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16 pages, 2029 KB  
Article
X-Ray and Optical Orientation of Modified Cotton Fibers
by Abdurrahman Ishaq and Yunusa Umar
Textiles 2026, 6(2), 40; https://doi.org/10.3390/textiles6020040 (registering DOI) - 30 Mar 2026
Abstract
The effect of structure on the properties of cotton fibers is yet to be fully understood even after many years of research. This is due to the presence of convolutions that occur at various intervals in cotton fibers. An attempt was made in [...] Read more.
The effect of structure on the properties of cotton fibers is yet to be fully understood even after many years of research. This is due to the presence of convolutions that occur at various intervals in cotton fibers. An attempt was made in this investigation to remove these convolutions using liquid ammonia treatment. The optical and X-ray orientation angles of two varieties of G. hirsutum cotton fibers were investigated at various stages of maturity, and results were compared. An American upland variety was also studied. Four-hour treatment of cotton fibers in liquid ammonia at a temperature of −50 °C ensures a complete change of the lattice structure from cellulose I polymorph to cellulose III polymorph. The cellulose I lattice structure is restored by boiling it in distilled water for 24 h. X-ray diffractograms confirm these conversions. Mature fibers after treatments are devoid of convolutions and are rounded in appearance with no central lumen. The scanning electron micrographs revealed these morphological structures. A close correlation exists between the optical and X-ray orientation measurements and are both strongly dependent on fiber maturity. In all the varieties studied, a maturity ratio of at least 0.8 is required for a cotton fiber to be of commercial value, in terms of strength and durability The progressive build-up of both the primary and secondary walls as the fiber matures shows a gradual decrease in helix angles and, hence, an increase in the orientation of the fibrils, conforming to the constant pitch model. The effect of convolutions on both the optical and X-ray orientation angle is found to be higher than 10%. Full article
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27 pages, 6773 KB  
Article
EasyBOPT: A Digitally Standardized Protocol to Simplify and Reproduce the Biologically Oriented Preparation Technique (BOPT)—Technique Description and Case Series
by Rubén Agustín-Panadero, Ignazio Loi, Ana Roig-Vanaclocha, José Amengual-Lorenzo, César Chust-López, Marina García-Selva, Miguel Gómez-Polo and Blanca Serra-Pastor
J. Clin. Med. 2026, 15(7), 2591; https://doi.org/10.3390/jcm15072591 - 28 Mar 2026
Viewed by 53
Abstract
Background: The Biologically Oriented Preparation Technique (BOPT) protocol has demonstrated excellent clinical and biological outcomes in restorations with vertical preparation designs. However, its provisional phase remains highly dependent on the operator’s skill. The EasyBOPT (eBOPT) protocol introduces a standardized digital workflow aimed [...] Read more.
Background: The Biologically Oriented Preparation Technique (BOPT) protocol has demonstrated excellent clinical and biological outcomes in restorations with vertical preparation designs. However, its provisional phase remains highly dependent on the operator’s skill. The EasyBOPT (eBOPT) protocol introduces a standardized digital workflow aimed at simplifying this process and enhancing its reproducibility. The primary objective of this study is to describe the eBOPT protocol and to compare its clinical outcomes with the conventional BOPT approach in a prospective case series. Materials and Methods: A case series was conducted including ten patients requiring full-coverage restorations in the maxillary anterior region. The study protocol was registered on 15 July 2024 at ClinicalTrials.gov, with the following registry name: Periodontal outcomes and digital volumetric variation following BOPT restorations, and with the following registration number: NCT06485999. Five patients were treated using the conventional BOPT protocol and five with the eBOPT protocol. Both groups followed identical diagnostic, preparation, and definitive restoration phases, differing only in the provisionalization technique. In the eBOPT group, a digital workflow based on dual scanning (physiologic and retracted gingiva), “best-fit” alignment, and CAD-CAM fabrication of a standardized 45° emergence provisional restoration was employed. Operative time per tooth, gingival healing time, and the need for additional adjustments were recorded. Results: The mean clinical time per tooth was significantly lower with the eBOPT protocol (12.30 ± 1.50 min) compared to the conventional protocol (31.20 ± 2.10 min; p < 0.001). The mean gingival healing time was also reduced with eBOPT (4.4 ± 0.9 weeks) relative to the traditional approach (9.6 ± 1.5 weeks; p = 0.0014). Only the conventional group required additional provisional adjustments (80% of cases; p = 0.048). Conclusions: The EasyBOPT protocol enables faster, more predictable, and less operator-dependent provisionalization while maintaining the biological stability and gingival health achieved with conventional BOPT. This digital workflow simplifies the clinical application of the BOPT concept and enhances its reproducibility. Full article
(This article belongs to the Section Dentistry, Oral Surgery and Oral Medicine)
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17 pages, 1166 KB  
Article
An Integrated 60 GHz Radar and AI-Guided Infrared System for Non-Contact Heart Rate and Body Temperature Monitoring
by Sangwook Sim and Changgyun Kim
Appl. Sci. 2026, 16(7), 3272; https://doi.org/10.3390/app16073272 - 27 Mar 2026
Viewed by 139
Abstract
The growing need for remote patient monitoring, accelerated by the global pandemic and an aging population, necessitates the development of advanced non-contact technologies for measuring vital signs. In this study, an integrated, non-contact system for accurately measuring heart rate (HR) and body temperature [...] Read more.
The growing need for remote patient monitoring, accelerated by the global pandemic and an aging population, necessitates the development of advanced non-contact technologies for measuring vital signs. In this study, an integrated, non-contact system for accurately measuring heart rate (HR) and body temperature (BT) is developed and validated. The proposed system combines a 60 GHz radar sensor and infrared (IR) sensor for HR and BT measurements, respectively, enhanced with advanced signal processing and an AI-based computer vision algorithm. A Window Filter and a Peak Uniformity algorithm were applied to the raw radar signal to mitigate noise and motion artifacts. For Temp measurement, an IR sensor with a narrow five-degree field of view (FOV) was integrated with a YOLO Pose-based tracking system using a camera and servo motors to automatically orient the sensor towards the user’s face. The system was validated with 30 healthy adult participants, benchmarked against a MAX30102 PPG sensor and Braun ThermoScan 7 for BT and BT measurements, respectively. The advanced signal processing reduced the HR Mean Absolute Error from 13.73 BPM to 5.28 BPM (p = 0.002), while the AI-guided IR sensor reduced the BT MAE from 4.10 °C to 1.64 °C (p < 0.001). These findings demonstrate that integrating 60 GHz radar with AI-driven tracking provides a promising approach for home-based trend monitoring. Full article
(This article belongs to the Special Issue AI-Based Biomedical Signal Processing—2nd Edition)
35 pages, 1965 KB  
Review
A Review and Perspective of Techniques for Autonomous Robotic Ultrasound Acquisitions
by Yanding Qin, Lele Dang, Fan Ren, Zhuomao Li, Lijun Duan, Hongpeng Wang and Jianda Han
Sensors 2026, 26(7), 2081; https://doi.org/10.3390/s26072081 - 27 Mar 2026
Viewed by 137
Abstract
Ultrasound (US) imaging is a widely used diagnostic method in clinics. Real-time-generated US images are used for rapid diagnosis without harm to patients. The quality of US imaging highly depends on the skill of the physician due to the differences among physicians. Techniques [...] Read more.
Ultrasound (US) imaging is a widely used diagnostic method in clinics. Real-time-generated US images are used for rapid diagnosis without harm to patients. The quality of US imaging highly depends on the skill of the physician due to the differences among physicians. Techniques for autonomous robotic ultrasound (AU-RUS) acquisitions are expected to become an effective means to improve the level of US diagnosis, reduce the workload of physicians, and improve the standardization of US imaging quality. This paper aims to summarize the current research status of techniques for AU-RUS acquisitions, and to discuss the research trends and challenges regarding related technologies. Firstly, the techniques for AU-RUS acquisitions and systems are outlined. The techniques for teleoperated or autonomous US acquisitions are briefly discussed. Representative RUS acquisition systems are introduced. Then, the current research status of AU-RUS acquisitions is reviewed from four research directions: force sensitivity and control, scanning path-planning and positioning, US treatment guidance, and US image processing technology and quality assessment optimization. This review provides a decision-oriented autonomy perspective by mapping typical methods to workflow components across the stages of perception, decision-making, and execution. We identify major deployment bottlenecks, including safety-verifiable autonomy and failure recovery, motion compensation under deformation, and the lack of standardized, clinically meaningful US image quality metrics. Finally, the shortcomings of current research are summarized and analyzed, and the research trends and challenges for AU-RUS acquisitions are prospected. Full article
(This article belongs to the Special Issue Recent Advances in Medical Robots: Design and Applications)
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34 pages, 9746 KB  
Article
A Four-Dimensional Historical Building Defect Information Modeling (HBDIM) Framework Integrating Digital Documentation and Nanomaterial Consolidation for Sustainable Stucco Conservation
by Ahmad Baik, Amer Habibullah, Ahmed Sallam, Tarek Salah and Mohamed Saleh
Sustainability 2026, 18(7), 3244; https://doi.org/10.3390/su18073244 - 26 Mar 2026
Viewed by 239
Abstract
This study proposes a four-dimensional Historical Building Defect Information Modeling (HBDIM) framework designed to support the documentation, diagnosis, and conservation of deteriorated historic stucco elements. The framework integrates multi-source digital documentation techniques, including terrestrial laser scanning (TLS), high-resolution photogrammetry, and automated total station [...] Read more.
This study proposes a four-dimensional Historical Building Defect Information Modeling (HBDIM) framework designed to support the documentation, diagnosis, and conservation of deteriorated historic stucco elements. The framework integrates multi-source digital documentation techniques, including terrestrial laser scanning (TLS), high-resolution photogrammetry, and automated total station measurements with laboratory-based material diagnostics to create a unified digital environment for defect detection and conservation assessment. The approach was applied to the Baron Empain Palace in Egypt as a representative case study of complex architectural heritage affected by material deterioration. Within the HBDIM workflow, point cloud processing and defect-oriented information modeling were used to identify and spatially localize deterioration features such as cracking, erosion, and material loss. Laboratory investigations—including computed tomography (CT), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and X-ray fluorescence (XRF)—were conducted to evaluate the effectiveness of calcium hydroxide nanoparticle consolidation treatments and to relate microstructural material behavior to spatially mapped defects within the digital model. Mechanical testing demonstrated a significant improvement in material performance, with treated stucco samples exhibiting an average compressive strength increase of approximately 69.06% compared to untreated specimens. The results demonstrate that integrating digital documentation, defect-oriented modeling, and material diagnostics within a four-dimensional framework provides a robust platform for linking geometric deterioration patterns with material-level conservation performance. By embedding diagnostic data and treatment outcomes within a temporally structured digital model, the HBDIM approach supports preventive conservation strategies, long-term monitoring, and data-driven decision-making in sustainable heritage management. Full article
(This article belongs to the Special Issue Cultural Heritage Conservation and Sustainable Development)
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28 pages, 12752 KB  
Article
An Automatic Update Framework for As-Designed Pipeline BIM Model Based on Laser Scanning Point Cloud
by Xinru Wang, Bin Yang and Tianjia Lu
Buildings 2026, 16(7), 1295; https://doi.org/10.3390/buildings16071295 (registering DOI) - 25 Mar 2026
Viewed by 204
Abstract
Accurately reconstructing Mechanical, Electrical and Plumbing (MEP) systems from laser-scanned point clouds is often hindered by structural occlusions, sensor noise, and extreme scale imbalance between large pipes and small fittings. This study presents a hybrid framework, driven by both knowledge and data, for [...] Read more.
Accurately reconstructing Mechanical, Electrical and Plumbing (MEP) systems from laser-scanned point clouds is often hindered by structural occlusions, sensor noise, and extreme scale imbalance between large pipes and small fittings. This study presents a hybrid framework, driven by both knowledge and data, for automated pipeline BIM updating. To tackle scale variance, we implement a coarse-to-fine segmentation strategy using Density-Based Spatial Clustering of Applications with Noise (DBSCAN) to isolate pipeline instances before segmentation with PointNeXt. Furthermore, a logic-based refinement module integrates geometric and topological priors from the design BIM to correct coordinate deviations in incomplete datasets. Finally, graph isomorphism analysis enables automated topological mapping between unstructured point cloud instances and structured BIM components. Experimental results from a dense shopping center case study demonstrate that the framework achieves a semantic segmentation mIoU of 74.45% and reduces the average spatial coordinate error to within 7 mm. Notably, the automated workflow compressed the modeling time from 3–5 days to approximately 3 h, offering a robust solution for digital twin-oriented facility management. Full article
(This article belongs to the Section Construction Management, and Computers & Digitization)
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24 pages, 1081 KB  
Article
Fashion Futures as Design Scenarios for the Triple Transition Framework
by Paola Bertola, Chiara Colombi, Manuela Celi and Victoria Rodriguez Schön
Platforms 2026, 4(2), 5; https://doi.org/10.3390/platforms4020005 - 24 Mar 2026
Viewed by 149
Abstract
This article explores how fashion, as a culture-intensive industry, can act as a testbed for ecosystem-centred sustainability transitions. Building on debates on the Triple Transition (green, digital, resilience) and the four pillars of sustainability (environmental, social, economic, cultural), the study addresses a theoretical [...] Read more.
This article explores how fashion, as a culture-intensive industry, can act as a testbed for ecosystem-centred sustainability transitions. Building on debates on the Triple Transition (green, digital, resilience) and the four pillars of sustainability (environmental, social, economic, cultural), the study addresses a theoretical and methodological gap: while transition agendas and sustainability frameworks are well developed at policy and conceptual levels, there is limited empirical integration of these frameworks into design-oriented methods capable of guiding situated organisational decisions in fashion and cultural and creative industries. It proposes a design- and futures-driven methodology that combines intuitive-logics scenario building, horizon scanning and a customised three-axis Polar Map. The Polar Map translates the Triple Transition into three composite orientations: Bios, Techné and Resilience, used to structure four narrative scenarios applied to the fashion ecosystem: Trailblazing Agency, Other-than-Human Agency, Constructive Agency and Normative Agency. Each scenario assembles concepts, weak signals and case examples into plausible configurations of the fashion value chain and its ecosystem. The results show how these scenarios act as meta-narratives, orienting devices and boundary objects that support futures literacy, make the cultural and intangible consequences of design decisions explicit and reveal interdependencies across value chains. Conceptually, the work operationalises combined transitions and the four pillars of sustainability in a flagship CCI; methodologically, it advances a design-oriented adaptation of scenario practices; and practically, it offers organisations narrative tools to rehearse ecosystem-centred innovation pathways. The conclusion reflects on structural constraints and methodological directions for further hybridisation within foresight methods. Full article
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15 pages, 5247 KB  
Article
Differentiated Stem Cell-Seeded Gelatin/PLA/P(3HB-co-4HB) Meniscal Scaffold with Biocompatibility and Mechanical Strength
by Peng Li, Xiaoxin Cheng, Wuwei Li, Haiqing Yang and Yubi Jiang
Polymers 2026, 18(6), 774; https://doi.org/10.3390/polym18060774 - 23 Mar 2026
Viewed by 285
Abstract
Laceration is one of the most common meniscus injuries, which can cause knee joint dysfunction. The treatment of meniscus injuries remains one of the greatest challenges in orthopedics. In this study, a three-dimensional sponge-like Poly(lactic acid)/Poly(3-hydroxybutyrate-co-4-hydroxybutyrate) (PLA/P(3HB-co-4HB)) scaffold with oriented microtubules was fabricated [...] Read more.
Laceration is one of the most common meniscus injuries, which can cause knee joint dysfunction. The treatment of meniscus injuries remains one of the greatest challenges in orthopedics. In this study, a three-dimensional sponge-like Poly(lactic acid)/Poly(3-hydroxybutyrate-co-4-hydroxybutyrate) (PLA/P(3HB-co-4HB)) scaffold with oriented microtubules was fabricated using an improved gradient thermal phase separation technique. The scaffold surface was modified by adsorbing gelatin. The surface-modified scaffolds and the unmodified scaffolds were divided into two groups. All preparation parameters were adjusted to meet tissue engineering requirements. The prepared scaffolds were tested for porosity, compression modulus, hydrophilicity, and degradability. Following scaffold preparation, induced differentiated rabbit bone marrow mesenchymal stem cells (BMSCs) were seeded to evaluate scaffold cytocompatibility. Cell proliferation was observed in the two scaffold groups, and cell viability was analyzed using CCK-8 assay, scanning electron microscopy (SEM), and confocal microscopy. Histological staining was performed to comparatively study cell synthetic function. Subsequently, tissue reconstruction and regeneration were evaluated following subcutaneous implantation of gelatin/PLA/P(3HB-co-4HB) scaffolds loaded with induced differentiated BMSCs in the dorsal regions of athymic nude mice. Results demonstrated that the gelatin/PLA/P(3HB-co-4HB) scaffold exhibited good cell compatibility, providing a suitable microenvironment for cell proliferation and differentiation. Furthermore, the scaffold supported the growth of seeded induced differentiated rabbit MSCs in vivo, maintaining meniscus cell phenotyping and function. The cell-laden scaffold has the potential to generate meniscus fibrocartilage. Full article
(This article belongs to the Special Issue Smart and Bio-Medical Polymers: 3rd Edition)
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34 pages, 2031 KB  
Article
Heritage 4.0: How Applied 3D Technologies and Digital Twins Are Redefining Cultural Preservation Beyond Replication
by Antreas Kantaros, Theodore Ganetsos, Stavroula Nakou and Nikolaos Laskaris
Heritage 2026, 9(3), 123; https://doi.org/10.3390/heritage9030123 - 21 Mar 2026
Viewed by 287
Abstract
This work examines how digital technologies, particularly 3D imaging, additive man-ufacturing, and digital twins, contribute to a more interactive and process-oriented understanding of cultural preservation. Building on practical experience with museum scanning and 3D reproduction, the study introduces the Heritage 4.0 Cycle, a [...] Read more.
This work examines how digital technologies, particularly 3D imaging, additive man-ufacturing, and digital twins, contribute to a more interactive and process-oriented understanding of cultural preservation. Building on practical experience with museum scanning and 3D reproduction, the study introduces the Heritage 4.0 Cycle, a conceptual framework that structures digital heritage management into four iterative phases: Capture, Curate, Connect, and Co-create. The model integrates technological, ethical, and social aspects of preservation, describing how cultural heritage operates as a living system supported by data, interpretation, and participation. Findings indicate that 3D technologies function as mediators between tangible and intangible heritage, promoting inclusivity, collaborative learning, and sustainable engagement. The framework aligns digital preservation practices with broader objectives of education, innovation, and community development. By formalizing Heritage 4.0 into a structured and iterative framework, this study contributes a transferable model that supports sustainable and smart cultural ecosystems by aligning digital documentation, ethical curation, participatory engagement, and digital twin-enabled connectivity within a coherent heritage management strategy Full article
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18 pages, 7894 KB  
Article
Laser Surface Microtexturing for Enhanced Adhesive Bonding in Steel–Polymer and Steel–Ceramic Joints
by Szymon Tofil, Leonardo Orazi, Vincenzina Siciliani, Cyril Mauclair, António B. Pereira, Sascha Stribick, Felix Hartmann, Jianhua Yao, Qunli Zhang, Liang Wang and Shuyang Lin
Appl. Sci. 2026, 16(6), 3010; https://doi.org/10.3390/app16063010 - 20 Mar 2026
Viewed by 144
Abstract
Laser surface microtexturing has emerged as an effective approach for improving the performance of adhesive joints between dissimilar materials. In this study, the influence of laser-generated micrometric surface features on the mechanical behavior of hybrid adhesive joints was investigated for two material systems: [...] Read more.
Laser surface microtexturing has emerged as an effective approach for improving the performance of adhesive joints between dissimilar materials. In this study, the influence of laser-generated micrometric surface features on the mechanical behavior of hybrid adhesive joints was investigated for two material systems: structural steel bonded to polyamide (PA66) and structural steel bonded to technical ceramic (Al2O3). Single-lap joints were manufactured using a two-component epoxy adhesive with two nominal bond-line thicknesses (0.1 mm and 1.0 mm). Prior to bonding, selected surfaces were modified by ultrashort-pulse laser microtexturing, producing well-defined circular features with characteristic depths on the order of tens of micrometers. The resulting microstructures were characterized using optical and scanning electron microscopy, and their geometric parameters were quantified through profilometric measurements. Mechanical performance was evaluated under shear and bending loading conditions. The results demonstrate a substantial increase in joint strength for laser-microtextured surfaces compared with non-textured references for both material combinations. The effect of surface microtexturing was more pronounced than the influence of adhesive layer thickness within the investigated range. These findings confirm that laser-induced surface microtexturing is a versatile and application-oriented surface preparation method capable of enhancing the reliability of adhesive bonding in hybrid metal–polymer and metal–ceramic assemblies. Full article
(This article belongs to the Special Issue The Applications of Laser-Based Manufacturing for Material Science)
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16 pages, 3777 KB  
Article
From Film Processing to Microphase Orientation: Structure–Property Relationships in Commercial PBSA/PLA Blend Films
by Guru Geertz, Stefan Böhler, Bastian Barton, Frank Malz, Andreas Bohn, Olaf Kahle, Robert Brüll and Jens Balko
Polymers 2026, 18(6), 761; https://doi.org/10.3390/polym18060761 - 20 Mar 2026
Viewed by 268
Abstract
The commercialization of poly(butylene succinate-co-adipate) (PBSA), a biodegradable and potentially fully biobased random copolyester, is still ongoing. Due to its high relevance as mono material or as blend component in flexible film applications, a sound understanding of compounding, further processing and film properties [...] Read more.
The commercialization of poly(butylene succinate-co-adipate) (PBSA), a biodegradable and potentially fully biobased random copolyester, is still ongoing. Due to its high relevance as mono material or as blend component in flexible film applications, a sound understanding of compounding, further processing and film properties is necessary. In this work, PBSA, poly (lactic acid) (PLA) and blends at three different compositions thereof were processed into flat films and blown films, respectively. Investigating the films with X-ray diffraction (XRD), multivariate confocal Raman microscopy (CRM) and scanning electron microscopy (SEM) revealed the semicrystalline order as well as the blend morphology. While PBSA is semicrystalline, PLA remains amorphous after the processing step. As imaged by CRM, flat films exhibit lamellar-like domains formed during uniaxial stretching and rapid cooling, whereas blown films show no pronounced preferential orientation. Tensile tests in both the machine and transverse directions demonstrate the versatility of PBSA and its blends in spanning a wide range of mechanical strength and flexibility, covering and partly exceeding the stiffness and strength ranges typically reported for commodity polyolefins while exhibiting reduced ductility. Differential scanning calorimetry (DSC) and dynamic mechanical analysis (DMA) provide further insights into the thermal properties of the pure and blend materials. Full article
(This article belongs to the Special Issue Polymers for Circular Packaging Materials)
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28 pages, 1987 KB  
Article
RACI–AHP–BIM Methodology in Projects with High Functional Complexity and Conservation Constraints
by Urszula Kwast-Kotlarek and Mariusz Szóstak
Infrastructures 2026, 11(3), 105; https://doi.org/10.3390/infrastructures11030105 - 19 Mar 2026
Viewed by 126
Abstract
The article presents an integrated RACI–AHP–BIM methodology that supports responsibility management, decision-making, and information management in complex construction projects delivered under the design–build model, with particular emphasis on conservation-orientated investments. The approach combines three complementary components: the RACI responsibility matrix, the analytic hierarchy [...] Read more.
The article presents an integrated RACI–AHP–BIM methodology that supports responsibility management, decision-making, and information management in complex construction projects delivered under the design–build model, with particular emphasis on conservation-orientated investments. The approach combines three complementary components: the RACI responsibility matrix, the analytic hierarchy process (AHP), and building information modeling (BIM). The methodology is validated on a higher-education conservation project using a BIM execution plan (BEP), scan-to-BIM procedures, and structured decision-making. The integration of RACI with BIM reduced accountability gaps and improved stakeholder coordination, while linking AHP with BIM data enabled data-driven design decisions using the BOCR model. The findings demonstrate measurable benefits, including clearer responsibility allocation, improved interdisciplinary coordination, and more transparent decision-making. The application of laser scanning and scan-to-BIM supported the creation of a digital model of historic elements for both design and future facility management. The main contribution is a holistic integration of RACI, AHP, and BIM into a unified methodology for conservation-orientated projects with high functional complexity, providing a reference framework for public-sector investment management. Full article
(This article belongs to the Special Issue Modern Digital Technologies for the Built Environment of the Future)
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27 pages, 5146 KB  
Article
Impact of Printing Parameters on the Surface Morphology and Thermal Stability of Sustainable FDM Filaments: A Taguchi-Based Factorial Design Study
by Erman Zurnacı
Appl. Sci. 2026, 16(6), 2904; https://doi.org/10.3390/app16062904 - 18 Mar 2026
Viewed by 151
Abstract
The increasing demand for sustainable materials has accelerated the development of environmentally friendly filaments for fused deposition modeling (FDM). In this study, the surface roughness and thermal degradation behavior of sustainable PLA-based filaments, including PLA, recycled PLA (Re–PLA), and wood-filled PLA (Wood–PLA), were [...] Read more.
The increasing demand for sustainable materials has accelerated the development of environmentally friendly filaments for fused deposition modeling (FDM). In this study, the surface roughness and thermal degradation behavior of sustainable PLA-based filaments, including PLA, recycled PLA (Re–PLA), and wood-filled PLA (Wood–PLA), were systematically investigated under different FDM printing conditions. A full factorial experimental design was employed to identify the dominant processing parameters and optimize surface quality. Surface roughness was evaluated using values Ra, Rz, and Rq parameters measured on three different surface orientations (top surface at 0°, top surface at 45°, and side surface). Scanning electron microscopy (SEM) was used to examine the relationship between roughness measurements and surface morphology, while thermogravimetric analysis (TGA) was performed to evaluate the thermal degradation behavior of the filaments in relation to printing temperature. The results have shown that filament material is the most important parameter affecting surface roughness. While Wood–PLA exhibited the highest roughness due to fiber-induced surface heterogeneity, recycled Re–PLA showed moderate surface irregularities resulting from degradation compared to pure PLA. Despite a rougher filament surface prior to production, recycled PLA exhibited a surface morphology similar to that of pure PLA after printing, influenced by the processing parameters. Furthermore, SEM findings indicated that the Ra parameter predominantly reflects macro-scale surface topography, while local microstructural heterogeneity can be better characterized by complementary roughness parameters such as Rz. These findings support optimizing printing conditions to improve surface quality and more widespread use of sustainable FDM filaments in applications where surface roughness is critical. Full article
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11 pages, 6346 KB  
Article
The Anisotropic Permeability Insights of Nano-Scale Pore Networks Evolution in the Overmature Shales
by Yanshuai Tang, Tianguo Tang, Xiaohang Bao, Xiujiang Fan and Lei Zhou
Minerals 2026, 16(3), 315; https://doi.org/10.3390/min16030315 - 17 Mar 2026
Viewed by 172
Abstract
Permeability is affected by nanopores and pore structure, and anisotropic permeability is the result of shale lamination, orientation, and stratification of minerals. To understand the reasons for permeability anisotropy, the pore networks of over-mature shale has been studied. The mineral compositions, petrophysical properties, [...] Read more.
Permeability is affected by nanopores and pore structure, and anisotropic permeability is the result of shale lamination, orientation, and stratification of minerals. To understand the reasons for permeability anisotropy, the pore networks of over-mature shale has been studied. The mineral compositions, petrophysical properties, and pore structures of the Lower Cambrian Niutitang Formation shales were analyzed using subcritical gas adsorption, field-emission scanning electron microscopic, and X-ray micro-computed tomographic methods. Quartz, clay minerals, and carbonate are the dominant minerals in the shales. The bedding-parallel and bedding-perpendicular permeabilities are 1.25–46.21 × 10−2 and 1.38–6.62 × 10−2 mD, respectively. The anisotropy of permeability, which is the ratio between the bedding-parallel and bedding-perpendicular permeability, is 0.21–26.87. The micropore and Barrett–Joyner–Halenda pore volumes are 0.54–3.62 and 0.05–0.69 mL/100 g, respectively. The bedding-parallel permeability is correlated positively with the micropore and Barrett–Joyner–Halenda pore volumes. Thin-section observations indicate the shales exhibit a bedding-parallel alignment of phyllosilicate minerals and planar deformation bands. The scanning electron microscopy shows deformation of the lamination and parallel alignment of the clay minerals due to compaction or differential compaction over coarser-grained quartz grains. The scanning electron microscopy images and subcritical gas adsorption data indicate that the pore fracture system is parallel to bedding and formed after diagenesis. Furthermore, X-ray micro-computed tomographic analysis shows that the micro-fractures are also preferentially oriented, parallel to bedding. Full article
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12 pages, 3645 KB  
Proceeding Paper
Towards Predictive Models of Mechanical Properties in 3D-Printed Polymers: An Exploratory Study
by Bruno A. G. Sousa, César M. A. Vasques and Adélio M. S. Cavadas
Eng. Proc. 2026, 124(1), 79; https://doi.org/10.3390/engproc2026124079 - 16 Mar 2026
Viewed by 205
Abstract
Additive manufacturing, particularly 3D printing, is increasingly shaping the production of polymer-based components, enabling complex geometries and tailored functional performance. Yet, predicting their mechanical behavior remains challenging due to material anisotropy and sensitivity to processing conditions. This work presents an exploratory study designed [...] Read more.
Additive manufacturing, particularly 3D printing, is increasingly shaping the production of polymer-based components, enabling complex geometries and tailored functional performance. Yet, predicting their mechanical behavior remains challenging due to material anisotropy and sensitivity to processing conditions. This work presents an exploratory study designed to provide the experimental basis for the development and calibration of predictive models of mechanical properties in 3D-printed components. Standard ISO 527-2 Type 1A specimens were fabricated using thermoplastic PLA (polylactic acid) with systematic variations in layer orientation, infill overlap, and printing velocity. Mechanical characterization was carried out through uniaxial tensile testing to determine tensile strength and stiffness of the material specimens, while scanning electron microscopy (SEM) provided complementary insights into interlayer bonding, filament alignment, porosity, and fracture morphology. Results showed that material type and processing strategies strongly influenced mechanical response, with SEM highlighting microstructural features that govern interlayer adhesion and failure mechanisms. These findings contribute to a deeper understanding of process–structure–property relationships in additive manufacturing and establish the groundwork for predictive model development. Ongoing efforts will integrate these experimental insights into numerical simulations employing homogenized material models, thereby enhancing design optimization and reliability of 3D-printed structural components. Full article
(This article belongs to the Proceedings of The 6th International Electronic Conference on Applied Sciences)
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