Search Results (101)

Fine migration is widely recognized as a primary cause of production decline in unconsolidated sandstone reservoirs. Migrated fines may accumulate within pore throats and obstruct flow channels, or they may be transported into the wellbore with the produced fluids, leading to operational issues such as wellbore plugging, pump sticking, and equipment abrasion. Despite extensive studies on fine migration, the role of particle wettability has received limited attention. In this study, the mineralogical composition of formation particles was first characterized using X-ray diffraction (XRD) and quantitative clay analysis. Surface modification experiments were then conducted to investigate the effect of hexadecylamine (HDA) on particle wettability and to determine the optimal reaction conditions. Surface characterization techniques were employed to elucidate the modification mechanism. Subsequently, sand-packed tube displacement experiments were performed to evaluate the influence of wettability alteration on fine migration behavior. The underlying mechanisms were further interpreted through interfacial thermodynamic analysis. Two potential field application schemes are proposed to facilitate practical implementation in oilfield operations. The results indicate that the water contact angle of formation particles increased from 0° to 150° when treated with 0.8 wt% HDA for 24 h. Surface characterization confirms that HDA molecules were physically adsorbed onto the particle surfaces. Displacement experiments demonstrate that the permeability reduction rate decreases significantly with increasing particle hydrophobicity. Thermodynamic analysis suggests that the work of adhesion on the modified particle surface was reduced by 93.3%, thereby weakening fluid–particle interfacial coupling and suppressing fine mobilization. This study provides a wettability-based approach for mitigating permeability damage caused by fine migration in unconsolidated sandstone reservoirs. Full article

The redox mechanisms of silica-supported Ni particles were investigated using their in situ X-ray absorption fine structure, providing mechanistic insights into partially reduced NiO and partially oxidized metallic Ni. The results of surface oxidation of partially reduced NiO particles at room temperature revealed that the surface was not fully covered with metallic Ni and that metallic Ni had also formed within the particle interior. During NiO particle reduction, the process initiates at specific surface sites, and before the metallic Ni phase fully covers the surface, O²⁻ ions are expelled from the particle. Conversely, the oxidation of metallic Ni particles progresses inward from the surface, with an accompanying increase in the thickness of the NiO layer that forms upon O₂ exposure at room temperature. This mechanism is supported by observations that the reduction of a thin NiO shell on metallic Ni particles was completed below 200 °C, while reduction temperatures shifted to higher values as the NiO layer thickness increased. The distinct oxidation and reduction mechanisms are attributed to differences in the migration direction of O²⁻ ions. During reduction, it is proposed that O²⁻ ions within the particles migrate to the surface along the interface between the NiO phase and the metallic Ni phase. This study elucidates the detailed mechanism behind the redox interconversion between NiO and metallic Ni in solid catalyst particles. Full article

This study presents a distribution-optimized mesostructure estimation method for statistically modeling near-surface aggregate size distributions in concrete by optimizing the spatial arrangement of polydisperse spherical aggregates with respect to formwork boundaries. The approach is based on minimizing the deviation between a generated cumulative aggregate volume function and an idealized linear target function corresponding to a constant area fraction along the specimen depth. To enable efficient computation for systems containing a large number of aggregates, grain size groups derived from the grading curve are represented using symmetric Beta distributions, allowing each group to be described by a single shape parameter. The resulting optimization problem is solved using a derivative-free Powell algorithm. The method inherently captures wall effects, leading to a migration of smaller aggregates toward the specimen boundaries to compensate for the geometric constraints of bigger aggregates. Experimental validation was performed for a single concrete mixture and specimen geometry by determining the depth-dependent mean bulk density of a concrete cube using incremental surface grinding combined with high-resolution 3D laser scanning. The optimized mesostructure shows strong agreement with measured density profiles for the investigated specimen. While the validation is limited to a single mixture and geometry, the results indicate that the proposed method is a computationally efficient approach for incorporating wall effects into mesoscale concrete models. Furthermore, increasing aggregate volume fractions intensify the near-surface accumulation of fine particles. Full article

The large volumes of fine flotation tailings constitute a persistent challenge for the conventional treatment of minerals due to their wide particle size distribution and their low metal contents. In this work, the potential of passive inertial microfluidics for the selective redistribution of mineral particles from actual copper flotation tailings is studied. A suspension of tailings was treated in a rectangular microfluidic channel in a laminar regime, without an external magnetic field or sheath flux. The solid fractions obtained were characterized in terms of particle size distribution, phase composition and element content. The microfluidic treatment induced a systematic distribution of the particles between the output fractions. The central fraction was enriched with coarser particles, the median particle size increasing from about 15 µm in the feed to about 20 µm, and had high concentrations of Cu, Fe, Ag and Zn, with enrichment factors reaching 2.0 to 2.7 depending on the element. On the other hand, the lateral fraction was mainly composed of finer particles (D50 ≈ 13 µm) and depleted in metalliferous phases. The elemental mass balance confirmed that the observed enrichment results from selective redistribution rather than from a loss of material. These results indicate that the separation of the particles cannot be explained solely by size effects and are consistent with a preferential migration of the denser and metal-rich particles towards stable inertial focusing trajectories. Full article

Tailings backfilling (TB) is widely recognized as an environmentally friendly and engineering safe technique to enhance mining efficiency. However, the heterogeneous particle distribution in TB slurry, also-named the segregation phenomenon, can significantly affect the mechanical strength of the backfill, especially under high goaf conditions. Therefore, elucidating the spatial distribution characteristics of particles during high-goaf filling has become a crucial research focus for improving the mechanical behavior of tailings backfill. A systematic experimental investigation was conducted in this study, incorporating the similarity principle, to analyze the migration behavior of backfill slurry particles and to clarify how the different backfill heights influence the spatial distribution of fine, medium, and coarse particles. The results indicate a clear vertical variation in PSD. Based on statistical analysis of samples collected from different backfill height experiments, coarse particle content increased progressively from the upper to lower layers (median: 16.2%, 23.6%, and 25.0%), while medium-sized particles remained relatively stable (37.0%, 37.3%, 37.0%). Fine particles dominated overall but decreased with layers (45.6%, 38.8%, 38.3%). Coarse particles tended to settle downward due to gravitational forces, whereas fine particles migrated upward. The distribution of medium-sized particles remained largely homogeneous. Fine and coarse particles were subjected to opposing driving forces. Meanwhile, particles maintained an approximately symmetrical distribution in the horizontal direction. Moreover, when the backfill height exceeded 800 mm, a notable intensification of stratification occurred, indicating a strong height-dependent transition in segregation behavior. In contrast, in the horizontal direction, the PSD showed no clear dependence on backfill height. These findings provide new insights into the mechanisms of particle segregation within backfill materials, offering a theoretical foundation and experimental support for optimizing PSD within the backfill body and elucidating the collapse mechanisms of high goafs. Full article

Prolonged water injection in unconsolidated sandstone reservoirs can induce pore rearrangement and modify flow pathways, thereby affecting reservoir performance. However, quantitative characterization of pore evolution in both temporal and spatial dimensions remains limited. This study investigates the mechanisms of pore-structure evolution during extended injection through a series of multi-scale experiments. Scanning electron microscopy and X-ray diffraction analyses were employed to compare mineral composition and microstructural characteristics before and after injection, while in situ nuclear magnetic resonance (NMR) monitoring captured the dynamic evolution process, enabling pore-size classification from T₂ spectra and fractal assessment of structural complexity. Segmented NMR measurements at different distances further resolved spatial heterogeneity. The results show that prolonged water injection reduced permeability by 10.4–32.1%, whereas porosity exhibited only minor variation, indicating that the decline in flow capacity is primarily controlled by pore–throat structural adjustment rather than pore volume loss. Mineralogical redistribution and fine-particle migration decreased the median pore radius by 21.5–51.8% and the micropore fractal dimension by 23.8–76.5%, with stronger responses observed at higher permeabilities, while meso- and macropore fractal dimensions remained nearly unchanged, indicating preferential modification of micropores with preservation of the main connected flow framework. Consistently, NMR responses reveal pronounced spatial heterogeneity along the flow direction. The NMR signal changes at the injection end were 11.2–18.4% and 7.7–21.7% during the early and intermediate stages, respectively, both exceeding those at the distal end (2.9–12.4% and 1.9–17.1%). These results indicate a downstream-attenuating structural modification gradient. The findings provide new insights into pore-structure evolution during prolonged water injection and offer a scientific basis for optimizing water-injection strategies in unconsolidated sandstone reservoirs. Full article

Spiral separators commonly face the issue of particle misplacement during fine particle separation, which severely limits separation accuracy. This study employs a coupled CFD-DEM numerical simulation method to systematically investigate the influence mechanism of transverse inclination angle (10°, 15°, 20°) on particle moving behavior. The results show that the separation process exhibits distinct stage characteristics, which can be divided into an initial stage (first 1/3 turn), a transition stage (1/3 to 2 turns), and a quasi-steady stage (after 2 turns). A steeper angle (20°) optimizes the flow field, reducing the inner low-velocity zone and widening the high-velocity core, which promotes inward migration of particles. This enhances the enrichment of high-density particles while effectively suppressing their mixing into the clean coal product at the outer edge. For difficult-to-separate fine particles below 0.1 mm, although complete separation is challenging, increasing the transverse inclination angle still shows a clear reduction in the misplacement of high-density particles, providing a controllable approach for improving the quality of the outer edge product. This study offers theoretical insights and design guidance for optimizing spiral separator structures and enhancing fine coal separation efficiency. Full article

Particle migration is a pore-scale process that fundamentally controls pore-structure evolution and seepage behavior in granular porous media. This study investigates fine particles migration in coarse-grained sediments and its effects on pore structure and permeability by combining low-field nuclear magnetic resonance (LF-NMR) experiments with coupled CFD–DEM simulations. The evolution of fine particles migration rate, porosity variation, and permeability was analyzed under different fluid injection velocities and fines concentrations. Higher injection velocities accelerate fines initiation and early-stage migration by increasing hydrodynamic drag forces, whereas their influence diminishes at later stages due to pore-structure confinement and localized particle retention. At a constant injection velocity, increasing fines concentration suppresses early fines mobilization owing to enhanced interparticle interactions and pore throat blockage. As seepage continues, progressive fines release and export enlarge pore space and enhance permeability. Spatial analyses reveal that fines migration is governed by localized retention and rearrangement within pore throats. Within the investigated parameter ranges and timescales, system evolution is dominated by internal erosion and pore unclogging rather than sustained macroscopic clogging. These results provide mechanistic experimental–numerical insight into fines migration and seepage stability in granular porous media, with direct relevance to hydrate-bearing sediments and other fine-sensitive geological systems. Full article

To investigate the effects of repeated drying and wetting on the mechanical properties and meso-fabric of metal tailings, lead-zinc tailings from Hunan Province were studied. A self-developed apparatus was used to simulate the cyclic drying-wetting processes. Combined with triaxial shear tests and stereomicroscopic image analysis, the changes in macroscopic mechanical properties and meso-fabric, as well as their correlation mechanisms, were investigated. The results indicate that the wet-dry cycles did not alter the strain-softening characteristics of the tailings’ stress-strain curves; however, they significantly intensified the degree of softening during the later stages of cycling (4–6 cycles). The static strength exhibited a trend characterized by “initial gradual degradation → temporary recovery → further deterioration” with an increasing number of cycles. After six cycles, the strength was significantly reduced compared to the initial state. The effective cohesion (c′) fluctuated markedly, with an amplitude of 31.1%, while the variation in the effective internal friction angle (φ′) was only 6.02%, indicating that dry-wet cycles have a more pronounced effect on the cohesion of tailings. At the microscopic level, the dry-wet cycling process promoted the upward migration of fine particles ranging from 0 to 60 µm, resulting in a decrease in the proportion of smaller particles in the lower layer. The porosity increased overall, with the lower layer rising from 44.06% to 54.26%. Pore evolution was dominated by the enlargement of pores larger than 150 µm. The macro-meso correlation analysis revealed that “fine particle migration → expansion of pores → loss of cementitious material” was the core driving factor for the deterioration of macroscopic mechanics, and the macroscopic mechanical response was the external manifestation of the adjustment of the microscopic structure. This research can provide certain theoretical support for the long-term safe operation and stability improvement of tailings dams. Full article

Liners made of natural materials, such as expansive soil with sand, have a wide range of applications, including geotechnical and geoenvironmental applications. Besides being environmentally friendly, these materials are locally available and can be constructed at a low cost. The concern regarding these liners is sustainability and serviceability in the long run. The research conducted revealed significant degradation in hydraulic performance after periods of operation under continuous flow, which was attributed to the migration of fines. This study investigated the stabilization of these liners by using biopolymers as a cementitious agent to prevent the migration of fines and enhance sustainability in the long run. Two different biopolymers were examined in this study, including guar gum (GG) and sodium alginate (SA). The hydraulic conductivity tests were conducted in the laboratory under continuous flow for a long period (i.e., more than 360 days). The results revealed that incorporating biopolymers into these liners is of great significance for enhancing their sustainability and hydraulic performance stability. Further in-depth identification of the interaction mechanisms demonstrates that biopolymer–soil interactions create cross-links between soil particles through adhesive bonding, forming a cementitious gel that stabilizes fines and enhances the stability of the liners’ internal structure. Both examined biopolymers show significant stabilization of fines and stable hydraulic performance within the acceptable range, with high superiority of SA with EC20. The outcomes of this study are valuable for conducting an adequate and sustainable design for liner protection layers as hydraulic barriers or covers. Full article

Drill-and-blast tunnel construction continuously releases high-intensity dust during drilling, blasting, and shotcreting, while conventional forced ventilation is often insufficient to control dust migration and worker exposure. This study develops three-dimensional Euler–Lagrange gas–solid two-phase models for these three typical processes to clarify the spatiotemporal dispersion of polydisperse dust and to explore effective control strategies. The simulations show that all processes generate a persistent high-concentration dust belt near the tunnel face, and a low-velocity recirculation zone at the crown acts as a structural hotspot of dust accumulation that is difficult to purge by longitudinal ventilation. Particle size strongly affects dispersion behaviour: coarse particles rapidly settle near the source under gravity, whereas fine and medium-sized particles remain suspended for long periods and can be transported over long distances, particularly after blasting. Based on these findings, a rail-mounted purification system with a dynamically adjustable position along the tunnel is proposed, and its preferred deployment zones are determined to work synergistically with the main airflow. The system is designed to perform near-source and crown-targeted removal, providing an engineering-oriented “dynamic local purification plus overall ventilation dilution” pathway for improving air quality in drill-and-blast tunnel construction. Full article

Advanced oxidation processes (AOPs) are increasingly used for the remediation of soils contaminated with petroleum hydrocarbons, as they rapidly mineralize recalcitrant fractions to CO₂ and H₂O. However, the effects of AOPs on the geotechnical properties of such soils remain not well understood. In this study, the influences of a combined oxidation system of sodium percarbonate (SPC), nanoscale zero-valent iron (nZVI), and sodium persulfate (PS) on the geotechnical behavior of petroleum hydrocarbon-contaminated soil were investigated. A series of tests, including basic geotechnical index, pH, Atterberg limits, particle size distribution, and consolidated undrained triaxial compression test, were conducted to explore the geotechnical responses and underlying mechanisms associated with the dual AOPs treatment. The results indicate that the diesel-contaminated soil exhibited slightly higher LL and PI compared with the natural soil. For the treated soils, LL and PI remained essentially unchanged with increasing SPC dosage. The particle-size distribution first migrated to finer fractions and then reverted to a coarser mode. The strongest fining was observed at 2% SPC, whereas higher SPC dosages induced aggregation and the formation of larger agglomerates. Consolidated undrained triaxial tests indicate that diesel contamination reduced undrained stiffness and strength. The nZVI–PS treatment without SPC produced a partial recovery in stiffness and a slight increase in the friction angle. With increasing SPC dosage, the soils exhibited a nonmonotonic response in stiffness and shear strength, where low SPC enhanced apparent cohesion and higher SPC weakened bonds while partially restoring frictional resistance. These findings suggest that advanced oxidation of petroleum hydrocarbon–contaminated soils requires a trade-off. This trade-off is between contaminant degradation efficiency and the preservation of geotechnical performance to ensure the reuse of the remediated soil. Full article

This paper proposes a hybrid photovoltaic (PV) Maximum Power Point Tracking (MPPT) strategy to tackle local optima, slow dynamic response, and steady-state oscillations under partial shading conditions (PSC). The method combines an Improved Whale Migration Algorithm (IWMA) with a variable-step Incremental Conductance (VINC) technique. IWMA employs a Tent–Logistic–Cosine chaotic initialization, dynamic weight coefficients, random feedback, and a distance-sensitive term to enhance population diversity, strengthen global exploration, and reduce the risk of convergence to local maxima. The VINC stage adaptively adjusts the step size based on incremental conductance, providing fine local refinement around the global maximum power point (GMPP) and suppressing steady-state power ripple. Extensive MATLAB/Simulink simulations with multiple random trials show that the proposed IWMA-VINC strategy consistently outperforms the Whale Migration Algorithm (WMA), A Simplified Particle Swarm Optimization Algorithm Combining Natural Selection and Conductivity Incremental Approach (NSNPSO-INC), and the Grey Wolf Optimizer and Whale Optimization Algorithm (GWO-WOA) under both static and dynamic PSC, achieving the highest tracking accuracies (99.74% static, 99.44% dynamic), higher average output power, shorter convergence times, and the smallest variance across trials. These results demonstrate that IWMA-VINC offers a robust and high-performance MPPT solution for PV systems operating in complex illumination environments. Full article

Ultrafine particles, as raw materials for various industries such as construction and environmental protection, are currently obtained through repeated ball milling and multiple classifications, but classification efficiency remains at a low level. Based on the principle of hydrocyclone classification, this paper designs a hydrocyclone with a triple-vortex finder structure that can achieve finer particle size distributions without altering the main structure of the hydrocyclone. The classification performance of the triple-vortex finder hydrocyclone is investigated through numerical analysis and experimental methods, with numerical comparisons made to single-vortex finder and double-vortex finder structures. The results indicate that with an increase in the number of vortex finders, the static pressure and tangential velocity gradually decrease, reducing the likelihood of tangential vortex formation while meeting classification requirements. The axial velocity in the triple-vortex finder structure is significantly reduced, which extends the residence time within the hydrocyclone and facilitates sufficient particle classification. As the number of vortex finders increases, the zero-velocity envelope surface (LZVV) gradually migrates inward, enlarging the external swirling classification space. Through numerical and experimental analyses, it is found that the triple-vortex finder hydrocyclone exhibits the highest classification efficiency, the strongest cutting ability, and the best classification accuracy. Compared to the single-vortex finder structure, the cutting particle size of the triple-vortex finder hydrocyclone decreases by 2.5 µm, and the content of fine particles in the underflow is reduced by 4.36 percentage points, effectively decreasing the fine particle content in the underflow. The quality efficiency improves by 18.85 percentage points compared to the single-vortex finder, while the quantity efficiency shows no significant decline. The obtained data provide a theoretical foundation and data support for the structural design of the new hydrocyclone. Full article

The utilization of hydrocyclones dates back more than a century. As the key channel for multiphase flow, the inlet chamber exerts a notable influence on the separation efficiency of hydrocyclones. Conventional feed bodies mainly adopt straight lines as guidelines. During the transition of fluid from linear motion to circumferential motion, significant kinetic energy loss and particle misalignment are exhibited, resulting in relatively low classification accuracy of the hydrocyclone. Therefore, in this study, a hydrocyclone featuring a complex curved inlet chamber structure was designed, and numerical analysis was employed to examine the particle distribution and aggregation characteristics within both the inlet chamber and the hydrocyclone. Supplemented with RSM/VOF/TFM simulations and quartz sand experimental validation, this study compares the separation performance of the complex curved inlet with the conventional linear inlet. The results indicate the following: when particle sizes are small, particles are dispersed throughout the hydrocyclone and inlet chamber, exhibiting a disordered state, which leads to poor classification performance. As particle size increases, particles gradually form layers along the radial direction; larger particles tend to accumulate on the hydrocyclone wall. When the particle concentration is maintained within a specific range, it promotes the migration of fine particles toward the center, thereby reducing the likelihood of fine particles entering the outer vortex and allowing for more precise classification of fine particles. As the particle concentration increases, the cutting ability of the hydrocyclone progressively diminishes; when the concentration exceeds 20%, the maximum underflow recovery rate for particles smaller than 50 µm is only 60%, resulting in significant coarse overflow and a notable decrease in classification precision. Furthermore, as the inlet concentration increases, the dispersion index for 0.5 µm particles ranges from 0.6 to 1.6, for 4 µm particles from 0.6 to 1.4, and for 60 µm particles from 0.6 to 1. The decreasing dispersion index indicates an increasing classification force, which aids in the formation of a coarse particle layer on the wall. The conclusions and data obtained provide a theoretical foundation and empirical support for the design of innovative inlet chamber structures. Full article