Search Results (6,180)

This study evaluated the physical and mechanical properties of acrylic resins used for interim fixed prostheses, with and without metal reinforcement, before and after aging. A total of 138 samples were divided into three groups: VIPI + Wire (control), VIPI, and Diamond D. Samples were assessed for microhardness, porosity, roughness, and flexural strength. Aging was simulated using 500 thermocycling cycles at 5 and 55 ± 1 °C. Data were analyzed using ANOVA and Tukey’s test. Group Diamond D did not fracture during flexural testing, but it exhibited significantly lower microhardness at both baseline and after aging. Before aging, Group Diamond D had higher roughness than Group VIPI, which exhibited greater porosity. Aging increased the microhardness of Group VIPI and the roughness of Group Diamond D. The percentage of porosity decreased significantly for Groups VIPI + Wire and VIPI, and pore size was reduced in all groups. Based on the results obtained from Diamond D material, this resin does not meet the required properties for the proposed indication for temporary fixed prostheses, whereas VIPI with reinforcement showed superior properties and greater stability after aging. Full article

Aim: Fixed dental prostheses (FDPs) are increasingly fabricated from high-strength ceramic materials; however, their fracture behavior under flexurally dominated loading remains incompletely understood. This in vitro study aimed to compare the mechanical performance and fracture mechanisms of four FDP material systems under standardized bending conditions. Materials and Methods: Three-unit CAD/CAM-fabricated FDPs were produced from metal-ceramic (P1), zirconia-ceramic (P2), monolithic zirconia (P3), and monolithic lithium disilicate (P4) materials (n = 9 per group). Specimens were subjected to three-point bending until failure. Crack initiation load, maximum load, displacement, and stiffness were recorded, and fracture behavior was analyzed using stereomicroscopy, micro-computed tomography (μCT), and scanning electron microscopy (SEM). Results: Metal-ceramic FDPs (P1) exhibited the highest crack initiation load (0.89 kN) and maximum load (1.91 kN), with failure predominantly occurring through ceramic veneer delamination without complete framework fracture. Monolithic zirconia FDPs (P3) demonstrated the most brittle failure behavior, characterized by abrupt fracture and unstable crack propagation immediately after crack initiation. Zirconia-ceramic (P2) and lithium disilicate (P4) FDPs showed intermediate mechanical performance, with lithium disilicate exhibiting greater resistance to catastrophic failure (F_max = 0.94 kN) compared with zirconia–ceramic FDPs. Conclusions: These findings refine current assumptions regarding the mechanical reliability of monolithic zirconia FDPs under flexural loading and highlight the importance of fracture behavior, rather than peak strength alone, in material selection. Lithium disilicate and metal-ceramic systems exhibited more favorable damage-tolerant responses under static flexural loading. These findings should be interpreted within the limitations of this in vitro model and should not be directly extrapolated to long-term clinical performance. Full article

To solve the problems of easy fracture of reaming cutter arms and mechanical jamming leading to equipment damage when mechanical reaming equipment is used for anchor hole reaming in soft rock roadways, this study proposes the development of a high-efficiency reaming device with a simple structure. This study combines theoretical analysis, numerical simulation, and laboratory experiments to systematically investigate the key parameters of high-pressure water jet reaming equipment. The results show that under the same conditions, the maximum velocity of the high-pressure water jet decreases with an increase in the number of nozzles and the nozzle spacing. Although the correlation between the maximum jet velocity and nozzle angle is weak, the jet velocity acting on the anchor hole wall reaches its peak at a nozzle angle of 60°. Based on the simulation results, a 1:1 scale nozzle model was manufactured using 3D printing technology, and high-pressure water jet reaming experiments and bolt pull-out tests were carried out at a pressure of 20 MPa. The experimental results demonstrate that the optimal reaming effect is achieved with a nozzle configuration of 3 nozzles, 10 mm spacing, and a nozzle angle range of 45–60°. Specifically, after reaming with the nozzle at a 60° angle and 10 mm spacing, the bolt anchoring force reaches 51.99 kN, representing a 41.16% increase in anchoring strength compared with conventional anchoring. This research provides technical support for the engineering application of anchor hole reaming technology in soft rock roadways and is of great significance for improving the support effect of soft rock roadways. Full article

In this paper, the effects of 4 wt.% of silicon on the microstructure and mechanical properties of AM50 magnesium alloys fabricated by the casting method are presented. New AM50/Si material and the base AM50 alloy were gravity cast into a metal mould under the same conditions for comparison. Analyses of the alloys’ microstructures were carried out by light microscopy (with differential interface contrast), scanning electron microscopy (with an energy dispersive X-ray spectrometer), as well as X-ray diffraction (XRD). In as-cast conditions, both materials were composed of α-Mg solid solution, α + γ eutectic (where γ is Al₁₂Mg₁₇), Al₈Mn₅ intermetallic phases and discontinuous γ precipitates. The AM50/Si material also consisted of the Mg₂Si phase. This structural constituent appeared in the form of primary crystals with regular polygonal morphology and an α + Mg₂Si eutectic in the form of “Chinese script”. In the microstructure of the AM50/Si material, the Mn₃SiAl₉ ternary phase was also identified. The detailed analyses presented in this paper revealed that the new ternary Mn₃SiAl₉ structural compound caused a reduction in the volume fraction of the Al₈Mn₅ phase but did not completely replace it. These two phases formed competitively. The fabricated material exhibited higher tensile and compression strength as well as yield strength in comparison with the AM50 alloy. Additionally, analyses of the fracture surfaces of the AM50/Si material carried out using scanning electron microscopy (SEM) were presented. Full article

Polymer gel profile control technology can effectively modify water flow channels in water-flooded oil reservoirs and enhance oil recovery. However, most polymer gel systems exhibit poor performance, such as low strength, not suitable for high-temperature and high-salinity reservoir conditions, leading to ineffective water shutoff. To address this challenge in complex formations of high-temperature, high-salinity fractured reservoirs, a temperature- and salt-tolerant polymer gel system with delayed crosslinking was developed based on the concept of slow hydrogen-bond crosslinking. Laboratory evaluations demonstrated that a gel system formulated with 0.4 wt% HPAM and 0.2 wt% PEI (HPAM/PEI) achieved a gel strength grade of G index. Even at 100 °C or a salinity of 200,000 ppm, the HPAM/PEI system maintained a gel strength grade of F, indicating excellent temperature resistance and shear stability. The slow hydrogen-bond crosslinking mechanism endowed the system with delayed gelation characteristics. Sandpack and core flooding experiments confirmed that the HPAM/PEI system could form high-strength gels in situ with low polymer retention. After treatment, the permeability of the core was reduced by over 99%, and the effective blocking duration exceeded 12 months. This study provides a theoretical foundation for applying the HPAM/PEI gel system in deep profile control and water shutoff in high-temperature and high-salinity reservoirs. Full article

The development of protective coatings that integrate self-healing and environmental tolerance is vital for extending substrate lifespan. In this study, a multifunctional hydrogel composite coating is developed based on a waterborne polyacrylate dynamic covalent network containing oxime–carbamate bonds. The functional monomer MEOC, which contains an oxime–carbamate dynamic bond, was synthesized and incorporated into the waterborne polyacrylate matrix to form a hydrogel network (OC-PA) with intrinsic self-healing capability. Prussian blue (PB) and nano-SiO₂ were incorporated to form a photothermal functional layer, imparting hydrophobicity and converting light into heat for de-icing, while also activating dynamic bond rearrangement within the substrate. When the MEOC content was 7 wt% and the PB content was 2 wt%, the coating temperature rose to 110 °C within 2 min under 0.6 W/cm² irradiation, and the scratch healed within 5 min. After 1 h of fracture repair, the tensile strength reached 6.68 MPa, with a repair rate as high as 92.91%, and de-icing time was reduced from 343 s to 183 s. The coating achieved a water contact angle >100°. At −20 °C, the icing delay time increased by 215%. The hydrogel coating also exhibited excellent abrasion resistance, chemical stability, UV aging resistance, and anti-fouling properties, offering a durable solution for demanding environments. Full article

Metal Digital light processing (MDLP) offers high resolution and excellent surface quality, but the final properties of printed parts are highly dependent on post-processing. In this study, the effects of debinding, decarburization, and sintering on the shape fidelity, microstructure, and mechanical properties of MDLP-fabricated 316L stainless steel were systematically investigated. The optimal post-processing route consisted of debinding in an inert atmosphere, decarburization in air within 400–600 °C, and sintering at 1370 °C for 4 h under flowing nitrogen. Under these conditions, the sintered parts achieved a relative density of 98.03 ± 0.23%, hardness of 380.63 ± 9.15 HV, elastic modulus of 213.47 ± 5.5 GPa, tensile strength of 519.7 ± 22 MPa, and elongation at fracture of 76.8 ± 9.3%. Microstructural analysis showed that increasing the sintering temperature reduced porosity and smoothed the morphology of Cr-rich oxygen-containing second phase regions, thereby alleviating stress concentration and improving mechanical properties. This study provides an effective post-processing strategy for MDLP-fabricated 316L stainless steel and examines the microstructural origins of the observed property evolution. Full article

This study investigates the influence of adhesive type on the bond performance between CFRP plates and steel interfaces through static tensile double-shear tests. Three types of adhesives (Araldite 420A/B, 2015-1, Sikadur-30CN) were tested under four bond lengths. The results indicate that adhesive strength significantly affects failure characteristics, with distinct material performance differences observed. Bond length influences the stress distribution, enhancing dispersion while potentially altering damage progression. High-performance adhesives exhibit superior shear resistance and fracture energy due to improved viscous properties, whereas moderately plastic adhesives achieve adaptive deformation and durable bonding by enhancing the flow and substrate contact. These findings provide a theoretical basis for material selection in CFRP-strengthened steel structures and offer actionable guidance for structural repair engineering applications. Full article

Numerical simulation of sequential fracturing in horizontal wells for shale gas and oil extraction requires careful consideration of mechanical interactions between proppant and fracture surfaces—a challenge that remains largely unresolved. This study proposes a novel phase-field model featuring a strain-based formulation and a width-dependent proppant reaction force. Unlike previous studies, we integrate an empirical propped force solution, adapted from established work to account for rock properties and proppant support, to capture nonlinear fracture closure. Results show that reaction stress models significantly dictate propped geometry. The model’s fracture length, width, and closure predictions are validated against theoretical solutions. We conducted a sensitivity analysis to evaluate how fracture deflection angles and widths vary with dimensionless fracture spacing, in situ stress contrast, and proppant strength. Numerical results show that proppants induce pronounced morphological asymmetry and distinct geometric discrepancies. Specifically, the heterogeneous support provided by proppants and the resulting stress redistribution alter fracture propagation paths, leading to an 8% reduction in fracture length and a marked difference in fracture orientation of approximately 80° between supported and unsupported fractures, highlighting the important role of proppants in governing fracture geometry. Both dimensionless fracture spacing and in situ stress contrast strongly influence fracture deflection, with proppant strength also contributing. The propped-force formulation is further extended to nonplanar fractures, enabling application to sequential fracturing with multiple fractures. These results highlight fracture propagation mechanisms and demonstrate the robustness of the proposed phase-field model. Full article

In this study, the microstructure and mechanical properties of ultrasonic welded joints between large-diameter aluminum wire and Cu (Ni-plated copper) terminals were systematically investigated, to reveal the underlying fracture mechanisms. The cross-sectional morphology, interfacial microstructure, and mechanical properties of the two types of welded joints are investigated. The results indicate that ultrasonic welding produces well-structured Al-Cu and Al-Ni joints. Under the same welding process parameters, the Al-Cu joint exhibits many pores, while the Al-Ni joint has no pores in its microstructure. The interfacial region of the Al-Cu joint presents various morphologies, such as flat bonding, interlocking, and eddy current patterns, whereas the Al-Ni joint interface is flat. No significant atomic diffusion phenomenon occurs between the interfaces of the two types of joints. The tensile strength of the Al-Cu joint is 53 MPa, with fracture modes including ductile fracture and brittle fracture, whereas the tensile strength of the Al-Ni joint is 50 MPa, with a failure mode of pull-out fracture. In working conditions requiring ultrasonic welding of aluminum and copper, nickel-plated copper can be used as a substitute for copper to prevent electrochemical corrosion between aluminum and copper. Full article

To address severe strata pressure induced by large end-area hanging spans and poor caving of thick, hard roofs in western coal mines, this study takes the 1302 working face of Zhujiamao Coal Mine as a case study. A multiscale mechanical model is developed to describe the progressive evolution of a stratified hard roof from a continuous beam to a cantilever beam and finally to an arched triangular hanging roof. Limit criteria for the maximum hanging length under bending and shear failure are derived, indicating that bending governs end-area roof instability. The theoretical results show good agreement with field observations and numerical simulations, providing guidance for liquid nitrogen fracturing target selection. Coupled FLAC3D-3DEC simulations reveal the staged deformation of overlying strata and clarify the spatial correspondence between the “O-X” fracture pattern and the arched triangular hanging roof. Based on these findings, a collaborative weakening strategy integrating directional drilling, hydraulic pre-cracking, and deep liquid nitrogen fracturing is proposed. Field observations and comparative tests confirm that this method effectively forms a three-dimensional fracture network, reduces roof stiffness and strength, shortens the caving interval, lowers peak shield resistance, and promotes stable caving of the end-area hanging roof. Full article

Additive manufacturing (AM) using powder bed fusion (PBF) has been the predominant printing method used over the last decade. The capability of this approach to produce complex parts with high precision has attracted the attention of major industries as a potential tool for replacing traditional manufacturing technologies. 15-5 PH stainless steel is one of the alloys being studied as a candidate for PBF processes. Its superior strength and corrosion resistance have made it a highly attractive option in numerous industries, including the automotive, nuclear, and petrochemical industries. To enhance the properties of 15-5 PH stainless-steel AM parts following printing, one can use a thermal treatment such as age hardening. However, very little research exists regarding the functional properties of AM parts made from this alloy after heat treatment. This study aims to evaluate the effect of H1150M age hardening heat treatment following printing on the properties of 15-5 PH steel, particularly regarding its mechanical properties and environmental behavior. The microstructure was studied using both optical and electron microscopy, along with X-ray diffraction (XRD) analysis. The mechanical properties were examined by tensile testing and fracture toughness assessment. Corrosion behavior was analyzed in terms of potentiodynamic polarization and using impedance spectroscopy. The results obtained have shown that over-aging caused by H1150M heat treatment has a detrimental effect on the mechanical and environmental behavior of the tested alloy. This was primarily attributed to the formation of an austenitic phase within the inherent martensitic matrix, the generation of brittle phases (mainly carbonitrides of Cr and Nb) and a reduction in grain size. Full article

In order to verify the feasibility of in situ repair of underwater local dry laser welding (ULDLW) on nuclear power reactor components, this work investigates the microstructure and mechanical properties of 304L austenitic stainless steel repaired by ULDLW using ER308L filler metal. Comprehensive comparison would be made between the ULDLW and conventional in-air laser welding to evaluate their applicability. The results demonstrate that the rapid cooling rate inherent to the underwater environment significantly influences solidification behavior and microstructural evolution. The weld metal (WM) solidifies in the ferritic–austenitic (FA) mode, with an increased proportion of lathy δ-ferrite at the expense of skeletal morphology compared to the in-air welds. Electron backscatter diffraction (EBSD) analysis reveals the substantial grain refinement in underwater welds, with average grain sizes of 39.4 μm versus 47.3 μm for in-air weld bead, accompanied by a higher fraction of low-angle grain boundaries (LAGBs). These microstructural modifications yield superior mechanical properties: underwater weld bead exhibits ultimate tensile strength (UTS) of 685.6 MPa, elongation of 57.5%, and impact toughness of 22.6 J, significantly exceeding the corresponding values for in-air welds (663.9 MPa, 51.8%, and 18.6 J, respectively). Fractographic analysis confirms ductile fracture mechanisms in both conditions. The enhanced performance is attributed to grain refinement strengthening via the Hall–Petch relationship and the increased LAGBs fraction, which impedes dislocation motion and crack propagation. Full article

Wollastonite is a natural meta-silicate mineral material with fibrous characteristics. In this paper, wollastonite with different aspect ratios obtained after grinding was used as a mineral admixture to replace cement for preparing ultra-high-toughness cement-based composites (UHTCCs). The effects of wollastonite on the fluidity, compressive strength, flexural strength, and tensile properties of UHTCCs were investigated, and the crack morphology and micro-topography of the tensile specimens after fracture were observed. The experimental results show that when the wollastonite replacement ratio exceeds 4%, it exerts a negative effect on the fluidity of UHTCCs, and wollastonite with a larger aspect ratio has a more significant negative impact. Relying on the bridging effect, replacing cement with wollastonite can significantly improve the flexural strength and compressive strength of UHTCCs. However, when the replacement ratio exceeds 6%, the strength enhancement effect of wollastonite with a larger aspect ratio begins to decrease. When the cement replacement ratio of wollastonite is up to 6%, it can increase the initial cracking strength, tensile strength and tensile strain of UHTCCs. At the same replacement ratio, wollastonite with a larger aspect ratio shows a better reinforcing effect. According to the observation of post-fracture crack morphology, the cracks of UHTCCs change from the original smooth cracks to tortuous ones after cement is partially replaced by wollastonite. Replacing a part of cement with wollastonite optimizes the performance relationship among PE fibers, the matrix, and the PE fiber–matrix interface, and it enhances their synergistic effect. This not only raises the initial tensile cracking strength of UHTCCs but also improves its tensile strain. In particular, wollastonite with a larger aspect ratio exhibits a more pronounced reinforcing effect. Full article

To address the technical challenges of difficult deduction, limited field measurement, and ambiguous instability determination of roof separation critical values in mining roadways within the weakly cemented coal-bearing strata of Xinjiang, this paper proposes a discrete element method that integrates the fracture of anchor bolt and anchor cable support materials with the damage degree of the surrounding rock. Taking a specific mine in the Hosh Tolgay coalfield as the research object, a systematic study was conducted. The research process was as follows. (1) Model parameter calibration was performed. Intact rock parameters were obtained through laboratory basic mechanical tests, and rock mass parameters were corrected based on reduction empirical formulas and the Hoek–Brown criterion. Numerical model verification showed that the errors between the simulated and theoretical values of the elastic modulus, compressive strength, and tensile strength of the rock mass were all less than 10%, indicating that the corrected parameters are reasonable. (2) The critical damage values of the rock mass considering a non-constant confining pressure environment were proposed. Through triaxial compression simulations, the differential evolution patterns of rapid damage increase in sandy mudstone under low confining pressure and stable damage accumulation in coal were revealed, thereby clarifying the damage thresholds for rock mass instability under different confining pressures. (3) A large-scale model was established to analyze the evolution laws of the fracture field, support field, and displacement field of the roadway surrounding rock. A comprehensive determination method for the instability of the roof anchored bearing structure was proposed. By comparing the damage thresholds of the scaled rock mass and the roadway surrounding rock and analyzing the fracture conditions of the roadway support system, a dual-criterion consisting of surrounding rock damage and support material fracture was constructed. Based on this criterion theory, the critical values for deep and shallow separation were obtained. The research results indicate that the evolution patterns of damage in coal and sandy mudstone differ with confining pressure. The sandy mudstone layers in the shallow part of the roof are more sensitive to mining-induced unloading disturbances. Consequently, the surrounding rock damage and support fracture of the mine roof exhibit distinct distribution characteristics: the dominant failure of the roadway is shear failure, with wide-range coalescence of shallow fractures and gradual development of deep fractures, alongside the concentrated failure of shallow anchor bolts and partial failure of deep anchor cables. Based on the instability state of the roof monitoring zones, the critical value for shallow separation was determined to be 90.7 mm, and the critical value for deep separation was 129.03 mm. These results are very close to the field measured values, verifying the engineering applicability of the method. This paper reveals the damage characteristics of the rock mass and surrounding rock in weakly cemented strata, as well as the mechanism of roof separation initiation and evolution. The proposed method for determining critical values provides a scientific and feasible practical reference for the support optimization and monitoring and early warning of roadway roofs in weakly cemented strata, possessing significant engineering value for ensuring safe and efficient mine production. Full article