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Keywords = sweep frequency impedance

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23 pages, 3698 KB  
Article
Design of a Thin-Film Lithium Niobate Electro-Optic Modulator with Three-Dimensional L-Shaped Traveling-Wave Electrodes
by Yingbo Liu, Haiou Li, Yue Li, Yuxiang Hao and Liangpeng Qin
Photonics 2026, 13(5), 502; https://doi.org/10.3390/photonics13050502 - 19 May 2026
Viewed by 630
Abstract
The systematic influence of signal electrode width on electro-optic bandwidth and insertion loss in L-type traveling-wave lithium niobate modulators has not yet been comprehensively quantified, limiting the parametric engineering design of this device configuration. This study presents a full-band systematic simulation sweep of [...] Read more.
The systematic influence of signal electrode width on electro-optic bandwidth and insertion loss in L-type traveling-wave lithium niobate modulators has not yet been comprehensively quantified, limiting the parametric engineering design of this device configuration. This study presents a full-band systematic simulation sweep of signal electrode width and three auxiliary geometric parameters in an L-type traveling-wave lithium niobate Mach–Zehnder modulator, combined with optical mode simulation to establish joint microwave–optical optimization constraints. The study reveals the coupled modulating effect of signal electrode width on characteristic impedance, velocity mismatch, and transmission loss; it elucidates the competition mechanism underlying non-monotonic high-frequency loss behavior; and it identifies the complete impedance-neutral characteristic of the electrode–waveguide contact width as an independent loss-tuning degree of freedom decoupled from the impedance constraint. Full-system validation confirms that the final design simultaneously satisfies broadband impedance matching, low insertion loss, and high electro-optic bandwidth. The results are distilled into four quantitative design rules that provide simulation-driven guidance directly applicable to the engineering design of L-type thin-film lithium niobate modulators, advancing the systematic establishment of a parametric design methodology for this device configuration. Full article
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12 pages, 2082 KB  
Article
Design and Experimental Validation of a Dynamic Frequency Sweeping Algorithm for Optimized Impedance Matching in Semiconductor RF Power Systems Under Pulse-Mode Operation
by Zhaolong Fan, Zhifeng Wang, Long Xu, Lili Hou, Long Yao, Siao Zeng and Mingqing Liu
Micromachines 2026, 17(3), 376; https://doi.org/10.3390/mi17030376 - 20 Mar 2026
Viewed by 724
Abstract
The design and implementation of a dynamic frequency sweeping algorithm for a 3 kW RF power source are underpinned by theoretical principles aimed at optimizing impedance matching under pulse-mode operation. The algorithm dynamically adjusts the output frequency within a predefined range to align [...] Read more.
The design and implementation of a dynamic frequency sweeping algorithm for a 3 kW RF power source are underpinned by theoretical principles aimed at optimizing impedance matching under pulse-mode operation. The algorithm dynamically adjusts the output frequency within a predefined range to align the source impedance Zsource with the conjugate of the load impedance Z*load, maximizing the power transfer efficiency and minimizing the reflection coefficient Γ. This is achieved by leveraging the maximum power transfer theorem and adapting to dynamic load variations, such as those induced by the plasma state transitions. The algorithm incorporates adaptive step size adjustments based on the rate of change of Γ, predictive frequency initialization using historical data, and real-time impedance monitoring to ensure efficient convergence within the constrained pulse “ON” time (TON). Integration with pulse mode requires synchronization with the pulse signal, fast convergence, and optimized search strategies. Experimental validation on a 13.56 MHz, 3 kW Automatic Sweep Generator testbed operating at 20 kHz pulse modulation with a 50% duty cycle demonstrates a linear and stable sweep, achieving impedance matching and low reflected power within 5.0172 ms. These findings highlight the algorithm’s potential for high-precision applications, such as RF plasma excitation, and underscore the importance of adaptive techniques in dynamic RF systems. Full article
(This article belongs to the Special Issue Emerging Technologies and Applications for Semiconductor Industry)
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21 pages, 5143 KB  
Article
BP Neural Network-Based Adaptive Phase-Locked Loop for Impedance Measurement with Dynamic Operating Conditions
by Zhiren Liu, Jian Dai, Chengkai Peng, Xuan Zhao and Zhixiang Zou
Electronics 2026, 15(4), 781; https://doi.org/10.3390/electronics15040781 - 12 Feb 2026
Viewed by 503
Abstract
With the development of modern power systems, impedance measurement has become a key approach for stability assessment of power-electronic-dominated grids. In particular, frequency-sweep–based impedance measurement is widely adopted due to its effectiveness in characterizing system dynamics. However, owing to the limited adaptability of [...] Read more.
With the development of modern power systems, impedance measurement has become a key approach for stability assessment of power-electronic-dominated grids. In particular, frequency-sweep–based impedance measurement is widely adopted due to its effectiveness in characterizing system dynamics. However, owing to the limited adaptability of conventional phase-locked loop (PLL), grid-following (GFL) converters encounter significant challenges in maintaining stable operation during frequency-sweep signal injection, especially under non-power-frequency excitation and grid disturbances. To address these issues, this paper proposes an adaptive PLL scheme based on a backpropagation (BP) neural network. This scheme fully leverages the nonlinear mapping and adaptive learning capabilities of the BP neural network, which significantly enhances the robustness and stability adaptability of the synchronization component against small disturbances during the impedance measurement process. A hybrid strategy combining offline parameter tuning and online adaptive adjustment is adopted to improve reliability under varying operating conditions. Comprehensive simulation studies and hardware-in-the-loop (HIL) experimental results verify the effectiveness of the proposed method in improving stability and impedance measurement accuracy in frequency-sweep–based applications. Full article
(This article belongs to the Special Issue Planning, Scheduling and Control of Grids with Renewables)
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17 pages, 3951 KB  
Article
Development of a Flexible Microneedle Array Electrode with a High Signal-to-Noise Ratio for Surface Bioelectrical Signal Recording
by Bo Jiang, Ye Wang, Ruiqing Li, Yan Zhou, Lihua Ma, Dingjie Suo and Guangying Pei
Biosensors 2026, 16(2), 108; https://doi.org/10.3390/bios16020108 - 7 Feb 2026
Viewed by 992
Abstract
Microneedle array (MNA) electrodes have garnered significant attention for their capacity to record high-fidelity surface bioelectrical signals over extended periods and convenience. However, accuracy limitations in 3D-printed metal MNA electrodes, particularly concerning surface roughness and insufficient tip sharpness, have been reported. Additionally, the [...] Read more.
Microneedle array (MNA) electrodes have garnered significant attention for their capacity to record high-fidelity surface bioelectrical signals over extended periods and convenience. However, accuracy limitations in 3D-printed metal MNA electrodes, particularly concerning surface roughness and insufficient tip sharpness, have been reported. Additionally, the prevalent use of nonporous metal substrates often results in poor flexibility. This study proposes a novel MNA electrode featuring a lightweight flexible substrate and sharp, smooth microneedles. Utilizing micron-level metal 3D printing with 316L stainless steel, we fabricated the electrodes in a single step. We evaluated the MNA electrode-skin interface impedance via frequency sweep and assessed mechanical properties using porcine skin, followed by the collection and analysis of bioelectrical signals. The results demonstrate that the contact impedance of the MNA electrode is comparable to that of standard gold cup electrodes, with validated flexibility and strength. Furthermore, the MNA electrodes achieved a high signal-to-noise ratio and minimal motion artifacts during recording, thereby enhancing both comfort and signal quality. The efficient production process facilitates the broader application of metal MNA electrodes. Full article
(This article belongs to the Special Issue Recent Advances in Microneedle Array Electrodes in Biomedicine)
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19 pages, 6578 KB  
Article
High-Resolution Spatiotemporal-Coded Differential Eddy-Current Array Probe for Defect Detection in Metal Substrates
by Qi Ouyang, Yuke Meng, Lun Huang and Yun Li
Sensors 2026, 26(2), 537; https://doi.org/10.3390/s26020537 - 13 Jan 2026
Cited by 1 | Viewed by 600
Abstract
To address the problems of weak geometric features, low signal response amplitude, and insufficient spatial resolvability of near-surface defects in metal substrates, a high-resolution spatiotemporal-coded eddy-current array probe is proposed. The probe adopts an array topology with time-multiplexed excitation and adjacent differential reception, [...] Read more.
To address the problems of weak geometric features, low signal response amplitude, and insufficient spatial resolvability of near-surface defects in metal substrates, a high-resolution spatiotemporal-coded eddy-current array probe is proposed. The probe adopts an array topology with time-multiplexed excitation and adjacent differential reception, achieving a balance between high common-mode rejection ratio and high-density spatial sampling. First, a theoretical electromagnetic coupling model between the probe and the metal substrate is established, and finite-element simulations are conducted to investigate the evolution of the skin effect, eddy-current density distribution, and differential impedance response over an excitation frequency range of 1–10 MHz. Subsequently, a 64-channel M-DECA probe and an experimental testing platform are developed, and frequency-sweeping experiments are carried out under different excitation conditions. Experimental results indicate that, under a 50 kHz excitation frequency, the array eddy-current response achieves an optimal trade-off between signal amplitude and spatial geometric consistency. Furthermore, based on the pixel-to-physical coordinate mapping relationship, the lateral equivalent diameters of near-surface defects with different characteristic scales are quantitatively characterized, with relative errors of 6.35%, 4.29%, 3.98%, 3.50%, and 5.80%, respectively. Regression-based quantitative analysis reveals a power-law relationship between defect area and the amplitude of the differential eddy-current array response, with a coefficient of determination R2=0.9034 for the bipolar peak-to-peak feature. The proposed M-DECA probe enables high-resolution imaging and quantitative characterization of near-surface defects in metal substrates, providing an effective solution for electromagnetic detection of near-surface, low-contrast defects. Full article
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20 pages, 3539 KB  
Article
Real-Time Monitoring of NIH/3T3 Cell Growth and Drug Reaction Using Impedance Biosensors and Comparison with Biological Assays
by Seok-kyu Kim, Gayoung Lee, Yeeun Kim, Dahyun Kang and Moongyu Jang
Biosensors 2025, 15(12), 788; https://doi.org/10.3390/bios15120788 - 1 Dec 2025
Viewed by 1307
Abstract
Impedance biosensors are manufactured on glass slides using a semiconductor process to monitor cell growth and cell–drug reactions in real time, and the results are compared with biological assay results to confirm the validity of impedance measurement method. Approximately 10,000 cells per well [...] Read more.
Impedance biosensors are manufactured on glass slides using a semiconductor process to monitor cell growth and cell–drug reactions in real time, and the results are compared with biological assay results to confirm the validity of impedance measurement method. Approximately 10,000 cells per well were cultured for 48 h, after which 6.67 μg/mL puromycin was injected to observe apoptosis over the following 48 h. A frequency sweep from 1 kHz to 1 MHz was performed to determine the optimal frequency range, identifying 367–440 kHz as the most sensitive for detecting impedance changes. Impedance was measured every 10 min for 96 h. Capacitance gradually increased during cell proliferation, while after drug administration, a transient increase occurred within 9 h, followed by a rapid decline, indicating cell death within 24 h. The sensor utilized Electrical Cell–substrate Impedance Sensing (ECIS) to detect real-time changes in cell status without the need for staining or destruction. Comparison with conventional biological assays such as MTS and FACS confirmed that the impedance biosensor provided higher sensitivity and quantitative accuracy in monitoring both cell proliferation and apoptosis. This study demonstrates that the developed biosensor enables label-free, non-invasive, and continuous monitoring of cellular behaviors with acceptable coincidence with 3 different biological assay results. Impedance biosensor presents a promising alternative to conventional biological assays and offers potential applications in drug screening, cytotoxicity evaluation, and real-time biological monitoring. Full article
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18 pages, 7499 KB  
Article
Transformer Winding Fault Locating Using Frequency Domain Reflectometry (FDR) Technology
by Hao Yun, Yizhou Zhang, Yufei Sun, Liang Wang, Lulin Xu, Daning Zhang and Jialu Cheng
Electronics 2025, 14(15), 3117; https://doi.org/10.3390/electronics14153117 - 5 Aug 2025
Cited by 2 | Viewed by 1287
Abstract
Detecting power transformer winding degradations at an early stage is very important for the safe operation of nuclear power plants. Most transformer failures are caused by insulation breakdown; the winding turn-to-turn short circuit fault is frequently encountered. Experience has shown that routine testing [...] Read more.
Detecting power transformer winding degradations at an early stage is very important for the safe operation of nuclear power plants. Most transformer failures are caused by insulation breakdown; the winding turn-to-turn short circuit fault is frequently encountered. Experience has shown that routine testing techniques, e.g., winding resistance, leakage inductance, and sweep frequency response analysis (SFRA), are not sensitive enough to identify minor turn-to-turn short defects. The SFRA technique is effective only if the fault is in such a condition that the flux distribution in the core is prominently distorted. This paper proposes the frequency domain reflectometry (FDR) technique for detecting and locating transformer winding defects. FDR measures the wave impedance and its change along the measured windings. The wire over a plane model is selected as the transmission line model for the transformer winding. The effectiveness is verified through lab experiments on a twist pair cable simulating the transformer winding and field testing on a real transformer. The FDR technique successfully identified and located the turn-to-turn short fault that was not detected by other testing techniques. Using FDR as a complementary tool for winding condition assessment will be beneficial. Full article
(This article belongs to the Section Power Electronics)
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11 pages, 4207 KB  
Proceeding Paper
Portable, Energy-Autonomous Electrochemical Impedance Spectroscopy (EIS) System Based on Python and Single-Board Computer
by Jhon Alvaro Cuastuza and Carlos Andrés Rosero-Zambrano
Eng. Proc. 2025, 87(1), 89; https://doi.org/10.3390/engproc2025087089 - 9 Jul 2025
Cited by 1 | Viewed by 1428
Abstract
We develop a modular, wireless, solar- and battery-powered system for detecting chlorpyrifos (LorsbanTM 2.5% DP) in water using electrochemical impedance spectroscopy (EIS). The system integrates a Raspberry Pi Zero 2W for data processing, Python-based software (version 3.12.2), and a solar charge manager [...] Read more.
We develop a modular, wireless, solar- and battery-powered system for detecting chlorpyrifos (LorsbanTM 2.5% DP) in water using electrochemical impedance spectroscopy (EIS). The system integrates a Raspberry Pi Zero 2W for data processing, Python-based software (version 3.12.2), and a solar charge manager to power all components via a lithium-ion battery and solar panel. A commercial EmStat Pico Module and an amperometric biosensor with acetylcholinesterase (AChE) detect chlorpyrifos. Nine water samples with varying concentrations were tested using a 20 Hz–200 kHz frequency sweep and 15 mV excitation. Bode plots and statistical analyses confirmed statistically significant impedance variation as a function of chlorpyrifos concentration, validating the system as a portable, sensitive, and effective tool for environmental monitoring. Full article
(This article belongs to the Proceedings of The 5th International Electronic Conference on Applied Sciences)
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15 pages, 797 KB  
Article
Incremental Capacity and Voltammetry of Batteries, and Implications for Electrochemical Impedance Spectroscopy
by Christopher Dunn, Jonathan Scott, Marcus Wilson, Michael Mucalo and Michael Cree
Metrology 2025, 5(2), 31; https://doi.org/10.3390/metrology5020031 - 3 Jun 2025
Cited by 1 | Viewed by 2345
Abstract
Incremental capacity analysis (ICA), where incremental charge (Q) movements associated with changes in potential are tracked, and cyclic voltammetry (CV), where current response to a linear voltage sweep is recorded, are used to investigate the properties of electrochemical systems. Electrochemical impedance spectroscopy (EIS), [...] Read more.
Incremental capacity analysis (ICA), where incremental charge (Q) movements associated with changes in potential are tracked, and cyclic voltammetry (CV), where current response to a linear voltage sweep is recorded, are used to investigate the properties of electrochemical systems. Electrochemical impedance spectroscopy (EIS), on the other hand, is a powerful, non-destructive technique that can be used to determine small-signal AC impedance over a wide frequency range. It is frequently used to design battery equivalent-circuit models. This manuscript explores the relationships between ICA, CV and EIS and demonstrates how sweep rate in CV is related to charging (C) rate in ICA. In addition, it shows the connection between observations linked to rate of charge movement in CV and ICA and intermittent, irregular behavior seen in EIS when performed on a battery. It also explains the use of an additional DC stimulus during EIS to ensure reliability of battery impedance data and to facilitate equivalent-circuit modeling, and suggests a method for obtaining data analogous to CV from a whole battery without risking its destruction. Full article
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25 pages, 4089 KB  
Article
Taguchi Method-Based Synthesis of a Circular Antenna Array for Enhanced IoT Applications
by Wided Amara, Ramzi Kheder, Ridha Ghayoula, Issam El Gmati, Amor Smida, Jaouhar Fattahi and Lassaad Latrach
Telecom 2025, 6(1), 7; https://doi.org/10.3390/telecom6010007 - 14 Jan 2025
Cited by 4 | Viewed by 2467
Abstract
Linear antenna arrays exhibit radiation patterns that are restricted to a half-space and feature axial radiation, which can be a significant drawback for applications that require omnidirectional coverage. To address this limitation, the synthesis method utilizing the Taguchi approach, originally designed for linear [...] Read more.
Linear antenna arrays exhibit radiation patterns that are restricted to a half-space and feature axial radiation, which can be a significant drawback for applications that require omnidirectional coverage. To address this limitation, the synthesis method utilizing the Taguchi approach, originally designed for linear arrays, can be effectively extended to two-dimensional or planar antenna arrays. In the context of a linear array, the synthesis process primarily involves determining the feeding law and/or the spatial distribution of the elements along a single axis. Conversely, for a planar array, the synthesis becomes more complex, as it requires the identification of the complex weighting of the feed and/or the spatial distribution of sources across a two-dimensional plane. This adaptation to planar arrays is facilitated by substituting the direction θ with the pair of directions (θ,ϕ), allowing for a more comprehensive coverage of the angular domain. This article focuses on exploring various configurations of planar arrays, aiming to enhance their performance. The primary objective of these configurations is often to minimize the levels of secondary lobes and/or array lobes while enabling a full sweep of the angular space. Secondary lobes can significantly impede system performance, particularly in multibeam applications, where they restrict the minimum distance for frequency channel reuse. This restriction is critical, as it affects the overall efficiency and effectiveness of communication systems that rely on precise beamforming and frequency allocation. By investigating alternative planar array designs and their synthesis methods, this research seeks to provide solutions that improve coverage, reduce interference from secondary lobes, and ultimately enhance the functionality of antennas in diverse applications, including telecommunications, radar systems, and wireless communication. Full article
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14 pages, 6132 KB  
Article
Design of Two Compact Wideband Monopoles Through Loading with Linear Approximated Lumped Components
by Jiansen Ma, Weiping Cao and Xinhua Yu
Micromachines 2024, 15(12), 1477; https://doi.org/10.3390/mi15121477 - 7 Dec 2024
Cited by 2 | Viewed by 2071
Abstract
In this paper, two ultra-wideband monopoles in a colinear structure are presented for application in remote terrestrial communication systems. The antennas consist of a loaded monopole with a hat and an elevated loaded monopole located in the upper position. All lumped loads are [...] Read more.
In this paper, two ultra-wideband monopoles in a colinear structure are presented for application in remote terrestrial communication systems. The antennas consist of a loaded monopole with a hat and an elevated loaded monopole located in the upper position. All lumped loads are modeled as linear frequency-dependent components to approximate the practical component property for achieving ultra-wideband characteristics, since the constant value property of a component is only present in a relatively narrow band. The antennas are simulated by the method of moments (MoM) with asymptotic waveform evaluation (AWE) to speed up frequency sweep across a wide bandwidth. For proper simulation with the AWE process, the parallel RLC load with linear frequency-dependent components is modeled in a corresponding impedance function. With the optimized load parameters, one antenna covers 30–750 MHz with a VSWR < 3.5 and the other one covers 800 MHz–3000 MHz with a VSWR < 2.5, which are promising results for terrestrial omnidirectional applications. Full article
(This article belongs to the Special Issue RF MEMS and Microsystems)
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11 pages, 4563 KB  
Article
A Spectroscopy Solution for Contactless Conductivity Detection in Capillary Electrophoresis
by Tomas Drevinskas, Audrius Maruška, Hirotaka Ihara, Makoto Takafuji, Linas Jonušauskas, Domantas Armonavičius, Mantas Stankevičius, Kristina Bimbiraitė-Survilienė, Elzbieta Skrzydlewska, Ona Ragažinskienė, Yutaka Kuwahara, Shoji Nagaoka, Vilma Kaškonienė and Loreta Kubilienė
Micromachines 2024, 15(12), 1430; https://doi.org/10.3390/mi15121430 - 28 Nov 2024
Cited by 1 | Viewed by 2484
Abstract
This paper introduces a novel contactless single-chip detector that utilizes impedance-to-digital conversion technology to measure impedance in the microfluidic channel or capillary format analytical device. The detector is designed to operate similarly to capacitively coupled contactless conductivity detectors for capillary electrophoresis or chromatography [...] Read more.
This paper introduces a novel contactless single-chip detector that utilizes impedance-to-digital conversion technology to measure impedance in the microfluidic channel or capillary format analytical device. The detector is designed to operate similarly to capacitively coupled contactless conductivity detectors for capillary electrophoresis or chromatography but with the added capability of performing frequency sweeps up to 200 kHz. At each recorded data point, impedance and phase-shift data can be extracted, which can be used to generate impedance versus frequency plots, or phase-shift versus frequency plots. Real and imaginary parts can also be calculated from the data, allowing for the generation of Nyquist diagrams. This detector represents the first of its kind in the contactless conductivity class to provide spectrum-type data, as demonstrated in capillary electrophoresis experiments. Full article
(This article belongs to the Special Issue Flows in Micro- and Nano-Systems)
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21 pages, 9179 KB  
Article
Analysis of Influence of Grid-Following and Grid-Forming Static Var Generators on High-Frequency Resonance in Doubly Fed Induction Generator-Based Wind Farms
by Yong Sun, Hongbin Wu, Xiaozhe Song, Haifeng Zhang, Yifu Zhang, Jikai Chen and Hongpeng Liu
Electronics 2024, 13(19), 3879; https://doi.org/10.3390/electronics13193879 - 30 Sep 2024
Cited by 6 | Viewed by 2419
Abstract
In Doubly Fed Induction Generator (DFIG)-based wind farms with Static Var Generators (SVGs), high-frequency resonance will be more like to occur when an unloaded cable is put into operation, which will threaten the stable operation of the wind farm. To address this issue, [...] Read more.
In Doubly Fed Induction Generator (DFIG)-based wind farms with Static Var Generators (SVGs), high-frequency resonance will be more like to occur when an unloaded cable is put into operation, which will threaten the stable operation of the wind farm. To address this issue, the influence of power outer loops on the impedance of grid-connected inverters is considered. Based on harmonic linearization, theoretical models for the sequence impedances of DFIGs, Grid-following (GFL) SVGs, and Grid-forming (GFM) SVGs are established. The correctness of the three models is verified by impedance scanning using the frequency sweep method. Through a comparative analysis of these sequence impedances, it is found that unlike the GFM SVG (which exhibits inductive impedance), the GFL SVG exhibits capacitive impedance in the high-frequency band, which leads to negative damping characteristics in the high-frequency band for the wind farm system with the grid-following SVG; thereby, the risk of high-frequency resonance also increases accordingly. On the contrary, GFM control adopted by SVGs can effectively eliminate the negative damping region in the high-frequency band for wind farms to suppress high-frequency resonance. Meanwhile, for grid-forming SVGs, the parameter variations in power synchronous loops have no significant impact on the suppressing effect of high-frequency resonance for wind farms. Finally, an electromagnetic simulation model for a DFIG-based wind farm system with an SVG is established using the StarSim-HIL (hardware-in-the-loop) experiment platform, and the simulation results validate the correctness of the theoretical analysis. Full article
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8 pages, 1953 KB  
Proceeding Paper
Impedance Matching Optimization of RF Networks
by Miroslav Tomov, Stanimir Sadinov and Boris Arsov
Eng. Proc. 2024, 70(1), 46; https://doi.org/10.3390/engproc2024070046 - 12 Aug 2024
Cited by 1 | Viewed by 3200
Abstract
The subject of this publication is a synthesized description of an S-parameter linear analysis for the improvement of a particular RF amplifier. The model is applied in a simulation environment as a 100–500 MHz two-port device under test with control of the input [...] Read more.
The subject of this publication is a synthesized description of an S-parameter linear analysis for the improvement of a particular RF amplifier. The model is applied in a simulation environment as a 100–500 MHz two-port device under test with control of the input and output impedance of the RF amplifier. The main goal of the exploration is to achieve a near-perfect impedance match in the input and output stages of a particular RF amplifying schematic. For that purpose, a computing sub-application was created and used in the simulation environment of Keysight Genesys. An appropriate sweep of the parameters’ values of the respective elements of the schematic allows simultaneous changes of the working point position on the diagrams corresponding to the maximum efficient operating mode of the amplifier for the operating frequency range. The upgrade of the initial schematic design usually achieves much better performance and overall behavior of the RF amplifiers from the perspective of the optimum gain and efficiency. Full article
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26 pages, 3870 KB  
Article
Circular Economy of Construction and Demolition Waste for Nanocomposite Cement: XRD, NMR, Vickers, Voltammetric and EIS Characterization
by Roxana Rada, Daniela Lucia Manea, Simona Rada and Radu Fechete
Nanomaterials 2024, 14(15), 1239; https://doi.org/10.3390/nano14151239 - 23 Jul 2024
Cited by 3 | Viewed by 1686
Abstract
In this paper, we present the structural, mechanical and electrical properties of composite cement materials that can be widely used as substituent for cement. We start with the characterization of a composite cement sample using an analysis of X-ray diffraction (XRD) and nuclear [...] Read more.
In this paper, we present the structural, mechanical and electrical properties of composite cement materials that can be widely used as substituent for cement. We start with the characterization of a composite cement sample using an analysis of X-ray diffraction (XRD) and nuclear magnetic resonance (NMR) spectra. The measurements of the Vickers hardness, cyclic and sweep linear voltammetry and electrochemical impedance spectroscopy (EIS) of composite cement materials were also recorded. This study compared the effect of the different nanocomposites added to cement on the mitigation of the alkali–silica reaction, which is responsible for the swelling, cracking and deleterious behavior of the material. The enhancement in Vickers hardness was more pronounced for composite cement materials. In contrast, the values of Vickers hardness decreased for the composite cement containing mortar and the control sample, suggesting that the long-term performance of cement was compromised. In order to obtain information about the bulk resistance of the composite cement material, electrochemical impedance spectroscopy (EIS) data were employed. The results suggest that for composite cement materials, there is an improvement in bulk electrical resistance, which can be attributed to the lower amounts of cracks and swelling due to lower expansion. In the control sample, a reduction in the bulk resistance suggests the formation of microcracks, which cause the aging and degradation of the material. The intersection of arcs in the EIS spectrum of the mixed composite cement sample gradually increased by an alkaline exposure of up to 21 days and finally shifted towards a low value of high frequency with an increase in alkaline exposure of up to 28 days. Full article
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