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Search Results (476)

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Keywords = high-reflection coating

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10 pages, 1309 KiB  
Proceeding Paper
A Sustainable Approach to Cooking: Design and Evaluation of a Sun-Tracking Concentrated Solar Stove
by Hasan Ali Khan, Malik Hassan Nawaz, Main Omair Gul and Mazhar Javed
Mater. Proc. 2025, 23(1), 4; https://doi.org/10.3390/materproc2025023004 - 29 Jul 2025
Viewed by 78
Abstract
Access to clean cooking remains a major challenge in rural and off-grid areas where traditional fuels are costly, harmful, or scarce. Solar cooking offers a sustainable solution, but many existing systems suffer from fixed positioning and low efficiency. This study presents a low-cost, [...] Read more.
Access to clean cooking remains a major challenge in rural and off-grid areas where traditional fuels are costly, harmful, or scarce. Solar cooking offers a sustainable solution, but many existing systems suffer from fixed positioning and low efficiency. This study presents a low-cost, dual-axis solar tracking parabolic dish cooker designed for such regions, featuring adjustable pot holder height and portability for ease of use. The system uses an Arduino UNO, LDR sensors, and a DC gear motor to automate sun tracking, ensuring optimal alignment throughout the day. A 0.61 m parabolic dish with ≥97% reflective silver-coated mirrors concentrates sunlight to temperatures exceeding 300 °C. Performance tests in April, June, and November showed boiling times as low as 3.37 min in high-irradiance conditions (7.66 kWh/m2/day) and 6.63 min under lower-irradiance conditions (3.86 kWh/m2/day). Compared to fixed or single-axis systems, this design achieved higher thermal efficiency and reliability, even under partially cloudy skies. Built with locally available materials, the system offers an affordable, clean, and effective cooking solution that supports energy access, health, and sustainability in underserved communities. Full article
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24 pages, 6934 KiB  
Article
In Situ High-Resolution Optical Microscopy Survey of the Initial Reactivity of Multiphase ZnAlMgSi Coating on Steel
by Guilherme Adinolfi Colpaert Sartori, Oumayma Gabsi, Tiago Machado Amorim, Viacheslav Shkirskiy and Polina Volovitch
Metals 2025, 15(8), 821; https://doi.org/10.3390/met15080821 - 23 Jul 2025
Viewed by 245
Abstract
The initial reactivity of a multiphase ZnAlMgSi coating with an Al content > 30 wt.% was studied by in situ reflective microscopy under alternating applied potentials +50 mV/−50 mV vs. open-circuit potential in 5 wt.% NaCl and 5 wt.% Na2SO4 [...] Read more.
The initial reactivity of a multiphase ZnAlMgSi coating with an Al content > 30 wt.% was studied by in situ reflective microscopy under alternating applied potentials +50 mV/−50 mV vs. open-circuit potential in 5 wt.% NaCl and 5 wt.% Na2SO4 aqueous solutions. In both environments, galvanic coupling between different coating phases and the anodic behavior decreased in the order binary ZnAl > binary Zn/Zn2Mg > Zn2Mg > Al(Zn); dendrites were evidenced for the coating exposed alone as well as in galvanic coupling with steel. Contrary to the observations known for Zn-rich ZnAlMg coatings, pure Zn2Mg was less reactive than the pure ZnAl phase, underlining the importance of the microstructure for reactivity. Si-needles were systematically cathodic, and Al(Zn) dendrites have shown cathodic behavior in some couplings. In the configuration of coupling with steel, corrosion started at the interfaces “binary ZnAl/steel substrate” or “binary ZnAl/Si particle”. The distribution and nature of the corrosion products formed during the experiment were assessed using X-ray microanalysis in scanning electron microscopy and confocal Raman microscopy. In the sulfate environment, a homogenous and stable corrosion product layer formed from the first steps of the degradation; this was in contrast to the chloride environment, where no surface film formed on the dendrites. Full article
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23 pages, 7773 KiB  
Article
Strengthening-Effect Assessment of Smart CFRP-Reinforced Steel Beams Based on Optical Fiber Sensing Technology
by Bao-Rui Peng, Fu-Kang Shen, Zi-Yi Luo, Chao Zhang, Yung William Sasy Chan, Hua-Ping Wang and Ping Xiang
Photonics 2025, 12(7), 735; https://doi.org/10.3390/photonics12070735 - 18 Jul 2025
Viewed by 289
Abstract
Carbon fiber-reinforced polymer (CFRP) laminates have been widely coated on aged and damaged structures for recovering or enhancing their structural performance. The health conditions of the coated composite structures have been given high attention, as they are critically important for assessing operational safety [...] Read more.
Carbon fiber-reinforced polymer (CFRP) laminates have been widely coated on aged and damaged structures for recovering or enhancing their structural performance. The health conditions of the coated composite structures have been given high attention, as they are critically important for assessing operational safety and residual service life. However, the current problem is the lack of an efficient, long-term, and stable monitoring technique to characterize the structural behavior of coated composite structures in the whole life cycle. For this reason, bare and packaged fiber Bragg grating (FBG) sensors have been specially developed and designed in sensing networks to monitor the structural performance of CFRP-coated composite beams under different loads. Some optical fibers have also been inserted in the CFRP laminates to configure the smart CFRP component. Detailed data interpretation has been conducted to declare the strengthening process and effect. Finite element simulation and simplified theoretical analysis have been conducted to validate the experimental testing results and the deformation profiles of steel beams before and after the CFRP coating has been carefully checked. Results indicate that the proposed FBG sensors and sensing layout can accurately reflect the structural performance of the composite beam structure, and the CFRP coating can share partial loads, which finally leads to the downward shift in the centroidal axis, with a value of about 10 mm. The externally bonded sensors generally show good stability and high sensitivity to the applied load and temperature-induced inner stress variation. The study provides a straightforward instruction for the establishment of a structural health monitoring system for CFRP-coated composite structures in the whole life cycle. Full article
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15 pages, 2902 KiB  
Article
Synergistic Integration of MXene Photothermal Conversion and TiO2 Radiative Cooling in Bifunctional PLA Fabrics for Adaptive Personal Thermal Management
by Tianci Han and Yunjie Yin
Solids 2025, 6(3), 37; https://doi.org/10.3390/solids6030037 - 12 Jul 2025
Viewed by 290
Abstract
Polylactic acid (PLA) fabrics exhibit significant sunlight reflectivity and high emissivity within the atmospheric window, making them suitable as the foundational material for this study. This research involves the modification of one side of the fabric with hydrophilic agents and titanium dioxide (TiO [...] Read more.
Polylactic acid (PLA) fabrics exhibit significant sunlight reflectivity and high emissivity within the atmospheric window, making them suitable as the foundational material for this study. This research involves the modification of one side of the fabric with hydrophilic agents and titanium dioxide (TiO2), while the opposite side is treated with MXene and subsequently coated with polydimethylsiloxane (PDMS) to inhibit oxidation of the MXene. Through these surface modifications, a thermal management fabric based on PLA was successfully developed, capable of passively regulating temperature in response to environmental conditions and user requirements. The study discusses the optimal concentrations of TiO2 and MXene for the fabric, and characterizes and evaluates the functional surface of the PLA. Surface morphology analyses and tests indicate that the resulting functional PLA fabrics possess excellent ultraviolet (UV) resistance, favorable air permeability, high sunlight reflectivity on the TiO2-treated side, and superior photothermal conversion capabilities on the MXene-treated side. Furthermore, photothermal effect tests conducted under a light intensity of 1000 W/m2 reveal that the MXene-treated fabric exhibits a heating effect of approximately 25 °C, while the TiO2-treated side demonstrates a cooling effect exceeding 5 °C. This study developed PLA functional fabrics with heating and cooling capabilities. Full article
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19 pages, 3564 KiB  
Article
Surface Ice Detection Using Hyperspectral Imaging and Machine Learning
by Steve Vanlanduit, Arnaud De Vooght and Thomas De Kerf
Sensors 2025, 25(14), 4322; https://doi.org/10.3390/s25144322 - 10 Jul 2025
Viewed by 304
Abstract
Ice formation on critical infrastructure such as wind turbine blades can lead to severe performance degradation and safety hazards. This study investigates the use of hyperspectral imaging (HSI) combined with machine learning to detect and classify ice on various coated and uncoated surfaces. [...] Read more.
Ice formation on critical infrastructure such as wind turbine blades can lead to severe performance degradation and safety hazards. This study investigates the use of hyperspectral imaging (HSI) combined with machine learning to detect and classify ice on various coated and uncoated surfaces. Hyperspectral reflectance data were acquired using a push-broom HSI system under controlled laboratory conditions, with ice and rime ice generated using a thermoelectric cooling setup. Support Vector Machine (SVM) and Random Forest (RF) classifiers were trained on uncoated aluminum samples and evaluated on surfaces with different coatings to assess model generalization. Both models achieved high classification accuracy, though performance declined on black-coated surfaces due to increased absorbance by the coating. The study further examined the impact of spectral band reduction to simulate different sensor types (e.g., NIR vs. SWIR), revealing that model performance is sensitive to wavelength range, with SVM performing optimally in a reduced band set and RF benefiting from the full spectral range. A multiclass classification approach using RF successfully distinguished between glaze and rime ice, offering insights into more targeted mitigation strategies. The results confirm the potential of HSI and machine learning as robust tools for surface ice monitoring in safety-critical environments. Full article
(This article belongs to the Section Optical Sensors)
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17 pages, 6013 KiB  
Article
The Effect of Injection Molding Processing Parameters on Chrome-Plated Acrylonitrile Butadiene Styrene-Based Automotive Parts: An Industrial Scale
by Yunus Emre Polat, Mustafa Oksuz, Aysun Ekinci, Murat Ates and Ismail Aydin
Polymers 2025, 17(13), 1787; https://doi.org/10.3390/polym17131787 - 27 Jun 2025
Viewed by 562
Abstract
In recent years, plastic decorative materials have been used in the automotive industry due to their advantages such as being environmentally friendly, aesthetic, light and economically affordable. Plastic decorative materials can exhibit high strength and metallic reflection with metal coatings. Chrome plating is [...] Read more.
In recent years, plastic decorative materials have been used in the automotive industry due to their advantages such as being environmentally friendly, aesthetic, light and economically affordable. Plastic decorative materials can exhibit high strength and metallic reflection with metal coatings. Chrome plating is generally preferred in the production of decorative plastic parts in the automotive industry. In this study, the effect of injection molding processing parameters on the metal–polymer adhesion of chrome-plated acrylonitrile butadiene styrene (ABS) was investigated. The ABS-based front grille frames are fabricated by means of using an industrial-scale injection molding machine. Then, the fabricated ABS-based front grille frame was plated with chrome by means of the electroplating method. The metal–polymer adhesion was investigated as a function of the injection molding processing parameters by means of a cross-cut test and scanning electron microscope (SEM). As a result, it was determined that the optimal injection process parameters, a cooling time of 18 s, a mold temperature of 70 °C, injection rates of 45-22-22-20-15-10 mm/s, and packing pressures of 110-100-100 bar, were effective in enhancing polymer–metal adhesion for the ABS-based front grille frame. Full article
(This article belongs to the Special Issue Advances in Polymer Molding and Processing)
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17 pages, 4222 KiB  
Article
Grooved High-Reflective Films for Ultraviolet Emission Enhancement
by Hengrui Zhang, Zhanhua Huang and Lin Zhang
Photonics 2025, 12(7), 644; https://doi.org/10.3390/photonics12070644 - 25 Jun 2025
Viewed by 276
Abstract
Conventional ultraviolet microplasma sources typically lack a back-reflection structure, resulting in radiative power loss from the backside. To enhance the emission efficiency of ultraviolet microplasma devices around 220 nm, we propose a multilayer reflective coating composed of alternating high- and low-refractive-index layers of [...] Read more.
Conventional ultraviolet microplasma sources typically lack a back-reflection structure, resulting in radiative power loss from the backside. To enhance the emission efficiency of ultraviolet microplasma devices around 220 nm, we propose a multilayer reflective coating composed of alternating high- and low-refractive-index layers of Al2O3 and SiO2, within a V-shaped groove. Key structural parameters, including the number of alternating film layer pairs, groove width, and light source position, are investigated to show their effects on ultraviolet reflection characteristics. The results show that reducing the groove width greatly enhances light reflection. When the groove width is 6.5 μm, the device exhibits a reflection efficiency of 47.82% and power enhancement of 91.66%, representing improvements of 2.5-fold and 4.2-fold, respectively, compared to non-optimized cases. Device performance is also influenced by the offset of the light source, which is more sensitive along the horizontal direction. This study provides a practical solution for developing high-efficiency ultraviolet emission devices. Full article
(This article belongs to the Special Issue Recent Progress in Integrated Photonics)
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18 pages, 4595 KiB  
Article
Solution Mixing Synthesis of Epoxy Nanocomposites Reinforced with MWCNTs and Graphene: Thermal Stability and EMI Shielding Effectiveness Study
by Natalia Drakopoulou, Tatiana Giannakopoulou, Christos Trapalis and Petroula A. Tarantili
J. Compos. Sci. 2025, 9(7), 326; https://doi.org/10.3390/jcs9070326 - 24 Jun 2025
Viewed by 353
Abstract
In this work, the critical properties of epoxy resin reinforced with carbon-based nanoparticles were examined in order to improve its performance in protective coating applications. Epoxy resin composites with commercial multi-walled carbon nanotubes (MWCNTs) and graphene (GP) nanoplates were prepared via solution mixing. [...] Read more.
In this work, the critical properties of epoxy resin reinforced with carbon-based nanoparticles were examined in order to improve its performance in protective coating applications. Epoxy resin composites with commercial multi-walled carbon nanotubes (MWCNTs) and graphene (GP) nanoplates were prepared via solution mixing. In addition, hybrid composites with 50:50 w/w MWCNTs/GP were also examined. The characterization of the EMI shielding effectiveness revealed that epoxy resin composites reinforced with MWCNTs presented the best performance. Composites with the same content of graphene exhibited much lower shielding results. As confirmed by electrical conductivity measurements, this outcome can be explained by the fact that the electrical percolation threshold in the composites reinforced with MWCNTs was met (around 5 phr), while the conductive network in the composites with graphene was not completely developed. An analysis of the mechanisms that contributed to EMI shielding for each type of specimen showed that, in the case of MWCNT composites, the main mechanism that determined the response of the material was reflection rather than absorption. It was also observed that by increasing the MWCNT content, the shielding efficiency of the composites was enhanced. In the case of graphene composites, the absorption and reflection remained at low levels, resulting in high transmission and therefore poor shielding. Regarding the examined hybrid composites (MWCNTs:GP at 50:50 w/w), it seemed that the MWCNT content determined their shielding performance. Full article
(This article belongs to the Special Issue Feature Papers in Journal of Composites Science in 2025)
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20 pages, 3209 KiB  
Article
Experimental Evaluation of GAGG:Ce Crystalline Scintillator Properties Under X-Ray Radiation
by Anastasios Dimitrakopoulos, Christos Michail, Ioannis Valais, George Fountos, Ioannis Kandarakis and Nektarios Kalyvas
Crystals 2025, 15(7), 590; https://doi.org/10.3390/cryst15070590 - 23 Jun 2025
Viewed by 576
Abstract
The scope of this study was to evaluate the response of Ce-doped gadolinium aluminum gallium garnet (GAGG:Ce) crystalline scintillator under medical X-ray irradiation for medical imaging applications. A 10 × 10 × 10 mm3 crystal was irradiated at X-ray tube voltages ranging [...] Read more.
The scope of this study was to evaluate the response of Ce-doped gadolinium aluminum gallium garnet (GAGG:Ce) crystalline scintillator under medical X-ray irradiation for medical imaging applications. A 10 × 10 × 10 mm3 crystal was irradiated at X-ray tube voltages ranging from 50 kVp to 150 kVp. The crystal’s compatibility with several commercially available optical photon detectors was evaluated using the spectral matching factor (SMF) along with the absolute efficiency (AE) and the effective efficiency (EE). In addition, the energy-absorption efficiency (EAE), the quantum-detection efficiency (QDE) as well as the zero-frequency detective quantum detection efficiency DQE(0) were determined. The crystal demonstrated satisfactory AE values as high as 26.3 E.U. (where 1 E.U. = 1 μW∙m−2/(mR∙s−1)) at 150 kVp, similar, or in some cases, even superior to other cerium-doped scintillator materials. It also exhibits adequate DQE(0) performance ranging from 0.99 to 0.95 across all the examined X-ray tube voltages. Moreover, it showed high spectral compatibility with commonly used photoreceptors in modern day such as complementary metal–oxide–semiconductors (CMOS) and charge-coupled-devices (CCD) with SMF values of 0.95 for CCD with broadband anti-reflection coating and 0.99 for hybrid CMOS blue. The aforementioned properties of this scintillator material were indicative of its superior efficiency in the examined medical energy range, compared to other commonly used scintillators. Full article
(This article belongs to the Special Issue Exploring New Materials for the Transition to Sustainable Energy)
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17 pages, 2097 KiB  
Article
Study on the Optical Properties and Lattice Thermal Conductivity of Ti2AlB2
by Shengzhao Wang, Jinfan Song and Bin Liu
Colloids Interfaces 2025, 9(3), 41; https://doi.org/10.3390/colloids9030041 - 19 Jun 2025
Viewed by 376
Abstract
In this paper, the optical properties and lattice thermal conductivity of Ti2AlB2 were studied by first-principles calculations. The real part of the dielectric constant, ε1, attains a significant value of 47.26 at 0.12 eV, indicating strong polarization capabilities [...] Read more.
In this paper, the optical properties and lattice thermal conductivity of Ti2AlB2 were studied by first-principles calculations. The real part of the dielectric constant, ε1, attains a significant value of 47.26 at 0.12 eV, indicating strong polarization capabilities and energy storage capacity. Regarding optical properties, Ti2AlB2 exhibits significant absorption peaks at photon energies of 4.19 eV, 6.78 eV, and 10.61 eV, and 14.32 eV, with absorption coefficients of 184,168.1 cm−1, 228,860.8 cm−1, 366,350.8 and 303,440.6 cm−1, indicating a strong absorption capacity. The loss function exhibits peaks at 19.80 eV and the refractive index reaches a maximum of 8.30 at 0.01 eV. Reflectivity is notably higher in the 0–5 eV range, exceeding 44%, which demonstrates excellent reflective properties. This suggests that Ti2AlB2 has potential as an optical coating material across certain frequency bands. The lattice thermal conductivity of Ti2AlB2 is obtained at 27.2 W/(m·K). The phonon relaxation time is greater in the low-frequency region, suggesting that phonons have a longer duration of action during the heat transport process, which may contribute to higher thermal conductivity. Although the phonon group velocity is generally low, several factors influence thermal conductivity, including phonon relaxation time and Grüneisen parameters. The high Grüneisen parameter of Ti2AlB2 indicates strong anharmonic vibrations, which may enhance phonon scattering and consequently reduce thermal conductivity. However, Ti2AlB2 still exhibits some lattice thermal conductivity, suggesting that the contributions of phonon relaxation time and group velocity to its thermal conductivity may be more significant. The unique optical properties and thermal conductivity of Ti2AlB2 indicate its potential applications in optical coatings and high-temperature structural materials. Full article
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22 pages, 4799 KiB  
Article
Design and Deposition of Ultra-Broadband Beam-Splitting Coatings
by Yunyun Shi, Haochuan Li, Sibao Zhang, Changxin Luo, Jiangheng Sun, Chenrui Lv, Jiaoteng Ding and Yongsheng Yao
Coatings 2025, 15(6), 695; https://doi.org/10.3390/coatings15060695 - 9 Jun 2025
Viewed by 362
Abstract
This study aims to develop a stress-optimized ultra-broadband beam-splitting coating that integrates four spectral bands by analyzing the beam-splitting properties of coatings spanning visible to medium and long-wave infrared regions. A beam-splitting coating was deposited on a Ge substrate using ion-beam-assisted thermal evaporation, [...] Read more.
This study aims to develop a stress-optimized ultra-broadband beam-splitting coating that integrates four spectral bands by analyzing the beam-splitting properties of coatings spanning visible to medium and long-wave infrared regions. A beam-splitting coating was deposited on a Ge substrate using ion-beam-assisted thermal evaporation, employing Ge, ZnS, and YbF3 as coating materials. The designed coating exhibits high reflectance in the 0.5–0.8 μm and 0.9–1.7 μm wavelength bands while maintaining high transmittance in the 3–5 μm and 8–12 μm bands. The optimal deposition process for a single-layer coating was established, at a 45° incidence angle, the beam-splitting coating achieved an average reflectance (Rave) of 86.6% in the 0.9–1.7 μm band and 93.7% in the 0.9–1.7 μm band, alongside an average transmittance (Tave) of 91.36% in the 3–5 μm band and 91.3% in the 8–12 μm band. The antireflection coating achieved a single-side Tave of 98.5% in the 3–5 μm band and 97% in the 8–12 μm band. The coating uniformity exceeded 99.6%. To optimize the surface profile, a single-layer Ge coating was added to the rear surface, resulting in a root mean square deviation of less than 0.0007 μm, achieved the same precision of the surface profile successfully. The deposited beam-splitting coating possessed high surface profile precision, and successfully achieved high reflectance in the visible to short-wave infrared range and high transmittance in the medium- and long-wave infrared range. The coating demonstrated excellent adhesion, abrasion resistance, and structural integrity, with no wrinkling, cracking, or delamination. Full article
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18 pages, 9850 KiB  
Article
Structural Water Content in Pigment-Grade TiO2 Particles Coated with Al2O3 and SiO2, and Their Effect on Polypropylene Photodegradation
by Edgar F. Armendáriz-Alonso, Nancy Rivera-García, J. Antonio Moreno-Razo, Luis Octavio Meza-Espinoza, Miguel A. Waldo-Mendoza and Elías Pérez
Coatings 2025, 15(6), 685; https://doi.org/10.3390/coatings15060685 - 6 Jun 2025
Viewed by 543
Abstract
The influence of structural water in alumina (Al2O3) and silica (SiO2) coated titanium dioxide (TiO2) pigments on the photodegradation behavior of polypropylene (PP) composites was investigated. Four commercial rutile TiO2 pigments with varying surface [...] Read more.
The influence of structural water in alumina (Al2O3) and silica (SiO2) coated titanium dioxide (TiO2) pigments on the photodegradation behavior of polypropylene (PP) composites was investigated. Four commercial rutile TiO2 pigments with varying surface inorganic coatings were incorporated into PP plaques and subjected to accelerated UV weathering to simulate outdoor exposure. Photodegradation was assessed through gloss retention measurements, the carbonyl index (CI), and stress at break retention, while pigment morphology and composition were analyzed using transmission electron microscopy (TEM) and energy-dispersive X-ray spectroscopy (EDS). Surface charge and water content were determined through the zeta potential (ζ), Karl Fischer titration, thermogravimetric analysis (TGA), and Diffuse Reflectance Infrared Fourier Transform Spectroscopy (DRIFTS). The results showed that low-alumina coating alone led to the lowest photodegradation resistance, the highest CI, and the lowest stress at break retention. In contrast, increasing alumina content enhanced photostability, reaching its maximum for combined alumina–silica coatings, which mitigated electron–hole pair migration. PP composites with high alumina–silica-coated TiO2 exhibited higher gloss retention (36%) compared to low-alumina samples (21%). Furthermore, statistical analysis using ANOVA revealed significant differences in coating content and ζ potential among the pigment grades. These findings provide novel insights into oxide-water interactions and the impact of structural water on the photodegradation of polymer composites. Full article
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15 pages, 4691 KiB  
Article
Comparison of Continuous and Pulsed Low-Power DC Sputtered Ti Thin Films Deposited at Room Temperature
by Anna Maria Reider, Ariane Kronthaler, Fabio Zappa, Alexander Menzel, Felix Laimer and Paul Scheier
Surfaces 2025, 8(2), 36; https://doi.org/10.3390/surfaces8020036 - 31 May 2025
Viewed by 792
Abstract
Titanium thin films with thicknesses of up to 105 nm were deposited on borosilicate glass implementing low-power continuous (25 W) and pulsed (85 W, with an ultra-low duty cycle) DC magnetron sputtering. The characteristics of the resulting films were studied via atomic force [...] Read more.
Titanium thin films with thicknesses of up to 105 nm were deposited on borosilicate glass implementing low-power continuous (25 W) and pulsed (85 W, with an ultra-low duty cycle) DC magnetron sputtering. The characteristics of the resulting films were studied via atomic force microscopy (AFM), X-ray photoelectron spectroscopy (XPS), VIS spectroscopy, and four-point-probe measurements. Both deposition modes yield films with low surface roughness, and AFM analysis showed no topographical features indicative of columnar-and-void structures. The films exhibited high optical reflectivity and stable transmittance and reflectance across the visible spectrum. The electric resistivity could be measured even at single nanometer thickness, emphasizing the metallic character of the films and approaching the bulk titanium value at higher film thicknesses. The low power regime of magnetron sputter deposition not only offers the possibility of studying the development of physical characteristics during the growth of ultra-thin films but also provides the advantage of extremely low heat development and no evident mechanical stress on the substrate during the coating process. These results outline a path for low-power DC sputtering as a reliable approach for studying the evolution of functional properties in ultra-thin films and for the gentle fabrication of coatings where thermal stress must be avoided, making the method compatible with temperature-sensitive applications. Full article
(This article belongs to the Special Issue Surface Engineering of Thin Films)
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10 pages, 1167 KiB  
Article
Investigation of UV Picosecond Laser Damage Threshold of Anti-Reflection Coated Windows
by Priyadarshani Narayanasamy, Martin Mydlář, Hana Turčičová, Mihai George Mureșan, Ondřej Novák, Jan Vanda and Jan Brajer
J. Manuf. Mater. Process. 2025, 9(6), 180; https://doi.org/10.3390/jmmp9060180 - 29 May 2025
Viewed by 700
Abstract
Long-term stability and laser-induced damage resistance of optical components in the UV region are critical for enhancing their performance in UV high-power laser applications. This study evaluates the laser-induced damage threshold (LIDT) of commercially available UV optical windows with anti-reflective (AR) coating, produced [...] Read more.
Long-term stability and laser-induced damage resistance of optical components in the UV region are critical for enhancing their performance in UV high-power laser applications. This study evaluates the laser-induced damage threshold (LIDT) of commercially available UV optical windows with anti-reflective (AR) coating, produced through various coating techniques and designed for high-power lasers. A third-harmonic (343 nm) wavelength with good beam quality was generated in the picosecond regime to investigate the LIDT of optical components. The LIDT for each sample was measured under controlled conditions and compared based on their coating techniques. The sample coated with Al2O3/SiO2 through ion beam sputtering has the best LIDT value, of 0.6 J/cm2, among the tested samples, based on the hundred-thousand-pulses methodology. The damage threshold curve and the corresponding damage morphology are discussed in detail, and these findings provide insights into the durability and susceptibility of UV optics for advanced laser systems available in the market. Full article
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12 pages, 1455 KiB  
Article
Hydrothermal Synthesis of Nanocomposites Combining Tungsten Trioxide and Zinc Oxide Nanosheet Arrays for Improved Photocatalytic Degradation of Organic Dye
by Chien-Yie Tsay, Tao-Ying Hsu, Gang-Juan Lee, Chin-Yi Chen, Yu-Cheng Chang, Jing-Heng Chen and Jerry J. Wu
Nanomaterials 2025, 15(10), 772; https://doi.org/10.3390/nano15100772 - 21 May 2025
Viewed by 411
Abstract
Both tungsten trioxide (WO3) nanosheet arrays and tungsten trioxide/zinc oxide (WO3/ZnO) nanocomposites were grown on fluorine-doped tin oxide (FTO) coated glass slides using a hydrothermal method to develop a visible-light-driven photocatalyst with easy reusability. Field emission scanning electron microscopy [...] Read more.
Both tungsten trioxide (WO3) nanosheet arrays and tungsten trioxide/zinc oxide (WO3/ZnO) nanocomposites were grown on fluorine-doped tin oxide (FTO) coated glass slides using a hydrothermal method to develop a visible-light-driven photocatalyst with easy reusability. Field emission scanning electron microscopy (FE-SEM) observations confirmed the formation of irregular oxide nanosheet arrays on the FTO surfaces. X-ray diffraction (XRD) analysis revealed the presence of hexagonal WO3 and wurtzite ZnO crystal phases. UV-Vis diffuse reflectance spectroscopy showed that integrating ZnO nanostructures with WO3 nanosheets resulted in a blue shift of the absorption edge and a reduced absorption capacity in the visible-light region. Photoluminescence (PL) spectra indicated that the WO 0.5/ZnO 2.0 sample exhibited the lowest electron-hole recombination rate among the WO3/ZnO nanocomposite sample. Photocatalytic degradation tests demonstrated that all WO3/ZnO nanocomposite samples had higher photodegradation rates for a 10 ppm methylene blue (MB) aqueous solution under visible-light irradiation compared to pristine WO3 nanosheet arrays. Among them, the WO 0.5/ZnO 2.0 sample showed the highest photocatalytic efficiency. Furthermore, it exhibited excellent recyclability and high photodegradation stability over three cycles. Full article
(This article belongs to the Section Synthesis, Interfaces and Nanostructures)
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