military vehicles is very important. The paper deals with the study of selected aluminum honeycomb sandwich materials subjected to static and dynamic compressive loading. The used equipment includes: static strength machine, drop hammer and Split Hopkinson Pressure Bar (SHPB). The results show the influence of applied strain rate on the strength properties, especially Plateau stress, of the tested material. In each of the discussed cases, an increase in the value of plateau stresses in the entire strain range was noted with an increase in the strain rate, with an average of 10 to 19%. This increase is mostly visible in the final phase of structure destruction, and considering the geometrical parameters of the samples, the plateau stress increase was about 0.3 MPa between samples with the smallest and largest cell size for the SHPB test and about 0.15 MPa for the drop hammer test. Full article
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37 pages, 33340 KiB  
Article
Designing of the Electromechanical Drive for Automated Hot Plate Welder Using Load Optimization with Genetic Algorithm
by Krzysztof Wałęsa, Krzysztof Talaśka and Dominik Wilczyński
Materials 2022, 15(5), 1787; https://doi.org/10.3390/ma15051787 - 27 Feb 2022
Cited by 6 | Viewed by 1996
Abstract
Drive and conveyor belts are widely used in the mining and processing industry. One of the types often used is the belt with a cross-section and a diameter of several millimeters, made of weldable thermoplastic elastomer. Their production process requires the joining of [...] Read more.
Drive and conveyor belts are widely used in the mining and processing industry. One of the types often used is the belt with a cross-section and a diameter of several millimeters, made of weldable thermoplastic elastomer. Their production process requires the joining of the ends to obtain a closed loop. This operation is often performed by butt welding using the hot plate method. Taking into account the industrial requirements, the authors made an effort to design the automated welding machine for this type of belt. The work that had been conducted was finished with the implementation of the device for serial belt production. One of the stages of the design process of the welding machine consisted of developing a solution for the electromechanical drive system. The paper presents a design and the selection of the key components of the drive system, in particular, the electrical executive elements. Firstly, on the basis of the functional requirements of individual working mechanisms, the kinematic structure of the drives was developed, and the influence of the workload on power consumption was described. Then, using known technological parameters, experimental research of the plasticization operation was performed. On the basis of the results obtained, a mathematical model of the correlation between the plasticization force and technological parameters was derived. Using the derived model, the optimization of the technological parameters was made by using a genetic algorithm. The work led to the choice of an effective electric motor, which is the main component of the designed drive system. Full article
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11 pages, 2459 KiB  
Article
Evaluation of In Doped GaAs Alloys to Optimize Electronic, Thermoelectric and Mechanical Properties
by Aiyeshah Alhodaib
Materials 2022, 15(5), 1781; https://doi.org/10.3390/ma15051781 - 26 Feb 2022
Cited by 1 | Viewed by 1671
Abstract
The electronic, mechanical and transport properties of the In substitution in GaAs are investigated by the TB-mBJ potential, BoltzTraP code and Charpin tensor matrix analysis using Wien2k code. The formation energies of the alloys Ga1−xInxAs (x = 0.0, 0.25, [...] Read more.
The electronic, mechanical and transport properties of the In substitution in GaAs are investigated by the TB-mBJ potential, BoltzTraP code and Charpin tensor matrix analysis using Wien2k code. The formation energies of the alloys Ga1−xInxAs (x = 0.0, 0.25, 0.50, 0.75 and 1.0) confirm that they are thermodynamically favorable. The directional symmetry changes when increasing the In concentration and reduces the bandgap from 1.55 eV (GaAs) to 0.57 eV (InAs), as well as reducing the electrical conductivity and increasing the Seebeck coefficient. The thermoelectric performance is depicted by the power factor without including lattice vibration. The elastic properties’ analysis shows mechanical stability, and elastic moduli decrease with an increasing In in GaAs, which converts the brittle nature to ductile. The Debye temperature, hardness and thermal conductivity decrease, thus, increasing their importance for device fabrications. Full article
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26 pages, 7703 KiB  
Article
Design and Experimental Research of a New Film-Picking Mulch Film Recovery Machine with Impurity Separation Function
by Jianhao Dong, Shuzhuo Li, Xinsheng Bi, Guangheng Wang, Jikui Wang, Wensheng Wang and Ningze Tong
Processes 2022, 10(3), 455; https://doi.org/10.3390/pr10030455 - 24 Feb 2022
Cited by 1 | Viewed by 1719
Abstract
When the film is under no stress, it does not show any stiffness or capability to withstand loads. Therefore, with the help of ANSYS motion, the author applied pre-stress, controlled point coordinates and the equation of equivalent stress surface and used form-finding conditions [...] Read more.
When the film is under no stress, it does not show any stiffness or capability to withstand loads. Therefore, with the help of ANSYS motion, the author applied pre-stress, controlled point coordinates and the equation of equivalent stress surface and used form-finding conditions to explore the equilibrium state of the films in different depths. The author established curve fitting equations and designed a new membrane-removing mulch film recovery machine. The author also analyzed key components and separately established regression equations between recovery rate, damage rate, release rate and the working angle of film picking mechanism, as well as the regression equation between the depth of picking mechanism into the soil and the working angle of clamping conveyor. Then the author conducted the variance analysis on these regression equations. By using Design Expert 8.0.6 to optimize the solution, when the working angle of the pick-up mechanism is 27.31°, the depth of the pick-up mechanism is 73.0 mm. The working angle of the clamping and conveying device is 38.33°, the recovery rate is 93.9% and the damage rate is 89.3%. The test result shows that when parameters are set as above values, the recovery rate of residual film is 92.5%, the release rate is 87.6% and the error values of damage rate and release rate are both lower than 1.5%, which have verified the feasibility of the optimization solution. The experimental result can work as a reference for the optimum working parameters of the new membrane-removing mulch film recovery machine. Full article
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10 pages, 4069 KiB  
Article
Prediction and Process Analysis of Tensile Properties of Sinter-Hardened Alloy Steel by Artificial Neural Network
by Zhaoqiang Tan, Zijun Qin, Qing Zhang, Yong Liu and Feng Liu
Metals 2022, 12(3), 381; https://doi.org/10.3390/met12030381 - 23 Feb 2022
Viewed by 1408
Abstract
Sinter-hardening is an emerging powder metallurgy process by which the consolidation of powder and the hardening of dense bulk samples are integrated into one step. In this study, to understand the complex effects of sinter-hardening parameters on the properties of the Fe-Cr-Ni (Cu)-C [...] Read more.
Sinter-hardening is an emerging powder metallurgy process by which the consolidation of powder and the hardening of dense bulk samples are integrated into one step. In this study, to understand the complex effects of sinter-hardening parameters on the properties of the Fe-Cr-Ni (Cu)-C alloy, an artificial neural network (ANN) with the topology of a nonlinear multi-layered perceptron was designed to predict the ultimate tensile strength and elongation, considering parameters including chemical composition, sintering temperature, and cooling rate. The predictability of the ANN was verified by experiments, indicating that this method is adequate to quantitatively ascribe steel properties to powder metallurgy parameters in the view of improving process robustness. Full article
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15 pages, 9786 KiB  
Article
Microstructure, Hot Deformation Behavior, and Textural Evolution of Mg-3Sn-2Al-1Zn-0.6Nd Alloy
by Yuhang Guo, Yibo Dai, Pan Chen, Qianhao Zang and Zhenya Zhang
Metals 2022, 12(2), 364; https://doi.org/10.3390/met12020364 - 21 Feb 2022
Cited by 3 | Viewed by 1561
Abstract
To prepare wrought magnesium alloys with excellent plastic deformation properties, Mg-3Sn-2Al-1Zn-0.6Nd alloys were prepared. A hot compression test of Mg-3Sn-2Al-1Zn-0.6Nd alloy was carried out on a thermo-mechanical simulator. The hot deformation behavior of the alloys was studied, and the constitutive equations and the [...] Read more.
To prepare wrought magnesium alloys with excellent plastic deformation properties, Mg-3Sn-2Al-1Zn-0.6Nd alloys were prepared. A hot compression test of Mg-3Sn-2Al-1Zn-0.6Nd alloy was carried out on a thermo-mechanical simulator. The hot deformation behavior of the alloys was studied, and the constitutive equations and the processing map at the strain of 0.8 were established. The processing map exhibited the stable domain (temperature range of 320–350 °C and strain rate range of 0.001–0.04 s−1) with the high power dissipation efficiency (>30%). A large number of fine dynamic recrystallization (DRX) grains and deformed twinning existed in the alloy after the hot deformation. The dominant texture of the Mg-3Sn-2Al-1Zn-0.6Nd alloy is <0001>//CD texture after the hot deformation. The continuous dynamic recrystallization (CDRX) and discontinuous dynamic recrystallization (DDRX) were the dominant recrystallization mechanisms, and {101¯2} extension twinning also occurred in the alloy during the hot deformation. Full article
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26 pages, 51246 KiB  
Article
Large Deflections of Thin-Walled Plates under Transverse Loading—Investigation of the Generated In-Plane Stresses
by Gilad Hakim and Haim Abramovich
Materials 2022, 15(4), 1577; https://doi.org/10.3390/ma15041577 - 20 Feb 2022
Cited by 10 | Viewed by 4189
Abstract
Thin-walled plates subjected to transverse loading undergoing large deflection have been the topic of a large number of studies. However, there is still a lack of information about the nature and the distribution membrane stresses generated under large deflections. The purpose of this [...] Read more.
Thin-walled plates subjected to transverse loading undergoing large deflection have been the topic of a large number of studies. However, there is still a lack of information about the nature and the distribution membrane stresses generated under large deflections. The purpose of this paper is to calculate and display the distribution of the generated stresses and the respective deflections on the entire rectangular plate area. Finite element analysis results for thin-walled plates with aspect ratios of 1, 2 and 5, on movable and immovable edges simply supported and clamped boundary conditions are clearly visualized. The distribution of the normal and shear stresses enables a good understanding of the plate critical points locations. It was found that strong tensile and compressive membrane stresses exist at various points near the plate edges, creating potential failure hazards. Full article
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19 pages, 9226 KiB  
Article
Microstructure Analysis and Segmented Constitutive Model for Ni-Cr-Co-Based Superalloy during Hot Deformation
by Hongyu Li, Wei Feng, Wuhao Zhuang and Lin Hua
Metals 2022, 12(2), 357; https://doi.org/10.3390/met12020357 - 18 Feb 2022
Cited by 3 | Viewed by 1797
Abstract
In a thermal simulator of Gleeble-3500, isothermal hot compression tests were performed on a Ni-Cr-Co-based superalloy at deformation temperatures ranging from 1323 K to 1423 K and with strain rates of 0.01, 0.1, 1, and 5 s−1. We obtained the true [...] Read more.
In a thermal simulator of Gleeble-3500, isothermal hot compression tests were performed on a Ni-Cr-Co-based superalloy at deformation temperatures ranging from 1323 K to 1423 K and with strain rates of 0.01, 0.1, 1, and 5 s−1. We obtained the true stress–strain curves, and the microstructures of deformed samples were analyzed by electron backscatter diffraction (EBSD) technique. The segmented constitutive models were developed to predict the flow stress, and the dynamic recrystallization grain size model was established to evaluate the microstructure evolution for a Ni-Cr-Co-based superalloy. It is found that discontinuous dynamic recrystallization (DDRX) and continuous dynamic recrystallization (CDRX) appear simultaneously in the Ni-Cr-Co-based superalloy during hot deformation, with the latter not being active. Comparison between the experimental and predicted results indicates that the proposed models can describe and interpret the work-hardening and dynamic softening behaviors as well as the evolution characteristic of dynamic recrystallization grain size of the Ni-Cr-Co-based superalloy. In the error analysis of the segmented constitutive models, correlation coefficient (R) is 0.988 and average absolute relative error (AARE) is 6.94%, and for the AGS of DRX, R is 0.974 and AARE is 5.83%, which both have good accuracy. Full article
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21 pages, 7521 KiB  
Article
Progressive Collapse of the Base-Isolated Frame Structures Supported by Stepped Foundation in Mountainous City
by Youfa Yang, Anxu Chen and Tianhang Yang
Appl. Sci. 2022, 12(4), 2151; https://doi.org/10.3390/app12042151 - 18 Feb 2022
Cited by 6 | Viewed by 1516
Abstract
Base-isolated frames supported by stepped foundation in mountainous areas possess their own particularity, so its progressive collapse dynamic response performance and dynamic effect propagation path are very different from those of ordinary flat ground-isolated structural systems. In order to study the progressive collapse [...] Read more.
Base-isolated frames supported by stepped foundation in mountainous areas possess their own particularity, so its progressive collapse dynamic response performance and dynamic effect propagation path are very different from those of ordinary flat ground-isolated structural systems. In order to study the progressive collapse performance of the base-isolated frames supported by stepped foundation in mountainous areas under two-directional coupled dynamic excitation, a four-span three-story plane frame demolition column test was simulated to verify the reliability of the computing platform. The common ground motion and three types of long-period ground motions were selected, and the two-dimensional dynamic coupling of the ordinary flat ground isolation structure and the base-isolated frames supported by stepped foundation in mountainous areas was obtained based on the demolition method. First, the seismic isolation structure was subjected to the collapse dynamic response under the vertical unbalanced load, then the collapse dynamic response under the vertical unbalanced load and the horizontal seismic coupling excitation was made; the two were compared and analyzed. It can be used as a reference for the design of progressive collapse of the frame structure of the base-isolated frames supported by stepped foundation in mountainous areas. Full article
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13 pages, 2335 KiB  
Article
Experimental Investigation on the Effect of Dry Ice Compression on the Poisson Ratio
by Aleksandra Biszczanik, Jan Górecki, Mateusz Kukla, Krzysztof Wałęsa and Dominik Wojtkowiak
Materials 2022, 15(4), 1555; https://doi.org/10.3390/ma15041555 - 18 Feb 2022
Cited by 11 | Viewed by 1788
Abstract
In the processing of waste materials, attention must be given to the efficient use of energy. The pelletization of dry ice is a good example of such processes. A literature review shows that in the pelletizers available on the market, the force applied [...] Read more.
In the processing of waste materials, attention must be given to the efficient use of energy. The pelletization of dry ice is a good example of such processes. A literature review shows that in the pelletizers available on the market, the force applied in the process is excessive. As a result, the efficiency of the utilization of inputs, including electricity and carbon dioxide, is at a very low level. This article presents the results of experimental research on the effect of the degree of dry ice compression on the value of the Poisson ratio. The first part of this article presents the research methodology and a description of the test stand, developed specifically for this research, bearing in mind the unique properties of carbon dioxide in the solid state. The results presented show the behavior of dry ice during compression in a rectangular chamber for different final densities of the finished product. As a result, it is possible to determine the values of the Poisson ratio as a function of density, using for this purpose four mathematical models. The findings of this research may be useful for research work focused on the further development of this process, such as by using the Drucker–Prager/Cap numerical model to optimize the geometric parameters of the parts and components of the main unit of the machine used in the extrusion process of dry ice. Full article
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17 pages, 76036 KiB  
Article
Numerical Simulation and Defect Identification in the Casting of Co-Cr Alloy
by Raimundo Silva, Rui Madureira, José Silva, Rui Soares, Ana Reis, Rui Neto, Filomena Viana, Omid Emadinia and Rui Silva
Metals 2022, 12(2), 351; https://doi.org/10.3390/met12020351 - 17 Feb 2022
Cited by 4 | Viewed by 2260
Abstract
The development of biomaterials, particularly metallic ones, is one of the focuses of the scientific community, mainly due to an increase of average life expectancy and an improvement of the casted materials combined with better mechanical properties and defect-free products. The use of [...] Read more.
The development of biomaterials, particularly metallic ones, is one of the focuses of the scientific community, mainly due to an increase of average life expectancy and an improvement of the casted materials combined with better mechanical properties and defect-free products. The use of cobalt alloys in applications, such as knee, hip, and dental prostheses, is the result of their good ability to maintain mechanical properties and biocompatibility over long periods of use. Numerical methods are becoming more important, as they help product improvement in a faster and economic way. This work focuses on the development of a numerical model in ProCAST®, comparing the shrinkage porosity and cooling curves with real castings. When correlating simulation results with available experimental data, it is possible to understand that the formulated model demonstrates an acceptable solution in terms of precision (shrinkage porosity and cooling curve). The alloy’s thermal properties and heat conditions were iteratively changed until the developed numerical model turned out a viable tool for this specific alloy when used in the investment casting process. Full article
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13 pages, 2666 KiB  
Article
Kinetics of Carbon Partitioning of Q&P Steel: Considering the Morphology of Retained Austenite
by Yaowen Xu, Fei Chen, Zhen Li, Gengwei Yang, Siqian Bao, Gang Zhao, Xinping Mao and Jun Shi
Metals 2022, 12(2), 344; https://doi.org/10.3390/met12020344 - 16 Feb 2022
Cited by 5 | Viewed by 1961
Abstract
The diffusion of carbon atoms from martensite to retained austenite (RA) is controlled by the carbon partitioning kinetics when the quenching and partitioning (Q&P) process is conducted. The RA is divided into film-like and blocky ones in morphology. This research aims to study [...] Read more.
The diffusion of carbon atoms from martensite to retained austenite (RA) is controlled by the carbon partitioning kinetics when the quenching and partitioning (Q&P) process is conducted. The RA is divided into film-like and blocky ones in morphology. This research aims to study the influence of the morphology of RA on the kinetics of carbon partitioning mainly by developing a numerical simulation. A one-step Q&P process was modeled at the partitioning temperature of 330–292 °C, with a partitioning time ranging from 106 to 5 × 103 s. The finite element method was employed to solve the carbon diffusion equation. A thermomechanical simulator Gleeble-3500 was used to conduct the corresponding Q&P heat treatment, and the RA was examined by X-ray diffraction. The results show that the film-like RA will be enriched in carbon within a short time at first, followed by a decrease in carbon concentration due to the massive absorption of carbon by blocky RA, leading the stable film-like RA to become unstable again. The end of the kinetics of carbon partitioning was the concentration determined by the constrained carbon equilibrium (CCE) model, provided that the CCE condition was employed in this study. It took quite a long time (thousands of seconds) to complete the carbon partitioning globally, which was influenced by the partitioning temperature. Full article
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20 pages, 5644 KiB  
Article
Probability-Based Crack Width Estimation Model for Flexural Members of Underground RC Box Culverts
by Sang-Hyo Kim, Syed Haider Ali Shah, Sang-Kyun Woo, Inyeop Chu and Chungwook Sim
Appl. Sci. 2022, 12(4), 2063; https://doi.org/10.3390/app12042063 - 16 Feb 2022
Cited by 3 | Viewed by 2369
Abstract
Crack control for slabs and beams in current design practices in Korea are based on the Frosch’s model, which is adapted in ACI 318. It is more difficult to have consistent quality control in underground construction sites, such as the RC box culverts [...] Read more.
Crack control for slabs and beams in current design practices in Korea are based on the Frosch’s model, which is adapted in ACI 318. It is more difficult to have consistent quality control in underground construction sites, such as the RC box culverts used for electric power distribution built below the ground level. There are more discrepancies between the as-built dimensions and the design dimensions provided in drawings in these structures. Due to this variability in construction error, the crack widths measured in such structures have higher potential to have more differences than the calculated values. Although crack control is a serviceability concern, if the owner chooses to have a target crack width that needs better control, crack width estimations can be improved by considering such construction variability. The probability-based crack width model suggested in this study will allow minimizing the discrepancies between the measured and calculated crack widths and provide reliable estimations of crack widths. Typical size of slabs and beams ranging between 300 mm (12 in.) to 500 mm (20 in.) used in underground RC box culverts in Korea were tested under the four-point bending test program. The thicker specimens had smaller bar spacings which created more cracks with smaller crack widths. However, with smaller crack widths generated in these specimens, there were more errors between the measurements and calculated values. From site investigations in Korea, the thickness of slabs in underground box culverts varied the most among all parameters. As a result, the bottom concrete covers had the highest variability. Bottom concrete covers and bar spacings are the two most important parameters in concrete crack control. A probability-based crack width estimation model for flexural members was developed in this study to consider this construction variability. Monte Carlo simulations were performed to evaluate the probabilistic characteristics of the design surface crack widths with a target width of either 0.3 mm (12 mils) or 0.5 mm (20 mils). The probabilistic models of design variables included in the crack width estimation model were generated based on field-collected information from construction sites in Korea. Because the surface crack widths in RC flexural members are sensitive to the construction errors of concrete cover depths, and since there are differences between the assumed and actual stress distribution closer to the reinforcing bars, the probability of having surface cracks of 0.3 mm width (12 mils) is found to be quite high, such as 89% at the positive moment region (mid-span, bottom surface) of the top slab in RC box culverts and 45% for the negative moment region (support area, top surface) of the top slab with current design practice. In order to ensure crack widths to be smaller than the design target width, probability-based crack width factors are recommended in this study to improve estimations depending on the selected target reliability levels. Full article
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11 pages, 3474 KiB  
Article
Structural, Morphological, Optical and Electrical Characterization of Gahnite Ferroan Nano Composite Derived from Fly Ash Silica and ZnO Mixture
by Sushree Saraswati Panda, Hara Prasada Tripathy, Priyabrata Pattanaik, Dilip Kumar Mishra, Sushanta Kumar Kamilla, Asimananda Khandual, William Holderbaum, Richard Sherwood, Gary Hawkins and Shyam Kumar Masakapalli
Materials 2022, 15(4), 1388; https://doi.org/10.3390/ma15041388 - 14 Feb 2022
Cited by 2 | Viewed by 1701
Abstract
The synthesis of a high value-added product, gahnite ferroan nano composite, from a mixture of fly ash silica and ZnO is a low-cost and non-expensive technique. The XRD pattern clearly reveals the synthesized product from fly ash after leaching is a product of [...] Read more.
The synthesis of a high value-added product, gahnite ferroan nano composite, from a mixture of fly ash silica and ZnO is a low-cost and non-expensive technique. The XRD pattern clearly reveals the synthesized product from fly ash after leaching is a product of high-purity gahnite ferroan composite. The grains are mostly cubical in shape. The optical band gap of powdered gahnite ferroan nano composite is 3.37 eV, which acts as a UV protector. However, the bulk sample shows that the 500 to 700 nm wavelength of visible light is absorbed, and UV light is allowed to pass through. So, the bulk sample acts as a band pass filter of UV light which can be used in many optical applications for conducting UV-irradiation activity. Dielectric permittivity and dielectric loss increase with a rise in temperature. The increase in the ac conductivity at higher temperatures denotes the negative temperature coefficient resistance (NTCR) behavior of the material. Full article
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17 pages, 12357 KiB  
Article
Pneumatic Bionic Hand with Rigid-Flexible Coupling Structure
by Chang Chen, Jiteng Sun, Long Wang, Guojin Chen, Ming Xu, Jing Ni, Rizauddin Ramli, Shaohui Su and Changyong Chu
Materials 2022, 15(4), 1358; https://doi.org/10.3390/ma15041358 - 13 Feb 2022
Cited by 9 | Viewed by 2878
Abstract
This paper presents a rigid-flexible composite of bionic hand structure design scheme solution for solving the problem of low load on the soft gripping hand. The bionic hand was designed based on the Fast Pneumatic Network (FPN) approach, which can produce a soft [...] Read more.
This paper presents a rigid-flexible composite of bionic hand structure design scheme solution for solving the problem of low load on the soft gripping hand. The bionic hand was designed based on the Fast Pneumatic Network (FPN) approach, which can produce a soft finger bending drive mechanism. A soft finger bending driver was developed and assembled into a human-like soft gripping hand which includes a thumb for omnidirectional movement and four modular soft fingers. An experimental comparison of silicone rubber materials with different properties was conducted to determine suitable materials. The combination of 3D printing technology and mold pouring technology was adopted to complete the prototype preparation of the bionic hand. Based on the second-order Yeoh model, a soft bionic finger mathematical model was established, and ABAQUS simulation analysis software was used for correction to verify the feasibility of the soft finger bending. We adopted a pneumatic control scheme based on a motor micro-pump and developed a human–computer interface through LabView. A comparative experiment was carried out on the bending performance of the finger, and the experimental data were analyzed to verify the accuracy of the mathematical model and simulation. In this study, the control system was designed, and the human-like finger gesture and grasping experiments were carried out. Full article
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13 pages, 3034 KiB  
Article
Optimization of Repair Process Parameters for Open-Arc Surfacing Welding of Grinding Rolls Based on the Response Surface Method
by Jin Wang, Min Wei, Jimiao He, Yuqi Wang and Changrong Ren
Processes 2022, 10(2), 321; https://doi.org/10.3390/pr10020321 - 08 Feb 2022
Cited by 3 | Viewed by 1763
Abstract
The dilution rate of surfacing layers and the quality of weld forming are important factors affecting the quality of surfacing layers in open-arc surfacing. They are determined by the interaction of various surfacing parameters. In this paper, the response surface method is used [...] Read more.
The dilution rate of surfacing layers and the quality of weld forming are important factors affecting the quality of surfacing layers in open-arc surfacing. They are determined by the interaction of various surfacing parameters. In this paper, the response surface method is used to optimize the process parameters of open-arc surfacing welding. Mathematical models of the surfacing current, surfacing voltage, surfacing speed, dilution rate and weld residual height were established, and the reliability of the models was verified by variance analysis. By performing an analysis of the perturbation diagram and response surface diagram, the influence law of each influencing factor on the response value was obtained. The parameters of surfacing welding were optimized by setting optimization targets, and the experimental results of optimized parameters were compared with the predicted results. The optimized surfacing parameters were tested by grinding roller surfacing repair. The experimental results show that the quality of the grinding roller can meet the repair requirements. This shows that the model can be used to guide the surface repair of rollers and is of great significance to ensure the surface-repair quality of rollers. Full article
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15 pages, 5496 KiB  
Article
Finite Element Analysis on Welding-Induced Distortion of Automotive Rear Chassis Component
by Jin-Jae Kim, Moonki Bae, Myoung-Pyo Hong and Young-Suk Kim
Metals 2022, 12(2), 287; https://doi.org/10.3390/met12020287 - 07 Feb 2022
Cited by 1 | Viewed by 2276
Abstract
Welding-induced distortion is a major concern for the industrial joining practice. The welding-induced distortion at the weldment between the coupled torsion beam axle (CTBA) of the automotive rear chassis parts and trailing arm connected to the wheel hub axle module seriously affects the [...] Read more.
Welding-induced distortion is a major concern for the industrial joining practice. The welding-induced distortion at the weldment between the coupled torsion beam axle (CTBA) of the automotive rear chassis parts and trailing arm connected to the wheel hub axle module seriously affects the tow angle, camber angle, and caster of the wheel axle. In this paper, the welding process between CTBA and trailing arm was numerically analyzed via SYSWELD (i.e., a finite element analysis code), using the material properties predicted via J-MatPro SW, material properties software, considering the thermo-mechanical-metallurgical properties of materials. From the numerical study for the weldment of CTBA and trailing arm, we predicted the welding and thermal distortions, temperature variation, microstructure, and residual stress at the concerned area. As a result, the temperature of the welded area was predicted between 102 °C and 840 °C at the end of weldment and converged to room temperature after 1000 s. The maximum portion of the martensite structure at the welded area was expected to be 55%. The expected distortions of the trailing arm after the weldment were 0.52 mm, −1.47 mm, and 0.44 mm in the x, y, and z-directions, respectively. Finally, the limitations of this research and recommendations are presented. Full article
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15 pages, 5761 KiB  
Article
Analysis of Behaviors of the Railway Subgrade with a New Waterproof Seal Layer
by Wubin Wang, Zhixing Deng, Yunbin Niu, Yandong Li, Zhichao Huang, Minqi Dong and Qian Su
Materials 2022, 15(3), 1180; https://doi.org/10.3390/ma15031180 - 03 Feb 2022
Cited by 1 | Viewed by 1828
Abstract
This study proposes a new waterproof sealing layer to reduce the impact of water on subgrade beds. The proposed waterproof sealing layer is composed of a polyurethane adhesive (PA) mixture, which aims to control interlaminar deformation and prevent seepage. A variety of laboratory [...] Read more.
This study proposes a new waterproof sealing layer to reduce the impact of water on subgrade beds. The proposed waterproof sealing layer is composed of a polyurethane adhesive (PA) mixture, which aims to control interlaminar deformation and prevent seepage. A variety of laboratory tests were first performed to analyze the attenuation characteristics and mechanical properties of various polyurethane polymer (PP)-improved gravel mixtures under thermohydraulic coupling effects. In addition, a waterproof performance model test of the PP-improved gravel layer was conducted to investigate its waterproof and drainage performance and hydraulic damage mechanism. Finally, the feasibility and effectiveness of the surface structure of the waterproof drainage subgrade bed containing the PA mixture was tested in combination with the treatment project of the Ciyaowan station of the Baoshen heavy-haul railway. According to the experimental and model results, (1) the waterproof layer containing the polyurethane mixture exhibited satisfactory stiffness, elasticity and flexibility. The waterproof layer containing the polyurethane mixture also controlled the deformation between layers, and its mechanical properties remained stable. (2) The waterproof layer with the dense polyurethane mixture performed well in terms of the waterproof aspect, and no infiltration occurred under cyclic load (3). Long-term field monitoring revealed that the effect of the implementation of a PP-improved gravel layer to treat mud pumping was remarkable. The settlement of the PP-improved gravel layer only reached 13.21 mm, and the settlement remained stable in the later stage. Full article
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12 pages, 3807 KiB  
Article
Microstructure and Texture of an Aluminum Plate Produced by Multipass Cold Rolling and Graded Annealing Process
by Yunlei Wang, Fangzhou Yang, Liping Ren, Qi Liu, Yu Cao and Guangjie Huang
Metals 2022, 12(2), 260; https://doi.org/10.3390/met12020260 - 29 Jan 2022
Cited by 7 | Viewed by 2861
Abstract
In order to explore the microstructure, texture, individual performance, and grain size characteristic evolution law during the process of multipass cold rolling, graded annealing process, the experimental design, research approach, and methodology were investigated using the equipment of optical microscope (OM), X-ray diffraction [...] Read more.
In order to explore the microstructure, texture, individual performance, and grain size characteristic evolution law during the process of multipass cold rolling, graded annealing process, the experimental design, research approach, and methodology were investigated using the equipment of optical microscope (OM), X-ray diffraction (XRD), electron backscattered diffraction (EBSD), and transmission electron microscope (TEM). The results show that a low interannealing temperature could strengthen the cubic texture after finished product annealing, and a high volume fraction of cubic texture components was subsequently obtained. In view of the nucleation advantage of cubic texture, the Cube-{001}<100> texture formation after annealing was promoted by the cold-rolled texture of Cu-{112}<111> and S-{123}<634>, which mainly depended on the decomposition of Cu and S textures, finally, they were consumed and transformed from Cu and S textures into a cubic texture. In addition, the dislocation configuration and corrosion pit density were clearly visible and distinctive in the observation space of aluminum foil. Full article
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14 pages, 9262 KiB  
Article
Effects of Cold Rolling Deformation and Solution Treatment on Microstructural, Mechanical, and Corrosion Properties of a Biocompatible Ti-Nb-Ta-Zr Alloy
by Mariana Lucia Angelescu, Alexandru Dan, Elena Ungureanu, Nicoleta Zarnescu-Ivan and Bogdan Mihai Galbinasu
Metals 2022, 12(2), 248; https://doi.org/10.3390/met12020248 - 28 Jan 2022
Cited by 5 | Viewed by 1984
Abstract
One of the most important requirements for a metallic biomaterial is the mechanical biocompatibility, which means excellent mechanical properties—high strength and fatigue strength, but low elastic modulus, to be mechanically harmonized with hard tissues. In order to improve the mechanical and biocompatible performance [...] Read more.
One of the most important requirements for a metallic biomaterial is the mechanical biocompatibility, which means excellent mechanical properties—high strength and fatigue strength, but low elastic modulus, to be mechanically harmonized with hard tissues. In order to improve the mechanical and biocompatible performance of the Ti-25.5Nb-4.5Ta-8.0Zr wt% alloy, the influence of cold plastic deformation and solution treatment on its properties were investigated. The Ti-25.5Nb-4.5Ta-8.0Zr wt% alloy was fabricated by melting in a cold crucible furnace (in levitation) and then subjected to several treatment schemes, which include cold rolling and different solution treatments. Microstructural and mechanical characteristics of specimens in as-cast and thermo-mechanically processed condition were determined by SEM microscopy and tensile testing, for different structural states: initial as-cast/as-received, cold rolled and solution treated at different temperatures (800, 900, and 1000 °C) and durations (5, 10, 15, and 20 min), with water quenching. It was concluded that both cold rolling and solution treatment have important positive effects on structural and mechanical properties of the biomaterial, increasing mechanical strength and decreasing the elastic modulus. Samples in different structural states were also corrosion tested and the results provided important information on determining the optimal processing scheme to obtain a high-performance biomaterial. The final processing route chosen consists of a cold rolling deformation with a total deformation degree of 60%, followed by a solution heat treatment at 900 °C with maintenance duration of 5 min and water quenching. By applying this thermo-mechanical processing scheme, the Ti-25.5Nb-4.5Ta-8.0Zr wt% alloy showed an elastic modulus of 56 GPa (5% higher than in the as-cast state), an ultimate tensile strength of 1004 MPa (41.8% higher than in the as-cast state), a yield strength of 718 MPa (40.6% higher than in the as-cast state), and increased corrosion resistance (the corrosion rate decreased by 50% compared to the as-cast state). Full article
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11 pages, 3543 KiB  
Article
Effect of Ti Addition on the Precipitation Mechanism and Precipitate Size in Nb-Microalloyed Steels
by Jun Xing, Guohui Zhu, Baoqiao Wu, Hanlin Ding and Hongbo Pan
Metals 2022, 12(2), 245; https://doi.org/10.3390/met12020245 - 27 Jan 2022
Cited by 4 | Viewed by 1874
Abstract
The effect of Ti microalloying on the precipitation of NbC particles in Nb-microalloyed and Nb-Ti-microalloyed steels was investigated by scanning transmission electron microscopy. The experimental results illustrate that NbC precipitates tend to be formed via a conventional “nucleation and growth” mechanism in Ti-free [...] Read more.
The effect of Ti microalloying on the precipitation of NbC particles in Nb-microalloyed and Nb-Ti-microalloyed steels was investigated by scanning transmission electron microscopy. The experimental results illustrate that NbC precipitates tend to be formed via a conventional “nucleation and growth” mechanism in Ti-free steel, while the particles would be precipitated as a complex form of TiN cuboid core and NbC hemispherical cap in Ti-Nb-microalloyed steel with 0.009 wt.% Ti and 0.0046 wt.% N. Ti microalloying contributed to the refinement of the precipitate size, and an enhancement of the volume fraction of NbC particles was also found based on the experimental observations. Full article
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26 pages, 4894 KiB  
Article
Robust and General Model to Forecast the Heat Transfer Coefficient for Flow Condensation in Multi Port Mini/Micro-Channels
by Seyyed Hossein Hosseini, Mohamed Arselene Ayari, Amith Khandakar, Mohammad Amin Moradkhani, Mehdi Jowkar, Mohammad Panahi, Goodarz Ahmadi and Jafar Tavoosi
Processes 2022, 10(2), 243; https://doi.org/10.3390/pr10020243 - 26 Jan 2022
Cited by 6 | Viewed by 2169
Abstract
A general correlation for predicting the two-phase heat transfer coefficient (HTC) during condensation inside multi-port mini/micro-channels was presented. The model was obtained by correlating the two-phase multiplier, φtp with affecting parameters using the genetic programming (GP) method. An extensive database containing [...] Read more.
A general correlation for predicting the two-phase heat transfer coefficient (HTC) during condensation inside multi-port mini/micro-channels was presented. The model was obtained by correlating the two-phase multiplier, φtp with affecting parameters using the genetic programming (GP) method. An extensive database containing 3503 experimental data samples was gathered from 21 different sources, including a broad range of operating parameters. The newly obtained correlation fits the broad range of measured data analyzed with an average absolute relative deviation (AARD) of 16.87% and estimates 84.73% of analyzed data points with a relative error of less than 30%. Evaluation of previous correlations was also conducted using the same database. They showed the AARD values ranging from 36.94% to 191.19%. However, the GP model provides more accurate results, AARD lower than 17%, by considering the surface tension effects. Finally, the effect of various operating parameters on the HTC was studied using the proposed correlation. Full article
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8 pages, 3768 KiB  
Article
Numerical Analysis of Electron Beam Welding Deformation for the Vacuum Vessel Lower Port Stub of 316L Stainless Steel
by Haibiao Ji, Jia Tao, Jiefeng Wu, Zhihong Liu, Jianguo Ma, Xiaowei Xia, Xiaodong Lin and Xiang Gao
Metals 2022, 12(2), 224; https://doi.org/10.3390/met12020224 - 25 Jan 2022
Cited by 1 | Viewed by 2071
Abstract
The China Fusion Engineering Test Reactor vacuum vessel has strict tolerances requirements and a large number of fully penetrated joints in the manufacturing and assembly processes. As the most complicated component of vacuum vessel, port stubs have stricter tolerance requirements, to guarantee the [...] Read more.
The China Fusion Engineering Test Reactor vacuum vessel has strict tolerances requirements and a large number of fully penetrated joints in the manufacturing and assembly processes. As the most complicated component of vacuum vessel, port stubs have stricter tolerance requirements, to guarantee the high assembly accuracy with the vacuum vessel. Due to the small deformation of electron beam welding, this method is adopted for the welding of port stub. However, welding deformation cannot be avoided, thus it is necessary to carry out finite element analysis to analyze and control the welding deformation of the port stub. In this paper, based on thermo-elastic–plastic theory, the double ellipsoid and cone-shaped hybrid heat source can accurately outline the electron beam weld pool contour of the 316L stainless steel with 50 mm thickness, which is further verified by the welding process experiment. The above hybrid heat source is applied to analyze the welding deformation of the lower port stub, and according to the deformation simulation results, the welding fixture is designed to reduce the welding deformation. The welding deformation analysis can effectively provide theoretical data support and practical guidance for the actual electron beam welding process of port stub. Full article
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23 pages, 3197 KiB  
Article
Correlation Degree and Clustering Analysis-Based Alarm Threshold Optimization
by Guixin Zhang and Zhenlei Wang
Processes 2022, 10(2), 224; https://doi.org/10.3390/pr10020224 - 25 Jan 2022
Cited by 3 | Viewed by 2206
Abstract
In industrial practice, excessive alarms and high alarm rates are mostly generated from unreasonable settings to variable alarm thresholds, which have become the significant causes of impact on operation stability and plant safety. A correlation degree and clustering analysis-based approach was presented to [...] Read more.
In industrial practice, excessive alarms and high alarm rates are mostly generated from unreasonable settings to variable alarm thresholds, which have become the significant causes of impact on operation stability and plant safety. A correlation degree and clustering analysis-based approach was presented to optimize the variable alarm thresholds in this paper. The correlation degrees of variables are first obtained by analyzing correlation relationships among them. Second, the variables are grouped according to the gray correlation coefficients and clustering analysis, given the weight for fault alarm rate (FAR) in each group. An objective function about the FAR, missed alarm rate (MAR), and the maximum acceptable FAR and MAR is then established with variable weight. Eventually, based on an optimization algorithm, the objective function can be optimized for obtaining the optimal alarm threshold. Cases study of the Tennessee Eastman (TE) industrial simulation process and an actual industrial ethylene production process, in comparison to the initial situation, show that the method can effectively reduce FAR according to correlation degrees among variables in the system, and decrease the number of alarms with reduction rates of 40.5% and 35.3%, respectively. Full article
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16 pages, 67665 KiB  
Article
AZ31 Sheet Forming by Clustering Ball Spinning-Analysis of Damage Evolution Using a Modified GTN Model
by Zhiqing Hu, Lijia Da, Jia Xi and Xinchen Li
Metals 2022, 12(2), 220; https://doi.org/10.3390/met12020220 - 25 Jan 2022
Cited by 1 | Viewed by 1976
Abstract
Clustering ball spinning (CBS) forming is a novel approach to manufacturing a complex curved surface. In order to explore the forming limit of magnesium alloy in the CBS forming process, the modified GTN model was incorporated into the FE simulation to analyze the [...] Read more.
Clustering ball spinning (CBS) forming is a novel approach to manufacturing a complex curved surface. In order to explore the forming limit of magnesium alloy in the CBS forming process, the modified GTN model was incorporated into the FE simulation to analyze the damage evolution. The theoretical analyses are conducted to investigate the deformation mechanism and to explore the stress state in the CBS forming process. The numerical results show that the modified GTN model can predict the result more accurately compared with the standard GTN model, and the damage parameters for GTN model are determined by the experiments. Besides, the forming limit of AZ31 magnesium alloy can be improved by CBS forming method. To explore the reason for the increased forming limit, the microstructure of curved surface was tested by electron backscattered scattering detection (EBSD). The results demonstrate that the deformation of magnesium alloy plate by the CBS method is dominated initially by the extension twinning, and non-basal slip systems are activated with the development of forming process. Full article
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12 pages, 3532 KiB  
Article
Study of Cutting Power and Power Efficiency during Straight-Tooth Cylindrical Milling Process of Particle Boards
by Rongrong Li, Qian Yao, Wei Xu, Jingya Li and Xiaodong (Alice) Wang
Materials 2022, 15(3), 879; https://doi.org/10.3390/ma15030879 - 24 Jan 2022
Cited by 21 | Viewed by 2297
Abstract
The cutting power consumption of milling has direct influence on the economic benefits of manufacturing particle boards. The influence of the milling parameters on the cutting power were investigated in this study. Experiments and data analyses were conducted based on the response surface [...] Read more.
The cutting power consumption of milling has direct influence on the economic benefits of manufacturing particle boards. The influence of the milling parameters on the cutting power were investigated in this study. Experiments and data analyses were conducted based on the response surface methodology. The results show that the input parameters had significant effects on the cutting power. The high rake angle reduced the cutting force. Thus, the cutting power decreased with the increase in the rake angle and the cutting energy consumption was also reduced. The cutting power increased with the rotation speed of the main shaft and the depth of milling induced the impact resistance between the milling tool and particle board and the material removal rate. The p-values of the created models and input parameters were less than 0.05, which meant they were significant for cutting power and power efficiency. The depth of milling was the most important factor, followed by the rotation speed of the main shaft and then the rake angle. Due to the high values of R2 of 0.9926 and 0.9946, the quadratic models were chosen for creating the relationship between the input parameters and response parameters. The predicted values of cutting power and power efficiency were close to the actual values, which meant the models could perform good predictions. To minimize the cutting power and maximize the power efficiency for the particle board, the optimized parameters obtained via the response surface methodology were 2°, 6991.7 rpm, 1.36 mm for rake angle, rotation speed of the main shaft and depth of milling, respectively. The model further predicted that the optimized parameters combination would achieve cutting power and power efficiency values of 52.4 W and 11.9%, respectively, with the desirability of 0.732. In this study, the influence of the input parameters on the cutting power and power efficiency are revealed and the created models were useful for selecting the milling parameters for particle boards, to reduce the cutting power. Full article
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12 pages, 16293 KiB  
Article
Effect of the Flame Retardants and Glass Fiber on the Polyamide 66/Polyphenylene Oxide Composites
by Zhenya Zhang, Mingcheng Yang, Kunpeng Cai, Yang Chen, Shubo Liu, Wentao Liu and Jilin Liu
Materials 2022, 15(3), 813; https://doi.org/10.3390/ma15030813 - 21 Jan 2022
Cited by 6 | Viewed by 1960
Abstract
In this work, polyamide 66/polyphenylene oxide (PA66/PPO) composites, including the flame retardants 98 wt% aluminum diethylphosphinate + 2 wt% polydimethylsiloxane (P@Si), Al(OH)3-coated red phosphorus (RP*), and glass fiber (GF), were systematically studied, respectively. The limiting oxygen index (LOI), UL-94 vertical burning [...] Read more.
In this work, polyamide 66/polyphenylene oxide (PA66/PPO) composites, including the flame retardants 98 wt% aluminum diethylphosphinate + 2 wt% polydimethylsiloxane (P@Si), Al(OH)3-coated red phosphorus (RP*), and glass fiber (GF), were systematically studied, respectively. The limiting oxygen index (LOI), UL-94 vertical burning level, and thermal and mechanical properties of the PA66/PPO composites were characterized. The results showed that the P@Si and RP flame retardants both improved the LOI value and UL-94 vertical burning level of the PA66/PPO composites, and PA66/PPO composites passed to the UL-94 V-0 level when the contents of P@Si and RP* flame retardants were 16 wt% and 8 wt%. On the other hand, the mechanical properties of the PA66/PPO composites were reduced from a ductile to a brittle fracture mode. The addition of GF effectively made up for these defects and improved the mechanical properties of the PA66/PPO composites containing the P@Si and RP*, but it did not change the fracture mode. P@Si and RP* flame retardants improved the thermal decomposition of PA66/PPO/GF composites and reduced the maximum mass loss rates, showing that the PA66/PPO/GF composites containing the P@Si and RP* flame retardants could be used in higher-temperature fields. Full article
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10 pages, 3656 KiB  
Article
Microstructure Evolution and Shear Strength of the Cu/Au80Sn20/Cu Solder Joints with Multiple Reflow Temperatures
by Chaoyu Chen, Mingxu Sun, Zhi Cheng and Yao Liang
Materials 2022, 15(3), 780; https://doi.org/10.3390/ma15030780 - 20 Jan 2022
Cited by 4 | Viewed by 2154
Abstract
In order to present the multiple reflow process during electronic packaging, the influence of the different short-time reheating temperatures on the microstructure and shear strength of the Cu/Au80Sn20/Cu solder joints was studied and discussed. The results showed that high-quality Cu/Au80Sn20/Cu solder joints were [...] Read more.
In order to present the multiple reflow process during electronic packaging, the influence of the different short-time reheating temperatures on the microstructure and shear strength of the Cu/Au80Sn20/Cu solder joints was studied and discussed. The results showed that high-quality Cu/Au80Sn20/Cu solder joints were obtained with 30 °C for 3 min. The joints were mainly composed of the ζ-(Au,Cu)5Sn intermetallic compound (IMC) with an average thickness of 8 μm between Cu and solder matrix, and (ζ-(Au,Cu)5Sn +δ-(Au,Cu)Sn) eutectic structure in the solder matrix. With an increase in the multiple reflow temperature from 180 °C to 250 °C, the microstructure of the joint interface showed little change due to the barrier effect of the formed ζ IMC layer and the limitation of short-time reheating on the element diffusion. The eutectic structures in the solder matrix were coarsened and transformed from lamellar to the bulk morphology. The shear strength of the as-welded joint reached 31.5 MPa. The joint shear strength decreased slightly with reheating temperatures lower than 200 °C, while it decreased significantly (by about 10%) with reheating temperatures above 250 °C compared to the as-welded joint. The shear strength of the joints was determined by the brittle solder matrix, showing that the joint strength decreased with the coarsening of the δ phase in the eutectic structure. Full article
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14 pages, 2758 KiB  
Article
Parameter Measurement of Edible Sunflower Exudates and Calibration of Discrete Element Simulation Parameters
by Xiaoxiao Sun, Bin Li, Yang Liu and Xiaolong Gao
Processes 2022, 10(2), 185; https://doi.org/10.3390/pr10020185 - 18 Jan 2022
Cited by 7 | Viewed by 1614
Abstract
To improve the accuracy of the parameters used in discrete element simulation tests in the process of clearing fresh sunflowers, this study took the extracts of fresh sunflower as the research object and used a combination of physical experiments and simulation experiments to [...] Read more.
To improve the accuracy of the parameters used in discrete element simulation tests in the process of clearing fresh sunflowers, this study took the extracts of fresh sunflower as the research object and used a combination of physical experiments and simulation experiments to calibrate the discrete element simulation parameters. First, the composition of the edible sunflower extract is determined, and then, the physical test method is used to determine the characteristics of the edible sunflower extract material. Based on the results of the physical test as a simulation basis, the Plackett–Burman test is used to screen the significance of the test parameters, and the screening results show that the shear modulus, static friction coefficient, and collision recovery coefficient of sunflower kernels have significant effects on the simulated angle of repose. On the basis of the steepest climbing test, the Box–Behnken test is carried out to obtain the simulated angle of repose and significance. The second-order regression equation of texture parameters is optimized with the actual physical angle of repose (24.68°) as the target value to obtain the optimal parameter combination. Finally, through the two-sample T test, p > 0.05 is obtained, indicating that the simulated angle of repose and the actual physical test angle of repose are not significantly different, and the relative error is 0.923%, which verifies the reliability of the optimal simulation parameter combination. The research results show that the calibrated simulation parameter combination can be used in discrete element simulation tests of the extraction process of sunflower extracts. Full article
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24 pages, 7672 KiB  
Article
Semi-Infinite Structure Analysis with Bimodular Materials with Infinite Element
by Wang Huang, Jianjun Yang, Jan Sladek, Vladimir Sladek and Pihua Wen
Materials 2022, 15(2), 641; https://doi.org/10.3390/ma15020641 - 15 Jan 2022
Cited by 3 | Viewed by 1551
Abstract
The modulus of elasticity of some materials changes under tensile and compressive states is simulated by constructing a typical material nonlinearity in a numerical analysis in this paper. The meshless Finite Block Method (FBM) has been developed to deal with 3D semi-infinite structures [...] Read more.
The modulus of elasticity of some materials changes under tensile and compressive states is simulated by constructing a typical material nonlinearity in a numerical analysis in this paper. The meshless Finite Block Method (FBM) has been developed to deal with 3D semi-infinite structures in the bimodular materials in this paper. The Lagrange polynomial interpolation is utilized to construct the meshless shape function with the mapping technique to transform the irregular finite domain or semi-infinite physical solids into a normalized domain. A shear modulus strategy is developed to present the nonlinear characteristics of bimodular material. In order to verify the efficiency and accuracy of FBM, the numerical results are compared with both analytical and numerical solutions provided by Finite Element Method (FEM) in four examples. Full article
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16 pages, 7990 KiB  
Article
A Study on the Electromagnetic–Thermal Coupling Effect of Cross-Slot Frequency Selective Surface
by Yi Lu, Juan Chen, Jianxing Li and Wenjing Xu
Materials 2022, 15(2), 640; https://doi.org/10.3390/ma15020640 - 15 Jan 2022
Cited by 3 | Viewed by 1867
Abstract
In high-power microwave applications, the electromagnetic-thermal effect of frequency selective surface (FSS) cannot be ignored. In this paper, the electromagnetic-thermal coupling effects of cross-slot FSS were studied. We used an equivalent circuit method and CST software to analyze the electromagnetic characteristics of cross-slot [...] Read more.
In high-power microwave applications, the electromagnetic-thermal effect of frequency selective surface (FSS) cannot be ignored. In this paper, the electromagnetic-thermal coupling effects of cross-slot FSS were studied. We used an equivalent circuit method and CST software to analyze the electromagnetic characteristics of cross-slot FSS. Then, we used multi-field simulation software COMSOL Multiphysics to study the thermal effect of the FSSs. To verify the simulation results, we used a horn antenna with a power of 20 W to radiate the FSSs and obtain the stable temperature distribution of the FSSs. By using simulations and experiments, it is found that the maximum temperature of the cross-slot FSS appears in the middle of the cross slot. It is also found that the FSS with a narrow slot has severer thermal effect than that with a wide slot. In addition, the effects of different incident angles on the temperature variation of FSS under TE and TM polarization were also studied. It is found that in TE polarization, with the increase in incident angle, the maximum stable temperature of FSS increases gradually. In TM polarization, with the increase in incident angle, the maximum stable temperature of FSS decreases gradually. Full article
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17 pages, 8822 KiB  
Article
Investigation of the Mechanical and Liquid Absorption Properties of a Rice Straw-Based Composite for Ayurvedic Treatment Tables
by Abhishek Sadananda Madival, Deepak Doreswamy, Shripathi Adiga Handady, Krishna Raghava Hebbar and Shobha Karabylu Lakshminarayana
Materials 2022, 15(2), 606; https://doi.org/10.3390/ma15020606 - 14 Jan 2022
Cited by 6 | Viewed by 1707
Abstract
Managing rice crop stubble is one of the major challenges witnessed in the agricultural sector. This work attempts to investigate the physical, mechanical, and liquid absorption properties of rice straw (RS)-reinforced polymer composite for assessing its suitability to use as an ayurvedic treatment [...] Read more.
Managing rice crop stubble is one of the major challenges witnessed in the agricultural sector. This work attempts to investigate the physical, mechanical, and liquid absorption properties of rice straw (RS)-reinforced polymer composite for assessing its suitability to use as an ayurvedic treatment table. This material is expected to be an alternative for wooden-based ayurvedic treatment tables. The results showed that the addition of rice straw particles (RSp) up to 60% volume in epoxy reduced the density of the composite material by 46.20% and the hardness by 15.69%. The maximum tensile and flexural strength of the RSp composite was 17.53 MPa and 43.23 MPa, respectively. The scanning electron microscopy (SEM) analysis showed deposits of silica in the form of phytoliths in various size and shapes on the outer surface of RS. The study also revealed that the water absorption rate (WA) was less than 7.8% for the test samples with 45% volume of RSp. Interestingly the test samples showed greater resistance to the absorption of Kottakal Dhanvantaram Thailam (<2%). In addition, the developed samples showed resistance towards bacterial and fungal growth under the exposure of treatment oils and water. Full article
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16 pages, 4659 KiB  
Article
Continuous Prediction Model of Carbon Content in 120 t Converter Blowing Process
by Dazhi Wang, Fang Gao, Lidong Xing, Jianhua Chu and Yanping Bao
Metals 2022, 12(1), 151; https://doi.org/10.3390/met12010151 - 14 Jan 2022
Cited by 2 | Viewed by 1885
Abstract
A continuous prediction model of carbon content of 120 t BOF is established in this paper. Based on the three-stage decarburization theory and combined with the production process of 120 t converter, the effects of oxygen lance height and top blowing oxygen flow [...] Read more.
A continuous prediction model of carbon content of 120 t BOF is established in this paper. Based on the three-stage decarburization theory and combined with the production process of 120 t converter, the effects of oxygen lance height and top blowing oxygen flow rate are also considered in the model. The explicit finite difference method is used to realize continuous prediction of carbon content in the converter blowing process. The model parameters such as ultimate carbon content in molten pool are calculated according to the actual data of 120 t BOF, which improves the hit rate of the model. Process verification and end-point verification for the continuous prediction model have been carried out, and the results of process verification indicate that the continuous prediction model established in the paper basically accords with the actual behavior of decarburization. Moreover, the hit ratio of the continuous prediction model reached 85% for the prediction of end-point carbon content within a tolerance of ±0.02%. Full article
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14 pages, 8594 KiB  
Article
Compressive Rheological Behavior and Microstructure Evolution of a Semi-Solid CuSn10P1 Alloy at Medium Temperature and Low Strain
by Zhangxing Liu, Rongfeng Zhou, Wentao Xiong, Zilong He, Tao Liu and Yongkun Li
Metals 2022, 12(1), 143; https://doi.org/10.3390/met12010143 - 12 Jan 2022
Cited by 6 | Viewed by 1549
Abstract
Copper–tin alloys are widely used in the machining and molding of sleeves, bearings, bearing housings, gears, etc. They are a material used in heavy-duty, high-speed and high-temperature situations and subject to strong friction conditions due to their high strength, high modulus of elasticity, [...] Read more.
Copper–tin alloys are widely used in the machining and molding of sleeves, bearings, bearing housings, gears, etc. They are a material used in heavy-duty, high-speed and high-temperature situations and subject to strong friction conditions due to their high strength, high modulus of elasticity, low coefficient of friction and good wear and corrosion resistance. Although copper–tin alloys are excellent materials, a higher performance of mechanical parts is required under extreme operating conditions. Plastic deformation is an effective way to improve the overall performance of a workpiece. In this study, medium-temperature compression tests were performed on a semi-solid CuSn10P1 alloy using a Gleeble 1500D testing machine at different temperatures (350−440 °C) and strain rates (0.1−10 s−1) to obtain its medium-temperature deformation characteristics. The experimental results show that the filamentary deformation marks appearing during the deformation are not single twins or slip lines, but a mixture of dislocations, stacking faults and twins. Within the experimental parameters, the filamentary deformation marks increase with increasing strain and decrease with increasing temperature. Twinning subdivides the grains into lamellar sheets, and dislocation aggregates are found near the twinning boundaries. The results of this study are expected to make a theoretical contribution to the forming of copper–tin alloys in post-processing processes such as rolling and forging. Full article
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20 pages, 6262 KiB  
Article
A Comparative Study on the Microstructures and Mechanical Properties of Al-10Si-0.5Mg Alloys Prepared under Different Conditions
by Minghao Guo, Ming Sun, Junhui Huang and Song Pang
Metals 2022, 12(1), 142; https://doi.org/10.3390/met12010142 - 12 Jan 2022
Cited by 8 | Viewed by 1947
Abstract
Fabrication condition greatly influences the microstructures and properties of Al alloys. However, most of the available reports focus on a single fabrication technique, indicating there is still a lack of systematic comparisons among wider ranges of fabrication methods. In this paper, with conventional [...] Read more.
Fabrication condition greatly influences the microstructures and properties of Al alloys. However, most of the available reports focus on a single fabrication technique, indicating there is still a lack of systematic comparisons among wider ranges of fabrication methods. In this paper, with conventional casting (via sand/Fe/Cu mold) and additive manufacturing (AM, via selective laser melting, SLM) methods, the effects of cooling rate () on the microstructures and mechanical properties of hypoeutectic Al-10Si-0.5Mg alloy are systematically investigated. The results show that with increasing cooling rate from sand-mold condition to SLM condition, the grain size (d) is continuously refined from ~3522 ± 668 μm to ~10 μm, and the grain morphology is gradually refined from coarse dendrites to a mixed grain structure composed of columnar plus fine grains (~10 μm). The eutectic Si particles are effectively refined from blocky shape under sand/Fe-mold conditions to needle-like under Cu-mold conditions, and finally to fine fibrous network under SLM condition. The tensile yield strength and elongation is greatly improved from 125 ± 5 MPa (sand-mold) to 262 ± 3 MPa (SLM) and from 0.8 ± 0.2% (sand-mold) to 4.0 ± 0.2% (SLM), respectively. The strengthening mechanism is discussed, which is mainly ascribed to the continuous refinement of grains and Si particles and an increase in super-saturation of Al matrix with increasing cooling rate. Full article
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19 pages, 6702 KiB  
Article
Experimental Study of the Dynamic Characteristics of a New Antidrainage Subgrade Structure for High-Speed Railways in Diatomaceous Earth Areas
by Qian Su, Zhixing Deng, Xun Wang, Wenyi Jia and Yunbin Niu
Materials 2022, 15(2), 532; https://doi.org/10.3390/ma15020532 - 11 Jan 2022
Cited by 3 | Viewed by 1629
Abstract
The experience needed to carry out engineering and construction in diatomaceous earth areas is currently lacking. This project studies the new Hang Shaotai high-speed railway passing through a diatomaceous earth area in Shengzhou, Zhejiang Province, and analyzes the hydrological and mechanical properties of [...] Read more.
The experience needed to carry out engineering and construction in diatomaceous earth areas is currently lacking. This project studies the new Hang Shaotai high-speed railway passing through a diatomaceous earth area in Shengzhou, Zhejiang Province, and analyzes the hydrological and mechanical properties of diatomaceous earth on the basis of a field survey and laboratory. Moreover, a new antidrainage subgrade structure was proposed to address the rainy local environment, and field excitation tests were performed to verify the antidrainage performance and stability of the new subgrade structure. Finally, the dynamic characteristics and deformation of the diatomaceous earth roadbed were examined. The hydrophysical properties of diatomaceous earth in the area are extremely poor, and the disintegration resistance index ranges from 3.1% to 9.0%. The antidrainage subgrade structure has good water resistance and stability under dynamic loading while submerged in water. After 700,000 loading cycles, the dynamic stress and vibration acceleration of the surface of the subgrade bed stabilized at approximately 6.37 kPa and 0.94 m/s2, respectively. When the number of excitations reached 2 million, the settlement of the diatomaceous earth foundation was 0.08 mm, and there was basically negligible postwork settlement of the diatomaceous earth foundation. These results provide new insights for engineering construction in diatomaceous earth areas. Full article
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12 pages, 24812 KiB  
Article
Response Surface Optimization for Antioxidant Extraction and Attributes Liking from Roasted Rice Germ Flavored Herbal Tea
by Sriwiang Rittisak, Ratchanee Charoen, Natthaya Choosuk, Wanticha Savedboworn and Wiboon Riansa-ngawong
Processes 2022, 10(1), 125; https://doi.org/10.3390/pr10010125 - 07 Jan 2022
Cited by 3 | Viewed by 2176
Abstract
The optimal process conditions when examining the antioxidant potential, total polyphenol content, and attribute liking in roasted rice germ flavored herbal tea were investigated using response surface methodology (RSM). The influence upon the extraction process of time and temperature was assessed using a [...] Read more.
The optimal process conditions when examining the antioxidant potential, total polyphenol content, and attribute liking in roasted rice germ flavored herbal tea were investigated using response surface methodology (RSM). The influence upon the extraction process of time and temperature was assessed using a full factorial design on three levels with two variables (32), involving five central point replicates. Extraction temperature (70 °C, 80 °C, and 90 °C) and extraction time (3 min, 4.5 min, and 6 min) served as independent variables, while the dependent variables were allocated to the regression equation to determine antioxidant activity (R2 = 0.941) along with total polyphenol content (R2 = 0.849), flavor liking score (R2 = 0.758), and overall liking score (R2 = 0.816). Following experimentation, it was determined that the optimal time and temperature conditions to maximize total polyphenol content, antioxidant activity, flavor, and overall liking score were in a range of 86 °C to 90 °C for 3.4 min to 5.9 min. When these conditions were imposed, the antioxidant potential, total polyphenol content, flavor, and overall liking score were >70% for DPPH scavenging activity, >75 mgGAE/g, >6.7 (like moderately), and >6.5 (like moderately), respectively. Full article
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12 pages, 4529 KiB  
Article
Modeling of Grouting Penetration in Porous Medium with Influence of Grain Distribution and Grout–Water Interaction
by Mengmeng Zhou, Fengshuai Fan, Zhuo Zheng and Chenyang Ma
Processes 2022, 10(1), 77; https://doi.org/10.3390/pr10010077 - 30 Dec 2021
Cited by 3 | Viewed by 2444
Abstract
In this study, a numerical model of grouting penetration in a porous medium is established. The fluid flow in the interstices of the porous medium is directly modeled by Navier–Stokes equations. The grouting process is considered as a two-phase flow problem, and the [...] Read more.
In this study, a numerical model of grouting penetration in a porous medium is established. The fluid flow in the interstices of the porous medium is directly modeled by Navier–Stokes equations. The grouting process is considered as a two-phase flow problem, and the level set method is used to characterize the interaction between grout and groundwater. The proposed model has considered the nuances for each grain during grouting penetration, instead of representing the fluid flow as a continuum process. In the simulation, three kinds of porosity (0.3; 0.4; 0.5) and two kinds of grain size distribution (0.5~1 mm; 1~2 mm) are used. Results show that: the pressure drop along penetration distance is approximately in a linear trend. The variation of filling degree along grouting distance approximately obeys a quadratic polynomial function. The injection pressure is influenced by the porosity and grain size of the porous medium, especially by the former. A theoretical analysis is carried out to propose an analytical solution of the grouting penetration. The analytical solution gives a good estimation when the grain amounts in the porous medium are small, and the difference becomes larger as the grain amounts increase. Full article
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15 pages, 5764 KiB  
Article
Understanding the Failure Mechanism of Thermal Barrier Coatings Considering the Local Bulge at the Interface between YSZ Ceramic and Bond Layer
by Zhi-Yuan Wei and Hong-Neng Cai
Materials 2022, 15(1), 275; https://doi.org/10.3390/ma15010275 - 30 Dec 2021
Cited by 5 | Viewed by 1948
Abstract
The TC/BC interface morphology in APS TBC is one of the important factors leading to crack propagation and coating failure. Long cracks are found near the bulge on the TC/BC interface. In this study, the TBC model with the bulge on the interface [...] Read more.
The TC/BC interface morphology in APS TBC is one of the important factors leading to crack propagation and coating failure. Long cracks are found near the bulge on the TC/BC interface. In this study, the TBC model with the bulge on the interface is developed to explore the influence of the bulge on the coating failure. Dynamic TGO growth and crack propagation are considered in the model. The effects of the bulge on the stress state and crack propagation in the ceramic layer are examined. Moreover, the effects of the distribution and number of bulges are also investigated. The results show that the bulge on the interface results in the redistribution of local stress. The early cracking of the ceramic layer occurs near the top of the bulge. One bulge near the peak or valley of the interface leads to a coating life reduction of about 75% compared with that without a bulge. The increase in the number of bulges further decreases the coating life, which is independent of the bulge location. The results in this work indicate that a smooth TC/BC interface obtained by some possible surface treatments may be an optional scenario for improving coating life. Full article
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11 pages, 2747 KiB  
Article
Optimization of Machining Parameters for Milling Zirconia Ceramics by Polycrystalline Diamond Tool
by Xuefeng Yan, Shuliang Dong, Xianzhun Li, Zhonglin Zhao, Shuling Dong and Libao An
Materials 2022, 15(1), 208; https://doi.org/10.3390/ma15010208 - 28 Dec 2021
Cited by 9 | Viewed by 1690
Abstract
Zirconia ceramics are widely used in many fields because of their excellent physical and mechanical properties. However, there are some challenges to machine zirconia ceramics with high processing efficiency. In order to optimize parameters for milling zirconia ceramics by polycrystalline diamond tool, finite [...] Read more.
Zirconia ceramics are widely used in many fields because of their excellent physical and mechanical properties. However, there are some challenges to machine zirconia ceramics with high processing efficiency. In order to optimize parameters for milling zirconia ceramics by polycrystalline diamond tool, finite element method was used to simulate machining process based on Johnson-Cook constitutive model. The effects of spindle speed, feed rate, radial and axial cutting depth on cutting force, tool flank wear and material removal rate were investigated. The results of the simulation experiment were analyzed and optimized by the response surface method. The optimal parameter combination was obtained when the spindle speed, feed rate, radial and axial cutting depth were 8000 r/min, 90.65 mm/min, 0.10 mm and 1.37 mm, respectively. Under these conditions, the cutting force was 234.81 N, the tool flank wear was 33.40 μm when the milling length was 60 mm and the material removal rate was 44.65 mm3/min. Full article
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18 pages, 4260 KiB  
Article
A Sustainable Process to Produce Manganese and Its Alloys through Hydrogen and Aluminothermic Reduction
by Jafar Safarian
Processes 2022, 10(1), 27; https://doi.org/10.3390/pr10010027 - 24 Dec 2021
Cited by 6 | Viewed by 4091
Abstract
Hydrogen and aluminum were used to produce manganese, aluminum–manganese (AlMn) and ferromanganese (FeMn) alloys through experimental work, and mass and energy balances. Oxide pellets were made from Mn oxide and CaO powder, followed by pre-reduction by hydrogen. The reduced MnO pellets were then [...] Read more.
Hydrogen and aluminum were used to produce manganese, aluminum–manganese (AlMn) and ferromanganese (FeMn) alloys through experimental work, and mass and energy balances. Oxide pellets were made from Mn oxide and CaO powder, followed by pre-reduction by hydrogen. The reduced MnO pellets were then smelted and reduced at elevated temperatures through CaO flux and Al reductant addition, yielding metallic Mn. Changing the amount of the added Al for the aluminothermic reduction, with or without iron addition led to the production of Mn metal, AlMn alloy and FeMn alloy. Mass and energy balances were carried out for three scenarios to produce these metal products with feasible material flows. An integrated process with three main steps is introduced; a pre-reduction unit to pre-reduce Mn ore, a smelting-aluminothermic reduction unit to produce metals from the pre-reduced ore, and a gas treatment unit to do heat recovery and hydrogen looping from the pre-reduction process gas. It is shown that the process is sustainable regarding the valorization of industrial waste and the energy consumptions for Mn and its alloys production via this process are lower than current commercial processes. Ferromanganese production by this process will prevent the emission of about 1.5 t CO2/t metal. Full article
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11 pages, 2659 KiB  
Article
Half Metallic Ferromagnetism and Transport Properties of Zinc Chalcogenides ZnX2Se4 (X = Ti, V, Cr) for Spintronic Applications
by Mohsen Al-Qhtani, Ghulam M. Mustafa, Nasheeta Mazhar, Sonia Bouzgarrou, Qasim Mahmood, Abeer Mera, Zaki I. Zaki, Nasser Y. Mostafa, Saad H. Alotaibi and Mohammed A. Amin
Materials 2022, 15(1), 55; https://doi.org/10.3390/ma15010055 - 22 Dec 2021
Cited by 7 | Viewed by 2937 | Correction
Abstract
In ferromagnetic semiconductors, the coupling of magnetic ordering with semiconductor character accelerates the quantum computing. The structural stability, Curie temperature (Tc), spin polarization, half magnetic ferromagnetism and transport properties of ZnX2Se4 (X = Ti, V, Cr) chalcogenides for [...] Read more.
In ferromagnetic semiconductors, the coupling of magnetic ordering with semiconductor character accelerates the quantum computing. The structural stability, Curie temperature (Tc), spin polarization, half magnetic ferromagnetism and transport properties of ZnX2Se4 (X = Ti, V, Cr) chalcogenides for spintronic and thermoelectric applications are studied here by density functional theory (DFT). The highest value of Tc is perceived for ZnCr2Se4. The band structures in both spin channels confirmed half metallic ferromagnetic behavior, which is approved by integer magnetic moments (2, 3, 4) μB of Ti, V and Cr based spinels. The HM behavior is further measured by computing crystal field energy ΔEcrystal, exchange energies Δx(d), Δx (pd) and exchange constants (Noα and Noβ). The thermoelectric properties are addressed in terms of electrical conductivity, thermal conductivity, Seebeck coefficient and power factor in within a temperature range 0–400 K. The positive Seebeck coefficient shows p-type character and the PF is highest for ZnTi2Se4 (1.2 × 1011 W/mK2) among studied compounds. Full article
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